DE10108484A1 - Verbessertes Verfahren zur Herstelung von Polyetherpolyolen - Google Patents

Verbessertes Verfahren zur Herstelung von Polyetherpolyolen

Info

Publication number
DE10108484A1
DE10108484A1 DE10108484A DE10108484A DE10108484A1 DE 10108484 A1 DE10108484 A1 DE 10108484A1 DE 10108484 A DE10108484 A DE 10108484A DE 10108484 A DE10108484 A DE 10108484A DE 10108484 A1 DE10108484 A1 DE 10108484A1
Authority
DE
Germany
Prior art keywords
dmc
polyether polyols
polyol
catalyst
polyaddition
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Withdrawn
Application number
DE10108484A
Other languages
German (de)
English (en)
Inventor
Joerg Hofmann
Stephan Ehlers
Bernd Klinksiek
Lars Obendorf
Christian Steinlein
Bert Klesczewski
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Covestro Deutschland AG
Original Assignee
Bayer AG
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Bayer AG filed Critical Bayer AG
Priority to DE10108484A priority Critical patent/DE10108484A1/de
Priority to MXPA03007533A priority patent/MXPA03007533A/es
Priority to DE50203140T priority patent/DE50203140D1/de
Priority to PT02714155T priority patent/PT1368407E/pt
Priority to RU2003128531/04A priority patent/RU2301815C2/ru
Priority to BRPI0207766-3A priority patent/BR0207766B1/pt
Priority to EP02714155A priority patent/EP1368407B1/de
Priority to ES02714155T priority patent/ES2242003T3/es
Priority to HK04109847.2A priority patent/HK1066819B/xx
Priority to JP2002568010A priority patent/JP4112985B2/ja
Priority to CA002438647A priority patent/CA2438647A1/en
Priority to CNB028054350A priority patent/CN1215104C/zh
Priority to CZ20032222A priority patent/CZ297775B6/cs
Priority to AT02714155T priority patent/ATE295861T1/de
Priority to PCT/EP2002/001398 priority patent/WO2002068503A1/de
Priority to KR1020037010984A priority patent/KR100799036B1/ko
Priority to PL369335A priority patent/PL207572B1/pl
Priority to HU0303259A priority patent/HU227020B1/hu
Priority to US10/078,951 priority patent/US6776925B2/en
Priority to TW091102855A priority patent/TWI232228B/zh
Publication of DE10108484A1 publication Critical patent/DE10108484A1/de
Withdrawn legal-status Critical Current

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2696—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the process or apparatus used
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1868—Stationary reactors having moving elements inside resulting in a loop-type movement
    • B01J19/1881—Stationary reactors having moving elements inside resulting in a loop-type movement externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/24—Stationary reactors without moving elements inside
    • B01J19/2455—Stationary reactors without moving elements inside provoking a loop type movement of the reactants
    • B01J19/2465—Stationary reactors without moving elements inside provoking a loop type movement of the reactants externally, i.e. the mixture leaving the vessel and subsequently re-entering it
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Health & Medical Sciences (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Toxicology (AREA)
  • Polyethers (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
  • Cephalosporin Compounds (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Preparation Of Compounds By Using Micro-Organisms (AREA)
DE10108484A 2001-02-22 2001-02-22 Verbessertes Verfahren zur Herstelung von Polyetherpolyolen Withdrawn DE10108484A1 (de)

Priority Applications (20)

Application Number Priority Date Filing Date Title
DE10108484A DE10108484A1 (de) 2001-02-22 2001-02-22 Verbessertes Verfahren zur Herstelung von Polyetherpolyolen
MXPA03007533A MXPA03007533A (es) 2001-02-22 2002-02-11 Procedimiento mejorado para preparacion de polioleteres.
DE50203140T DE50203140D1 (de) 2001-02-22 2002-02-11 Verbessertes verfahren zur herstellung von polyetherpolyolen
PT02714155T PT1368407E (pt) 2001-02-22 2002-02-11 Processo melhorado para a preparacao de polieter-poliois
RU2003128531/04A RU2301815C2 (ru) 2001-02-22 2002-02-11 Способ получения полиэфирполиолов
BRPI0207766-3A BR0207766B1 (pt) 2001-02-22 2002-02-11 processo aperfeiÇoado para a preparaÇço de poliÉter-poliàis.
EP02714155A EP1368407B1 (de) 2001-02-22 2002-02-11 Verbessertes verfahren zur herstellung von polyetherpolyolen
ES02714155T ES2242003T3 (es) 2001-02-22 2002-02-11 Procedimiento mejorado para la preparacion de polioleteres.
HK04109847.2A HK1066819B (en) 2001-02-22 2002-02-11 Improved method for producing polyether polyols
JP2002568010A JP4112985B2 (ja) 2001-02-22 2002-02-11 改良されたポリエーテルポリオールの製造方法
CA002438647A CA2438647A1 (en) 2001-02-22 2002-02-11 Improved method for producing polyether polyols
CNB028054350A CN1215104C (zh) 2001-02-22 2002-02-11 制备聚醚多元醇的改进方法
CZ20032222A CZ297775B6 (cs) 2001-02-22 2002-02-11 Zlepsený zpusob výroby polyetherpolyolu
AT02714155T ATE295861T1 (de) 2001-02-22 2002-02-11 Verbessertes verfahren zur herstellung von polyetherpolyolen
PCT/EP2002/001398 WO2002068503A1 (de) 2001-02-22 2002-02-11 Verbessertes verfahren zur herstellung von polyetherpolyolen
KR1020037010984A KR100799036B1 (ko) 2001-02-22 2002-02-11 폴리에테르 폴리올의 개선된 제조 방법
PL369335A PL207572B1 (pl) 2001-02-22 2002-02-11 Sposób wytwarzania polieteropolioli
HU0303259A HU227020B1 (en) 2001-02-22 2002-02-11 Improved method for producing polyether polyols
US10/078,951 US6776925B2 (en) 2001-02-22 2002-02-19 Process for the preparation of polyether polyols
TW091102855A TWI232228B (en) 2001-02-22 2002-02-20 Improved process for the preparation of polyether polyols

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE10108484A DE10108484A1 (de) 2001-02-22 2001-02-22 Verbessertes Verfahren zur Herstelung von Polyetherpolyolen

Publications (1)

Publication Number Publication Date
DE10108484A1 true DE10108484A1 (de) 2002-09-05

Family

ID=7675084

Family Applications (2)

Application Number Title Priority Date Filing Date
DE10108484A Withdrawn DE10108484A1 (de) 2001-02-22 2001-02-22 Verbessertes Verfahren zur Herstelung von Polyetherpolyolen
DE50203140T Expired - Lifetime DE50203140D1 (de) 2001-02-22 2002-02-11 Verbessertes verfahren zur herstellung von polyetherpolyolen

Family Applications After (1)

Application Number Title Priority Date Filing Date
DE50203140T Expired - Lifetime DE50203140D1 (de) 2001-02-22 2002-02-11 Verbessertes verfahren zur herstellung von polyetherpolyolen

Country Status (18)

Country Link
US (1) US6776925B2 (cg-RX-API-DMAC7.html)
EP (1) EP1368407B1 (cg-RX-API-DMAC7.html)
JP (1) JP4112985B2 (cg-RX-API-DMAC7.html)
KR (1) KR100799036B1 (cg-RX-API-DMAC7.html)
CN (1) CN1215104C (cg-RX-API-DMAC7.html)
AT (1) ATE295861T1 (cg-RX-API-DMAC7.html)
BR (1) BR0207766B1 (cg-RX-API-DMAC7.html)
CA (1) CA2438647A1 (cg-RX-API-DMAC7.html)
CZ (1) CZ297775B6 (cg-RX-API-DMAC7.html)
DE (2) DE10108484A1 (cg-RX-API-DMAC7.html)
ES (1) ES2242003T3 (cg-RX-API-DMAC7.html)
HU (1) HU227020B1 (cg-RX-API-DMAC7.html)
MX (1) MXPA03007533A (cg-RX-API-DMAC7.html)
PL (1) PL207572B1 (cg-RX-API-DMAC7.html)
PT (1) PT1368407E (cg-RX-API-DMAC7.html)
RU (1) RU2301815C2 (cg-RX-API-DMAC7.html)
TW (1) TWI232228B (cg-RX-API-DMAC7.html)
WO (1) WO2002068503A1 (cg-RX-API-DMAC7.html)

Families Citing this family (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US6596842B2 (en) 2001-07-16 2003-07-22 Shell Oil Company Polymerizing alkylene oxide with sound or radiation treated DMC
EP1369448A1 (de) * 2002-06-07 2003-12-10 Bayer Ag Verfahren zur Herstellung von polymeren Kondensaten und ihre Verwendung
CN1320029C (zh) * 2005-05-31 2007-06-06 抚顺佳化聚氨酯有限公司 一种聚醚多元醇的制备方法
DE102008012613A1 (de) 2008-03-05 2009-09-10 Bayer Materialscience Ag Verfahren zur Herstellung von Polycarbonat nach dem Phasengrenzflächenverfahren
KR20120088696A (ko) * 2009-10-05 2012-08-08 아사히 가라스 가부시키가이샤 연질 폴리우레탄 폼의 제조 방법 및 시트
WO2012006264A1 (en) * 2010-07-08 2012-01-12 Dow Global Technologies Llc Polyurethanes made using zinc catalysts
JP5734633B2 (ja) * 2010-12-09 2015-06-17 三井化学株式会社 アルキレンオキサイド付加物の製造方法
US8663565B2 (en) * 2011-02-11 2014-03-04 Xerox Corporation Continuous emulsification—aggregation process for the production of particles
WO2015110447A1 (de) 2014-01-24 2015-07-30 Bayer Materialscience Ag Verfahren zur herstellung von polycarbonat nach dem phasengrenzflächenverfahren
GB201810380D0 (en) * 2018-06-25 2018-08-08 Rosehill Polymers Group Ltd Continuous reaction system,vessel and method
EP3719052B1 (de) 2019-04-03 2022-03-02 Covestro Deutschland AG Verfahren zur herstellung von polycarbonat mit reduziertem phosgenüberschuss

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Publication number Priority date Publication date Assignee Title
FR1181577A (fr) * 1956-08-23 1959-06-17 Bayer Ag Appareil mélangeur
GB1063525A (en) 1963-02-14 1967-03-30 Gen Tire & Rubber Co Organic cyclic oxide polymers, their preparation and tires prepared therefrom
US3829505A (en) 1970-02-24 1974-08-13 Gen Tire & Rubber Co Polyethers and method for making the same
US3941849A (en) 1972-07-07 1976-03-02 The General Tire & Rubber Company Polyethers and method for making the same
DE3039510A1 (de) * 1980-10-20 1982-06-03 Hoechst Ag, 6000 Frankfurt Vorrichtung und verfahren zum dispergieren und loesen von polymerpulvern
US4533254A (en) 1981-04-17 1985-08-06 Biotechnology Development Corporation Apparatus for forming emulsions
US5159092A (en) * 1989-09-22 1992-10-27 Buss Ag Process for the safe and environmentally sound production of highly pure alkylene oxide adducts
JP2653236B2 (ja) 1990-10-05 1997-09-17 旭硝子株式会社 ポリエーテル化合物の製造方法
US5158922A (en) 1992-02-04 1992-10-27 Arco Chemical Technology, L.P. Process for preparing metal cyanide complex catalyst
JPH05247199A (ja) * 1992-03-04 1993-09-24 Asahi Glass Co Ltd ポリエーテル類の製造方法
US5470813A (en) 1993-11-23 1995-11-28 Arco Chemical Technology, L.P. Double metal cyanide complex catalysts
US5712216A (en) 1995-05-15 1998-01-27 Arco Chemical Technology, L.P. Highly active double metal cyanide complex catalysts
DE4416343C2 (de) 1994-05-09 1996-10-17 Karlsruhe Forschzent Statischer Mikro-Vermischer
KR100372853B1 (ko) * 1994-05-09 2003-05-09 바이엘 악티엔게젤샤프트 마이크로구조 혼합을 이용하여 화학반응을 수행하는 방법 및 장치
US5482908A (en) 1994-09-08 1996-01-09 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
US5545601A (en) 1995-08-22 1996-08-13 Arco Chemical Technology, L.P. Polyether-containing double metal cyanide catalysts
US5767323A (en) * 1995-12-22 1998-06-16 Arco Chemical Technology, L.P. Process for preparing polyoxyalkylene polyether polyols having low levels of transition metals through double metal cyanide complex polyoxyalkylation
US5777177A (en) 1996-02-07 1998-07-07 Arco Chemical Technology, L.P. Preparation of double metal cyanide-catalyzed polyols by continuous addition of starter
US5627120A (en) 1996-04-19 1997-05-06 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
JPH1029213A (ja) * 1996-07-15 1998-02-03 Toray Dow Corning Silicone Co Ltd 液状材料連続混合装置
US5689012A (en) * 1996-07-18 1997-11-18 Arco Chemical Technology, L.P. Continuous preparation of low unsaturation polyoxyalkylene polyether polyols with continuous additon of starter
US5714428A (en) 1996-10-16 1998-02-03 Arco Chemical Technology, L.P. Double metal cyanide catalysts containing functionalized polymers
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DE19757574A1 (de) 1997-12-23 1999-06-24 Bayer Ag Verbesserte Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen
CN1273217C (zh) 1997-10-13 2006-09-06 拜尔公司 用于生产聚醚多元醇的晶态双金属氰化物催化剂
DE19810269A1 (de) 1998-03-10 2000-05-11 Bayer Ag Verbesserte Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen
DE19842383A1 (de) 1998-09-16 2000-03-23 Bayer Ag Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen
DE19913260C2 (de) 1999-03-24 2001-07-05 Bayer Ag Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen
DE19906985A1 (de) 1999-02-19 2000-08-31 Bayer Ag Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen
DE19924672A1 (de) 1999-05-28 2000-11-30 Bayer Ag Doppelmetallcyanic-Katalysatoren für die Herstellung von Polyetherpolyolen
DE19928156A1 (de) * 1999-06-19 2000-12-28 Bayer Ag Aus Polyetherpolyolen hergestellte Polyurethan-Weichschäume
DE10108485A1 (de) * 2001-02-22 2002-09-05 Bayer Ag Verbessertes Verfahren zur Herstellung von Polyetherpolyolen

Also Published As

Publication number Publication date
CA2438647A1 (en) 2002-09-06
ATE295861T1 (de) 2005-06-15
DE50203140D1 (de) 2005-06-23
CZ297775B6 (cs) 2007-03-28
ES2242003T3 (es) 2005-11-01
TWI232228B (en) 2005-05-11
HUP0303259A2 (hu) 2003-12-29
MXPA03007533A (es) 2003-12-11
PT1368407E (pt) 2005-09-30
JP4112985B2 (ja) 2008-07-02
KR20030094256A (ko) 2003-12-11
HK1066819A1 (en) 2005-04-01
BR0207766B1 (pt) 2011-07-26
JP2005506393A (ja) 2005-03-03
HUP0303259A3 (en) 2008-03-28
RU2003128531A (ru) 2005-03-27
KR100799036B1 (ko) 2008-01-28
US20020169229A1 (en) 2002-11-14
CN1505650A (zh) 2004-06-16
PL207572B1 (pl) 2011-01-31
EP1368407B1 (de) 2005-05-18
WO2002068503A1 (de) 2002-09-06
CZ20032222A3 (cs) 2003-11-12
US6776925B2 (en) 2004-08-17
EP1368407A1 (de) 2003-12-10
PL369335A1 (en) 2005-04-18
BR0207766A (pt) 2004-04-27
HU227020B1 (en) 2010-05-28
RU2301815C2 (ru) 2007-06-27
CN1215104C (zh) 2005-08-17

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Legal Events

Date Code Title Description
8127 New person/name/address of the applicant

Owner name: BAYER MATERIALSCIENCE AG, 51373 LEVERKUSEN, DE

8139 Disposal/non-payment of the annual fee