CO5560606A2 - Hidratos cristalinos de derivados de anilida de acido nicotinico - Google Patents
Hidratos cristalinos de derivados de anilida de acido nicotinicoInfo
- Publication number
- CO5560606A2 CO5560606A2 CO04027791A CO04027791A CO5560606A2 CO 5560606 A2 CO5560606 A2 CO 5560606A2 CO 04027791 A CO04027791 A CO 04027791A CO 04027791 A CO04027791 A CO 04027791A CO 5560606 A2 CO5560606 A2 CO 5560606A2
- Authority
- CO
- Colombia
- Prior art keywords
- nicotinic acid
- hydrates
- acid derivatives
- trifluoromethyl
- chlorine
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/81—Amides; Imides
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/34—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom
- A01N43/40—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with one nitrogen atom as the only ring hetero atom six-membered rings
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C233/00—Carboxylic acid amides
- C07C233/64—Carboxylic acid amides having carbon atoms of carboxamide groups bound to carbon atoms of six-membered aromatic rings
- C07C233/66—Carboxylic acid amides having carbon atoms of carboxamide groups bound to carbon atoms of six-membered aromatic rings having the nitrogen atom of at least one of the carboxamide groups bound to a carbon atom of a hydrocarbon radical substituted by halogen atoms or by nitro or nitroso groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/81—Amides; Imides
- C07D213/82—Amides; Imides in position 3
Abstract
1.- Hidratos cristalinos de derivados sustituidos de anilida de ácido nicotínico de la fórmula Idonde A esR1 es fenilo que está sustituido por halógeno, R2 es metilo, difluorometilo, trifluorometilo, cloro, bromo o yodo, R3 es trifluorometilo o cloro.2.- Hidratos de acuerdo con la reivindicación 1, caracterizados porque están presentes en forma de monohidratos.3.- Procedimiento para preparar los hidratos de acuerdo con la reivindicación 1 ó 2, caracterizado porque comprende los siguientes pasos: a) disolver el anhidrato de I en un solvente orgánico hidrosoluble; y b) precipitar el hidrato de I por agregado de agua.
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10147034 | 2001-09-25 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CO5560606A2 true CO5560606A2 (es) | 2005-09-30 |
Family
ID=7700100
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CO04027791A CO5560606A2 (es) | 2001-09-25 | 2004-03-24 | Hidratos cristalinos de derivados de anilida de acido nicotinico |
Country Status (26)
| Country | Link |
|---|---|
| US (1) | US7087239B2 (es) |
| EP (1) | EP1432685B1 (es) |
| JP (1) | JP4401773B2 (es) |
| KR (2) | KR20090127446A (es) |
| CN (1) | CN1275943C (es) |
| AR (1) | AR036578A1 (es) |
| AT (1) | ATE290530T1 (es) |
| AU (1) | AU2002338695B2 (es) |
| BR (1) | BR0212685A (es) |
| CA (1) | CA2460654C (es) |
| CO (1) | CO5560606A2 (es) |
| DE (1) | DE50202440D1 (es) |
| DK (1) | DK1432685T3 (es) |
| EA (1) | EA007780B1 (es) |
| ES (1) | ES2238610T3 (es) |
| HU (1) | HUP0402129A3 (es) |
| IL (2) | IL160640A0 (es) |
| MX (1) | MXPA04002036A (es) |
| MY (1) | MY131952A (es) |
| NZ (1) | NZ531778A (es) |
| PL (1) | PL220091B1 (es) |
| PT (1) | PT1432685E (es) |
| SI (1) | SI1432685T1 (es) |
| TW (1) | TWI281469B (es) |
| UA (1) | UA80538C2 (es) |
| WO (1) | WO2003029219A1 (es) |
Families Citing this family (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE10307751A1 (de) | 2003-02-14 | 2004-08-26 | Basf Ag | Neue kristalline Modifikation des Anhydrates von Boscalid |
| AP2006003533A0 (en) * | 2003-08-26 | 2006-02-28 | Basf Ag | Method of plant growth promotion using amide compounds. |
| JP4970255B2 (ja) * | 2005-06-21 | 2012-07-04 | Ｍｅｉｊｉ Ｓｅｉｋａファルマ株式会社 | 新規殺虫、殺ダニ剤 |
| UA90035C2 (ru) | 2005-11-10 | 2010-03-25 | Басф Се | Фунгицидная смесь, которая содержит боскалид и пириметанил и способ борьбы с фитопатогенными грибами |
| CN101535278B (zh) * | 2006-10-13 | 2011-12-28 | 巴斯夫欧洲公司 | 2-氯-5-[3,6-二氢-3-甲基-2,6-二氧代-4-(三氟甲基)-1-(2h)嘧啶基]-4-氟-n-[[甲基(1-甲基乙基)氨基]磺酰基]苯甲酰胺的水合物 |
| ATE500232T1 (de) * | 2006-10-13 | 2011-03-15 | Basf Se | Kristalline form von 2-chlor-5-ä3,6-dihydro-3- methyl-2,6-dioxo-4-(trifluormethyl)-1-(2h)- pyrimidinylü-4-fluor-n-äämethyl-(1- methylethyl)aminoüsulfonylübenzamid |
| CA2697386A1 (en) * | 2007-08-09 | 2009-02-12 | Basf Se | Fungicidal mixtures |
| US20090280983A1 (en) * | 2008-05-08 | 2009-11-12 | Rui Luiz Correa Picanco | Fertilizer - pesticide throw-pack |
| CA2810578C (en) | 2010-09-09 | 2016-08-30 | Suncor Energy Inc. | Synergistic paraffinic oil and boscalid fungicides |
| CN103348982B (zh) | 2013-07-15 | 2016-06-15 | 江苏龙灯化学有限公司 | 一种杀真菌混合物 |
| CN103980192B (zh) * | 2014-01-20 | 2016-02-17 | 泰州百力化学股份有限公司 | 一种选择性合成不同晶型啶酰菌胺的方法 |
| GB2539022B (en) * | 2015-06-04 | 2018-02-07 | Rotam Agrochem Int Co Ltd | Process for preparing boscalid |
| GB2536979B (en) * | 2015-06-04 | 2019-03-13 | Rotam Agrochem Int Co Ltd | Process for preparing boscalid |
| GB2550138B (en) * | 2016-05-09 | 2019-06-12 | Rotam Agrochem Int Co Ltd | Process for preparing boscalid |
| GB2552696B (en) * | 2016-08-04 | 2020-03-04 | Rotam Agrochem Int Co Ltd | Process for preparing boscalid |
| GB2552699B (en) * | 2016-08-04 | 2021-03-10 | Rotam Agrochem Int Co Ltd | Process for preparing boscalid |
| GB2552697B (en) * | 2016-08-04 | 2021-03-10 | Rotam Agrochem Int Co Ltd | Process for the preparation of boscalid |
| CN106083712B (zh) * | 2016-08-23 | 2018-10-16 | 王正友 | 一种烟酰苯胺盐的合成方法 |
| MX2019003584A (es) | 2016-09-28 | 2019-06-10 | Upl Ltd | Proceso para la preparacion de la forma i de anhidrato de boscalid y la forma ii de anhidrato de boscalid. |
| CN114181141A (zh) * | 2021-12-09 | 2022-03-15 | 江阴苏利化学股份有限公司 | 一种啶酰菌胺晶型ⅰ的制备方法 |
| CN115536581A (zh) * | 2022-10-08 | 2022-12-30 | 河北兰升生物科技有限公司 | 高纯度啶酰菌胺晶型i的制备方法 |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IL103614A (en) * | 1991-11-22 | 1998-09-24 | Basf Ag | Carboxamides for controlling botrytis and certain novel such compounds |
| DE4231517A1 (de) * | 1992-09-21 | 1994-03-24 | Basf Ag | Carbonsäureanilide, Verfahren zu ihrer Herstellung und sie enthaltende Mittel zur Bekämpfung von Schadpilzen |
| DE4322211A1 (de) * | 1993-07-03 | 1995-01-12 | Basf Ag | Wäßrige, mehrphasige, stabile Fertigformulierung für Pflanzenschutz-Wirkstoffe und Verfahren zu ihrer Herstellung |
| DE4331416A1 (de) * | 1993-12-09 | 1995-06-14 | Bayer Ag | Verwendung von Phenylcarbonsäure-amiden als Kristallisationsinhibitoren |
| TW431861B (en) | 1997-12-18 | 2001-05-01 | Basf Ag | Fungicidal mixtures based on amide compounds and azoles |
| AU2003210237A1 (en) * | 2002-02-23 | 2003-09-09 | Bayer Cropscience Aktiengesellschaft | Microbicidal agents on the basis of biphenyl benzamide derivatives |
-
2002
- 2002-09-14 JP JP2003532469A patent/JP4401773B2/ja not_active Expired - Fee Related
- 2002-09-14 NZ NZ531778A patent/NZ531778A/en not_active IP Right Cessation
- 2002-09-14 PL PL370406A patent/PL220091B1/pl unknown
- 2002-09-14 DK DK02777103T patent/DK1432685T3/da active
- 2002-09-14 KR KR1020097024656A patent/KR20090127446A/ko not_active Application Discontinuation
- 2002-09-14 PT PT02777103T patent/PT1432685E/pt unknown
- 2002-09-14 DE DE50202440T patent/DE50202440D1/de not_active Expired - Lifetime
- 2002-09-14 CN CNB028187539A patent/CN1275943C/zh not_active Expired - Fee Related
- 2002-09-14 CA CA2460654A patent/CA2460654C/en not_active Expired - Lifetime
- 2002-09-14 EA EA200400414A patent/EA007780B1/ru not_active IP Right Cessation
- 2002-09-14 KR KR1020047004263A patent/KR100949627B1/ko active IP Right Grant
- 2002-09-14 AU AU2002338695A patent/AU2002338695B2/en not_active Ceased
- 2002-09-14 HU HU0402129A patent/HUP0402129A3/hu unknown
- 2002-09-14 WO PCT/EP2002/010320 patent/WO2003029219A1/de active Application Filing
- 2002-09-14 EP EP02777103A patent/EP1432685B1/de not_active Expired - Lifetime
- 2002-09-14 US US10/490,370 patent/US7087239B2/en not_active Expired - Lifetime
- 2002-09-14 MX MXPA04002036A patent/MXPA04002036A/es active IP Right Grant
- 2002-09-14 BR BR0212685-0A patent/BR0212685A/pt not_active Application Discontinuation
- 2002-09-14 ES ES02777103T patent/ES2238610T3/es not_active Expired - Lifetime
- 2002-09-14 AT AT02777103T patent/ATE290530T1/de active
- 2002-09-14 UA UA20040403075A patent/UA80538C2/uk unknown
- 2002-09-14 SI SI200230123T patent/SI1432685T1/xx unknown
- 2002-09-14 IL IL16064002A patent/IL160640A0/xx unknown
- 2002-09-25 TW TW091122015A patent/TWI281469B/zh not_active IP Right Cessation
- 2002-09-25 AR ARP020103603A patent/AR036578A1/es unknown
- 2002-09-25 MY MYPI20023580A patent/MY131952A/en unknown
-
2004
- 2004-02-26 IL IL160640A patent/IL160640A/en not_active IP Right Cessation
- 2004-03-24 CO CO04027791A patent/CO5560606A2/es not_active Application Discontinuation
Also Published As
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CO5560606A2 (es) | Hidratos cristalinos de derivados de anilida de acido nicotinico | |
| EP2269975B1 (en) | Method for producing aminothiazole derivative and production intermediate | |
| CO6140053A2 (es) | Proceso para fabricar 2-amino-5-halobenzamidas 3-sustituidas | |
| BR0313341A (pt) | Método para a preparação de uma oxazinona fundida e método para a preparação de um composto de fórmula iii | |
| BR0208805A (pt) | Uso de um derivado de pirazolina | |
| RS50672B (sr) | Postupak za pripremanje n-fenilpirazol-1-karboksamida | |
| AR063449A1 (es) | Proceso quimico para derivados de quinazolina, intermediarios | |
| PL94208B1 (es) | ||
| IS7550A (is) | Aðferð til framleiðslu á kvínólín-afleiðum | |
| PE20110100A1 (es) | Procedimiento de preparacion de n-[trans-4-[4-(ciclopropilmetil)-1-piperazinil]ciclohexil]-4-[[(7r)-7-etil-5,6,7,8-tetrahidro-5-metil-8-(1-metiletil)-6-oxo-2-pteridinil]amino]-3-metoxi-benzamida | |
| CO5601030A2 (es) | Derivados de quinolinona/benzoxazinona y usos de los mismos | |
| PE20040907A1 (es) | Derivados de anilinopirazol | |
| BRPI0411195A (pt) | método para a preparação de uma oxazinona fundida e método para a preparação de um composto | |
| Zhu et al. | An alternative route for synthesis of o-trifluoroacetylanilines as useful fluorine-containing intermediates | |
| EA200900629A1 (ru) | Способ сульфинилирования производной пиразола | |
| ES2422297T3 (es) | Proceso para la sulfinilación de un derivado de pirazol | |
| ME01297B (me) | Postupak i intermedijeri u dobijanju derivata n-(1-benzhidril-azetidin-3-il)-n-fenil-metilsulfonamida | |
| CN103275034B (zh) | 一类小分子cathepsin D抑制剂的制备方法 | |
| CN104003887B (zh) | 一种盐酸溴己新的制备方法 | |
| PE20020113A1 (es) | Un procedimiento para preparar compuestos de bifenilo | |
| PT1873145E (pt) | Método de produção de um derivado do ácido nicotínico ou de um seu sal | |
| PE20000558A1 (es) | Procedimiento mejorado para la preparacion de derivados de norbenzomorfano, valiosos farmaceuticamente | |
| HUP0003059A2 (hu) | Eljárás 2-alkiltiobenzoesav-származékok előállítására | |
| DK1678129T3 (da) | Forbedret fremgangsmåde til fremstilling af benzhydrylthioacetamid | |
| JP4351888B2 (ja) | スルファモイルオキシ基またはスルフィナモイルオキシ基が置換された芳香族化合物と求核剤との反応による芳香族化合物誘導体の製造方法 |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FC | Application refused |