DE1231696B - Verfahren zur Oxydation von Kohlenwasser-stoffen - Google Patents
Verfahren zur Oxydation von Kohlenwasser-stoffenInfo
- Publication number
- DE1231696B DE1231696B DES81678A DES0081678A DE1231696B DE 1231696 B DE1231696 B DE 1231696B DE S81678 A DES81678 A DE S81678A DE S0081678 A DES0081678 A DE S0081678A DE 1231696 B DE1231696 B DE 1231696B
- Authority
- DE
- Germany
- Prior art keywords
- hydrocarbon
- water
- condensed
- oxidation
- gaseous
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 229930195733 hydrocarbon Natural products 0.000 title claims description 50
- 150000002430 hydrocarbons Chemical class 0.000 title claims description 46
- 238000007254 oxidation reaction Methods 0.000 title claims description 28
- 230000003647 oxidation Effects 0.000 title claims description 25
- 238000000034 method Methods 0.000 title claims description 13
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 44
- 239000004215 Carbon black (E152) Substances 0.000 claims description 35
- 239000007788 liquid Substances 0.000 claims description 19
- 238000009833 condensation Methods 0.000 claims description 9
- 230000005494 condensation Effects 0.000 claims description 9
- 239000007789 gas Substances 0.000 claims description 6
- 150000001639 boron compounds Chemical class 0.000 claims description 5
- -1 metaboric acid Chemical class 0.000 claims description 5
- VGTPKLINSHNZRD-UHFFFAOYSA-N oxoborinic acid Chemical compound OB=O VGTPKLINSHNZRD-UHFFFAOYSA-N 0.000 claims description 5
- 238000000926 separation method Methods 0.000 claims description 5
- 239000000470 constituent Substances 0.000 claims description 3
- 150000001924 cycloalkanes Chemical class 0.000 claims description 3
- MYMOFIZGZYHOMD-UHFFFAOYSA-N Dioxygen Chemical compound O=O MYMOFIZGZYHOMD-UHFFFAOYSA-N 0.000 claims description 2
- 229910001882 dioxygen Inorganic materials 0.000 claims description 2
- 238000004064 recycling Methods 0.000 claims description 2
- 239000000463 material Substances 0.000 claims 2
- UAEPNZWRGJTJPN-UHFFFAOYSA-N methylcyclohexane Chemical compound CC1CCCCC1 UAEPNZWRGJTJPN-UHFFFAOYSA-N 0.000 description 26
- 238000006243 chemical reaction Methods 0.000 description 18
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 15
- GYNNXHKOJHMOHS-UHFFFAOYSA-N methyl-cycloheptane Natural products CC1CCCCCC1 GYNNXHKOJHMOHS-UHFFFAOYSA-N 0.000 description 13
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 12
- 229910052757 nitrogen Inorganic materials 0.000 description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 4
- 239000001301 oxygen Substances 0.000 description 4
- 229910052760 oxygen Inorganic materials 0.000 description 4
- 238000009835 boiling Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 239000000203 mixture Substances 0.000 description 3
- OFBQJSOFQDEBGM-UHFFFAOYSA-N n-pentane Natural products CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 3
- 239000011541 reaction mixture Substances 0.000 description 3
- 241000589614 Pseudomonas stutzeri Species 0.000 description 2
- 125000004432 carbon atom Chemical group C* 0.000 description 2
- 239000007795 chemical reaction product Substances 0.000 description 2
- 238000001816 cooling Methods 0.000 description 2
- 238000001704 evaporation Methods 0.000 description 2
- 230000008020 evaporation Effects 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 238000005406 washing Methods 0.000 description 2
- 150000001260 acyclic compounds Chemical class 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 239000001273 butane Substances 0.000 description 1
- 150000001923 cyclic compounds Chemical class 0.000 description 1
- BJZJDEOGMBZSLE-UHFFFAOYSA-N cyclohexane;hydrate Chemical compound O.C1CCCCC1 BJZJDEOGMBZSLE-UHFFFAOYSA-N 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 239000003517 fume Substances 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- QWTDNUCVQCZILF-UHFFFAOYSA-N isopentane Chemical compound CCC(C)C QWTDNUCVQCZILF-UHFFFAOYSA-N 0.000 description 1
- GQWOFANLKDZZMT-UHFFFAOYSA-N methylcyclohexane;hydrate Chemical compound O.CC1CCCCC1 GQWOFANLKDZZMT-UHFFFAOYSA-N 0.000 description 1
- IJDNQMDRQITEOD-UHFFFAOYSA-N n-butane Chemical compound CCCC IJDNQMDRQITEOD-UHFFFAOYSA-N 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 238000005191 phase separation Methods 0.000 description 1
- 239000007921 spray Substances 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/48—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxidation reactions with formation of hydroxy groups
- C07C29/50—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxidation reactions with formation of hydroxy groups with molecular oxygen only
- C07C29/52—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by oxidation reactions with formation of hydroxy groups with molecular oxygen only in the presence of mineral boron compounds with, when necessary, hydrolysis of the intermediate formed
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
- C07C2601/14—The ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US1231696XA | 1961-09-26 | 1961-09-26 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1231696B true DE1231696B (de) | 1967-01-05 |
Family
ID=22407104
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DES81678A Pending DE1231696B (de) | 1961-09-26 | 1962-09-26 | Verfahren zur Oxydation von Kohlenwasser-stoffen |
Country Status (2)
| Country | Link |
|---|---|
| DE (1) | DE1231696B (enrdf_load_stackoverflow) |
| NL (1) | NL283634A (enrdf_load_stackoverflow) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2652691A1 (de) * | 1975-11-22 | 1977-06-02 | Stamicarbon | Verfahren und vorrichtung zur oxidation von cyclo-alkanen |
Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1166679A (fr) * | 1957-02-06 | 1958-11-13 | Sinnova Ou Sadic | Procédé de synthèse des alcools |
| DE1078569B (de) * | 1957-09-28 | 1960-03-31 | Basf Ag | Verfahren zur Herstellung von Alkoholen und Ketonen durch Oxydation von cycloaliphatischen Kohlenwasserstoffen |
| DE1100020B (de) * | 1958-09-13 | 1961-02-23 | Inventa A G Fuer Forschung | Verfahren zur destillativen Zerlegung von Reaktionsgemischen, die aus der Oxydation von Cyclohexan stammen |
-
0
- NL NL283634D patent/NL283634A/xx unknown
-
1962
- 1962-09-26 DE DES81678A patent/DE1231696B/de active Pending
Patent Citations (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| FR1166679A (fr) * | 1957-02-06 | 1958-11-13 | Sinnova Ou Sadic | Procédé de synthèse des alcools |
| DE1078569B (de) * | 1957-09-28 | 1960-03-31 | Basf Ag | Verfahren zur Herstellung von Alkoholen und Ketonen durch Oxydation von cycloaliphatischen Kohlenwasserstoffen |
| DE1100020B (de) * | 1958-09-13 | 1961-02-23 | Inventa A G Fuer Forschung | Verfahren zur destillativen Zerlegung von Reaktionsgemischen, die aus der Oxydation von Cyclohexan stammen |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2652691A1 (de) * | 1975-11-22 | 1977-06-02 | Stamicarbon | Verfahren und vorrichtung zur oxidation von cyclo-alkanen |
Also Published As
| Publication number | Publication date |
|---|---|
| NL283634A (enrdf_load_stackoverflow) |
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