DE1518655C3 - Verfahren zur Herstellung von Nitroalkanen - Google Patents

Verfahren zur Herstellung von Nitroalkanen

Info

Publication number
DE1518655C3
DE1518655C3 DE1518655A DE1518655A DE1518655C3 DE 1518655 C3 DE1518655 C3 DE 1518655C3 DE 1518655 A DE1518655 A DE 1518655A DE 1518655 A DE1518655 A DE 1518655A DE 1518655 C3 DE1518655 C3 DE 1518655C3
Authority
DE
Germany
Prior art keywords
nitric acid
reaction
methane
temperature
acid
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired
Application number
DE1518655A
Other languages
German (de)
English (en)
Other versions
DE1518655B2 (de
DE1518655A1 (de
Inventor
Richard S. Egly
Emory E. Toops Jun.
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Commercial Solvents Corp Terre Haute Ind (vsta)
Original Assignee
Commercial Solvents Corp Terre Haute Ind (vsta)
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Commercial Solvents Corp Terre Haute Ind (vsta) filed Critical Commercial Solvents Corp Terre Haute Ind (vsta)
Publication of DE1518655A1 publication Critical patent/DE1518655A1/de
Publication of DE1518655B2 publication Critical patent/DE1518655B2/de
Application granted granted Critical
Publication of DE1518655C3 publication Critical patent/DE1518655C3/de
Expired legal-status Critical Current

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/0006—Controlling or regulating processes
    • B01J19/0013—Controlling the temperature of the process
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C201/00—Preparation of esters of nitric or nitrous acid or of compounds containing nitro or nitroso groups bound to a carbon skeleton
    • C07C201/06—Preparation of nitro compounds
    • C07C201/08—Preparation of nitro compounds by substitution of hydrogen atoms by nitro groups
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00121—Controlling the temperature by direct heating or cooling
    • B01J2219/00123—Controlling the temperature by direct heating or cooling adding a temperature modifying medium to the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B01J2219/00159—Controlling the temperature controlling multiple zones along the direction of flow, e.g. pre-heating and after-cooling
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00162—Controlling or regulating processes controlling the pressure
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
DE1518655A 1964-06-22 1965-06-19 Verfahren zur Herstellung von Nitroalkanen Expired DE1518655C3 (de)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US37686164A 1964-06-22 1964-06-22
US37668164A 1964-06-22 1964-06-22

Publications (3)

Publication Number Publication Date
DE1518655A1 DE1518655A1 (de) 1969-02-06
DE1518655B2 DE1518655B2 (de) 1975-01-09
DE1518655C3 true DE1518655C3 (de) 1975-09-04

Family

ID=27007503

Family Applications (1)

Application Number Title Priority Date Filing Date
DE1518655A Expired DE1518655C3 (de) 1964-06-22 1965-06-19 Verfahren zur Herstellung von Nitroalkanen

Country Status (6)

Country Link
BE (1) BE665694A (xx)
BR (1) BR6570539D0 (xx)
DE (1) DE1518655C3 (xx)
DK (1) DK120074B (xx)
GB (1) GB1088619A (xx)
NL (2) NL6507757A (xx)

Also Published As

Publication number Publication date
DE1518655B2 (de) 1975-01-09
BE665694A (xx) 1965-10-18
GB1088619A (en) 1967-10-25
NL6507757A (xx) 1965-12-23
NL128575C (xx)
BR6570539D0 (pt) 1973-12-27
DE1518655A1 (de) 1969-02-06
DK120074B (da) 1971-04-05

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Legal Events

Date Code Title Description
C3 Grant after two publication steps (3rd publication)
E77 Valid patent as to the heymanns-index 1977