DE2018713A1 - - Google Patents
Info
- Publication number
- DE2018713A1 DE2018713A1 DE19702018713 DE2018713A DE2018713A1 DE 2018713 A1 DE2018713 A1 DE 2018713A1 DE 19702018713 DE19702018713 DE 19702018713 DE 2018713 A DE2018713 A DE 2018713A DE 2018713 A1 DE2018713 A1 DE 2018713A1
- Authority
- DE
- Germany
- Prior art keywords
- exchange resins
- cation exchange
- hours
- solution
- hydrogen peroxide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims description 16
- 239000003054 catalyst Substances 0.000 claims description 11
- 238000000034 method Methods 0.000 claims description 8
- 230000002378 acidificating effect Effects 0.000 claims description 7
- 150000001735 carboxylic acids Chemical class 0.000 claims description 6
- 239000002253 acid Substances 0.000 claims description 5
- 239000003729 cation exchange resin Substances 0.000 claims description 5
- 229940023913 cation exchange resins Drugs 0.000 claims description 5
- 150000007513 acids Chemical class 0.000 claims description 4
- 150000002500 ions Chemical class 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 125000001931 aliphatic group Chemical group 0.000 claims description 3
- 125000003118 aryl group Chemical group 0.000 claims description 3
- 150000002148 esters Chemical class 0.000 claims description 3
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical group [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 2
- 125000005842 heteroatom Chemical group 0.000 claims description 2
- 229910052760 oxygen Inorganic materials 0.000 claims description 2
- 239000001301 oxygen Substances 0.000 claims description 2
- 229920000642 polymer Polymers 0.000 claims description 2
- 229920006395 saturated elastomer Polymers 0.000 claims description 2
- 239000000243 solution Substances 0.000 description 20
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 10
- 238000006243 chemical reaction Methods 0.000 description 9
- 239000000203 mixture Substances 0.000 description 6
- 229960000583 acetic acid Drugs 0.000 description 5
- 239000012362 glacial acetic acid Substances 0.000 description 5
- SCKXCAADGDQQCS-UHFFFAOYSA-N Performic acid Chemical compound OOC=O SCKXCAADGDQQCS-UHFFFAOYSA-N 0.000 description 3
- 239000003456 ion exchange resin Substances 0.000 description 3
- 229920003303 ion-exchange polymer Polymers 0.000 description 3
- YKYONYBAUNKHLG-UHFFFAOYSA-N n-Propyl acetate Natural products CCCOC(C)=O YKYONYBAUNKHLG-UHFFFAOYSA-N 0.000 description 3
- 125000000542 sulfonic acid group Chemical group 0.000 description 3
- KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 description 2
- 239000004793 Polystyrene Substances 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 230000000694 effects Effects 0.000 description 2
- 229920002223 polystyrene Polymers 0.000 description 2
- 229940090181 propyl acetate Drugs 0.000 description 2
- 239000012429 reaction media Substances 0.000 description 2
- 230000008961 swelling Effects 0.000 description 2
- NQPDZGIKBAWPEJ-UHFFFAOYSA-N valeric acid Chemical compound CCCCC(O)=O NQPDZGIKBAWPEJ-UHFFFAOYSA-N 0.000 description 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 1
- DKPFZGUDAPQIHT-UHFFFAOYSA-N Butyl acetate Natural products CCCCOC(C)=O DKPFZGUDAPQIHT-UHFFFAOYSA-N 0.000 description 1
- BQCADISMDOOEFD-UHFFFAOYSA-N Silver Chemical compound [Ag] BQCADISMDOOEFD-UHFFFAOYSA-N 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000007933 aliphatic carboxylic acids Chemical class 0.000 description 1
- 125000000217 alkyl group Chemical group 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 150000001768 cations Chemical class 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- FUZZWVXGSFPDMH-UHFFFAOYSA-N hexanoic acid Chemical compound CCCCCC(O)=O FUZZWVXGSFPDMH-UHFFFAOYSA-N 0.000 description 1
- 150000002927 oxygen compounds Chemical class 0.000 description 1
- 229920001467 poly(styrenesulfonates) Polymers 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 229910052709 silver Inorganic materials 0.000 description 1
- 239000004332 silver Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
- B01J31/06—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides containing polymers
- B01J31/08—Ion-exchange resins
- B01J31/10—Ion-exchange resins sulfonated
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C407/00—Preparation of peroxy compounds
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (11)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19702018713 DE2018713C3 (de) | 1970-04-18 | Verfahren zur Herstellung von Percarbonsäuren | |
| CH159171A CH544060A (de) | 1970-04-18 | 1971-02-03 | Verfahren zur Herstellung von Percarbonsäuren |
| NL7101911A NL171704C (nl) | 1970-04-18 | 1971-02-12 | Werkwijze voor het bereiden van percarbonzuren. |
| SU1625750A SU366600A3 (enrdf_load_stackoverflow) | 1970-04-18 | 1971-02-24 | |
| YU44571A YU36012B (en) | 1970-04-18 | 1971-02-24 | Process for the manufacture of percarboxylic acids |
| FR7110007A FR2092452A5 (enrdf_load_stackoverflow) | 1970-04-18 | 1971-03-22 | |
| BE765914A BE765914A (fr) | 1970-04-18 | 1971-04-16 | Procede pour la preparation d'acides percaboxyliques |
| AT324971A AT306692B (de) | 1970-04-18 | 1971-04-16 | Verfahren zur Herstellung von Percarbonsäuren |
| JP46025214A JPS5121967B1 (enrdf_load_stackoverflow) | 1970-04-18 | 1971-04-19 | |
| GB2689771A GB1338655A (en) | 1970-04-18 | 1971-04-19 | Production of percarboxylic acids |
| CA110719A CA923912A (en) | 1970-04-18 | 1971-04-19 | Process for the production of percarboxylic acids |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19702018713 DE2018713C3 (de) | 1970-04-18 | Verfahren zur Herstellung von Percarbonsäuren |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE2018713A1 true DE2018713A1 (enrdf_load_stackoverflow) | 1971-11-04 |
| DE2018713C3 DE2018713C3 (de) | 1976-02-26 |
Family
ID=
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0641777A1 (de) * | 1993-09-08 | 1995-03-08 | LAPORTE GmbH | Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Peroxycarbonsäuren |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| EP0641777A1 (de) * | 1993-09-08 | 1995-03-08 | LAPORTE GmbH | Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Peroxycarbonsäuren |
Also Published As
| Publication number | Publication date |
|---|---|
| BE765914A (fr) | 1971-09-16 |
| YU44571A (en) | 1981-02-28 |
| FR2092452A5 (enrdf_load_stackoverflow) | 1972-01-21 |
| GB1338655A (en) | 1973-11-28 |
| JPS5121967B1 (enrdf_load_stackoverflow) | 1976-07-06 |
| SU366600A3 (enrdf_load_stackoverflow) | 1973-01-16 |
| NL171704B (nl) | 1982-12-01 |
| NL7101911A (enrdf_load_stackoverflow) | 1971-10-20 |
| AT306692B (de) | 1973-04-25 |
| CA923912A (en) | 1973-04-03 |
| CH544060A (de) | 1973-11-15 |
| NL171704C (nl) | 1983-05-02 |
| YU36012B (en) | 1981-11-13 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| E77 | Valid patent as to the heymanns-index 1977 | ||
| 8339 | Ceased/non-payment of the annual fee |