DE1592276A1 - Verfahren zur Herstellung tongebundener Molekularsiebe - Google Patents
Verfahren zur Herstellung tongebundener MolekularsiebeInfo
- Publication number
- DE1592276A1 DE1592276A1 DE19651592276 DE1592276A DE1592276A1 DE 1592276 A1 DE1592276 A1 DE 1592276A1 DE 19651592276 DE19651592276 DE 19651592276 DE 1592276 A DE1592276 A DE 1592276A DE 1592276 A1 DE1592276 A1 DE 1592276A1
- Authority
- DE
- Germany
- Prior art keywords
- clay
- molecular sieve
- mixture
- synthesis
- production
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 239000002808 molecular sieve Substances 0.000 title claims description 44
- URGAHOPLAPQHLN-UHFFFAOYSA-N sodium aluminosilicate Chemical compound [Na+].[Al+3].[O-][Si]([O-])=O.[O-][Si]([O-])=O URGAHOPLAPQHLN-UHFFFAOYSA-N 0.000 title claims description 44
- 238000000034 method Methods 0.000 title claims description 38
- 239000004927 clay Substances 0.000 title claims description 34
- 238000004519 manufacturing process Methods 0.000 title claims description 7
- 239000000203 mixture Substances 0.000 claims description 25
- 230000015572 biosynthetic process Effects 0.000 claims description 17
- 238000003786 synthesis reaction Methods 0.000 claims description 17
- 238000002425 crystallisation Methods 0.000 claims description 9
- 230000008025 crystallization Effects 0.000 claims description 9
- 238000005342 ion exchange Methods 0.000 claims description 9
- 238000001035 drying Methods 0.000 claims description 3
- 239000011541 reaction mixture Substances 0.000 claims description 3
- 238000010304 firing Methods 0.000 claims description 2
- 150000002500 ions Chemical class 0.000 claims description 2
- 239000007791 liquid phase Substances 0.000 claims description 2
- 238000005299 abrasion Methods 0.000 description 12
- 238000000465 moulding Methods 0.000 description 11
- HNPSIPDUKPIQMN-UHFFFAOYSA-N dioxosilane;oxo(oxoalumanyloxy)alumane Chemical compound O=[Si]=O.O=[Al]O[Al]=O HNPSIPDUKPIQMN-UHFFFAOYSA-N 0.000 description 9
- 229910021536 Zeolite Inorganic materials 0.000 description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 8
- 239000010457 zeolite Substances 0.000 description 8
- 239000011230 binding agent Substances 0.000 description 6
- 239000000843 powder Substances 0.000 description 6
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 5
- 238000007796 conventional method Methods 0.000 description 5
- 239000012452 mother liquor Substances 0.000 description 5
- 238000012360 testing method Methods 0.000 description 5
- 238000000265 homogenisation Methods 0.000 description 4
- -1 silicic acid ester Chemical class 0.000 description 4
- 229910004298 SiO 2 Inorganic materials 0.000 description 3
- 229910052680 mordenite Inorganic materials 0.000 description 3
- 238000000926 separation method Methods 0.000 description 3
- 239000007787 solid Substances 0.000 description 3
- 238000005406 washing Methods 0.000 description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 2
- 229910000278 bentonite Inorganic materials 0.000 description 2
- 239000000440 bentonite Substances 0.000 description 2
- SVPXDRXYRYOSEX-UHFFFAOYSA-N bentoquatam Chemical compound O.O=[Si]=O.O=[Al]O[Al]=O SVPXDRXYRYOSEX-UHFFFAOYSA-N 0.000 description 2
- 238000005119 centrifugation Methods 0.000 description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 description 2
- NLYAJNPCOHFWQQ-UHFFFAOYSA-N kaolin Chemical compound O.O.O=[Al]O[Si](=O)O[Si](=O)O[Al]=O NLYAJNPCOHFWQQ-UHFFFAOYSA-N 0.000 description 2
- 229910052622 kaolinite Inorganic materials 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 239000011707 mineral Substances 0.000 description 2
- 229910052625 palygorskite Inorganic materials 0.000 description 2
- 229910052573 porcelain Inorganic materials 0.000 description 2
- 235000019353 potassium silicate Nutrition 0.000 description 2
- 229910052709 silver Inorganic materials 0.000 description 2
- 239000004332 silver Substances 0.000 description 2
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 2
- 238000001179 sorption measurement Methods 0.000 description 2
- BHPQYMZQTOCNFJ-UHFFFAOYSA-N Calcium cation Chemical compound [Ca+2] BHPQYMZQTOCNFJ-UHFFFAOYSA-N 0.000 description 1
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 description 1
- 241001122767 Theaceae Species 0.000 description 1
- YTAHJIFKAKIKAV-XNMGPUDCSA-N [(1R)-3-morpholin-4-yl-1-phenylpropyl] N-[(3S)-2-oxo-5-phenyl-1,3-dihydro-1,4-benzodiazepin-3-yl]carbamate Chemical compound O=C1[C@H](N=C(C2=C(N1)C=CC=C2)C1=CC=CC=C1)NC(O[C@H](CCN1CCOCC1)C1=CC=CC=C1)=O YTAHJIFKAKIKAV-XNMGPUDCSA-N 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 230000000996 additive effect Effects 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 229910052782 aluminium Inorganic materials 0.000 description 1
- WNROFYMDJYEPJX-UHFFFAOYSA-K aluminium hydroxide Chemical compound [OH-].[OH-].[OH-].[Al+3] WNROFYMDJYEPJX-UHFFFAOYSA-K 0.000 description 1
- ANBBXQWFNXMHLD-UHFFFAOYSA-N aluminum;sodium;oxygen(2-) Chemical compound [O-2].[O-2].[Na+].[Al+3] ANBBXQWFNXMHLD-UHFFFAOYSA-N 0.000 description 1
- 238000000137 annealing Methods 0.000 description 1
- 229960000892 attapulgite Drugs 0.000 description 1
- 239000011449 brick Substances 0.000 description 1
- 229910001424 calcium ion Inorganic materials 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 238000007596 consolidation process Methods 0.000 description 1
- 238000010908 decantation Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 235000013372 meat Nutrition 0.000 description 1
- 238000003801 milling Methods 0.000 description 1
- 239000008188 pellet Substances 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229910001414 potassium ion Inorganic materials 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 229910052710 silicon Inorganic materials 0.000 description 1
- 239000010703 silicon Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- 229910001388 sodium aluminate Inorganic materials 0.000 description 1
- 238000007711 solidification Methods 0.000 description 1
- 230000008023 solidification Effects 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000009495 sugar coating Methods 0.000 description 1
- 239000000725 suspension Substances 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/16—Alumino-silicates
- B01J20/18—Synthetic zeolitic molecular sieves
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
- B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
- B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
- B01J20/16—Alumino-silicates
- B01J20/18—Synthetic zeolitic molecular sieves
- B01J20/183—Physical conditioning without chemical treatment, e.g. drying, granulating, coating, irradiation
Landscapes
- Chemical & Material Sciences (AREA)
- Inorganic Chemistry (AREA)
- Analytical Chemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Silicates, Zeolites, And Molecular Sieves (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEV0029957 | 1965-12-17 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1592276A1 true DE1592276A1 (de) | 1970-12-03 |
Family
ID=7585290
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DE19651592276 Pending DE1592276A1 (de) | 1965-12-17 | 1965-12-17 | Verfahren zur Herstellung tongebundener Molekularsiebe |
Country Status (3)
| Country | Link |
|---|---|
| DE (1) | DE1592276A1 (enExample) |
| GB (1) | GB1139405A (enExample) |
| NL (1) | NL6600156A (enExample) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB8334610D0 (en) * | 1983-12-30 | 1984-02-08 | Bp Chem Int Ltd | Selective absorption of carbon monoxide on zeolites |
| JP3078850B2 (ja) * | 1990-12-28 | 2000-08-21 | 日揮ユニバーサル株式会社 | ゼオライト含有吸着組成物およびこの吸着組成物を含む吸着分解組成物 |
| US5616170A (en) * | 1995-08-11 | 1997-04-01 | The Boc Group, Inc. | Adsorptive separation of nitrogen from other gases |
| CN114130422B (zh) * | 2021-11-29 | 2024-04-12 | 江西省杰夫环保科技有限公司 | 一种深度脱氧银x分子筛净化剂的制备方法 |
| CN116637588A (zh) * | 2023-05-08 | 2023-08-25 | 江西萍乡市成宇陶瓷有限责任公司 | 一种高强度强吸附的沸石分子筛的制备方法 |
-
1965
- 1965-12-17 DE DE19651592276 patent/DE1592276A1/de active Pending
-
1966
- 1966-01-06 NL NL6600156A patent/NL6600156A/xx unknown
- 1966-03-01 GB GB894866A patent/GB1139405A/en not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| NL6600156A (enExample) | 1967-07-07 |
| GB1139405A (en) | 1969-01-08 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| DE1951907C3 (de) | Verfahren zur Herstellung eines zeolithischen Alumosilikats mit Faujasitstruktur | |
| DE69812872T2 (de) | Verfahren zur herstellung granulierter körper aus zeolith lsx mit einem geringen inerten bindemittegehalt | |
| DE69604377T2 (de) | Synthetischer ton für keramik und verfahren zu seiner herstellung | |
| US4818508A (en) | Process for preparing molecular sieve bodies | |
| DE60303500T2 (de) | Herstellung eines kristallinen, zeolithischen aluminosilikats des mfi-typs | |
| EP0102544B1 (de) | Verfahren zur Herstellung von harten, bruchfesten Katalysatoren aus Zeolith-Pulver | |
| DE2119723A1 (de) | Kristalline Zeolithe und Ver fahren zu deren Herstellung | |
| DE60005370T2 (de) | Mit aluminosilikat stabilisierte halogenierte polymere | |
| US2992068A (en) | Method for making synthetic zeolitic material | |
| DE2317454A1 (de) | Verfahren zur herstellung von aus vielen anorganischen grundteilchen zusammengesetzten mikroteilchen | |
| DE2446974A1 (de) | Verfahren zur herstellung von zeolith x-molekularsiebkoerpern | |
| DE1237992B (de) | Verfahren zur Herstellung von in Kieselsaeuregel oder Kieselsaeure-Metalloxyd-Mischgel eingebetteten kristallinen Aluminosilicat-Zeolithen | |
| DE4310792A1 (de) | Zeolithisches Material, Verfahren zur Regenerierung eines Katalysators für Crackverfahren sowie Verfahren zur Bereitstellung eines zeolithhaltigen Materials | |
| DE2205254A1 (de) | Verfahren zum Modifizieren von Tonen | |
| DE68912556T2 (de) | Zeolit-granulate mit zeolit-bindemittel. | |
| DE60115358T2 (de) | Geformter Katalysator zur Herstellung von Triethylendiamin, Verfahren zu dessen Herstellung, und Verfahren zur Herstellung von Triethylendiamin | |
| DE2256849A1 (de) | Hochfeste aktive aluminiumoxydformkoerper von niedriger dichte und verfahren zu deren herstellung | |
| DE1542194C3 (de) | Verfahren zur Herstellung eines nicht-kristallinen Kieselsäure Tonerde-Crackkatalysators | |
| DE1592276A1 (de) | Verfahren zur Herstellung tongebundener Molekularsiebe | |
| CH493426A (de) | Verfahren zur Verbesserung der physikalischen Eigenschaften von Alumino-Silikat-Zeolithen und deren Verwendung | |
| DE1545270A1 (de) | Katalysator zur Umwandlung von Kohlenwasserstoffen und Verfahren zur Herstellung derselben | |
| DE1224721B (de) | Verfahren zur Herstellung von geformten Zeolith-A-Koerpern | |
| DE112010004511B4 (de) | Verfahren zum herstellen eines zeoliths vom mtw-typ | |
| DE1567543A1 (de) | Verfahren zur Herstellung von Zeolithkoerpern | |
| AT266791B (de) | Verfahren zur Herstellung tongebundener Molokularsiebe |