DE1256993B - Verfahren zum Aufbringen eines Chromidueberzuges durch Kontaktabscheidung mit gegebenenfalls zusaetzlicher aeusserer EMK auf Metallkoerpern - Google Patents
Verfahren zum Aufbringen eines Chromidueberzuges durch Kontaktabscheidung mit gegebenenfalls zusaetzlicher aeusserer EMK auf MetallkoerpernInfo
- Publication number
- DE1256993B DE1256993B DEG37195A DEG0037195A DE1256993B DE 1256993 B DE1256993 B DE 1256993B DE G37195 A DEG37195 A DE G37195A DE G0037195 A DEG0037195 A DE G0037195A DE 1256993 B DE1256993 B DE 1256993B
- Authority
- DE
- Germany
- Prior art keywords
- chromium
- metal
- bath
- voltage
- chromide
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229910052751 metal Inorganic materials 0.000 title claims description 32
- 239000002184 metal Substances 0.000 title claims description 32
- 238000000576 coating method Methods 0.000 title claims description 26
- 241000501667 Etroplus Species 0.000 title claims description 24
- 239000011248 coating agent Substances 0.000 title claims description 22
- 238000000034 method Methods 0.000 title claims description 19
- 230000008021 deposition Effects 0.000 title claims description 9
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 claims description 44
- 229910052804 chromium Inorganic materials 0.000 claims description 32
- 239000011651 chromium Substances 0.000 claims description 32
- 150000003839 salts Chemical class 0.000 claims description 13
- 229910052783 alkali metal Inorganic materials 0.000 claims description 10
- 150000001844 chromium Chemical class 0.000 claims description 7
- 230000008018 melting Effects 0.000 claims description 7
- 238000002844 melting Methods 0.000 claims description 7
- 229910001515 alkali metal fluoride Inorganic materials 0.000 claims description 6
- 239000012298 atmosphere Substances 0.000 claims description 6
- 229910021563 chromium fluoride Inorganic materials 0.000 claims description 4
- 238000004519 manufacturing process Methods 0.000 claims description 4
- -1 Alkali metal chromium fluoride Chemical class 0.000 claims description 2
- 239000011261 inert gas Substances 0.000 claims 1
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 28
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 15
- 229910052742 iron Inorganic materials 0.000 description 14
- 150000001340 alkali metals Chemical class 0.000 description 8
- 238000000151 deposition Methods 0.000 description 8
- 229910052759 nickel Inorganic materials 0.000 description 7
- 230000002829 reductive effect Effects 0.000 description 7
- 229910000831 Steel Inorganic materials 0.000 description 6
- 239000010959 steel Substances 0.000 description 6
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000009792 diffusion process Methods 0.000 description 5
- 150000002500 ions Chemical class 0.000 description 5
- 239000000203 mixture Substances 0.000 description 5
- 229910052750 molybdenum Inorganic materials 0.000 description 5
- 239000011733 molybdenum Substances 0.000 description 5
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 4
- 230000015572 biosynthetic process Effects 0.000 description 4
- 210000004027 cell Anatomy 0.000 description 4
- 229910001430 chromium ion Inorganic materials 0.000 description 4
- 238000005260 corrosion Methods 0.000 description 4
- 230000007797 corrosion Effects 0.000 description 4
- 239000010410 layer Substances 0.000 description 4
- BASFCYQUMIYNBI-UHFFFAOYSA-N platinum Chemical compound [Pt] BASFCYQUMIYNBI-UHFFFAOYSA-N 0.000 description 4
- NROKBHXJSPEDAR-UHFFFAOYSA-M potassium fluoride Chemical compound [F-].[K+] NROKBHXJSPEDAR-UHFFFAOYSA-M 0.000 description 4
- 229910052799 carbon Inorganic materials 0.000 description 3
- 239000010960 cold rolled steel Substances 0.000 description 3
- 238000006073 displacement reaction Methods 0.000 description 3
- 238000002474 experimental method Methods 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 239000012535 impurity Substances 0.000 description 3
- 150000002739 metals Chemical class 0.000 description 3
- PUZPDOWCWNUUKD-UHFFFAOYSA-M sodium fluoride Inorganic materials [F-].[Na+] PUZPDOWCWNUUKD-UHFFFAOYSA-M 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 2
- 229910000792 Monel Inorganic materials 0.000 description 2
- 150000001845 chromium compounds Chemical class 0.000 description 2
- 239000004020 conductor Substances 0.000 description 2
- 230000003247 decreasing effect Effects 0.000 description 2
- 210000001787 dendrite Anatomy 0.000 description 2
- 239000007789 gas Substances 0.000 description 2
- 239000001257 hydrogen Substances 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- 238000007654 immersion Methods 0.000 description 2
- PQXKHYXIUOZZFA-UHFFFAOYSA-M lithium fluoride Chemical compound [Li+].[F-] PQXKHYXIUOZZFA-UHFFFAOYSA-M 0.000 description 2
- 230000007935 neutral effect Effects 0.000 description 2
- 229910052758 niobium Inorganic materials 0.000 description 2
- 239000010955 niobium Substances 0.000 description 2
- GUCVJGMIXFAOAE-UHFFFAOYSA-N niobium atom Chemical compound [Nb] GUCVJGMIXFAOAE-UHFFFAOYSA-N 0.000 description 2
- 229910052697 platinum Inorganic materials 0.000 description 2
- 235000003270 potassium fluoride Nutrition 0.000 description 2
- 239000011698 potassium fluoride Substances 0.000 description 2
- 239000002244 precipitate Substances 0.000 description 2
- 239000011833 salt mixture Substances 0.000 description 2
- 235000013024 sodium fluoride Nutrition 0.000 description 2
- 239000011775 sodium fluoride Substances 0.000 description 2
- 229910052715 tantalum Inorganic materials 0.000 description 2
- GUVRBAGPIYLISA-UHFFFAOYSA-N tantalum atom Chemical compound [Ta] GUVRBAGPIYLISA-UHFFFAOYSA-N 0.000 description 2
- FTBATIJJKIIOTP-UHFFFAOYSA-K trifluorochromium Chemical compound F[Cr](F)F FTBATIJJKIIOTP-UHFFFAOYSA-K 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 230000004584 weight gain Effects 0.000 description 2
- 235000019786 weight gain Nutrition 0.000 description 2
- 241001600451 Chromis Species 0.000 description 1
- 229910021554 Chromium(II) chloride Inorganic materials 0.000 description 1
- 229910000599 Cr alloy Inorganic materials 0.000 description 1
- 229910000604 Ferrochrome Inorganic materials 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229910021578 Iron(III) chloride Inorganic materials 0.000 description 1
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 description 1
- 239000004115 Sodium Silicate Substances 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 230000001464 adherent effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000012300 argon atmosphere Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 239000000788 chromium alloy Substances 0.000 description 1
- XBWRJSSJWDOUSJ-UHFFFAOYSA-L chromium(ii) chloride Chemical compound Cl[Cr]Cl XBWRJSSJWDOUSJ-UHFFFAOYSA-L 0.000 description 1
- 238000005254 chromizing Methods 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000002950 deficient Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 230000005611 electricity Effects 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 230000005496 eutectics Effects 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 229910002804 graphite Inorganic materials 0.000 description 1
- 239000010439 graphite Substances 0.000 description 1
- 238000000227 grinding Methods 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- 238000011065 in-situ storage Methods 0.000 description 1
- RBTARNINKXHZNM-UHFFFAOYSA-K iron trichloride Chemical compound Cl[Fe](Cl)Cl RBTARNINKXHZNM-UHFFFAOYSA-K 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 239000000155 melt Substances 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- 235000021110 pickles Nutrition 0.000 description 1
- 238000007747 plating Methods 0.000 description 1
- 229910052700 potassium Inorganic materials 0.000 description 1
- 239000011591 potassium Substances 0.000 description 1
- BGQMBPWATBYHMC-UHFFFAOYSA-J potassium;chromium(3+);tetrafluoride Chemical compound [F-].[F-].[F-].[F-].[K+].[Cr+3] BGQMBPWATBYHMC-UHFFFAOYSA-J 0.000 description 1
- 239000000843 powder Substances 0.000 description 1
- 239000011241 protective layer Substances 0.000 description 1
- NTHWMYGWWRZVTN-UHFFFAOYSA-N sodium silicate Chemical compound [Na+].[Na+].[O-][Si]([O-])=O NTHWMYGWWRZVTN-UHFFFAOYSA-N 0.000 description 1
- 229910052911 sodium silicate Inorganic materials 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- WFKWXMTUELFFGS-UHFFFAOYSA-N tungsten Chemical compound [W] WFKWXMTUELFFGS-UHFFFAOYSA-N 0.000 description 1
- 229910052721 tungsten Inorganic materials 0.000 description 1
- 239000010937 tungsten Substances 0.000 description 1
- 229910052720 vanadium Inorganic materials 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 230000004580 weight loss Effects 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25D—PROCESSES FOR THE ELECTROLYTIC OR ELECTROPHORETIC PRODUCTION OF COATINGS; ELECTROFORMING; APPARATUS THEREFOR
- C25D3/00—Electroplating: Baths therefor
- C25D3/66—Electroplating: Baths therefor from melts
-
- C—CHEMISTRY; METALLURGY
- C23—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; CHEMICAL SURFACE TREATMENT; DIFFUSION TREATMENT OF METALLIC MATERIAL; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL; INHIBITING CORROSION OF METALLIC MATERIAL OR INCRUSTATION IN GENERAL
- C23C—COATING METALLIC MATERIAL; COATING MATERIAL WITH METALLIC MATERIAL; SURFACE TREATMENT OF METALLIC MATERIAL BY DIFFUSION INTO THE SURFACE, BY CHEMICAL CONVERSION OR SUBSTITUTION; COATING BY VACUUM EVAPORATION, BY SPUTTERING, BY ION IMPLANTATION OR BY CHEMICAL VAPOUR DEPOSITION, IN GENERAL
- C23C18/00—Chemical coating by decomposition of either liquid compounds or solutions of the coating forming compounds, without leaving reaction products of surface material in the coating; Contact plating
- C23C18/54—Contact plating, i.e. electroless electrochemical plating
Landscapes
- Chemical & Material Sciences (AREA)
- Metallurgy (AREA)
- Electrochemistry (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Electroplating And Plating Baths Therefor (AREA)
- Electrolytic Production Of Metals (AREA)
- Electrodes For Compound Or Non-Metal Manufacture (AREA)
- Secondary Cells (AREA)
- Physical Vapour Deposition (AREA)
- Electroplating Methods And Accessories (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US17719662A | 1962-03-05 | 1962-03-05 | |
| US451053A US3232853A (en) | 1962-03-05 | 1965-04-26 | Corrosion resistant chromide coating |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1256993B true DE1256993B (de) | 1967-12-21 |
Family
ID=26873027
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEG37195A Pending DE1256993B (de) | 1962-03-05 | 1963-03-04 | Verfahren zum Aufbringen eines Chromidueberzuges durch Kontaktabscheidung mit gegebenenfalls zusaetzlicher aeusserer EMK auf Metallkoerpern |
| DEG45410A Pending DE1300411B (de) | 1962-03-05 | 1965-12-09 | Verfahren zum Aufbringen eines Chromidueberzuges durch Kontaktabscheidung mit gegebenenfalls zusaetzlicher aeusserer EMK auf Metallkoerpern |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEG45410A Pending DE1300411B (de) | 1962-03-05 | 1965-12-09 | Verfahren zum Aufbringen eines Chromidueberzuges durch Kontaktabscheidung mit gegebenenfalls zusaetzlicher aeusserer EMK auf Metallkoerpern |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US3232853A (OSRAM) |
| BE (1) | BE673733A (OSRAM) |
| CH (1) | CH469813A (OSRAM) |
| DE (2) | DE1256993B (OSRAM) |
| FR (2) | FR1426879A (OSRAM) |
| GB (2) | GB1029474A (OSRAM) |
| NL (1) | NL6516143A (OSRAM) |
| SE (1) | SE331403B (OSRAM) |
Families Citing this family (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3489540A (en) * | 1966-11-10 | 1970-01-13 | Gen Electric | Process for nickeliding,cobaltiding and ironiding base metal compositions |
| US3489537A (en) * | 1966-11-10 | 1970-01-13 | Gen Electric | Aluminiding |
| US3489536A (en) * | 1966-11-10 | 1970-01-13 | Gen Electric | Process for scandiding metals |
| US3489539A (en) * | 1966-11-10 | 1970-01-13 | Gen Electric | Manganiding |
| US3489538A (en) * | 1966-11-10 | 1970-01-13 | Gen Electric | Process for yttriding and rare earthiding |
| US3489659A (en) * | 1967-07-03 | 1970-01-13 | Gen Electric | Process for lithiding |
| US3530371A (en) * | 1968-07-01 | 1970-09-22 | Varian Associates | Internal field-frequency control for impulse gyromagnetic resonance spectrometers |
| FR2069985B1 (OSRAM) * | 1969-12-19 | 1973-12-21 | Anvar | |
| US3930060A (en) * | 1972-05-04 | 1975-12-30 | Toyoda Chuo Kenkyusho Kk | Method for forming a carbide layer of a V-a group element of the periodic table on the surface of an iron, ferrous alloy or cemented carbide article |
| SE372043B (OSRAM) * | 1972-07-07 | 1974-12-09 | Nordstjernan Rederi Ab | |
| US3912827A (en) * | 1973-11-13 | 1975-10-14 | Toyota Chuo Kenkyusko Kk | Method for forming a chromium carbide layer on the surface of an iron, ferrous alloy or cemented carbide article |
| US4432839A (en) * | 1981-06-18 | 1984-02-21 | Diamond Shamrock Corporation | Method for making metallided foils |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1535339A (en) * | 1924-05-10 | 1925-04-28 | Peacock Samuel | Process for electrolytically depositing elemental chromium upon metals |
| US1845978A (en) * | 1927-03-18 | 1932-02-16 | Metal & Thermit Corp | Process for the electrolytic production of alpha particularly strong chromium coating |
| US1927773A (en) * | 1931-06-02 | 1933-09-19 | Purdue Research Foundation | Electroplating chromium, etc., on iron, etc. |
| GB659927A (en) * | 1948-04-05 | 1951-10-31 | American Electro Metal Corp | Improvements relating to the coating electrolytically of metal articles |
| US2828251A (en) * | 1953-09-30 | 1958-03-25 | Horizons Titanium Corp | Electrolytic cladding process |
| US2786809A (en) * | 1953-09-30 | 1957-03-26 | Horizons Titanium Corp | Electrolytic cladding |
| US2957782A (en) * | 1956-07-13 | 1960-10-25 | Boller Dev Corp | Process for coating ferrous metals |
| US2971899A (en) * | 1957-09-10 | 1961-02-14 | Gen Motors Corp | Method of electroplating aluminum |
-
1963
- 1963-03-01 GB GB8376/63A patent/GB1029474A/en not_active Expired
- 1963-03-04 DE DEG37195A patent/DE1256993B/de active Pending
- 1963-03-05 FR FR926814A patent/FR1426879A/fr not_active Expired
-
1965
- 1965-04-26 US US451053A patent/US3232853A/en not_active Expired - Lifetime
- 1965-11-09 GB GB47427/65A patent/GB1118299A/en not_active Expired
- 1965-11-30 CH CH1650365A patent/CH469813A/de unknown
- 1965-12-09 DE DEG45410A patent/DE1300411B/de active Pending
- 1965-12-10 NL NL6516143A patent/NL6516143A/xx unknown
- 1965-12-10 SE SE16054/65A patent/SE331403B/xx unknown
- 1965-12-13 FR FR42007A patent/FR1461813A/fr not_active Expired
- 1965-12-14 BE BE673733D patent/BE673733A/xx unknown
Also Published As
| Publication number | Publication date |
|---|---|
| SE331403B (OSRAM) | 1970-12-21 |
| BE673733A (OSRAM) | 1966-04-01 |
| GB1118299A (en) | 1968-06-26 |
| US3232853A (en) | 1966-02-01 |
| NL6516143A (OSRAM) | 1966-10-27 |
| FR1461813A (fr) | 1966-12-09 |
| GB1029474A (en) | 1966-05-11 |
| DE1300411B (de) | 1969-07-31 |
| FR1426879A (fr) | 1966-02-04 |
| CH469813A (de) | 1969-03-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| E77 | Valid patent as to the heymanns-index 1977 |