DE2004405A1 - Verfahren zur Herstellung von 1,3 Propylendiaminen und Di (1,3 propylen) triaminen - Google Patents
Verfahren zur Herstellung von 1,3 Propylendiaminen und Di (1,3 propylen) triaminenInfo
- Publication number
- DE2004405A1 DE2004405A1 DE19702004405 DE2004405A DE2004405A1 DE 2004405 A1 DE2004405 A1 DE 2004405A1 DE 19702004405 DE19702004405 DE 19702004405 DE 2004405 A DE2004405 A DE 2004405A DE 2004405 A1 DE2004405 A1 DE 2004405A1
- Authority
- DE
- Germany
- Prior art keywords
- propylene
- acrylonitrile
- propylenediamines
- triamines
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 9
- XFNJVJPLKCPIBV-UHFFFAOYSA-N trimethylenediamine Chemical class NCCCN XFNJVJPLKCPIBV-UHFFFAOYSA-N 0.000 title claims description 6
- -1 1,3 propylene Chemical group 0.000 title claims description 4
- 238000002360 preparation method Methods 0.000 title claims description 4
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 11
- NLHHRLWOUZZQLW-UHFFFAOYSA-N Acrylonitrile Chemical compound C=CC#N NLHHRLWOUZZQLW-UHFFFAOYSA-N 0.000 claims description 9
- 150000001412 amines Chemical class 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 238000005984 hydrogenation reaction Methods 0.000 claims description 5
- 229910052739 hydrogen Inorganic materials 0.000 claims description 4
- 239000001257 hydrogen Substances 0.000 claims description 4
- 150000008362 aminopropionitriles Chemical class 0.000 claims description 2
- 125000004432 carbon atom Chemical group C* 0.000 claims description 2
- 239000003795 chemical substances by application Substances 0.000 claims description 2
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 8
- WGYKZJWCGVVSQN-UHFFFAOYSA-N propylamine Chemical compound CCCN WGYKZJWCGVVSQN-UHFFFAOYSA-N 0.000 description 5
- BAVYZALUXZFZLV-UHFFFAOYSA-N Methylamine Chemical compound NC BAVYZALUXZFZLV-UHFFFAOYSA-N 0.000 description 4
- 229910021529 ammonia Inorganic materials 0.000 description 4
- 229910017052 cobalt Inorganic materials 0.000 description 3
- 239000010941 cobalt Substances 0.000 description 3
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 3
- 150000001875 compounds Chemical class 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- 239000003054 catalyst Substances 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 238000004519 manufacturing process Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- AGSPXMVUFBBBMO-UHFFFAOYSA-N beta-aminopropionitrile Chemical compound NCCC#N AGSPXMVUFBBBMO-UHFFFAOYSA-N 0.000 description 1
- 229910052799 carbon Inorganic materials 0.000 description 1
- 239000007859 condensation product Substances 0.000 description 1
- 150000004985 diamines Chemical class 0.000 description 1
- GKQPCPXONLDCMU-CCEZHUSRSA-N lacidipine Chemical compound CCOC(=O)C1=C(C)NC(C)=C(C(=O)OCC)C1C1=CC=CC=C1\C=C\C(=O)OC(C)(C)C GKQPCPXONLDCMU-CCEZHUSRSA-N 0.000 description 1
- QHJABUZHRJTCAR-UHFFFAOYSA-N n'-methylpropane-1,3-diamine Chemical compound CNCCCN QHJABUZHRJTCAR-UHFFFAOYSA-N 0.000 description 1
- AOHJOMMDDJHIJH-UHFFFAOYSA-N propylenediamine Chemical compound CC(N)CN AOHJOMMDDJHIJH-UHFFFAOYSA-N 0.000 description 1
- 239000011541 reaction mixture Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000010626 work up procedure Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/60—Preparation of compounds containing amino groups bound to a carbon skeleton by condensation or addition reactions, e.g. Mannich reaction, addition of ammonia or amines to alkenes or to alkynes or addition of compounds containing an active hydrogen atom to Schiff's bases, quinone imines, or aziranes
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/44—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers
- C07C209/48—Preparation of compounds containing amino groups bound to a carbon skeleton by reduction of carboxylic acids or esters thereof in presence of ammonia or amines, or by reduction of nitriles, carboxylic acid amides, imines or imino-ethers by reduction of nitriles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Priority Applications (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19702004405 DE2004405A1 (de) | 1970-01-31 | 1970-01-31 | Verfahren zur Herstellung von 1,3 Propylendiaminen und Di (1,3 propylen) triaminen |
| FR7102822A FR2077091A5 (enExample) | 1970-01-31 | 1971-01-28 | |
| NL7101151A NL7101151A (enExample) | 1970-01-31 | 1971-01-28 | |
| BE762237A BE762237A (fr) | 1970-01-31 | 1971-01-29 | Procede de preparation de 1,3-propylene diamines et de di-(1,3-propylene)-triamines |
| GB2235371A GB1330109A (en) | 1970-01-31 | 1971-04-19 | Manufacture of 1,3-propylene diamines and di-1,3-propylene tri amines |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19702004405 DE2004405A1 (de) | 1970-01-31 | 1970-01-31 | Verfahren zur Herstellung von 1,3 Propylendiaminen und Di (1,3 propylen) triaminen |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE2004405A1 true DE2004405A1 (de) | 1971-08-05 |
Family
ID=5761058
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19702004405 Pending DE2004405A1 (de) | 1970-01-31 | 1970-01-31 | Verfahren zur Herstellung von 1,3 Propylendiaminen und Di (1,3 propylen) triaminen |
Country Status (5)
| Country | Link |
|---|---|
| BE (1) | BE762237A (enExample) |
| DE (1) | DE2004405A1 (enExample) |
| FR (1) | FR2077091A5 (enExample) |
| GB (1) | GB1330109A (enExample) |
| NL (1) | NL7101151A (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3003729A1 (de) * | 1979-02-01 | 1980-08-14 | Suntech | Verfahren zum hydrieren von aliphatischen nitrilen |
| EP0391349A3 (en) * | 1989-04-07 | 1991-05-22 | Air Products And Chemicals, Inc. | Coproduction of propanediamine and alkylated aminopropylamines |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB1551127A (en) * | 1975-09-13 | 1979-08-22 | Basf Ag | Manufacture of polypropylenepolyamines |
| CN101817752B (zh) * | 2010-04-01 | 2012-11-21 | 大连理工大学 | 一种1,3-丙二胺的制备方法 |
-
1970
- 1970-01-31 DE DE19702004405 patent/DE2004405A1/de active Pending
-
1971
- 1971-01-28 FR FR7102822A patent/FR2077091A5/fr not_active Expired
- 1971-01-28 NL NL7101151A patent/NL7101151A/xx unknown
- 1971-01-29 BE BE762237A patent/BE762237A/xx unknown
- 1971-04-19 GB GB2235371A patent/GB1330109A/en not_active Expired
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE3003729A1 (de) * | 1979-02-01 | 1980-08-14 | Suntech | Verfahren zum hydrieren von aliphatischen nitrilen |
| EP0391349A3 (en) * | 1989-04-07 | 1991-05-22 | Air Products And Chemicals, Inc. | Coproduction of propanediamine and alkylated aminopropylamines |
Also Published As
| Publication number | Publication date |
|---|---|
| FR2077091A5 (enExample) | 1971-10-15 |
| NL7101151A (enExample) | 1971-08-03 |
| BE762237A (fr) | 1971-07-29 |
| GB1330109A (en) | 1973-09-12 |
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