DE1592748C3 - Verfahren zur Herstellung eines granulierten Mischdüngemittels - Google Patents
Verfahren zur Herstellung eines granulierten MischdüngemittelsInfo
- Publication number
- DE1592748C3 DE1592748C3 DE1592748A DE1592748A DE1592748C3 DE 1592748 C3 DE1592748 C3 DE 1592748C3 DE 1592748 A DE1592748 A DE 1592748A DE 1592748 A DE1592748 A DE 1592748A DE 1592748 C3 DE1592748 C3 DE 1592748C3
- Authority
- DE
- Germany
- Prior art keywords
- ammonium
- fertilizer
- phosphate
- granulation
- atomic ratio
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired
Links
- 239000003337 fertilizer Substances 0.000 title claims description 31
- 238000000034 method Methods 0.000 title claims description 13
- 238000004519 manufacturing process Methods 0.000 title claims description 6
- 239000007787 solid Substances 0.000 claims description 23
- 239000004254 Ammonium phosphate Substances 0.000 claims description 19
- 235000019289 ammonium phosphates Nutrition 0.000 claims description 19
- MNNHAPBLZZVQHP-UHFFFAOYSA-N diammonium hydrogen phosphate Chemical compound [NH4+].[NH4+].OP([O-])([O-])=O MNNHAPBLZZVQHP-UHFFFAOYSA-N 0.000 claims description 19
- 229910000148 ammonium phosphate Inorganic materials 0.000 claims description 17
- 238000005469 granulation Methods 0.000 claims description 17
- 230000003179 granulation Effects 0.000 claims description 17
- 239000000203 mixture Substances 0.000 claims description 12
- PAWQVTBBRAZDMG-UHFFFAOYSA-N 2-(3-bromo-2-fluorophenyl)acetic acid Chemical compound OC(=O)CC1=CC=CC(Br)=C1F PAWQVTBBRAZDMG-UHFFFAOYSA-N 0.000 claims description 9
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 claims description 9
- 229910052921 ammonium sulfate Inorganic materials 0.000 claims description 9
- 235000011130 ammonium sulphate Nutrition 0.000 claims description 9
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 7
- 239000004202 carbamide Substances 0.000 claims description 7
- 229910052757 nitrogen Inorganic materials 0.000 claims description 7
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 6
- LFVGISIMTYGQHF-UHFFFAOYSA-N ammonium dihydrogen phosphate Chemical compound [NH4+].OP(O)([O-])=O LFVGISIMTYGQHF-UHFFFAOYSA-N 0.000 claims description 6
- 239000008187 granular material Substances 0.000 claims description 6
- 229910000387 ammonium dihydrogen phosphate Inorganic materials 0.000 claims description 5
- 235000019837 monoammonium phosphate Nutrition 0.000 claims description 5
- 239000006012 monoammonium phosphate Substances 0.000 claims description 5
- 238000005550 wet granulation Methods 0.000 claims description 5
- 101000623895 Bos taurus Mucin-15 Proteins 0.000 claims description 4
- 239000000463 material Substances 0.000 claims description 4
- 239000000126 substance Substances 0.000 claims description 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 2
- ZRIUUUJAJJNDSS-UHFFFAOYSA-N ammonium phosphates Chemical class [NH4+].[NH4+].[NH4+].[O-]P([O-])([O-])=O ZRIUUUJAJJNDSS-UHFFFAOYSA-N 0.000 claims description 2
- 229910052700 potassium Inorganic materials 0.000 claims description 2
- 239000011591 potassium Substances 0.000 claims description 2
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims 6
- YYRMJZQKEFZXMX-UHFFFAOYSA-N calcium;phosphoric acid Chemical compound [Ca+2].OP(O)(O)=O.OP(O)(O)=O YYRMJZQKEFZXMX-UHFFFAOYSA-N 0.000 claims 6
- 239000002426 superphosphate Substances 0.000 claims 6
- 229910019142 PO4 Inorganic materials 0.000 claims 5
- 235000021317 phosphate Nutrition 0.000 claims 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims 4
- 235000021049 nutrient content Nutrition 0.000 claims 3
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims 3
- 239000010452 phosphate Substances 0.000 claims 3
- 239000005696 Diammonium phosphate Substances 0.000 claims 2
- 229910000388 diammonium phosphate Inorganic materials 0.000 claims 2
- 235000019838 diammonium phosphate Nutrition 0.000 claims 2
- 238000004090 dissolution Methods 0.000 claims 2
- 150000003013 phosphoric acid derivatives Chemical class 0.000 claims 2
- 239000000047 product Substances 0.000 claims 2
- 229910002651 NO3 Inorganic materials 0.000 claims 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 claims 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 claims 1
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims 1
- 230000002378 acidificating effect Effects 0.000 claims 1
- 230000009418 agronomic effect Effects 0.000 claims 1
- 230000009286 beneficial effect Effects 0.000 claims 1
- 239000007795 chemical reaction product Substances 0.000 claims 1
- 239000002131 composite material Substances 0.000 claims 1
- 239000000470 constituent Substances 0.000 claims 1
- 230000000694 effects Effects 0.000 claims 1
- 230000005484 gravity Effects 0.000 claims 1
- 238000012423 maintenance Methods 0.000 claims 1
- 235000015097 nutrients Nutrition 0.000 claims 1
- 229910052698 phosphorus Inorganic materials 0.000 claims 1
- 239000011574 phosphorus Substances 0.000 claims 1
- 150000003018 phosphorus compounds Chemical class 0.000 claims 1
- 108090000623 proteins and genes Proteins 0.000 claims 1
- 238000009736 wetting Methods 0.000 claims 1
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 description 8
- 239000001103 potassium chloride Substances 0.000 description 4
- 235000011164 potassium chloride Nutrition 0.000 description 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 2
- 238000007792 addition Methods 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 239000002367 phosphate rock Substances 0.000 description 1
- 125000004437 phosphorous atom Chemical group 0.000 description 1
- -1 potassium chloride Chemical compound 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 239000011435 rock Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/38—Condensed phosphates
- C01B25/40—Polyphosphates
- C01B25/405—Polyphosphates of ammonium
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B25/00—Phosphorus; Compounds thereof
- C01B25/16—Oxyacids of phosphorus; Salts thereof
- C01B25/26—Phosphates
- C01B25/28—Ammonium phosphates
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B19/00—Granulation or pelletisation of phosphatic fertilisers, other than slag
-
- C—CHEMISTRY; METALLURGY
- C05—FERTILISERS; MANUFACTURE THEREOF
- C05B—PHOSPHATIC FERTILISERS
- C05B7/00—Fertilisers based essentially on alkali or ammonium orthophosphates
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Fertilizers (AREA)
- Battery Electrode And Active Subsutance (AREA)
- Luminescent Compositions (AREA)
Applications Claiming Priority (5)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| GB32399/61A GB951476A (en) | 1961-09-07 | 1961-09-07 | Manufacture of solid ammonium phosphates |
| GB3239861 | 1961-09-08 | ||
| GB2352362A GB982341A (en) | 1962-06-19 | 1962-06-19 | Improvements in or relating to the production of granular fertilisers comprising monoammonium phosphate |
| GB2352162 | 1962-06-19 | ||
| GB2352262 | 1962-06-19 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| DE1592748A1 DE1592748A1 (de) | 1971-02-04 |
| DE1592748C3 true DE1592748C3 (de) | 1974-08-08 |
Family
ID=27516254
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE1592748A Expired DE1592748C3 (de) | 1961-09-07 | 1962-08-28 | Verfahren zur Herstellung eines granulierten Mischdüngemittels |
| DE19621592749 Withdrawn DE1592749B1 (de) | 1961-09-07 | 1962-09-07 | Kontinuierliches Zweistufenverfahren zur Herstellung eines Ammoniumphosphat enthaltenden festen Duengemittels |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19621592749 Withdrawn DE1592749B1 (de) | 1961-09-07 | 1962-09-07 | Kontinuierliches Zweistufenverfahren zur Herstellung eines Ammoniumphosphat enthaltenden festen Duengemittels |
Country Status (6)
Families Citing this family (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3507641A (en) * | 1966-12-29 | 1970-04-21 | Grace W R & Co | Preparation of slurry fertilizer by acid treatment of phosphate rock and ammoniation |
| US3512942A (en) * | 1967-05-26 | 1970-05-19 | Grace W R & Co | Apparatus for mining and refining phosphorus |
| GB1483739A (en) * | 1974-09-13 | 1977-08-24 | Scottish Agricultural Ltd | Manufacture of solid ammonium phosphate |
| GB1483853A (en) * | 1975-01-30 | 1977-08-24 | Scottish Agricultural Ind Ltd | Manufacture of solid ammonium phosphate |
| US4009245A (en) * | 1975-02-28 | 1977-02-22 | United States Steel Corporation | Process for the manufacture of monoammonium phosphate |
| US4081266A (en) * | 1975-12-22 | 1978-03-28 | Agrico Chemical Company | Stable fluid suspension fertilizer composition and method for producing same |
Family Cites Families (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1822040A (en) * | 1928-07-16 | 1931-09-08 | Swann Res Inc | Process for manufacture of di-ammonium phosphate |
| US1999926A (en) * | 1934-08-14 | 1935-04-30 | Garzia Joseph | Spaghetti and macaroni machine |
| US2136793A (en) * | 1935-12-11 | 1938-11-15 | Davison Chemical Corp | Treatment of superphosphate |
| US2287759A (en) * | 1940-03-15 | 1942-06-23 | Henry A Wallace | Process for the granulation of fertilizers |
| US2600253A (en) * | 1949-01-21 | 1952-06-10 | Dorr Co | Fertilizer manufacture |
| US2857262A (en) * | 1952-09-11 | 1958-10-21 | Tennessee Valley Authority | Method of manufacturing fertilizers by evaporating slurries containing fertilizer constituents |
| US2703276A (en) * | 1952-10-18 | 1955-03-01 | Monsanto Chemicals | Soil-conditioning fertilizer |
| DE1051871B (de) * | 1954-04-30 | 1959-03-05 | Dorr Oliver Inc | Kontinuierliches Verfahren zur Herstellung von hochwertigen, frei fliessenden, granulierten Diammoniumphosphatduengemitteln |
| US2902342A (en) * | 1955-01-27 | 1959-09-01 | Jr Bernard J Kerley | Method and apparatus for producing ammonium salts |
| US2965471A (en) * | 1955-04-01 | 1960-12-20 | Swift & Co | Method and apparatus for producing mixed fertilizers |
| US2957763A (en) * | 1957-04-08 | 1960-10-25 | Monsanto Chemicals | Process for producing mixed ammonium nitrate-monoammonium phosphate prills |
| US2946655A (en) * | 1957-08-22 | 1960-07-26 | Koppers Co Inc | Production of diammonium phosphate |
| US2963359A (en) * | 1957-10-23 | 1960-12-06 | Tennessee Corp | Process of manufacturing di-ammonium phosphate |
| US3005696A (en) * | 1957-12-06 | 1961-10-24 | Tennessee Valley Authority | Process for production of ammonium phosphate fertilizers |
| US3053622A (en) * | 1958-05-05 | 1962-09-11 | Int Minerals & Chem Corp | Granular fertilizer |
| US3037855A (en) * | 1958-05-23 | 1962-06-05 | Allied Chem | Process for pebbling by spraying a mixture of ammonium nitrate and ammonium phosphates |
| US3097833A (en) * | 1960-03-18 | 1963-07-16 | Scottish Agricultural Ind Ltd | Rotary reaction kiln |
-
0
- BE BE633834D patent/BE633834A/xx unknown
- BE BE622211D patent/BE622211A/xx unknown
- GB GB951475D patent/GB951475A/en active Active
-
1961
- 1961-09-07 GB GB32399/61A patent/GB951476A/en not_active Expired
-
1962
- 1962-08-04 BR BR142706/62A patent/BR6242706D0/pt unknown
- 1962-08-16 US US217264A patent/US3186827A/en not_active Expired - Lifetime
- 1962-08-17 US US217539A patent/US3226184A/en not_active Expired - Lifetime
- 1962-08-28 DE DE1592748A patent/DE1592748C3/de not_active Expired
- 1962-09-07 DE DE19621592749 patent/DE1592749B1/de not_active Withdrawn
- 1962-09-07 SE SE9720/62A patent/SE306946B/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE1592748A1 (de) | 1971-02-04 |
| US3186827A (en) | 1965-06-01 |
| US3226184A (en) | 1965-12-28 |
| GB951476A (en) | 1964-03-04 |
| DE1592749B1 (de) | 1971-09-09 |
| BE622211A (US06521211-20030218-C00004.png) | |
| BR6242706D0 (pt) | 1973-06-12 |
| BE633834A (US06521211-20030218-C00004.png) | |
| SE306946B (US06521211-20030218-C00004.png) | 1968-12-16 |
| GB951475A (US06521211-20030218-C00004.png) |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C3 | Grant after two publication steps (3rd publication) | ||
| E77 | Valid patent as to the heymanns-index 1977 | ||
| EHJ | Ceased/non-payment of the annual fee |