CN1930108B - 制备(甲基)丙烯酸的方法 - Google Patents

制备(甲基)丙烯酸的方法 Download PDF

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Publication number
CN1930108B
CN1930108B CN2005800069631A CN200580006963A CN1930108B CN 1930108 B CN1930108 B CN 1930108B CN 2005800069631 A CN2005800069631 A CN 2005800069631A CN 200580006963 A CN200580006963 A CN 200580006963A CN 1930108 B CN1930108 B CN 1930108B
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China
Prior art keywords
acrylic acid
meth
tower
methyl
distillation tower
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Expired - Fee Related
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CN2005800069631A
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English (en)
Chinese (zh)
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CN1930108A (zh
Inventor
姜成必
崔锡焕
河炅秀
高准锡
金荣培
禹富坤
朴敏正
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LG Corp
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LG Chemical Co Ltd
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Publication date
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Publication of CN1930108A publication Critical patent/CN1930108A/zh
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/03—Monocarboxylic acids
    • C07C57/04—Acrylic acid; Methacrylic acid
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/48—Separation; Purification; Stabilisation; Use of additives by liquid-liquid treatment

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
CN2005800069631A 2004-08-02 2005-07-27 制备(甲基)丙烯酸的方法 Expired - Fee Related CN1930108B (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
KR10-2004-0060909 2004-08-02
KR1020040060909 2004-08-02
KR20040060909 2004-08-02
PCT/KR2005/002432 WO2006014053A1 (en) 2004-08-02 2005-07-27 Method for producing (meth)acrylic acid

Publications (2)

Publication Number Publication Date
CN1930108A CN1930108A (zh) 2007-03-14
CN1930108B true CN1930108B (zh) 2010-12-29

Family

ID=35733258

Family Applications (1)

Application Number Title Priority Date Filing Date
CN2005800069631A Expired - Fee Related CN1930108B (zh) 2004-08-02 2005-07-27 制备(甲基)丙烯酸的方法

Country Status (9)

Country Link
US (1) US7632968B2 (https=)
EP (1) EP1773748B1 (https=)
JP (2) JP4732366B2 (https=)
KR (1) KR100634678B1 (https=)
CN (1) CN1930108B (https=)
AT (1) ATE468315T1 (https=)
DE (1) DE602005021361D1 (https=)
TW (1) TWI306451B (https=)
WO (1) WO2006014053A1 (https=)

Families Citing this family (16)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE602005021361D1 (de) 2004-08-02 2010-07-01 Lg Chemical Ltd Verfahren zur herstellung von (meth)acrylsäure
US8242308B2 (en) 2006-09-15 2012-08-14 Arkema Inc. Process for producing acrylic acid
JP5358582B2 (ja) * 2007-10-23 2013-12-04 エルジー・ケム・リミテッド （メタ）アクリル酸回収方法および（メタ）アクリル酸回収装置
JP5507111B2 (ja) * 2008-05-30 2014-05-28 ローム アンド ハース カンパニー 水性（メタ）アクリル酸の製造方法
FR2948365B1 (fr) * 2009-07-22 2011-09-09 Arkema France Procede de fabrication d'acide acrylique bio-ressource a partir de glycerol
BR112013022304B1 (pt) * 2011-03-11 2020-01-28 Lg Chemical Ltd método de recuperação contínua de ácido (met)acrílico
JP5821672B2 (ja) * 2012-02-07 2015-11-24 三菱化学株式会社 アクリル酸の製造方法
CN103193618B (zh) * 2013-03-20 2015-11-25 中国石油集团东北炼化工程有限公司吉林设计院 丙烷一步法制丙烯酸生产中的丙烯酸洗涤改进工艺
US10093551B2 (en) * 2014-09-23 2018-10-09 Basf Se Process and plant for treatment of secondary components obtained in acrolein and/or (meth)acrylic acid production
US11976154B2 (en) 2020-01-21 2024-05-07 ExxonMobil Engineering & Technology Company Devolatilization apparatus and process
KR102768883B1 (ko) * 2020-11-10 2025-02-14 주식회사 엘지화학 (메트)아크릴산의 제조 방법
KR102690125B1 (ko) * 2020-12-03 2024-07-30 주식회사 엘지화학 아크릴산의 제조 공정
KR102721330B1 (ko) * 2020-12-03 2024-10-23 주식회사 엘지화학 아크릴산 제조방법
FR3125040B1 (fr) 2021-07-09 2024-04-26 Snf Sa Procédé d’obtention de bio-monomère à partir de diméthylaminoethanol d’origine renouvelable
KR102855132B1 (ko) 2021-10-15 2025-09-04 주식회사 엘지화학 아크릴산 제조방법
KR102855127B1 (ko) 2021-10-15 2025-09-03 주식회사 엘지화학 아크릴산 제조방법

Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3717675A (en) * 1966-08-09 1973-02-20 Knapsack Ag Process for isolating acrylic acid from the reaction gases obtained by the oxidation of propylene or a acrolein
US4156633A (en) * 1974-10-07 1979-05-29 Celanese Corporation Acrylic acid purification
EP0009545A1 (en) * 1978-09-13 1980-04-16 The Standard Oil Company Acrylic acid recovery with recycle quench
CN1022237C (zh) * 1987-06-27 1993-09-29 三井东压化学株式会社 含异丁烯酸反应物气体的骤冷方法及骤冷液的处理方法
CN1247186A (zh) * 1998-08-26 2000-03-15 巴斯福股份公司 连续回收(甲基)丙烯酸的方法
CN1137079C (zh) * 1998-03-31 2004-02-04 巴斯福股份公司 丙烯酸和丙烯酸酯的制备方法
CN1524849A (zh) * 2003-01-14 2004-09-01 纯化丙烯腈的方法中冷凝的骤冷塔顶馏出物的循环

Family Cites Families (23)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPS4810452B1 (https=) * 1969-05-08 1973-04-03
BE786398A (fr) * 1971-07-21 1973-01-18 Basf Ag Procede de preparation de l'acide acrylique anhydre
GB1458397A (en) 1972-12-27 1976-12-15 Degussa Process for obtaining pure acrylic acid
JPS5125602A (en) 1974-08-19 1976-03-02 Mitsubishi Heavy Ind Ltd Hakuyoboira oyobi sonojokiondochosetsuhoho
US3921150A (en) * 1974-09-12 1975-11-18 Sperry Rand Corp Three-rank priority select register system for fail-safe priority determination
GB2146636B (en) * 1983-08-11 1987-02-04 Nippon Catalytic Chem Ind Process for producing acrylic acid
US4554054A (en) * 1983-12-09 1985-11-19 Rohm And Haas Company Methacrylic acid separation
JPS60186197U (ja) 1984-05-17 1985-12-10 徳山内燃機株式会社 熱可塑性材料からなる素材のチツプ化装置
JPS61218556A (ja) * 1985-03-25 1986-09-29 Nippon Shokubai Kagaku Kogyo Co Ltd アクリル酸の精製方法
JPH0615497B2 (ja) * 1985-10-24 1994-03-02 日本化薬株式会社 メタクリル酸の回収方法
JPH062700B2 (ja) 1985-10-29 1994-01-12 三井東圧化学株式会社 メタクロレインの分離法
JPH0759532B2 (ja) * 1987-06-27 1995-06-28 三井東圧化学株式会社 メタクリル酸生成ガスの急冷方法
JP2504777B2 (ja) * 1987-06-27 1996-06-05 三井東圧化学株式会社 反応ガスの急冷方法
JPH0441066Y2 (https=) 1987-06-29 1992-09-28
JP3028925B2 (ja) 1995-12-05 2000-04-04 株式会社日本触媒 アクリル酸の製造方法
DE19814387A1 (de) * 1998-03-31 1999-10-07 Basf Ag Verfahren zur Herstellung von Acrylsäure und Acrylsäureestern
EP1026145B1 (en) * 1999-01-29 2003-04-02 Mitsubishi Chemical Corporation Method for purifying acrylic acid
EP1163201B1 (de) * 1999-03-06 2003-08-20 Basf Aktiengesellschaft Verfahren zur herstellung von acrylsäure
JP2001226320A (ja) * 2000-02-14 2001-08-21 Nippon Shokubai Co Ltd アクリル酸の捕集方法およびアクリル酸の精製方法
JP2002128728A (ja) * 2000-10-19 2002-05-09 Mitsubishi Rayon Co Ltd メタクリル酸の精製方法
DE10063161A1 (de) * 2000-12-18 2002-06-20 Basf Ag Verfahren zum Abschrecken eines heißen (Meth)acrylsäure enthaltenden Gasgemisches
JP2003238485A (ja) * 2001-12-10 2003-08-27 Nippon Shokubai Co Ltd （メタ）アクリル酸の捕集方法および装置
DE602005021361D1 (de) 2004-08-02 2010-07-01 Lg Chemical Ltd Verfahren zur herstellung von (meth)acrylsäure

Patent Citations (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3717675A (en) * 1966-08-09 1973-02-20 Knapsack Ag Process for isolating acrylic acid from the reaction gases obtained by the oxidation of propylene or a acrolein
US4156633A (en) * 1974-10-07 1979-05-29 Celanese Corporation Acrylic acid purification
EP0009545A1 (en) * 1978-09-13 1980-04-16 The Standard Oil Company Acrylic acid recovery with recycle quench
CN1022237C (zh) * 1987-06-27 1993-09-29 三井东压化学株式会社 含异丁烯酸反应物气体的骤冷方法及骤冷液的处理方法
CN1137079C (zh) * 1998-03-31 2004-02-04 巴斯福股份公司 丙烯酸和丙烯酸酯的制备方法
CN1247186A (zh) * 1998-08-26 2000-03-15 巴斯福股份公司 连续回收(甲基)丙烯酸的方法
CN1524849A (zh) * 2003-01-14 2004-09-01 纯化丙烯腈的方法中冷凝的骤冷塔顶馏出物的循环

Also Published As

Publication number Publication date
KR100634678B1 (ko) 2006-10-13
JP4732366B2 (ja) 2011-07-27
US20060025629A1 (en) 2006-02-02
TWI306451B (en) 2009-02-21
JP2007522207A (ja) 2007-08-09
KR20060048785A (ko) 2006-05-18
US7632968B2 (en) 2009-12-15
ATE468315T1 (de) 2010-06-15
TW200611892A (en) 2006-04-16
JP5393713B2 (ja) 2014-01-22
EP1773748A1 (en) 2007-04-18
JP2011105776A (ja) 2011-06-02
CN1930108A (zh) 2007-03-14
EP1773748A4 (en) 2008-08-20
DE602005021361D1 (de) 2010-07-01
WO2006014053A1 (en) 2006-02-09
EP1773748B1 (en) 2010-05-19

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