CN1746277A - 适用于润滑螺纹接头的润滑涂层组合物 - Google Patents
适用于润滑螺纹接头的润滑涂层组合物 Download PDFInfo
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- CN1746277A CN1746277A CNA2005101063691A CN200510106369A CN1746277A CN 1746277 A CN1746277 A CN 1746277A CN A2005101063691 A CNA2005101063691 A CN A2005101063691A CN 200510106369 A CN200510106369 A CN 200510106369A CN 1746277 A CN1746277 A CN 1746277A
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- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2030/00—Specified physical or chemical properties which is improved by the additive characterising the lubricating composition, e.g. multifunctional additives
- C10N2030/52—Base number [TBN]
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2050/00—Form in which the lubricant is applied to the material being lubricated
- C10N2050/015—Dispersions of solid lubricants
- C10N2050/02—Dispersions of solid lubricants dissolved or suspended in a carrier which subsequently evaporates to leave a lubricant coating
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- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10N—INDEXING SCHEME ASSOCIATED WITH SUBCLASS C10M RELATING TO LUBRICATING COMPOSITIONS
- C10N2080/00—Special pretreatment of the material to be lubricated, e.g. phosphatising or chromatising of a metal
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- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Organic Chemistry (AREA)
- Engineering & Computer Science (AREA)
- General Engineering & Computer Science (AREA)
- Mechanical Engineering (AREA)
- Lubricants (AREA)
- Non-Disconnectible Joints And Screw-Threaded Joints (AREA)
- Paints Or Removers (AREA)
Abstract
Description
号码 | C | Si | Mn | P | S | Cu | Ni | Cr | Mo | 名称 |
1 | 0.24 | 0.30 | 1.30 | 0.02 | 0.01 | 0.04 | 0.07 | 0.17 | 0.04 | Mn钢 |
2 | 0.19 | 0.25 | 0.80 | 0.02 | 0.01 | 0.04 | 0.1 | 13.0 | 0.04 | 13Cr钢 |
溶剂 | A-1 | 矿油精(JIS K2201 4) |
A-2 | 二甲苯 | |
A-3 | 丁基溶纤剂 | |
碱式润滑剂 | B-1 | 碱式磺酸钙(b.n.:400mg KOH/g) |
B-2 | 碱式磺酸钡(b.n.:100mg KOH/g) | |
B-3 | 碱式水杨酸镁(b.n.:150mg KOH/g) | |
B-4 | 碱式石炭酸钙(b.n.:300mg KOH/g) | |
热塑性树脂粉末 | C-1 | 聚乙烯粉末(p.d.:20μm) |
C-2 | 丙烯酸树脂粉末(p.d.:2μm) | |
C-3 | 苯乙烯树脂粉末(p.d.:0.2μm) | |
极压剂 | D-1 | 硫化猪油(S:10%,s.n.:180mg KOH/g) |
D-2 | 二月桂基磷酸氢盐 | |
D-3 | 二烷基二硫代磷酸锌(Zn:8%,P:9%,S:17%) | |
其它润滑剂 | E-1 | 牛油脂肪酸钙皂(s.n.:20mg KOH/g) |
E-2 | 中性磺酸钙(b.n.:1mg KOH/g) | |
E-3 | 三羟甲基丙烷三油酸酯(s.n.:160mg KOH/g) | |
E-4 | 羊毛脂(s.n.:100mg KOH/g) | |
E-5 | 纯化矿物油(ISO VG46) |
标号 | Rmax(μm) | 表面糙化的方法 |
F-1 | 3 | 和机械加工后一样(没有表面糙化) |
F-2 | 5 | Cu电镀 |
F-3 | 20 | 喷砂 |
22 | 喷砂+Cu电镀 | |
F-4 | 10 | 磷酸锌处理 |
F-5 | 20,25 | 磷酸锰处理 |
35,40 | 喷砂+磷酸锰处理 | |
F-6 | 30 | 在Mn钢上扩散渗镀(喷锌) |
25 | 在13Cr钢上扩散渗镀(喷锌) |
载荷 | 每次增加100kgf |
温度 | 室温 |
试验时间 | 每一种载荷下保持30秒 |
转速 | 20rpm |
润滑涂层 | 只涂覆在凹面试验片上 |
试验A | 常规试验(没有鳞片) |
试验B | 加入鳞片后试验 |
实施例:碳(Mn)钢接头 | ||||||||||||
标号 | 1 | 2 | 3 | 4 | 5 | 6 | 7 | 8 | 9 | 10 | 11 | |
润滑涂层组合物(wt%) | A-1 | 50 | 50 | 50 | 50 | 60 | 60 | 60 | 50 | 50 | 20 | |
A-2 | 30 | 30 | ||||||||||
A-3 | 10 | 10 | 10 | 10 | ||||||||
B-1 | 25 | 5 | 25 | 25 | ||||||||
B-2 | 25 | 5 | 10 | |||||||||
B-3 | 25 | 5 | 10 | |||||||||
B-4 | 25 | 15 | 25 | |||||||||
C-1 | ||||||||||||
C-2 | ||||||||||||
C-3 | 0.5 | |||||||||||
D-1 | 1 | 2 | 5 | |||||||||
D-2 | 2 | 3 | ||||||||||
D-3 | 2 | 1 | 5 | |||||||||
E-1 | 10 | 10 | 5 | 5 | 4 | 10 | ||||||
E-2 | 5 | 12 | ||||||||||
E-3 | 10 | 13 | 10 | 5 | 10 | 10 | 20 | 10 | ||||
E-4 | 3 | 10 | 5 | 10 | 10 | 5 | 4.5 | |||||
E-5 | 5 | 9 | 10 | 10 | 13 | 5 | 2 | 10 | ||||
碱值 | 200 | 50 | 125 | 150 | 67 | 167 | 31 | 113 | 110 | 250 | 200 | |
粘度1 | 4.0 | 4.3 | 3.8 | 3.9 | 3.2 | 3.5 | 3.7 | 3.6 | 16 | 6.5 | 84 | |
厚度2 | 20 | 25 | 30 | 10 | 40 | 60 | 25 | 30 | 15 | 40 | 100 | |
凸面试验片的表面粗糙度(Rmax,μm) | F-1 | 3 | 3 | 3 | 3 | 3 | 3 | |||||
F-2 | ||||||||||||
F-3 | ||||||||||||
F-4 | 10 | 10 | 10 | 10 | 10 | |||||||
F-5 | ||||||||||||
F-6 | ||||||||||||
凹面试验片的表面粗糙度(Rmax,μm) | F-1 | 3 | ||||||||||
F-2 | 5 | |||||||||||
F-3 | 20 | 20 | 20 | 20 | ||||||||
F-4 | ||||||||||||
F-5 | 20 | 40 | 20 | 35 | ||||||||
F-6 | 30 | |||||||||||
润滑性A3 | 15 | 15 | 15 | 15 | 14 | 13 | 13 | 14 | 14 | 14 | 17 | |
润滑性B4 | 11 | 11 | 11 | 11 | 11 | 10 | 10 | 11 | 10 | 10 | 13 | |
防锈性 | ○ | ○ | ○ | ○ | ○ | ○ | □ | ○ | ○ | ○ | ○ |
碳(Mn)钢接头 | 不锈钢(13Cr)接头 | ||||||||||
标号 | 12 | 13 | 14 | 15 | 16 | 17 | 18 | 19 | 20 | 21 | |
润滑涂层组合物(wt%) | A-1 | 50 | 20 | 25 | 40 | 40 | 40 | 50 | 40 | ||
A-2 | 30 | 10 | 10 | 30 | 30 | ||||||
A-3 | 10 | 10 | |||||||||
B-1 | 20 | 25 | 20 | 20 | |||||||
B-2 | 25 | 25 | |||||||||
B-3 | 20 | 10 | 20 | ||||||||
B-4 | 10 | 25 | 30 | ||||||||
C-1 | 2 | 4 | 1 | 5 | |||||||
C-2 | 0.5 | 1 | 3 | 10 | |||||||
C-3 | 10 | 1 | |||||||||
D-1 | 2 | 2 | 2 | ||||||||
D-2 | 1 | 3 | |||||||||
D-3 | 4 | 2 | |||||||||
E-1 | 10 | 10 | |||||||||
E-2 | 5 | 10 | |||||||||
E-3 | 10 | 10 | 15 | 10 | 20 | 20 | 10 | ||||
E-4 | 4.5 | 7 | 10 | 25 | 5 | ||||||
E-5 | 20 | 10 | 33 | 16 | 16 | ||||||
碱值 | 50 | 183 | 42 | 154 | 83 | 143 | 133 | 50 | 160 | 100 | |
粘度1 | 67 | 250 | 144 | 182 | 132 | 15 | 7.8 | 115 | 238 | 166 | |
厚度2 | 80 | 300 | 150 | 180 | 120 | 25 | 35 | 80 | 200 | 150 | |
凸面试验片的表面粗糙度(Rmax,μm) | F-1 | 3 | 3 | 3 | 3 | 3 | |||||
F-2 | 5 | 5 | |||||||||
F-3 | 20 | 20 | |||||||||
F-4 | 1O | 10 | |||||||||
F-5 | |||||||||||
F-6 | |||||||||||
凹面试验片的表面粗糙度(Rmax,μm) | F-1 | 3 | |||||||||
F-2 | 5 | ||||||||||
F-3 | 20 | 22 | 22 | ||||||||
F-4 | |||||||||||
F-5 | 25 | 40 | 20 | ||||||||
F-6 | 25 | 25 | |||||||||
润滑性A3 | 15 | 15 | 15 | 15 | 16 | 14 | 13 | 16 | 14 | 15 | |
润滑性B4 | 12 | 12 | 12 | 12 | 13 | 10 | 10 | 12 | 11 | 12 | |
防锈性 | ○ | ○ | □ | ○ | ○ | ○ | ○ | ○ | ○ | ○ |
对比实施例(Mn钢接头) | 传统实施例 | ||||||||
标号 | 1 | 2 | 3 | 4 | 1 | 2 | 3 | 4 | |
润滑涂层组合物(wt%) | A-1 | 50 | 脂润滑—Mn钢(API规格),—进行脂补充涂覆 | 脂润滑—Mn钢(API规格),—不进行脂补充涂覆 | MoS2/环氧树脂涂覆—Mn钢(API规格),—不进行脂补充涂覆 | 脂润滑—13Cr钢(API规格),—进行脂补充涂覆 | |||
A-2 | 30 | ||||||||
A-3 | 10 | ||||||||
B-1 | 20 | ||||||||
B-2 | 50 | ||||||||
B-3 | |||||||||
B-4 | |||||||||
C-1 | 5 | ||||||||
C-2 | 3 | ||||||||
C-3 | |||||||||
D-1 | |||||||||
D-2 | 2 | ||||||||
D-3 | 2 | ||||||||
E-1 | |||||||||
E-2 | 30 | 25 | |||||||
E-3 | 10 | 10 | |||||||
E-4 | 8 | 10 | |||||||
E-5 | 40 | 75 | 20 | ||||||
碱值 | 50 | <l | 80 | <1 | - | - | - | - | |
粘度1 | 348 | 3.8 | 523 | 134 | - | - | - | - | |
厚度2 | 350 | 25 | 450 | 120 | 850 | 850 | 30 | 850 | |
凸面试验片的表面粗糙度(Rmax,μm) | F-1 | 3 | 3 | 3 | 3 | 3 | 3 | ||
F-2 | |||||||||
F-3 | |||||||||
F-4 | 10 | 10 | |||||||
F-5 | |||||||||
F-6 | |||||||||
凹面试验片的表面粗糙度(Rmax,μm) | F-1 | 3 | |||||||
F-2 | 20 | ||||||||
F-3 | 22 | ||||||||
F-4 | |||||||||
F-5 | 20 | 20 | 25 | 25 | 20 | ||||
F-6 | |||||||||
润滑性A3 | 8 | 4 | 9 | 7 | 15 | 8 | 10 | 14 | |
润滑性B4 | 6 | 3 | 7 | 5 | 11 | 5 | 5 | 10 | |
防锈性 | △ | × | ○ | △ | ○ | -* | △ | ○ |
Claims (26)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
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JP2000368895A JP4092871B2 (ja) | 2000-12-04 | 2000-12-04 | ねじ継手の潤滑処理に適した潤滑被膜形成用組成物 |
JP2000368895 | 2000-12-04 |
Related Parent Applications (1)
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CNB018200397A Division CN1280386C (zh) | 2000-12-04 | 2001-12-04 | 适用于润滑螺纹接头的润滑涂层组合物 |
Publications (2)
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CN1746277A true CN1746277A (zh) | 2006-03-15 |
CN100529030C CN100529030C (zh) | 2009-08-19 |
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CNB018200397A Expired - Lifetime CN1280386C (zh) | 2000-12-04 | 2001-12-04 | 适用于润滑螺纹接头的润滑涂层组合物 |
CNB2005101063691A Expired - Lifetime CN100529030C (zh) | 2000-12-04 | 2001-12-04 | 适用于润滑螺纹接头的润滑涂层组合物 |
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CNB018200397A Expired - Lifetime CN1280386C (zh) | 2000-12-04 | 2001-12-04 | 适用于润滑螺纹接头的润滑涂层组合物 |
Country Status (16)
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US (1) | US6869111B2 (zh) |
EP (1) | EP1350834B1 (zh) |
JP (1) | JP4092871B2 (zh) |
CN (2) | CN1280386C (zh) |
AR (1) | AR031897A1 (zh) |
AU (1) | AU2002222575A1 (zh) |
BR (1) | BR0115926B1 (zh) |
CA (1) | CA2430533C (zh) |
EG (1) | EG23042A (zh) |
ES (1) | ES2541767T3 (zh) |
MX (1) | MXPA03004952A (zh) |
MY (1) | MY141943A (zh) |
PL (1) | PL198006B1 (zh) |
RO (2) | RO123531B1 (zh) |
RU (1) | RU2246532C1 (zh) |
WO (1) | WO2002046338A1 (zh) |
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- 2000-12-04 JP JP2000368895A patent/JP4092871B2/ja not_active Expired - Lifetime
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- 2001-12-02 EG EG20011288A patent/EG23042A/xx active
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- 2001-12-04 EP EP01999621.4A patent/EP1350834B1/en not_active Expired - Lifetime
- 2001-12-04 PL PL362794A patent/PL198006B1/pl unknown
- 2001-12-04 RO ROA200600372A patent/RO123531B1/ro unknown
- 2001-12-04 ES ES01999621.4T patent/ES2541767T3/es not_active Expired - Lifetime
- 2001-12-04 AR ARP010105637A patent/AR031897A1/es active IP Right Grant
- 2001-12-04 RU RU2003119974/04A patent/RU2246532C1/ru active
- 2001-12-04 WO PCT/JP2001/010573 patent/WO2002046338A1/ja active Application Filing
- 2001-12-04 CN CNB018200397A patent/CN1280386C/zh not_active Expired - Lifetime
- 2001-12-04 BR BRPI0115926-7A patent/BR0115926B1/pt not_active IP Right Cessation
- 2001-12-04 RO ROA200300489A patent/RO121035B1/ro unknown
- 2001-12-04 CA CA002430533A patent/CA2430533C/en not_active Expired - Lifetime
- 2001-12-04 CN CNB2005101063691A patent/CN100529030C/zh not_active Expired - Lifetime
- 2001-12-04 AU AU2002222575A patent/AU2002222575A1/en not_active Abandoned
- 2001-12-04 MY MYPI20015522A patent/MY141943A/en unknown
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Cited By (4)
Publication number | Priority date | Publication date | Assignee | Title |
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CN104145074A (zh) * | 2012-02-23 | 2014-11-12 | 国际壳牌研究有限公司 | 连接器组件 |
CN104145074B (zh) * | 2012-02-23 | 2016-10-12 | 国际壳牌研究有限公司 | 连接器组件 |
CN104520414A (zh) * | 2012-08-06 | 2015-04-15 | 新日铁住金株式会社 | 管状螺纹接头及用于它的润滑被膜形成用组合物 |
CN114770984A (zh) * | 2022-06-17 | 2022-07-22 | 北京航空航天大学宁波创新研究院 | 风电叶片根部连接用螺栓套及其预埋强度提升方法 |
Also Published As
Publication number | Publication date |
---|---|
CN100529030C (zh) | 2009-08-19 |
MY141943A (en) | 2010-07-30 |
EP1350834A1 (en) | 2003-10-08 |
AR031897A1 (es) | 2003-10-08 |
RU2246532C1 (ru) | 2005-02-20 |
RO123531B1 (ro) | 2013-04-30 |
CN1280386C (zh) | 2006-10-18 |
EG23042A (en) | 2004-01-31 |
EP1350834A4 (en) | 2005-04-20 |
EP1350834B1 (en) | 2015-04-08 |
JP2002173692A (ja) | 2002-06-21 |
BR0115926B1 (pt) | 2011-05-17 |
RO121035B1 (ro) | 2006-11-30 |
CA2430533A1 (en) | 2002-06-13 |
ES2541767T3 (es) | 2015-07-24 |
PL362794A1 (en) | 2004-11-02 |
PL198006B1 (pl) | 2008-05-30 |
US6869111B2 (en) | 2005-03-22 |
MXPA03004952A (es) | 2005-02-14 |
CN1526006A (zh) | 2004-09-01 |
BR0115926A (pt) | 2003-12-23 |
WO2002046338A1 (en) | 2002-06-13 |
JP4092871B2 (ja) | 2008-05-28 |
AU2002222575A1 (en) | 2002-06-18 |
US20030111838A1 (en) | 2003-06-19 |
CA2430533C (en) | 2009-05-12 |
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