DE1908099A1 - Graphitischer Kohlenstoff,Verfahren zu seiner Herstellung sowie Kohlenwasserstoff-Trennverfahren - Google Patents
Graphitischer Kohlenstoff,Verfahren zu seiner Herstellung sowie Kohlenwasserstoff-TrennverfahrenInfo
- Publication number
- DE1908099A1 DE1908099A1 DE19691908099 DE1908099A DE1908099A1 DE 1908099 A1 DE1908099 A1 DE 1908099A1 DE 19691908099 DE19691908099 DE 19691908099 DE 1908099 A DE1908099 A DE 1908099A DE 1908099 A1 DE1908099 A1 DE 1908099A1
- Authority
- DE
- Germany
- Prior art keywords
- graphitic carbon
- carbon
- adsorption
- heptane
- heat
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 title claims description 124
- 229910052799 carbon Inorganic materials 0.000 title claims description 90
- 229930195733 hydrocarbon Natural products 0.000 title claims description 46
- 150000002430 hydrocarbons Chemical class 0.000 title claims description 45
- 238000000034 method Methods 0.000 title claims description 27
- 239000004215 Carbon black (E152) Substances 0.000 title claims description 20
- 238000000926 separation method Methods 0.000 title claims description 11
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- IMNFDUFMRHMDMM-UHFFFAOYSA-N N-Heptane Chemical compound CCCCCCC IMNFDUFMRHMDMM-UHFFFAOYSA-N 0.000 claims description 87
- 238000001179 sorption measurement Methods 0.000 claims description 52
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 30
- QHMGJGNTMQDRQA-UHFFFAOYSA-N dotriacontane Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCC QHMGJGNTMQDRQA-UHFFFAOYSA-N 0.000 claims description 23
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 22
- 239000002904 solvent Substances 0.000 claims description 21
- 239000002002 slurry Substances 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 12
- 239000001257 hydrogen Substances 0.000 claims description 11
- 229910052739 hydrogen Inorganic materials 0.000 claims description 11
- 229910052760 oxygen Inorganic materials 0.000 claims description 11
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 10
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 10
- 238000010438 heat treatment Methods 0.000 claims description 10
- 239000001301 oxygen Substances 0.000 claims description 10
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 9
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 claims description 9
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 claims description 9
- 238000011282 treatment Methods 0.000 claims description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 7
- 229910052717 sulfur Inorganic materials 0.000 claims description 7
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 6
- 238000002485 combustion reaction Methods 0.000 claims description 6
- 239000011593 sulfur Substances 0.000 claims description 6
- JXTPJDDICSTXJX-UHFFFAOYSA-N triacontane Chemical compound CCCCCCCCCCCCCCCCCCCCCCCCCCCCCC JXTPJDDICSTXJX-UHFFFAOYSA-N 0.000 claims description 6
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 claims description 5
- 150000004945 aromatic hydrocarbons Chemical class 0.000 claims description 5
- 238000006243 chemical reaction Methods 0.000 claims description 5
- 239000007789 gas Substances 0.000 claims description 5
- -1 n ~ H © xane Chemical compound 0.000 claims description 5
- 229910052757 nitrogen Inorganic materials 0.000 claims description 5
- 150000001298 alcohols Chemical class 0.000 claims description 3
- YDLYQMBWCWFRAI-UHFFFAOYSA-N n-Hexatriacontane Natural products CCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCCC YDLYQMBWCWFRAI-UHFFFAOYSA-N 0.000 claims description 3
- OLTHARGIAFTREU-UHFFFAOYSA-N triacontane Natural products CCCCCCCCCCCCCCCCCCCCC(C)CCCCCCCC OLTHARGIAFTREU-UHFFFAOYSA-N 0.000 claims description 3
- 238000010992 reflux Methods 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims description 2
- 239000008346 aqueous phase Substances 0.000 claims 1
- 239000012071 phase Substances 0.000 claims 1
- 238000005406 washing Methods 0.000 claims 1
- 239000010439 graphite Substances 0.000 description 35
- 229910002804 graphite Inorganic materials 0.000 description 35
- 239000000463 material Substances 0.000 description 27
- 239000000047 product Substances 0.000 description 27
- 239000007788 liquid Substances 0.000 description 17
- 239000003921 oil Substances 0.000 description 14
- 238000003795 desorption Methods 0.000 description 10
- 239000001993 wax Substances 0.000 description 9
- 238000009835 boiling Methods 0.000 description 8
- 150000001875 compounds Chemical class 0.000 description 6
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 6
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 5
- 125000003118 aryl group Chemical group 0.000 description 5
- 239000013078 crystal Substances 0.000 description 5
- 239000012188 paraffin wax Substances 0.000 description 5
- XKRFYHLGVUSROY-UHFFFAOYSA-N Argon Chemical compound [Ar] XKRFYHLGVUSROY-UHFFFAOYSA-N 0.000 description 4
- NHTMVDHEPJAVLT-UHFFFAOYSA-N Isooctane Chemical compound CC(C)CC(C)(C)C NHTMVDHEPJAVLT-UHFFFAOYSA-N 0.000 description 4
- 239000003575 carbonaceous material Substances 0.000 description 4
- JVSWJIKNEAIKJW-UHFFFAOYSA-N dimethyl-hexane Natural products CCCCCC(C)C JVSWJIKNEAIKJW-UHFFFAOYSA-N 0.000 description 4
- 239000003925 fat Substances 0.000 description 3
- 239000010687 lubricating oil Substances 0.000 description 3
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 3
- 239000002245 particle Substances 0.000 description 3
- 239000003208 petroleum Substances 0.000 description 3
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 description 2
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 2
- 239000003463 adsorbent Substances 0.000 description 2
- 230000001476 alcoholic effect Effects 0.000 description 2
- 229910052786 argon Inorganic materials 0.000 description 2
- 150000001491 aromatic compounds Chemical class 0.000 description 2
- 125000004429 atom Chemical group 0.000 description 2
- 239000002199 base oil Substances 0.000 description 2
- 239000006229 carbon black Substances 0.000 description 2
- 235000019241 carbon black Nutrition 0.000 description 2
- 229910002092 carbon dioxide Inorganic materials 0.000 description 2
- 239000001569 carbon dioxide Substances 0.000 description 2
- 239000010779 crude oil Substances 0.000 description 2
- 238000010828 elution Methods 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- HYBBIBNJHNGZAN-UHFFFAOYSA-N furfural Chemical compound O=CC1=CC=CO1 HYBBIBNJHNGZAN-UHFFFAOYSA-N 0.000 description 2
- 238000000227 grinding Methods 0.000 description 2
- 238000011068 loading method Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- HIXDQWDOVZUNNA-UHFFFAOYSA-N 2-(3,4-dimethoxyphenyl)-5-hydroxy-7-methoxychromen-4-one Chemical compound C=1C(OC)=CC(O)=C(C(C=2)=O)C=1OC=2C1=CC=C(OC)C(OC)=C1 HIXDQWDOVZUNNA-UHFFFAOYSA-N 0.000 description 1
- 238000004438 BET method Methods 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- 241000557626 Corvus corax Species 0.000 description 1
- 101100258093 Drosophila melanogaster stum gene Proteins 0.000 description 1
- 101100258095 Mus musculus Stum gene Proteins 0.000 description 1
- QBKSWRVVCFFDOT-UHFFFAOYSA-N SJ000286711 Natural products CC(C)C1=C(O)C(O)=C(C=O)C2=C(O)C(C=3C(O)=C4C(C=O)=C(O)C(O)=C(C4=CC=3C)C(C)C)=C(C)C=C21 QBKSWRVVCFFDOT-UHFFFAOYSA-N 0.000 description 1
- WOYYTQHMNDWRCW-JGWLITMVSA-N [(2r,3r,4r,5s)-2,3,4,5-tetrahydroxy-6-phosphonooxyhexyl] dihydrogen phosphate Chemical compound OP(=O)(O)OC[C@H](O)[C@@H](O)[C@H](O)[C@H](O)COP(O)(O)=O WOYYTQHMNDWRCW-JGWLITMVSA-N 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 230000000274 adsorptive effect Effects 0.000 description 1
- 239000003849 aromatic solvent Substances 0.000 description 1
- 239000001273 butane Substances 0.000 description 1
- 125000004432 carbon atom Chemical group C* 0.000 description 1
- 229910002091 carbon monoxide Inorganic materials 0.000 description 1
- 229910002090 carbon oxide Inorganic materials 0.000 description 1
- 239000003245 coal Substances 0.000 description 1
- 239000000567 combustion gas Substances 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- RTZKZFJDLAIYFH-UHFFFAOYSA-N ether Substances CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 1
- 150000002431 hydrogen Chemical class 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 230000002262 irrigation Effects 0.000 description 1
- 238000003973 irrigation Methods 0.000 description 1
- 238000004452 microanalysis Methods 0.000 description 1
- 238000001000 micrograph Methods 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 1
- 239000012454 non-polar solvent Substances 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 238000002336 sorption--desorption measurement Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B32/00—Carbon; Compounds thereof
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Carbon And Carbon Compounds (AREA)
- Treatment Of Liquids With Adsorbents In General (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Electroplating And Plating Baths Therefor (AREA)
- Solid-Sorbent Or Filter-Aiding Compositions (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB817468 | 1968-02-20 | ||
| GB8176/68A GB1261712A (en) | 1968-02-20 | 1968-02-20 | Separation of hydrocarbons using a graphitic carbon |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1908099A1 true DE1908099A1 (de) | 1969-10-09 |
Family
ID=26242006
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19691908099 Pending DE1908099A1 (de) | 1968-02-20 | 1969-02-19 | Graphitischer Kohlenstoff,Verfahren zu seiner Herstellung sowie Kohlenwasserstoff-Trennverfahren |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US3769199A (en, 2012) |
| AT (2) | AT306207B (en, 2012) |
| BE (1) | BE728704A (en, 2012) |
| CA (1) | CA935384A (en, 2012) |
| CH (1) | CH528443A (en, 2012) |
| DE (1) | DE1908099A1 (en, 2012) |
| FR (1) | FR2002260A1 (en, 2012) |
| IE (1) | IE33369B1 (en, 2012) |
| NL (1) | NL6902573A (en, 2012) |
| NO (1) | NO126918B (en, 2012) |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3855117A (en) * | 1970-12-14 | 1974-12-17 | British Petroleum Co | Graphite pellets |
| US3862026A (en) * | 1971-09-28 | 1975-01-21 | Gordon Charles Friend | Adsorption of n-paraffins with graphite-alumina pellets |
| US3965004A (en) * | 1972-11-10 | 1976-06-22 | Sun Shipbuilding & Drydock Company | Removal of contaminants from water |
| US5282975A (en) * | 1989-12-25 | 1994-02-01 | Technion Research And Development Foundation Ltd. | Removal of oil from water |
-
1969
- 1969-02-12 IE IE183/69A patent/IE33369B1/xx unknown
- 1969-02-13 CA CA042796A patent/CA935384A/en not_active Expired
- 1969-02-13 NO NO00582/69A patent/NO126918B/no unknown
- 1969-02-17 CH CH236569A patent/CH528443A/de not_active IP Right Cessation
- 1969-02-19 DE DE19691908099 patent/DE1908099A1/de active Pending
- 1969-02-19 FR FR6904218A patent/FR2002260A1/fr not_active Withdrawn
- 1969-02-19 NL NL6902573A patent/NL6902573A/xx unknown
- 1969-02-19 AT AT693970A patent/AT306207B/de not_active IP Right Cessation
- 1969-02-19 AT AT165369A patent/AT299123B/de not_active IP Right Cessation
- 1969-02-20 BE BE728704D patent/BE728704A/xx unknown
-
1971
- 1971-06-23 US US00156073A patent/US3769199A/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| AT306207B (de) | 1973-03-26 |
| US3769199A (en) | 1973-10-30 |
| BE728704A (en, 2012) | 1969-08-20 |
| AT299123B (de) | 1972-06-12 |
| IE33369B1 (en) | 1974-06-12 |
| CA935384A (en) | 1973-10-16 |
| CH528443A (de) | 1972-09-30 |
| FR2002260A1 (en, 2012) | 1969-10-17 |
| NO126918B (en, 2012) | 1973-04-09 |
| NL6902573A (en, 2012) | 1969-08-22 |
| IE33369L (en) | 1969-08-20 |
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