DE121976C - - Google Patents
Info
- Publication number
- DE121976C DE121976C DENDAT121976D DE121976DA DE121976C DE 121976 C DE121976 C DE 121976C DE NDAT121976 D DENDAT121976 D DE NDAT121976D DE 121976D A DE121976D A DE 121976DA DE 121976 C DE121976 C DE 121976C
- Authority
- DE
- Germany
- Prior art keywords
- nhc
- bases
- colorless
- oil
- base
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Active
Links
- AVKNGPAMCBSNSO-UHFFFAOYSA-N cyclohexylmethanamine Chemical compound NCC1CCCCC1 AVKNGPAMCBSNSO-UHFFFAOYSA-N 0.000 claims description 3
- 238000000034 method Methods 0.000 claims description 3
- 239000003638 chemical reducing agent Substances 0.000 claims description 2
- HUESUARLBCVSFD-UHFFFAOYSA-N cyclohex-2-en-1-ylmethanamine Chemical compound NCC1CCCC=C1 HUESUARLBCVSFD-UHFFFAOYSA-N 0.000 claims description 2
- DHEVPCATXWKCSP-UHFFFAOYSA-N n-chloro-1-cyclohexylmethanamine Chemical compound ClNCC1CCCCC1 DHEVPCATXWKCSP-UHFFFAOYSA-N 0.000 claims 1
- -1 isopropylmethylchlorhexahydrobenzylaniline Chemical compound 0.000 description 7
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 description 5
- 239000012230 colorless oil Substances 0.000 description 4
- 239000003921 oil Substances 0.000 description 4
- WQTVNGHNKXINJE-UHFFFAOYSA-N N-(cyclohexylmethyl)-N,2,3-trimethylaniline Chemical compound CC=1C(=C(N(CC2CCCCC2)C)C=CC1)C WQTVNGHNKXINJE-UHFFFAOYSA-N 0.000 description 3
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 3
- 238000006243 chemical reaction Methods 0.000 description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 3
- IGBBADDXMAUKGV-UHFFFAOYSA-N C(C)(C)C1=C(N(CC2CCCC=C2)C)C=CC=C1 Chemical compound C(C)(C)C1=C(N(CC2CCCC=C2)C)C=CC=C1 IGBBADDXMAUKGV-UHFFFAOYSA-N 0.000 description 2
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 2
- QUSNBJAOOMFDIB-UHFFFAOYSA-N Ethylamine Chemical compound CCN QUSNBJAOOMFDIB-UHFFFAOYSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 2
- GWLOCUSRCDRZKG-UHFFFAOYSA-N N-(cyclohex-2-en-1-ylmethyl)-N,2,3-trimethylaniline Chemical compound CC=1C(=C(N(CC2CCCC=C2)C)C=CC1)C GWLOCUSRCDRZKG-UHFFFAOYSA-N 0.000 description 2
- OEPRFNAFBHVOQK-UHFFFAOYSA-N N-chloro-N-(cyclohexylmethyl)-2,3,4-trimethylaniline Chemical compound CC1=C(C(=C(N(CC2CCCCC2)Cl)C=C1)C)C OEPRFNAFBHVOQK-UHFFFAOYSA-N 0.000 description 2
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 description 2
- 229960000583 acetic acid Drugs 0.000 description 2
- HXKFBZNJRZNEMJ-UHFFFAOYSA-N n-(cyclohexylmethyl)aniline Chemical compound C1CCCCC1CNC1=CC=CC=C1 HXKFBZNJRZNEMJ-UHFFFAOYSA-N 0.000 description 2
- 238000010992 reflux Methods 0.000 description 2
- 239000011734 sodium Substances 0.000 description 2
- 229910052708 sodium Inorganic materials 0.000 description 2
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 1
- ATBXDEZLHOIUCY-UHFFFAOYSA-N N-(cyclohex-2-en-1-ylmethyl)-N-methylpropan-2-amine Chemical compound C(C)(C)N(CC1CCCC=C1)C ATBXDEZLHOIUCY-UHFFFAOYSA-N 0.000 description 1
- KOJRFUCCPWZFIL-UHFFFAOYSA-N N-(cyclohexylmethyl)-1-methoxy-N,2-dimethylpropan-1-amine Chemical compound C(C)(C)C(N(C)CC1CCCCC1)OC KOJRFUCCPWZFIL-UHFFFAOYSA-N 0.000 description 1
- BUPPOBQAJKCHHT-UHFFFAOYSA-N N-(cyclohexylmethyl)-N-methyl-2-propan-2-ylaniline Chemical compound C(C)(C)C1=C(N(CC2CCCCC2)C)C=CC=C1 BUPPOBQAJKCHHT-UHFFFAOYSA-N 0.000 description 1
- 230000001476 alcoholic effect Effects 0.000 description 1
- 125000001931 aliphatic group Chemical group 0.000 description 1
- 238000009835 boiling Methods 0.000 description 1
- 238000004821 distillation Methods 0.000 description 1
- 239000003205 fragrance Substances 0.000 description 1
- 239000012362 glacial acetic acid Substances 0.000 description 1
- 229910052739 hydrogen Inorganic materials 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- ABHOJSQYRHGJHC-UHFFFAOYSA-N n-(cyclohexylmethyl)-n-methylpropan-2-amine Chemical compound CC(C)N(C)CC1CCCCC1 ABHOJSQYRHGJHC-UHFFFAOYSA-N 0.000 description 1
- GTWJETSWSUWSEJ-UHFFFAOYSA-N n-benzylaniline Chemical compound C=1C=CC=CC=1CNC1=CC=CC=C1 GTWJETSWSUWSEJ-UHFFFAOYSA-N 0.000 description 1
- UHZYTMXLRWXGPK-UHFFFAOYSA-N phosphorus pentachloride Chemical compound ClP(Cl)(Cl)(Cl)Cl UHZYTMXLRWXGPK-UHFFFAOYSA-N 0.000 description 1
- 238000010792 warming Methods 0.000 description 1
Landscapes
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE121976C true DE121976C (enExample) |
Family
ID=390939
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DENDAT121976D Active DE121976C (enExample) |
Country Status (1)
| Country | Link |
|---|---|
| DE (1) | DE121976C (enExample) |
-
0
- DE DENDAT121976D patent/DE121976C/de active Active
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