DE1618441C3 - Verfahren zur Herstellung von 2-lso-cyanato-2-methyl-propansulfonsäurechlorid - Google Patents
Verfahren zur Herstellung von 2-lso-cyanato-2-methyl-propansulfonsäurechloridInfo
- Publication number
- DE1618441C3 DE1618441C3 DE1618441A DE1618441A DE1618441C3 DE 1618441 C3 DE1618441 C3 DE 1618441C3 DE 1618441 A DE1618441 A DE 1618441A DE 1618441 A DE1618441 A DE 1618441A DE 1618441 C3 DE1618441 C3 DE 1618441C3
- Authority
- DE
- Germany
- Prior art keywords
- chloride
- methyl
- acid chloride
- preparation
- iso
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 238000000034 method Methods 0.000 title claims description 7
- 238000002360 preparation method Methods 0.000 title description 3
- QPJDMGCKMHUXFD-UHFFFAOYSA-N cyanogen chloride Chemical compound ClC#N QPJDMGCKMHUXFD-UHFFFAOYSA-N 0.000 claims description 11
- AKEJUJNQAAGONA-UHFFFAOYSA-N sulfur trioxide Chemical compound O=S(=O)=O AKEJUJNQAAGONA-UHFFFAOYSA-N 0.000 claims description 10
- VQTUBCCKSQIDNK-UHFFFAOYSA-N Isobutene Chemical group CC(C)=C VQTUBCCKSQIDNK-UHFFFAOYSA-N 0.000 claims description 7
- HVXDQMXCBWOKGQ-UHFFFAOYSA-N 2-isocyanato-2-methylpropane-1-sulfonyl chloride Chemical compound ClS(=O)(=O)CC(C)(C)N=C=O HVXDQMXCBWOKGQ-UHFFFAOYSA-N 0.000 claims description 5
- XTHPWXDJESJLNJ-UHFFFAOYSA-N chlorosulfonic acid Substances OS(Cl)(=O)=O XTHPWXDJESJLNJ-UHFFFAOYSA-N 0.000 claims description 5
- 239000011541 reaction mixture Substances 0.000 claims description 5
- KEQGZUUPPQEDPF-UHFFFAOYSA-N 1,3-dichloro-5,5-dimethylimidazolidine-2,4-dione Chemical compound CC1(C)N(Cl)C(=O)N(Cl)C1=O KEQGZUUPPQEDPF-UHFFFAOYSA-N 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 2
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 12
- 150000001875 compounds Chemical class 0.000 description 3
- 238000001816 cooling Methods 0.000 description 3
- 229910052739 hydrogen Inorganic materials 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- RAHZWNYVWXNFOC-UHFFFAOYSA-N Sulphur dioxide Chemical compound O=S=O RAHZWNYVWXNFOC-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 2
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 2
- 239000012442 inert solvent Substances 0.000 description 2
- 238000003756 stirring Methods 0.000 description 2
- 229910052717 sulfur Inorganic materials 0.000 description 2
- 238000005292 vacuum distillation Methods 0.000 description 2
- NGNBDVOYPDDBFK-UHFFFAOYSA-N 2-[2,4-di(pentan-2-yl)phenoxy]acetyl chloride Chemical compound CCCC(C)C1=CC=C(OCC(Cl)=O)C(C(C)CCC)=C1 NGNBDVOYPDDBFK-UHFFFAOYSA-N 0.000 description 1
- -1 2-isocyanato-2-methylpropansulfonsäurechlorid Chemical compound 0.000 description 1
- GLLIPPRGASTLQN-UHFFFAOYSA-N Cl.OS(Cl)(=O)=O Chemical compound Cl.OS(Cl)(=O)=O GLLIPPRGASTLQN-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 150000001805 chlorine compounds Chemical class 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 239000012948 isocyanate Substances 0.000 description 1
- 150000002513 isocyanates Chemical class 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 229920002635 polyurethane Polymers 0.000 description 1
- 239000004814 polyurethane Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000004753 textile Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G18/00—Polymeric products of isocyanates or isothiocyanates
- C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
- C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
- C08G18/71—Monoisocyanates or monoisothiocyanates
- C08G18/715—Monoisocyanates or monoisothiocyanates containing sulfur in addition to isothiocyanate sulfur
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D291/00—Heterocyclic compounds containing rings having nitrogen, oxygen and sulfur atoms as the only ring hetero atoms
- C07D291/02—Heterocyclic compounds containing rings having nitrogen, oxygen and sulfur atoms as the only ring hetero atoms not condensed with other rings
- C07D291/06—Six-membered rings
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF0052748 | 1967-06-21 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| DE1618441A1 DE1618441A1 (de) | 1970-10-29 |
| DE1618441B2 DE1618441B2 (cg-RX-API-DMAC10.html) | 1974-07-18 |
| DE1618441C3 true DE1618441C3 (de) | 1975-05-07 |
Family
ID=7105702
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE1618441A Expired DE1618441C3 (de) | 1967-06-21 | 1967-06-21 | Verfahren zur Herstellung von 2-lso-cyanato-2-methyl-propansulfonsäurechlorid |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US3580942A (cg-RX-API-DMAC10.html) |
| BE (1) | BE716688A (cg-RX-API-DMAC10.html) |
| CH (1) | CH499500A (cg-RX-API-DMAC10.html) |
| DE (1) | DE1618441C3 (cg-RX-API-DMAC10.html) |
| FR (1) | FR1570995A (cg-RX-API-DMAC10.html) |
| GB (1) | GB1220746A (cg-RX-API-DMAC10.html) |
| NL (1) | NL6808499A (cg-RX-API-DMAC10.html) |
Families Citing this family (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2637114A1 (de) * | 1976-08-18 | 1978-02-23 | Bayer Ag | Verfahren zur herstellung von isocyanaten |
-
1967
- 1967-06-21 DE DE1618441A patent/DE1618441C3/de not_active Expired
-
1968
- 1968-05-13 CH CH705968A patent/CH499500A/de not_active IP Right Cessation
- 1968-05-24 GB GB24882/68A patent/GB1220746A/en not_active Expired
- 1968-06-17 NL NL6808499A patent/NL6808499A/xx unknown
- 1968-06-17 BE BE716688D patent/BE716688A/xx unknown
- 1968-06-18 US US737859A patent/US3580942A/en not_active Expired - Lifetime
- 1968-06-21 FR FR1570995D patent/FR1570995A/fr not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| DE1618441B2 (cg-RX-API-DMAC10.html) | 1974-07-18 |
| US3580942A (en) | 1971-05-25 |
| NL6808499A (cg-RX-API-DMAC10.html) | 1968-12-23 |
| CH499500A (de) | 1970-11-30 |
| GB1220746A (en) | 1971-01-27 |
| FR1570995A (cg-RX-API-DMAC10.html) | 1969-06-13 |
| BE716688A (cg-RX-API-DMAC10.html) | 1968-12-02 |
| DE1618441A1 (de) | 1970-10-29 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE2512514C2 (de) | Verfahren zur Herstellung von aliphatischen Isocyanaten | |
| DE1618441C3 (de) | Verfahren zur Herstellung von 2-lso-cyanato-2-methyl-propansulfonsäurechlorid | |
| DE1668425A1 (de) | Verfahren zur Herstellung von Diorganoantimonacylaten | |
| EP0045425B1 (de) | Verfahren zur Halogenierung von gegebenenfalls substituierten 4-tert.-Butyltoluolen sowie die daraus erhaltenen Gemische aus gegebenenfalls substituierten 4-tert.-Butylbenzalhalogeniden, 4-tert.-Butylbenzylhalogeniden und 4-tert.-Butylbenzotrihalogeniden | |
| DE874313C (de) | Verfahren zur Herstellung von Tetrahydropyranderivaten | |
| DE2231438C3 (de) | Verfahren zur Herstellung von 2-Alkyl-2-formyl-1,3-dithiacy clopentanen bzw. 1,3-dithiacyclohexanen | |
| DE1668005B2 (de) | Verfahren zur Herstellung von Isopropenyl-phenyl-isocyanaten | |
| DE1418334B1 (de) | Verfahren zur Herstellung von 1,2,3,4,7,7-Hexachlorbicyclo[2,2,1]-2,5-heptadien aus Hexachlorcyclopentadien und Acetylen | |
| DE890339C (de) | Verfahren zur Herstellung von symm. 1, 2, 4, 5-Tetrachlorbenzol aus ª€-Heptachlorcyclohexan | |
| DE831240C (de) | Verfahren zur Herstellung von konzentrierter Ameisensaeure und Nitraten aus Formiaten und Salpetersaeure | |
| EP0001276A1 (de) | Verfahren zur Herstellung von Sulfonsäurechloriden | |
| DE1545614C3 (de) | Verfahren zur Herstellung von 2-Oxo-hexahydropyrimidinen | |
| DE946710C (de) | Verfahren zur Herstellung von N-disubstituierten Sulfamidsaeurechloriden | |
| DE2360248C3 (de) | Verfahren zur Herstellung von Estern von Thiolcarbaminsäuren | |
| DE650430C (de) | Verfahren zur Herstellung von Diphenylaetheraldehyd | |
| AT214425B (de) | Verfahren zur Herstellung von N-substituierten Malonimiden und deren Polymeren | |
| DE1795779C3 (de) | 3,4-O-cyclische Sulfite des Lincomycins, von dessen Analogen, 7-Deoxy-7-chlor-Derivaten sowie von deren Isomeren | |
| EP0375920A1 (de) | Verfahren zur Herstellung von gegebenenfalls substituierten Alkyl- oder Alkenylchloriden | |
| DE1024957B (de) | Verfahren zur Herstellung von ª‡, ª‰-Dichlor-ª‰-formylacrylsaeure (Mucochlorsaeure) | |
| AT233551B (de) | Verfahren zur Herstellung chlorsubstituierter Methylisocyaniddichloride | |
| DE1568007C (de) | Verfahren zur Herstellung von 1,1,2,2 Tetrachlor 1,2 bis (p chlorphenyl) athan | |
| DE2619574C3 (de) | Verfahren zur Herstellung von 3-Brompropionsäureamid | |
| DE1183483B (de) | Verfahren zur Herstellung von Fluorsulfonylisocyanat | |
| DE1643341B2 (de) | Verfahren zur Herstellung eines cyclischen Sutfinsäureesters | |
| EP0008445A1 (de) | Verfahren zur Herstellung von Benzoesäureanhydrid |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| E77 | Valid patent as to the heymanns-index 1977 | ||
| EHV | Ceased/renunciation |