DE1103922B - Verfahren zur Herstellung von ª-Chloraethanphosphonsaeuredichlorid - Google Patents
Verfahren zur Herstellung von ª-ChloraethanphosphonsaeuredichloridInfo
- Publication number
- DE1103922B DE1103922B DEF28744A DEF0028744A DE1103922B DE 1103922 B DE1103922 B DE 1103922B DE F28744 A DEF28744 A DE F28744A DE F0028744 A DEF0028744 A DE F0028744A DE 1103922 B DE1103922 B DE 1103922B
- Authority
- DE
- Germany
- Prior art keywords
- ethylene
- phosphorus trichloride
- acid dichloride
- oxygen
- preparation
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 238000000034 method Methods 0.000 title claims description 12
- 238000002360 preparation method Methods 0.000 title description 2
- FAIAAWCVCHQXDN-UHFFFAOYSA-N phosphorus trichloride Chemical compound ClP(Cl)Cl FAIAAWCVCHQXDN-UHFFFAOYSA-N 0.000 claims description 16
- VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 claims description 13
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 12
- 239000001301 oxygen Substances 0.000 claims description 12
- 229910052760 oxygen Inorganic materials 0.000 claims description 12
- 239000005977 Ethylene Substances 0.000 claims description 10
- 239000007789 gas Substances 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 4
- 239000000126 substance Substances 0.000 claims description 2
- 238000006243 chemical reaction Methods 0.000 description 10
- XHXFXVLFKHQFAL-UHFFFAOYSA-N phosphoryl trichloride Chemical compound ClP(Cl)(Cl)=O XHXFXVLFKHQFAL-UHFFFAOYSA-N 0.000 description 6
- VSCWAEJMTAWNJL-UHFFFAOYSA-K aluminium trichloride Chemical compound Cl[Al](Cl)Cl VSCWAEJMTAWNJL-UHFFFAOYSA-K 0.000 description 4
- 238000009835 boiling Methods 0.000 description 4
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 description 2
- 238000004821 distillation Methods 0.000 description 2
- UHZYTMXLRWXGPK-UHFFFAOYSA-N phosphorus pentachloride Chemical compound ClP(Cl)(Cl)(Cl)Cl UHZYTMXLRWXGPK-UHFFFAOYSA-N 0.000 description 2
- 238000010626 work up procedure Methods 0.000 description 2
- WSLDOOZREJYCGB-UHFFFAOYSA-N 1,2-Dichloroethane Chemical compound ClCCCl WSLDOOZREJYCGB-UHFFFAOYSA-N 0.000 description 1
- MLSZIADXWDYFKM-UHFFFAOYSA-N 1-dichlorophosphorylethene Chemical compound ClP(Cl)(=O)C=C MLSZIADXWDYFKM-UHFFFAOYSA-N 0.000 description 1
- RNFJDJUURJAICM-UHFFFAOYSA-N 2,2,4,4,6,6-hexaphenoxy-1,3,5-triaza-2$l^{5},4$l^{5},6$l^{5}-triphosphacyclohexa-1,3,5-triene Chemical compound N=1P(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP(OC=2C=CC=CC=2)(OC=2C=CC=CC=2)=NP=1(OC=1C=CC=CC=1)OC1=CC=CC=C1 RNFJDJUURJAICM-UHFFFAOYSA-N 0.000 description 1
- NJLHHACGWKAWKL-UHFFFAOYSA-N ClP(Cl)=O Chemical compound ClP(Cl)=O NJLHHACGWKAWKL-UHFFFAOYSA-N 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 1
- OAICVXFJPJFONN-UHFFFAOYSA-N Phosphorus Chemical compound [P] OAICVXFJPJFONN-UHFFFAOYSA-N 0.000 description 1
- 150000001408 amides Chemical class 0.000 description 1
- 150000001875 compounds Chemical class 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 239000003063 flame retardant Substances 0.000 description 1
- 230000000855 fungicidal effect Effects 0.000 description 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 description 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 description 1
- 238000009413 insulation Methods 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- RLOWWWKZYUNIDI-UHFFFAOYSA-N phosphinic chloride Chemical compound ClP=O RLOWWWKZYUNIDI-UHFFFAOYSA-N 0.000 description 1
- 229910052698 phosphorus Inorganic materials 0.000 description 1
- 239000011574 phosphorus Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 239000002994 raw material Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 239000007858 starting material Substances 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 229920003002 synthetic resin Polymers 0.000 description 1
- 239000000057 synthetic resin Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
- C07F9/42—Halides thereof
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08F—MACROMOLECULAR COMPOUNDS OBTAINED BY REACTIONS ONLY INVOLVING CARBON-TO-CARBON UNSATURATED BONDS
- C08F30/00—Homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and containing phosphorus, selenium, tellurium or a metal
- C08F30/02—Homopolymers or copolymers of compounds having one or more unsaturated aliphatic radicals, each having only one carbon-to-carbon double bond, and containing phosphorus, selenium, tellurium or a metal containing phosphorus
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Molecular Biology (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
Priority Applications (14)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| BE592086D BE592086A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1959-06-20 | ||
| BE592087D BE592087A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1959-06-20 | ||
| DEF28744A DE1103922B (de) | 1959-06-20 | 1959-06-20 | Verfahren zur Herstellung von ª-Chloraethanphosphonsaeuredichlorid |
| DEF29070A DE1108687B (de) | 1959-06-20 | 1959-07-31 | Verfahren zur Herstellung von ª-Chloraethanphosphonsaeuredichlorid |
| DEF29707A DE1138770B (de) | 1959-06-20 | 1959-10-27 | Verfahren zur Herstellung ungesaettigter Phosphonsaeuredichloride |
| DEF30546A DE1123667B (de) | 1959-06-20 | 1960-02-16 | Verfahren zur Herstellung von ª-Chloraethanphosphonsaeuredichlorid |
| US35876A US3206508A (en) | 1959-06-20 | 1960-06-14 | Process for preparing beta-chlorethane phosphonic acid dichloride |
| US36732A US3183264A (en) | 1959-06-20 | 1960-06-17 | Process for the manufacture of unsaturated phosphonic acid dichlorides |
| CH691960A CH391699A (de) | 1959-06-20 | 1960-06-17 | Verfahren zur Herstellung ungesättigter Phosphonsäuredichloride |
| CH692060A CH395083A (de) | 1959-06-20 | 1960-06-17 | Verfahren zur Herstellung von B-Chloräthanphosphonsäuredichlorid |
| GB21622/60A GB963882A (en) | 1959-06-20 | 1960-06-20 | Process for the manufacture of unsaturated phosphonic acid dichlorides |
| GB21626/60A GB963881A (en) | 1959-06-20 | 1960-06-20 | Process for preparing ª -chlorethane phosphonic acid dichloride |
| FR830573A FR1269130A (fr) | 1959-06-20 | 1960-06-20 | Procédé de préparation de dichlorures d'acides phosphoniques non saturés |
| FR830574A FR1269131A (fr) | 1959-06-20 | 1960-06-20 | Procédé de préparation du dichlorure de l'acide beta-chloréthane-phosphonique |
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DEF28744A DE1103922B (de) | 1959-06-20 | 1959-06-20 | Verfahren zur Herstellung von ª-Chloraethanphosphonsaeuredichlorid |
| DEF29070A DE1108687B (de) | 1959-06-20 | 1959-07-31 | Verfahren zur Herstellung von ª-Chloraethanphosphonsaeuredichlorid |
| DEF30546A DE1123667B (de) | 1959-06-20 | 1960-02-16 | Verfahren zur Herstellung von ª-Chloraethanphosphonsaeuredichlorid |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| DE1103922B true DE1103922B (de) | 1961-04-06 |
Family
ID=30448787
Family Applications (4)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEF28744A Pending DE1103922B (de) | 1959-06-20 | 1959-06-20 | Verfahren zur Herstellung von ª-Chloraethanphosphonsaeuredichlorid |
| DEF29070A Pending DE1108687B (de) | 1959-06-20 | 1959-07-31 | Verfahren zur Herstellung von ª-Chloraethanphosphonsaeuredichlorid |
| DEF29707A Pending DE1138770B (de) | 1959-06-20 | 1959-10-27 | Verfahren zur Herstellung ungesaettigter Phosphonsaeuredichloride |
| DEF30546A Pending DE1123667B (de) | 1959-06-20 | 1960-02-16 | Verfahren zur Herstellung von ª-Chloraethanphosphonsaeuredichlorid |
Family Applications After (3)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| DEF29070A Pending DE1108687B (de) | 1959-06-20 | 1959-07-31 | Verfahren zur Herstellung von ª-Chloraethanphosphonsaeuredichlorid |
| DEF29707A Pending DE1138770B (de) | 1959-06-20 | 1959-10-27 | Verfahren zur Herstellung ungesaettigter Phosphonsaeuredichloride |
| DEF30546A Pending DE1123667B (de) | 1959-06-20 | 1960-02-16 | Verfahren zur Herstellung von ª-Chloraethanphosphonsaeuredichlorid |
Country Status (5)
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3397122A (en) * | 1966-12-23 | 1968-08-13 | Knapsack Ag | Process for purifying beta-chloroethane phosphonic acid dichloride by treatment with a tertiary amine salt |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3402196A (en) * | 1962-08-31 | 1968-09-17 | Hooker Chemical Corp | Organophosphorus compounds and methods for the preparation thereof |
| US3976690A (en) * | 1975-09-15 | 1976-08-24 | Stauffer Chemical Company | Process for preparing alkane bis-dihalophosphines |
| DE3629579A1 (de) * | 1986-08-30 | 1988-03-03 | Hoechst Ag | Verfahren zur herstellung von 2-chlorethanphosphonsaeuredichlorid |
| DE3640357A1 (de) * | 1986-11-26 | 1988-06-09 | Hoechst Ag | Verfahren zur herstellung von phosphin- oder phosphonsaeurechloriden |
| DE3641100A1 (de) * | 1986-12-02 | 1988-06-09 | Hoechst Ag | Verfahren zur herstellung von 2-chlorethanphosphonsaeuredichlorid |
Family Cites Families (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| SU116882A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | ||||
| US2365466A (en) * | 1942-10-23 | 1944-12-19 | Du Pont | Organic compounds |
| US2388657A (en) * | 1943-04-15 | 1945-11-06 | Wingfoot Corp | Preparation of acid chlorides |
| US2495799A (en) * | 1945-05-17 | 1950-01-31 | Victor Chemical Works | Chloroalkyl phosphorous oxy and sulfodichlorides |
| US2683168A (en) * | 1950-12-22 | 1954-07-06 | California Research Corp | Preparation of organo phosphonyl chlorides |
| US2683169A (en) * | 1952-06-11 | 1954-07-06 | California Research Corp | Preparation of organo phosphonyl chlorides from organo halides |
| SU116882A1 (ru) * | 1958-03-01 | 1958-11-30 | М.И. Кабачник | Способ получени диалкиловых эфиров винилфосфиновой кислоты и замещенных диамидов |
-
0
- BE BE592086D patent/BE592086A/xx unknown
- BE BE592087D patent/BE592087A/xx unknown
-
1959
- 1959-06-20 DE DEF28744A patent/DE1103922B/de active Pending
- 1959-07-31 DE DEF29070A patent/DE1108687B/de active Pending
- 1959-10-27 DE DEF29707A patent/DE1138770B/de active Pending
-
1960
- 1960-02-16 DE DEF30546A patent/DE1123667B/de active Pending
- 1960-06-14 US US35876A patent/US3206508A/en not_active Expired - Lifetime
- 1960-06-17 CH CH691960A patent/CH391699A/de unknown
- 1960-06-17 CH CH692060A patent/CH395083A/de unknown
- 1960-06-17 US US36732A patent/US3183264A/en not_active Expired - Lifetime
- 1960-06-20 GB GB21622/60A patent/GB963882A/en not_active Expired
- 1960-06-20 GB GB21626/60A patent/GB963881A/en not_active Expired
Non-Patent Citations (1)
| Title |
|---|
| None * |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3397122A (en) * | 1966-12-23 | 1968-08-13 | Knapsack Ag | Process for purifying beta-chloroethane phosphonic acid dichloride by treatment with a tertiary amine salt |
Also Published As
| Publication number | Publication date |
|---|---|
| BE592086A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | |
| DE1123667B (de) | 1962-02-15 |
| BE592087A (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | |
| US3183264A (en) | 1965-05-11 |
| GB963881A (en) | 1964-07-15 |
| CH391699A (de) | 1965-05-15 |
| US3206508A (en) | 1965-09-14 |
| CH395083A (de) | 1965-07-15 |
| DE1108687B (de) | 1961-06-15 |
| DE1138770B (de) | 1962-10-31 |
| GB963882A (en) | 1964-07-15 |
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