DE1917647B2 - Verfahren zur kontinuierlichen herstellung von festem, rieselfoermigem trioxan - Google Patents
Verfahren zur kontinuierlichen herstellung von festem, rieselfoermigem trioxanInfo
- Publication number
- DE1917647B2 DE1917647B2 DE19691917647 DE1917647A DE1917647B2 DE 1917647 B2 DE1917647 B2 DE 1917647B2 DE 19691917647 DE19691917647 DE 19691917647 DE 1917647 A DE1917647 A DE 1917647A DE 1917647 B2 DE1917647 B2 DE 1917647B2
- Authority
- DE
- Germany
- Prior art keywords
- trioxane
- water
- solid
- continuous production
- shaped
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- BGJSXRVXTHVRSN-UHFFFAOYSA-N 1,3,5-trioxane Chemical compound C1OCOCO1 BGJSXRVXTHVRSN-UHFFFAOYSA-N 0.000 title claims description 34
- 238000000034 method Methods 0.000 title claims description 9
- 238000010924 continuous production Methods 0.000 title claims description 3
- 239000007787 solid Substances 0.000 title claims description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
- 238000002425 crystallisation Methods 0.000 description 4
- 230000008025 crystallization Effects 0.000 description 4
- 229910052757 nitrogen Inorganic materials 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 229920000098 polyolefin Polymers 0.000 description 3
- 239000003963 antioxidant agent Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 239000000498 cooling water Substances 0.000 description 2
- 239000013078 crystal Substances 0.000 description 2
- 239000003381 stabilizer Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 150000001412 amines Chemical class 0.000 description 1
- 150000001414 amino alcohols Chemical class 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000002349 favourable effect Effects 0.000 description 1
- 239000011888 foil Substances 0.000 description 1
- 239000007789 gas Substances 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 238000007654 immersion Methods 0.000 description 1
- 239000011261 inert gas Substances 0.000 description 1
- 238000007689 inspection Methods 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000000289 melt material Substances 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 150000002989 phenols Chemical class 0.000 description 1
- 239000012265 solid product Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D323/00—Heterocyclic compounds containing more than two oxygen atoms as the only ring hetero atoms
- C07D323/04—Six-membered rings
- C07D323/06—Trioxane
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J2/00—Processes or devices for granulating materials, e.g. fertilisers in general; Rendering particulate materials free flowing in general, e.g. making them hydrophobic
- B01J2/24—Obtaining flakes by scraping a solid layer from a surface
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Crystallography & Structural Chemistry (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
- Polyoxymethylene Polymers And Polymers With Carbon-To-Carbon Bonds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (6)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19691917647 DE1917647B2 (de) | 1969-04-05 | 1969-04-05 | Verfahren zur kontinuierlichen herstellung von festem, rieselfoermigem trioxan |
| FR7011937A FR2038277A1 (enExample) | 1969-04-05 | 1970-04-02 | |
| NL7004837A NL7004837A (enExample) | 1969-04-05 | 1970-04-03 | |
| US25561A US3689619A (en) | 1969-04-05 | 1970-04-03 | Continuous granulation of trioxane |
| BE748455D BE748455A (fr) | 1969-04-05 | 1970-04-03 | Procede continu pour preparer un trioxanne a l'etat granulaire et capable de s'ecouler librement |
| GB1295131D GB1295131A (enExample) | 1969-04-05 | 1970-04-03 |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19691917647 DE1917647B2 (de) | 1969-04-05 | 1969-04-05 | Verfahren zur kontinuierlichen herstellung von festem, rieselfoermigem trioxan |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE1917647A1 DE1917647A1 (de) | 1970-10-08 |
| DE1917647B2 true DE1917647B2 (de) | 1976-02-05 |
Family
ID=5730483
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19691917647 Withdrawn DE1917647B2 (de) | 1969-04-05 | 1969-04-05 | Verfahren zur kontinuierlichen herstellung von festem, rieselfoermigem trioxan |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US3689619A (enExample) |
| BE (1) | BE748455A (enExample) |
| DE (1) | DE1917647B2 (enExample) |
| FR (1) | FR2038277A1 (enExample) |
| GB (1) | GB1295131A (enExample) |
| NL (1) | NL7004837A (enExample) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH062706B2 (ja) * | 1986-06-24 | 1994-01-12 | 川崎化成工業株式会社 | 1,4,4a,9a−テトラヒドロアントラキノンの成型方法 |
| CN102558137B (zh) * | 2012-01-04 | 2015-02-04 | 上海蓝星聚甲醛有限公司 | 一种三聚甲醛结晶体的加工方法及加工系统 |
| CN114230550B (zh) * | 2021-12-27 | 2023-08-01 | 邢台旭阳科技有限公司 | 制备三聚甲醛结晶产品的方法和系统 |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CA731203A (en) * | 1966-03-29 | Wunder Friedrich | Process for granulating substances from the melt | |
| US2697249A (en) * | 1950-06-09 | 1954-12-21 | Standard Oil Co | Method and apparatus for the manufacture of particulate wax and wax objects |
-
1969
- 1969-04-05 DE DE19691917647 patent/DE1917647B2/de not_active Withdrawn
-
1970
- 1970-04-02 FR FR7011937A patent/FR2038277A1/fr not_active Withdrawn
- 1970-04-03 BE BE748455D patent/BE748455A/xx unknown
- 1970-04-03 GB GB1295131D patent/GB1295131A/en not_active Expired
- 1970-04-03 US US25561A patent/US3689619A/en not_active Expired - Lifetime
- 1970-04-03 NL NL7004837A patent/NL7004837A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| FR2038277A1 (enExample) | 1971-01-08 |
| GB1295131A (enExample) | 1972-11-01 |
| NL7004837A (enExample) | 1970-10-07 |
| DE1917647A1 (de) | 1970-10-08 |
| BE748455A (fr) | 1970-10-05 |
| US3689619A (en) | 1972-09-05 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| 8263 | Opposition against grant of a patent | ||
| 8230 | Patent withdrawn |