CN1562476A - 一种高活性和高稳定性铁锰费托合成催化剂及其制法 - Google Patents
一种高活性和高稳定性铁锰费托合成催化剂及其制法 Download PDFInfo
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- CN1562476A CN1562476A CN 200410012191 CN200410012191A CN1562476A CN 1562476 A CN1562476 A CN 1562476A CN 200410012191 CN200410012191 CN 200410012191 CN 200410012191 A CN200410012191 A CN 200410012191A CN 1562476 A CN1562476 A CN 1562476A
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- fischer
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- ferrimanganic
- tropsch synthetic
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- 239000003054 catalyst Substances 0.000 title claims abstract description 65
- 238000002360 preparation method Methods 0.000 title claims description 23
- 230000015572 biosynthetic process Effects 0.000 title abstract description 9
- 229910000616 Ferromanganese Inorganic materials 0.000 title 1
- DALUDRGQOYMVLD-UHFFFAOYSA-N iron manganese Chemical compound [Mn].[Fe] DALUDRGQOYMVLD-UHFFFAOYSA-N 0.000 title 1
- 238000001308 synthesis method Methods 0.000 title 1
- 229910052742 iron Inorganic materials 0.000 claims abstract description 14
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims abstract description 12
- 229910052710 silicon Inorganic materials 0.000 claims abstract description 12
- 239000010703 silicon Substances 0.000 claims abstract description 12
- 229910052791 calcium Inorganic materials 0.000 claims abstract description 9
- 229910052748 manganese Inorganic materials 0.000 claims abstract description 8
- 238000001035 drying Methods 0.000 claims abstract description 7
- 229910052700 potassium Inorganic materials 0.000 claims abstract description 3
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 49
- 239000011572 manganese Substances 0.000 claims description 28
- 239000011575 calcium Substances 0.000 claims description 23
- 229910004298 SiO 2 Inorganic materials 0.000 claims description 17
- 239000007787 solid Substances 0.000 claims description 16
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 14
- 239000012065 filter cake Substances 0.000 claims description 14
- 239000008367 deionised water Substances 0.000 claims description 12
- 229910021641 deionized water Inorganic materials 0.000 claims description 12
- 230000009257 reactivity Effects 0.000 claims description 12
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 12
- 229910021645 metal ion Inorganic materials 0.000 claims description 11
- 238000001556 precipitation Methods 0.000 claims description 11
- RMAQACBXLXPBSY-UHFFFAOYSA-N silicic acid Chemical compound O[Si](O)(O)O RMAQACBXLXPBSY-UHFFFAOYSA-N 0.000 claims description 9
- 238000010009 beating Methods 0.000 claims description 8
- 238000005406 washing Methods 0.000 claims description 8
- 229910021529 ammonia Inorganic materials 0.000 claims description 7
- 238000001914 filtration Methods 0.000 claims description 7
- 238000002156 mixing Methods 0.000 claims description 7
- 239000012266 salt solution Substances 0.000 claims description 7
- OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 claims description 5
- 230000002378 acidificating effect Effects 0.000 claims description 5
- BWHMMNNQKKPAPP-UHFFFAOYSA-L potassium carbonate Substances [K+].[K+].[O-]C([O-])=O BWHMMNNQKKPAPP-UHFFFAOYSA-L 0.000 claims description 5
- 238000005507 spraying Methods 0.000 claims description 5
- PWHULOQIROXLJO-UHFFFAOYSA-N Manganese Chemical compound [Mn] PWHULOQIROXLJO-UHFFFAOYSA-N 0.000 claims description 4
- WCUXLLCKKVVCTQ-UHFFFAOYSA-M Potassium chloride Chemical compound [Cl-].[K+] WCUXLLCKKVVCTQ-UHFFFAOYSA-M 0.000 claims description 4
- UIIMBOGNXHQVGW-UHFFFAOYSA-M Sodium bicarbonate Chemical compound [Na+].OC([O-])=O UIIMBOGNXHQVGW-UHFFFAOYSA-M 0.000 claims description 4
- SCVFZCLFOSHCOH-UHFFFAOYSA-M potassium acetate Chemical compound [K+].CC([O-])=O SCVFZCLFOSHCOH-UHFFFAOYSA-M 0.000 claims description 4
- 239000001103 potassium chloride Substances 0.000 claims description 4
- 235000011164 potassium chloride Nutrition 0.000 claims description 4
- 239000006188 syrup Substances 0.000 claims description 4
- 235000020357 syrup Nutrition 0.000 claims description 4
- 235000015320 potassium carbonate Nutrition 0.000 claims description 3
- 238000000247 postprecipitation Methods 0.000 claims description 2
- 239000002244 precipitate Substances 0.000 claims description 2
- 239000002002 slurry Substances 0.000 abstract description 16
- 238000003786 synthesis reaction Methods 0.000 abstract description 8
- 235000011114 ammonium hydroxide Nutrition 0.000 abstract description 7
- 230000000694 effects Effects 0.000 abstract description 7
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 abstract 2
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 abstract 1
- 229910002551 Fe-Mn Inorganic materials 0.000 abstract 1
- 238000001354 calcination Methods 0.000 abstract 1
- 229910052681 coesite Inorganic materials 0.000 abstract 1
- 229910052906 cristobalite Inorganic materials 0.000 abstract 1
- TYJJADVDDVDEDZ-UHFFFAOYSA-M potassium hydrogencarbonate Chemical compound [K+].OC([O-])=O TYJJADVDDVDEDZ-UHFFFAOYSA-M 0.000 abstract 1
- 239000000377 silicon dioxide Substances 0.000 abstract 1
- 235000012239 silicon dioxide Nutrition 0.000 abstract 1
- 229910052682 stishovite Inorganic materials 0.000 abstract 1
- 229910052905 tridymite Inorganic materials 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 17
- 238000000034 method Methods 0.000 description 9
- 230000002829 reductive effect Effects 0.000 description 9
- 239000007789 gas Substances 0.000 description 8
- 238000001694 spray drying Methods 0.000 description 8
- 238000006243 chemical reaction Methods 0.000 description 7
- 238000000975 co-precipitation Methods 0.000 description 7
- 239000002245 particle Substances 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 5
- 239000004005 microsphere Substances 0.000 description 5
- 238000005303 weighing Methods 0.000 description 5
- 230000008569 process Effects 0.000 description 4
- XTVVROIMIGLXTD-UHFFFAOYSA-N copper(II) nitrate Chemical compound [Cu+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O XTVVROIMIGLXTD-UHFFFAOYSA-N 0.000 description 3
- 239000000446 fuel Substances 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 238000004519 manufacturing process Methods 0.000 description 3
- 229910002091 carbon monoxide Inorganic materials 0.000 description 2
- 238000006555 catalytic reaction Methods 0.000 description 2
- 239000003245 coal Substances 0.000 description 2
- 239000010949 copper Substances 0.000 description 2
- 238000009826 distribution Methods 0.000 description 2
- 229910052739 hydrogen Inorganic materials 0.000 description 2
- MVFCKEFYUDZOCX-UHFFFAOYSA-N iron(2+);dinitrate Chemical compound [Fe+2].[O-][N+]([O-])=O.[O-][N+]([O-])=O MVFCKEFYUDZOCX-UHFFFAOYSA-N 0.000 description 2
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
- 239000011259 mixed solution Substances 0.000 description 2
- 239000003921 oil Substances 0.000 description 2
- 239000004215 Carbon black (E152) Substances 0.000 description 1
- UGFAIRIUMAVXCW-UHFFFAOYSA-N Carbon monoxide Chemical compound [O+]#[C-] UGFAIRIUMAVXCW-UHFFFAOYSA-N 0.000 description 1
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 description 1
- 229910002651 NO3 Inorganic materials 0.000 description 1
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 230000004913 activation Effects 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 239000000378 calcium silicate Substances 0.000 description 1
- 229960003340 calcium silicate Drugs 0.000 description 1
- 229910052918 calcium silicate Inorganic materials 0.000 description 1
- 235000012241 calcium silicate Nutrition 0.000 description 1
- OYACROKNLOSFPA-UHFFFAOYSA-N calcium;dioxido(oxo)silane Chemical compound [Ca+2].[O-][Si]([O-])=O OYACROKNLOSFPA-UHFFFAOYSA-N 0.000 description 1
- 239000012018 catalyst precursor Substances 0.000 description 1
- 239000003795 chemical substances by application Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 235000009508 confectionery Nutrition 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 230000009849 deactivation Effects 0.000 description 1
- WDNQRCVBPNOTNV-UHFFFAOYSA-N dinonylnaphthylsulfonic acid Chemical compound C1=CC=C2C(S(O)(=O)=O)=C(CCCCCCCCC)C(CCCCCCCCC)=CC2=C1 WDNQRCVBPNOTNV-UHFFFAOYSA-N 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 229930195733 hydrocarbon Natural products 0.000 description 1
- 150000002430 hydrocarbons Chemical class 0.000 description 1
- 239000001257 hydrogen Substances 0.000 description 1
- 125000004435 hydrogen atom Chemical class [H]* 0.000 description 1
- 230000002779 inactivation Effects 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- WPBNNNQJVZRUHP-UHFFFAOYSA-L manganese(2+);methyl n-[[2-(methoxycarbonylcarbamothioylamino)phenyl]carbamothioyl]carbamate;n-[2-(sulfidocarbothioylamino)ethyl]carbamodithioate Chemical compound [Mn+2].[S-]C(=S)NCCNC([S-])=S.COC(=O)NC(=S)NC1=CC=CC=C1NC(=S)NC(=O)OC WPBNNNQJVZRUHP-UHFFFAOYSA-L 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 239000003345 natural gas Substances 0.000 description 1
- 229910017604 nitric acid Inorganic materials 0.000 description 1
- 229910000027 potassium carbonate Inorganic materials 0.000 description 1
- 235000011181 potassium carbonates Nutrition 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000012827 research and development Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- 238000004062 sedimentation Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 238000009955 starching Methods 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
Landscapes
- Catalysts (AREA)
Abstract
Description
实施例 | 实施例1 | 实施例2 | 实施例3 | 实施例4 | 实施例5 |
催化剂粒径(μm) | 35-90 | 30-80 | 30-100 | 45-90 | 55-120 |
成品率(%) | 95 | 96 | 96.5 | 97 | 97.5 |
还原条件 | |||||
温度(℃) | 285 | 270 | 295 | 280 | 285 |
压力(MPa) | 0.2 | 0.1 | 0.2 | 0.3 | 0.5 |
空速(h-1) | 2000 | 1000 | 2000 | 1000 | 1000 |
气体及时间(h) | H2,20h | H2/CO=0.7,32h | H2/CO=0.7,20h | CO,16h | H2/CO=2.0,24h |
费托合成反应结果 | |||||
失活率(%/天) | 0.05 | 0.03 | 0.04 | 0.1 | 0.04 |
CO转化率(%) | 63 | 45 | 60 | 75 | 65 |
CO2选择性(%) | 28 | 23 | 39 | 29 | 32 |
C1(wt%) | 4.7 | 3.5 | 6.7 | 8.2 | 5.0 |
C2-4(wt%) | 12.1 | 10.7 | 14.4 | 16.9 | 11.7 |
C5 +(wt%) | 83.2 | 85.8 | 78.9 | 74.9 | 83.3 |
C2-4 =/C2-4 0 | 4.1 | 5.7 | 4.7 | 2.6 | 5.9 |
Claims (10)
Priority Applications (1)
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CN 200410012191 CN1270822C (zh) | 2004-03-16 | 2004-03-16 | 一种铁锰费托合成催化剂及其制法 |
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---|---|---|---|
CN 200410012191 CN1270822C (zh) | 2004-03-16 | 2004-03-16 | 一种铁锰费托合成催化剂及其制法 |
Publications (2)
Publication Number | Publication Date |
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CN1562476A true CN1562476A (zh) | 2005-01-12 |
CN1270822C CN1270822C (zh) | 2006-08-23 |
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Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101811050A (zh) * | 2010-05-05 | 2010-08-25 | 中国科学院山西煤炭化学研究所 | 一种有机疏水改性钴基费托合成催化剂及制备和应用 |
WO2010121516A1 (zh) * | 2009-04-22 | 2010-10-28 | 中科合成油技术有限公司 | 一种费托合成催化剂、其制备方法和应用 |
CN102441384A (zh) * | 2010-10-12 | 2012-05-09 | 中国石油化工股份有限公司 | 一种高活性稳定性负载型铁基合成气制低碳烯烃催化剂的制备方法 |
CN103230800A (zh) * | 2013-05-16 | 2013-08-07 | 神华集团有限责任公司 | 一种含镓铁基费托催化剂及其制备方法 |
CN104707620A (zh) * | 2015-03-16 | 2015-06-17 | 中科合成油技术有限公司 | 一种费托合成催化剂及其制备方法与应用 |
CN108620077A (zh) * | 2017-03-17 | 2018-10-09 | 神华集团有限责任公司 | 低温费托合成催化剂及其制备方法和应用 |
CN108620076A (zh) * | 2017-03-17 | 2018-10-09 | 神华集团有限责任公司 | 低温费托合成催化剂及其制备方法和应用 |
CN110732329A (zh) * | 2018-07-20 | 2020-01-31 | 国家能源投资集团有限责任公司 | 含钾硅溶胶及其制备方法和费托合成铁基催化剂及其制备方法和费托合成方法 |
CN110961097A (zh) * | 2018-09-30 | 2020-04-07 | 中国石油化工股份有限公司 | 一种费托合成催化剂及其制备方法和费托合成工艺 |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101396647B (zh) | 2007-09-29 | 2011-03-16 | 中科合成油技术有限公司 | 用于费-托合成的气-液-固三相悬浮床反应器及其应用 |
-
2004
- 2004-03-16 CN CN 200410012191 patent/CN1270822C/zh not_active Expired - Lifetime
Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
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WO2010121516A1 (zh) * | 2009-04-22 | 2010-10-28 | 中科合成油技术有限公司 | 一种费托合成催化剂、其制备方法和应用 |
RU2477654C1 (ru) * | 2009-04-22 | 2013-03-20 | Синфьюэлс Чайна Текнолоджи Ко., Лтд | Катализатор синтеза фишера-тропша, его изготовление и применение |
CN101811050A (zh) * | 2010-05-05 | 2010-08-25 | 中国科学院山西煤炭化学研究所 | 一种有机疏水改性钴基费托合成催化剂及制备和应用 |
CN102441384A (zh) * | 2010-10-12 | 2012-05-09 | 中国石油化工股份有限公司 | 一种高活性稳定性负载型铁基合成气制低碳烯烃催化剂的制备方法 |
CN103230800B (zh) * | 2013-05-16 | 2015-11-04 | 神华集团有限责任公司 | 一种含镓铁基费托催化剂及其制备方法 |
CN103230800A (zh) * | 2013-05-16 | 2013-08-07 | 神华集团有限责任公司 | 一种含镓铁基费托催化剂及其制备方法 |
CN104707620A (zh) * | 2015-03-16 | 2015-06-17 | 中科合成油技术有限公司 | 一种费托合成催化剂及其制备方法与应用 |
CN108620077A (zh) * | 2017-03-17 | 2018-10-09 | 神华集团有限责任公司 | 低温费托合成催化剂及其制备方法和应用 |
CN108620076A (zh) * | 2017-03-17 | 2018-10-09 | 神华集团有限责任公司 | 低温费托合成催化剂及其制备方法和应用 |
CN108620076B (zh) * | 2017-03-17 | 2021-04-06 | 国家能源投资集团有限责任公司 | 低温费托合成催化剂及其制备方法和应用 |
CN110732329A (zh) * | 2018-07-20 | 2020-01-31 | 国家能源投资集团有限责任公司 | 含钾硅溶胶及其制备方法和费托合成铁基催化剂及其制备方法和费托合成方法 |
CN110732329B (zh) * | 2018-07-20 | 2022-12-27 | 国家能源投资集团有限责任公司 | 含钾硅溶胶及其制备方法和费托合成铁基催化剂及其制备方法和费托合成方法 |
CN110961097A (zh) * | 2018-09-30 | 2020-04-07 | 中国石油化工股份有限公司 | 一种费托合成催化剂及其制备方法和费托合成工艺 |
CN110961097B (zh) * | 2018-09-30 | 2023-08-08 | 中国石油化工股份有限公司 | 一种费托合成催化剂及其制备方法和费托合成工艺 |
Also Published As
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Effective date of registration: 20130613 Address after: 010321 building, building 6, Zhungeer Qi new road, Inner Mongolia Patentee after: SYNFUELS CHINA INNER MONGOLIA Co.,Ltd. Address before: 101407 Beijing city Huairou District Yanqi Economic Development Zone C District No. 1 south two Street Park Patentee before: SYNFUELS CHINA TECHNOLOGY Co.,Ltd. |
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CX01 | Expiry of patent term |
Granted publication date: 20060823 |
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CX01 | Expiry of patent term |