DE2015401A1 - Verfahren zur Herstellung faserförmiger Alkalihexatitanate - Google Patents
Verfahren zur Herstellung faserförmiger AlkalihexatitanateInfo
- Publication number
- DE2015401A1 DE2015401A1 DE19702015401 DE2015401A DE2015401A1 DE 2015401 A1 DE2015401 A1 DE 2015401A1 DE 19702015401 DE19702015401 DE 19702015401 DE 2015401 A DE2015401 A DE 2015401A DE 2015401 A1 DE2015401 A1 DE 2015401A1
- Authority
- DE
- Germany
- Prior art keywords
- alkali
- reaction
- tio
- compounds
- melt
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000003513 alkali Substances 0.000 title claims description 47
- 238000000034 method Methods 0.000 title claims description 20
- 238000004519 manufacturing process Methods 0.000 title claims description 11
- 238000006243 chemical reaction Methods 0.000 claims description 38
- 229910010413 TiO 2 Inorganic materials 0.000 claims description 18
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 17
- 150000001875 compounds Chemical class 0.000 claims description 17
- 229910021653 sulphate ion Inorganic materials 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 9
- 150000003609 titanium compounds Chemical class 0.000 claims description 7
- 239000000376 reactant Substances 0.000 claims description 6
- 229910052700 potassium Inorganic materials 0.000 claims description 5
- -1 rhodanides Chemical class 0.000 claims description 5
- 229910052708 sodium Inorganic materials 0.000 claims description 5
- 229910052792 caesium Inorganic materials 0.000 claims description 3
- 229910052701 rubidium Inorganic materials 0.000 claims description 3
- 150000001242 acetic acid derivatives Chemical class 0.000 claims description 2
- 229910000272 alkali metal oxide Inorganic materials 0.000 claims description 2
- 150000004679 hydroxides Chemical class 0.000 claims description 2
- 150000002823 nitrates Chemical class 0.000 claims description 2
- 150000002826 nitrites Chemical class 0.000 claims description 2
- 150000003891 oxalate salts Chemical class 0.000 claims description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 2
- LLZRNZOLAXHGLL-UHFFFAOYSA-J titanic acid Chemical compound O[Ti](O)(O)O LLZRNZOLAXHGLL-UHFFFAOYSA-J 0.000 claims description 2
- 229910002651 NO3 Inorganic materials 0.000 claims 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims 1
- UCKMPCXJQFINFW-UHFFFAOYSA-N Sulphide Chemical compound [S-2] UCKMPCXJQFINFW-UHFFFAOYSA-N 0.000 claims 1
- 150000004703 alkoxides Chemical class 0.000 claims 1
- 150000004820 halides Chemical class 0.000 claims 1
- 239000000835 fiber Substances 0.000 description 27
- 239000011541 reaction mixture Substances 0.000 description 24
- 239000000155 melt Substances 0.000 description 18
- 239000011734 sodium Substances 0.000 description 17
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 14
- 239000010936 titanium Substances 0.000 description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 9
- 238000010438 heat treatment Methods 0.000 description 6
- 229910052751 metal Inorganic materials 0.000 description 6
- 239000002184 metal Substances 0.000 description 6
- 229910052697 platinum Inorganic materials 0.000 description 6
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 5
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 5
- 229910052760 oxygen Inorganic materials 0.000 description 5
- 239000001301 oxygen Substances 0.000 description 5
- 238000001816 cooling Methods 0.000 description 4
- 230000035484 reaction time Effects 0.000 description 4
- 229910052719 titanium Inorganic materials 0.000 description 4
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 4
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 3
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 3
- 238000010586 diagram Methods 0.000 description 3
- 239000012065 filter cake Substances 0.000 description 3
- 238000001914 filtration Methods 0.000 description 3
- 239000011810 insulating material Substances 0.000 description 3
- 239000011591 potassium Substances 0.000 description 3
- 230000002787 reinforcement Effects 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 2
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 2
- 239000002585 base Substances 0.000 description 2
- FLJPGEWQYJVDPF-UHFFFAOYSA-L caesium sulfate Chemical compound [Cs+].[Cs+].[O-]S([O-])(=O)=O FLJPGEWQYJVDPF-UHFFFAOYSA-L 0.000 description 2
- 239000002657 fibrous material Substances 0.000 description 2
- 230000007062 hydrolysis Effects 0.000 description 2
- 238000006460 hydrolysis reaction Methods 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- OTYBMLCTZGSZBG-UHFFFAOYSA-L potassium sulfate Chemical compound [K+].[K+].[O-]S([O-])(=O)=O OTYBMLCTZGSZBG-UHFFFAOYSA-L 0.000 description 2
- 229910052939 potassium sulfate Inorganic materials 0.000 description 2
- 235000011151 potassium sulphates Nutrition 0.000 description 2
- 230000005855 radiation Effects 0.000 description 2
- 230000003014 reinforcing effect Effects 0.000 description 2
- 229910052938 sodium sulfate Inorganic materials 0.000 description 2
- 235000011152 sodium sulphate Nutrition 0.000 description 2
- 229920003002 synthetic resin Polymers 0.000 description 2
- 239000000057 synthetic resin Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 229910017682 MgTi Inorganic materials 0.000 description 1
- 238000002441 X-ray diffraction Methods 0.000 description 1
- 239000010425 asbestos Substances 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- TVFDJXOCXUVLDH-UHFFFAOYSA-N caesium atom Chemical compound [Cs] TVFDJXOCXUVLDH-UHFFFAOYSA-N 0.000 description 1
- 239000007795 chemical reaction product Substances 0.000 description 1
- 230000000295 complement effect Effects 0.000 description 1
- 210000003298 dental enamel Anatomy 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 230000017525 heat dissipation Effects 0.000 description 1
- 239000012943 hotmelt Substances 0.000 description 1
- 239000012774 insulation material Substances 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 238000002386 leaching Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- INHCSSUBVCNVSK-UHFFFAOYSA-L lithium sulfate Inorganic materials [Li+].[Li+].[O-]S([O-])(=O)=O INHCSSUBVCNVSK-UHFFFAOYSA-L 0.000 description 1
- 239000000314 lubricant Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 230000035515 penetration Effects 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- CHWRSCGUEQEHOH-UHFFFAOYSA-N potassium oxide Chemical compound [O-2].[K+].[K+] CHWRSCGUEQEHOH-UHFFFAOYSA-N 0.000 description 1
- 229910001950 potassium oxide Inorganic materials 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000012744 reinforcing agent Substances 0.000 description 1
- 239000012779 reinforcing material Substances 0.000 description 1
- 229910052895 riebeckite Inorganic materials 0.000 description 1
- IGLNJRXAVVLDKE-UHFFFAOYSA-N rubidium atom Chemical compound [Rb] IGLNJRXAVVLDKE-UHFFFAOYSA-N 0.000 description 1
- 229910000344 rubidium sulfate Inorganic materials 0.000 description 1
- GANPIEKBSASAOC-UHFFFAOYSA-L rubidium(1+);sulfate Chemical compound [Rb+].[Rb+].[O-]S([O-])(=O)=O GANPIEKBSASAOC-UHFFFAOYSA-L 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
- C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
- C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/622—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
- C04B35/62227—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres
- C04B35/62231—Forming processes; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products obtaining fibres based on oxide ceramics
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01G—COMPOUNDS CONTAINING METALS NOT COVERED BY SUBCLASSES C01D OR C01F
- C01G23/00—Compounds of titanium
- C01G23/003—Titanates
- C01G23/005—Alkali titanates
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/10—Particle morphology extending in one dimension, e.g. needle-like
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/54—Particles characterised by their aspect ratio, i.e. the ratio of sizes in the longest to the shortest dimension
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01P—INDEXING SCHEME RELATING TO STRUCTURAL AND PHYSICAL ASPECTS OF SOLID INORGANIC COMPOUNDS
- C01P2004/00—Particle morphology
- C01P2004/60—Particles characterised by their size
- C01P2004/61—Micrometer sized, i.e. from 1-100 micrometer
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Ceramic Engineering (AREA)
- Inorganic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Geology (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Environmental & Geological Engineering (AREA)
- Life Sciences & Earth Sciences (AREA)
- Materials Engineering (AREA)
- Structural Engineering (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
Priority Applications (10)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19702015401 DE2015401A1 (de) | 1970-04-01 | 1970-04-01 | Verfahren zur Herstellung faserförmiger Alkalihexatitanate |
| US00127414A US3760068A (en) | 1970-04-01 | 1971-03-23 | Production of fibrous alkali metal hexatitanates |
| AT260171A AT305210B (de) | 1970-04-01 | 1971-03-26 | Verfahren zur Herstellung faserförmiger Alkalihexatitanate |
| AU27085/71A AU2708571A (en) | 1970-03-31 | 1971-03-29 | Production of fibrous alkali metal hexatitanates |
| ZA712001A ZA712001B (en) | 1970-04-01 | 1971-03-29 | Production of fibrous alkali metal hexatitanates |
| SU1638607A SU367593A3 (enExample) | 1970-04-01 | 1971-03-31 | |
| NL7104308A NL7104308A (enExample) | 1970-04-01 | 1971-03-31 | |
| FR7111549A FR2085771A1 (fr) | 1970-04-01 | 1971-04-01 | Procede de preparation d'hexatitanates alcalins fibreux |
| BE765169A BE765169A (fr) | 1970-04-01 | 1971-04-01 | Procede de preparation d'hexatitanates alcalins fibreux |
| GB2585071*A GB1309706A (en) | 1970-04-01 | 1971-04-19 | Process for the production of fibrous alkali metal hexatitanates |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19702015401 DE2015401A1 (de) | 1970-04-01 | 1970-04-01 | Verfahren zur Herstellung faserförmiger Alkalihexatitanate |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2015401A1 true DE2015401A1 (de) | 1971-10-21 |
Family
ID=5766763
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19702015401 Pending DE2015401A1 (de) | 1970-03-31 | 1970-04-01 | Verfahren zur Herstellung faserförmiger Alkalihexatitanate |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3760068A (enExample) |
| AT (1) | AT305210B (enExample) |
| AU (1) | AU2708571A (enExample) |
| BE (1) | BE765169A (enExample) |
| DE (1) | DE2015401A1 (enExample) |
| FR (1) | FR2085771A1 (enExample) |
| GB (1) | GB1309706A (enExample) |
| NL (1) | NL7104308A (enExample) |
| SU (1) | SU367593A3 (enExample) |
| ZA (1) | ZA712001B (enExample) |
Families Citing this family (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS516200A (en) * | 1974-07-05 | 1976-01-19 | Central Glass Co Ltd | Kaatsukadatsusuihonyoru chitansankarisenino seizohoho |
| US3952090A (en) * | 1974-10-23 | 1976-04-20 | Matsushita Electric Industrial Co., Ltd. | Method of making fibrous alkali titanates |
| JPS5943440B2 (ja) * | 1975-02-05 | 1984-10-22 | 松下電器産業株式会社 | アルカリチタネイト繊維材の製造方法 |
| JPS51122700A (en) * | 1975-03-20 | 1976-10-26 | Natl Inst For Res In Inorg Mater | Process for production of fiberous alkali metal titanate |
| US4152281A (en) * | 1978-04-17 | 1979-05-01 | General Electric Company | Molten salt synthesis of lead zirconate titanate solid solution powder |
| US4152280A (en) * | 1978-04-17 | 1979-05-01 | General Electric Company | Molten salt synthesis of modified lead zirconate titanate solid solution powder |
| JPH01301516A (ja) * | 1987-12-25 | 1989-12-05 | Titan Kogyo Kk | トンネル構造・六チタン酸カリウム繊維，その製造方法及びそれを含む複合材料 |
| RU2326051C1 (ru) * | 2006-08-11 | 2008-06-10 | Александр Владиленович Гороховский | Способ получения титаната калия |
| JP6706615B2 (ja) * | 2015-06-02 | 2020-06-10 | 東邦チタニウム株式会社 | チタン酸アルカリおよび摩擦材 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2370443A (en) * | 1936-12-28 | 1945-02-27 | Biefeld Karl | Nonmetallic electric resistance material and process for producing same |
| US2841470A (en) * | 1956-05-18 | 1958-07-01 | Du Pont | Process for preparing fibrous and waterinsoluble alkali metal titanates and new fibrous crystalline alkali metal tetratitanates obtained thereby |
-
1970
- 1970-04-01 DE DE19702015401 patent/DE2015401A1/de active Pending
-
1971
- 1971-03-23 US US00127414A patent/US3760068A/en not_active Expired - Lifetime
- 1971-03-26 AT AT260171A patent/AT305210B/de not_active IP Right Cessation
- 1971-03-29 ZA ZA712001A patent/ZA712001B/xx unknown
- 1971-03-29 AU AU27085/71A patent/AU2708571A/en not_active Expired
- 1971-03-31 SU SU1638607A patent/SU367593A3/ru active
- 1971-03-31 NL NL7104308A patent/NL7104308A/xx unknown
- 1971-04-01 FR FR7111549A patent/FR2085771A1/fr not_active Withdrawn
- 1971-04-01 BE BE765169A patent/BE765169A/xx unknown
- 1971-04-19 GB GB2585071*A patent/GB1309706A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| SU367593A3 (enExample) | 1973-01-23 |
| AU2708571A (en) | 1972-10-05 |
| US3760068A (en) | 1973-09-18 |
| AT305210B (de) | 1973-02-12 |
| ZA712001B (en) | 1971-12-29 |
| NL7104308A (enExample) | 1971-10-05 |
| BE765169A (fr) | 1971-10-01 |
| GB1309706A (en) | 1973-03-14 |
| FR2085771A1 (fr) | 1971-12-31 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| EP0807086B1 (de) | Verfahren zur herstellung von hydrotalciten | |
| DE68907731T2 (de) | Verfahren zur Herstellung von kristallinen gemischten Metalloxiden. | |
| DE2707229C2 (de) | Herstellung von Zink- und Erdalkalititanaten | |
| DE2015401A1 (de) | Verfahren zur Herstellung faserförmiger Alkalihexatitanate | |
| DE1165563B (de) | Verfahren zum Aufschluss von Ilmenit mit Salzsaeure | |
| DE3006262C2 (de) | Verfahren zur Herstellung von fasrigen Titansäure-Metallsalzen | |
| DE2233037A1 (de) | Metalloxidfasern | |
| DE1069884B (de) | Verfahren zur Herstellung von Titan | |
| DE2529961C3 (de) | Verfahren zur Herstellung von fasrigem Kaliumtitanat | |
| DE1467352A1 (de) | Verfahren zur Aufarbeitung von kieselerdehaltigen Zirkonerzen auf Zirkon | |
| US3755553A (en) | Method of producing salts of alkaline earth metals | |
| DE2133466A1 (de) | Verfahren zur Herstellung von kristallinem Zinkborat mit geringem Hydratwassergehalt | |
| DE2650012C2 (de) | Verfahren zur Aufarbeitung von Rückständen einer Chromatproduktion | |
| DE2517292A1 (de) | Verfahren zur herstellung von galliumoxid | |
| DE619568C (de) | Herstellung von Alkalititanaten | |
| EP0704408A1 (de) | Verfahren und Vorrichtungen zur Herstellung von Bismutoxid und Bismutlegierungsoxiden | |
| DE2835542A1 (de) | Verfahren zur herstellung von wasserfreien alkalichloroferraten (ii, iii) | |
| DE610117C (de) | Verfahren zur Herstellung von Alkalititanaten der Zusammensetzung M Ti O | |
| DE2037963A1 (de) | Anorganische Fasern | |
| AT223583B (de) | Verfahen zur Herstellung von Doppelsalzen des Niob- und bzw. oder Tantalpentachlorids mit Kaliumchlorid oder- fluorid | |
| DE1047183B (de) | Verfahren zur Herstellung faseriger, wasserunloeslicher Alkalititanate der Zusammensetzung M2Ti4O9 oder M2Ti6O13 | |
| US3424555A (en) | Process for converting alkali metal titanates into their pure titanium dioxide pseudomorphs | |
| DE1155103B (de) | Verfahren zur Herstellung von pulverfoermigem kristallinem Molybdaendisulfid und/oder Wolframdisulfid | |
| AT44772B (de) | Verfahren zur Aufbereitung der aus Pyriten und dergleichen erhaltenen zink- und kobalthältigen Lösungen. | |
| DE1583882C3 (de) | Verfahren zur Herstellung von metallischem Cäsium |