MX2019003584A - Proceso para la preparacion de la forma i de anhidrato de boscalid y la forma ii de anhidrato de boscalid. - Google Patents

Proceso para la preparacion de la forma i de anhidrato de boscalid y la forma ii de anhidrato de boscalid.

Info

Publication number
MX2019003584A
MX2019003584A MX2019003584A MX2019003584A MX2019003584A MX 2019003584 A MX2019003584 A MX 2019003584A MX 2019003584 A MX2019003584 A MX 2019003584A MX 2019003584 A MX2019003584 A MX 2019003584A MX 2019003584 A MX2019003584 A MX 2019003584A
Authority
MX
Mexico
Prior art keywords
anhydrate form
boscalid anhydrate
preparation
boscalid
relates
Prior art date
Application number
MX2019003584A
Other languages
English (en)
Inventor
Rajnikant Shroff Jaidev
Rajnikant Shroff Vikram
Manubhai Panchal Digish
Bhulabhai Patel Rakesh
Original Assignee
Upl Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Upl Ltd filed Critical Upl Ltd
Publication of MX2019003584A publication Critical patent/MX2019003584A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/81—Amides; Imides
    • C07D213/82—Amides; Imides in position 3
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/24—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with substituted hydrocarbon radicals attached to ring carbon atoms
    • C07D213/54—Radicals substituted by carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/56—Amides
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0004—Crystallisation cooling by heat exchange
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/0036—Crystallisation on to a bed of product crystals; Seeding
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D9/00—Crystallisation
    • B01D9/005—Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B63/00—Purification; Separation; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07B—GENERAL METHODS OF ORGANIC CHEMISTRY; APPARATUS THEREFOR
    • C07B2200/00—Indexing scheme relating to specific properties of organic compounds
    • C07B2200/13—Crystalline forms, e.g. polymorphs

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Physics & Mathematics (AREA)
  • Thermal Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Pyrrole Compounds (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Saccharide Compounds (AREA)
  • Separation Using Semi-Permeable Membranes (AREA)

Abstract

La presente invención se relaciona a un proceso novedoso para la preparación de la forma I de anhidrato de boscalid y la forma II de anhidrato de boscalid.
MX2019003584A 2016-09-28 2017-09-26 Proceso para la preparacion de la forma i de anhidrato de boscalid y la forma ii de anhidrato de boscalid. MX2019003584A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
IN201631033175 2016-09-28
PCT/IB2017/055821 WO2018060836A1 (en) 2016-09-28 2017-09-26 Process for preparation of boscalid anhydrate form i and boscalid anhydrate form ii

Publications (1)

Publication Number Publication Date
MX2019003584A true MX2019003584A (es) 2019-06-10

Family

ID=61759373

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2019003584A MX2019003584A (es) 2016-09-28 2017-09-26 Proceso para la preparacion de la forma i de anhidrato de boscalid y la forma ii de anhidrato de boscalid.

Country Status (6)

Country Link
US (1) US10934259B2 (es)
EP (1) EP3519388B1 (es)
CN (1) CN109790124B (es)
ES (1) ES2947574T3 (es)
MX (1) MX2019003584A (es)
WO (1) WO2018060836A1 (es)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109232411B (zh) * 2018-10-26 2021-10-01 广东广康生化科技股份有限公司 一种制备啶酰菌胺的方法
CN114181141A (zh) * 2021-12-09 2022-03-15 江阴苏利化学股份有限公司 一种啶酰菌胺晶型ⅰ的制备方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2003029219A1 (de) 2001-09-25 2003-04-10 Basf Aktiengesellschaft Kristalline hydrate von nicotinsaeurenilid- und benzoylanilid-derivaten
MXPA04003733A (es) * 2001-11-02 2004-07-23 Basf Ag Metodo para producir amidas del acido 2-halogeno-piridina-carboxilico.
DE10307751A1 (de) * 2003-02-14 2004-08-26 Basf Ag Neue kristalline Modifikation des Anhydrates von Boscalid
CN102015649B (zh) * 2008-05-08 2013-06-19 巴斯夫欧洲公司 制备芳基碳酰胺的方法
CN103980192B (zh) * 2014-01-20 2016-02-17 泰州百力化学股份有限公司 一种选择性合成不同晶型啶酰菌胺的方法
CN104478797A (zh) * 2014-12-09 2015-04-01 苏州至善化学有限公司 烟酰胺类杀菌剂啶酰菌胺的制备方法
CN104920366A (zh) * 2015-05-14 2015-09-23 京博农化科技股份有限公司 一种啶酰菌胺制剂的加工方法
GB2536979B (en) * 2015-06-04 2019-03-13 Rotam Agrochem Int Co Ltd Process for preparing boscalid
GB2539022B (en) * 2015-06-04 2018-02-07 Rotam Agrochem Int Co Ltd Process for preparing boscalid
GB2550138B (en) * 2016-05-09 2019-06-12 Rotam Agrochem Int Co Ltd Process for preparing boscalid

Also Published As

Publication number Publication date
CN109790124A (zh) 2019-05-21
CN109790124B (zh) 2022-09-13
US10934259B2 (en) 2021-03-02
EP3519388B1 (en) 2023-03-29
US20200031772A1 (en) 2020-01-30
EP3519388A4 (en) 2020-04-15
ES2947574T3 (es) 2023-08-11
EP3519388A1 (en) 2019-08-07
WO2018060836A1 (en) 2018-04-05

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