CN1548491A - 自消光树脂的合成工艺和紫外光固化漆膜坚韧的亚光面漆 - Google Patents
自消光树脂的合成工艺和紫外光固化漆膜坚韧的亚光面漆 Download PDFInfo
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- CN1548491A CN1548491A CNA031168825A CN03116882A CN1548491A CN 1548491 A CN1548491 A CN 1548491A CN A031168825 A CNA031168825 A CN A031168825A CN 03116882 A CN03116882 A CN 03116882A CN 1548491 A CN1548491 A CN 1548491A
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- moles
- acrylate
- affixture
- bisphenol
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
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- 239000011347 resin Substances 0.000 title claims abstract description 9
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- 238000003786 synthesis reaction Methods 0.000 title claims description 3
- 239000002966 varnish Substances 0.000 title abstract 2
- PXKLMJQFEQBVLD-UHFFFAOYSA-N bisphenol F Chemical compound C1=CC(O)=CC=C1CC1=CC=C(O)C=C1 PXKLMJQFEQBVLD-UHFFFAOYSA-N 0.000 claims abstract description 14
- GOOHAUXETOMSMM-UHFFFAOYSA-N Propylene oxide Chemical compound CC1CO1 GOOHAUXETOMSMM-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000000463 material Substances 0.000 claims abstract description 5
- 229920001228 polyisocyanate Polymers 0.000 claims abstract description 4
- 239000005056 polyisocyanate Substances 0.000 claims abstract description 4
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 16
- 239000003973 paint Substances 0.000 claims description 16
- NIXOWILDQLNWCW-UHFFFAOYSA-N Acrylic acid Chemical compound OC(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-N 0.000 claims description 12
- NIXOWILDQLNWCW-UHFFFAOYSA-M Acrylate Chemical compound [O-]C(=O)C=C NIXOWILDQLNWCW-UHFFFAOYSA-M 0.000 claims description 8
- 239000000377 silicon dioxide Substances 0.000 claims description 8
- 238000003756 stirring Methods 0.000 claims description 8
- 229920002635 polyurethane Polymers 0.000 claims description 7
- 239000004814 polyurethane Substances 0.000 claims description 7
- MNAHQWDCXOHBHK-UHFFFAOYSA-N 1-phenylpropane-1,1-diol Chemical compound CCC(O)(O)C1=CC=CC=C1 MNAHQWDCXOHBHK-UHFFFAOYSA-N 0.000 claims description 6
- 238000006243 chemical reaction Methods 0.000 claims description 6
- 239000000178 monomer Substances 0.000 claims description 6
- 239000000126 substance Substances 0.000 claims description 6
- 239000007788 liquid Substances 0.000 claims description 5
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- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 5
- 238000005516 engineering process Methods 0.000 claims description 4
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 4
- 238000000034 method Methods 0.000 claims description 4
- 238000006116 polymerization reaction Methods 0.000 claims description 4
- 125000000391 vinyl group Chemical group [H]C([*])=C([H])[H] 0.000 claims description 4
- 229920002554 vinyl polymer Polymers 0.000 claims description 4
- OMIGHNLMNHATMP-UHFFFAOYSA-N 2-hydroxyethyl prop-2-enoate Chemical compound OCCOC(=O)C=C OMIGHNLMNHATMP-UHFFFAOYSA-N 0.000 claims description 3
- GWZMWHWAWHPNHN-UHFFFAOYSA-N 2-hydroxypropyl prop-2-enoate Chemical compound CC(O)COC(=O)C=C GWZMWHWAWHPNHN-UHFFFAOYSA-N 0.000 claims description 3
- 239000003054 catalyst Substances 0.000 claims description 3
- ZMARGGQEAJXRFP-UHFFFAOYSA-N 1-hydroxypropan-2-yl 2-methylprop-2-enoate Chemical compound OCC(C)OC(=O)C(C)=C ZMARGGQEAJXRFP-UHFFFAOYSA-N 0.000 claims description 2
- AMULJSVDIHMAOX-UHFFFAOYSA-N 3-hydroxypropyl prop-2-enoate;prop-2-enoic acid Chemical compound OC(=O)C=C.OCCCOC(=O)C=C AMULJSVDIHMAOX-UHFFFAOYSA-N 0.000 claims description 2
- IAYPIBMASNFSPL-UHFFFAOYSA-N Ethylene oxide Chemical compound C1CO1 IAYPIBMASNFSPL-UHFFFAOYSA-N 0.000 claims description 2
- UKLDJPRMSDWDSL-UHFFFAOYSA-L [dibutyl(dodecanoyloxy)stannyl] dodecanoate Chemical compound CCCCCCCCCCCC(=O)O[Sn](CCCC)(CCCC)OC(=O)CCCCCCCCCCC UKLDJPRMSDWDSL-UHFFFAOYSA-L 0.000 claims description 2
- 125000003368 amide group Chemical group 0.000 claims description 2
- 239000012752 auxiliary agent Substances 0.000 claims description 2
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- 239000013530 defoamer Substances 0.000 claims description 2
- 239000012975 dibutyltin dilaurate Substances 0.000 claims description 2
- VLCAYQIMSMPEBW-UHFFFAOYSA-N methyl 3-hydroxy-2-methylidenebutanoate Chemical compound COC(=O)C(=C)C(C)O VLCAYQIMSMPEBW-UHFFFAOYSA-N 0.000 claims description 2
- 239000002994 raw material Substances 0.000 claims description 2
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- 239000000080 wetting agent Substances 0.000 claims description 2
- DVKJHBMWWAPEIU-UHFFFAOYSA-N toluene 2,4-diisocyanate Chemical compound CC1=CC=C(N=C=O)C=C1N=C=O DVKJHBMWWAPEIU-UHFFFAOYSA-N 0.000 claims 1
- 238000007259 addition reaction Methods 0.000 abstract description 4
- -1 ethylene epoxide Chemical class 0.000 abstract 3
- IISBACLAFKSPIT-UHFFFAOYSA-N bisphenol A Chemical compound C=1C=C(O)C=CC=1C(C)(C)C1=CC=C(O)C=C1 IISBACLAFKSPIT-UHFFFAOYSA-N 0.000 abstract 2
- JOYRKODLDBILNP-UHFFFAOYSA-N Ethyl urethane Chemical compound CCOC(N)=O JOYRKODLDBILNP-UHFFFAOYSA-N 0.000 abstract 1
- 239000005977 Ethylene Substances 0.000 abstract 1
- 239000003085 diluting agent Substances 0.000 abstract 1
- 230000035939 shock Effects 0.000 abstract 1
- 229920002803 thermoplastic polyurethane Polymers 0.000 abstract 1
- 239000011248 coating agent Substances 0.000 description 10
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- 238000000016 photochemical curing Methods 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- ZDQNWDNMNKSMHI-UHFFFAOYSA-N 1-[2-(2-prop-2-enoyloxypropoxy)propoxy]propan-2-yl prop-2-enoate Chemical compound C=CC(=O)OC(C)COC(C)COCC(C)OC(=O)C=C ZDQNWDNMNKSMHI-UHFFFAOYSA-N 0.000 description 2
- SMZOUWXMTYCWNB-UHFFFAOYSA-N 2-(2-methoxy-5-methylphenyl)ethanamine Chemical compound COC1=CC=C(C)C=C1CCN SMZOUWXMTYCWNB-UHFFFAOYSA-N 0.000 description 2
- 239000004593 Epoxy Substances 0.000 description 2
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical class OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 2
- HVVWZTWDBSEWIH-UHFFFAOYSA-N [2-(hydroxymethyl)-3-prop-2-enoyloxy-2-(prop-2-enoyloxymethyl)propyl] prop-2-enoate Chemical compound C=CC(=O)OCC(CO)(COC(=O)C=C)COC(=O)C=C HVVWZTWDBSEWIH-UHFFFAOYSA-N 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 150000001336 alkenes Chemical class 0.000 description 2
- SZXQTJUDPRGNJN-UHFFFAOYSA-N dipropylene glycol Chemical compound OCCCOCCCO SZXQTJUDPRGNJN-UHFFFAOYSA-N 0.000 description 2
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- JRZJOMJEPLMPRA-UHFFFAOYSA-N olefin Natural products CCCCCCCC=C JRZJOMJEPLMPRA-UHFFFAOYSA-N 0.000 description 2
- 238000002360 preparation method Methods 0.000 description 2
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- 125000004805 propylene group Chemical group [H]C([H])([H])C([H])([*:1])C([H])([H])[*:2] 0.000 description 2
- 238000010298 pulverizing process Methods 0.000 description 2
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- 239000000243 solution Substances 0.000 description 2
- IMNIMPAHZVJRPE-UHFFFAOYSA-N triethylenediamine Chemical compound C1CN2CCN1CC2 IMNIMPAHZVJRPE-UHFFFAOYSA-N 0.000 description 2
- DKEGCUDAFWNSSO-UHFFFAOYSA-N 1,8-dibromooctane Chemical compound BrCCCCCCCCBr DKEGCUDAFWNSSO-UHFFFAOYSA-N 0.000 description 1
- LCZVSXRMYJUNFX-UHFFFAOYSA-N 2-[2-(2-hydroxypropoxy)propoxy]propan-1-ol Chemical compound CC(O)COC(C)COC(C)CO LCZVSXRMYJUNFX-UHFFFAOYSA-N 0.000 description 1
- KMNCBSZOIQAUFX-UHFFFAOYSA-N 2-ethoxy-1,2-diphenylethanone Chemical compound C=1C=CC=CC=1C(OCC)C(=O)C1=CC=CC=C1 KMNCBSZOIQAUFX-UHFFFAOYSA-N 0.000 description 1
- NLGDWWCZQDIASO-UHFFFAOYSA-N 2-hydroxy-1-(7-oxabicyclo[4.1.0]hepta-1,3,5-trien-2-yl)-2-phenylethanone Chemical compound OC(C(=O)c1cccc2Oc12)c1ccccc1 NLGDWWCZQDIASO-UHFFFAOYSA-N 0.000 description 1
- 241000208140 Acer Species 0.000 description 1
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- 235000017491 Bambusa tulda Nutrition 0.000 description 1
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- 244000082204 Phyllostachys viridis Species 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- ZJCCRDAZUWHFQH-UHFFFAOYSA-N Trimethylolpropane Chemical compound CCC(CO)(CO)CO ZJCCRDAZUWHFQH-UHFFFAOYSA-N 0.000 description 1
- DAKWPKUUDNSNPN-UHFFFAOYSA-N Trimethylolpropane triacrylate Chemical compound C=CC(=O)OCC(CC)(COC(=O)C=C)COC(=O)C=C DAKWPKUUDNSNPN-UHFFFAOYSA-N 0.000 description 1
- 239000007983 Tris buffer Substances 0.000 description 1
- 239000002390 adhesive tape Substances 0.000 description 1
- 125000002947 alkylene group Chemical group 0.000 description 1
- 229910021529 ammonia Inorganic materials 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- VQLYBLABXAHUDN-UHFFFAOYSA-N bis(4-fluorophenyl)-methyl-(1,2,4-triazol-1-ylmethyl)silane;methyl n-(1h-benzimidazol-2-yl)carbamate Chemical compound C1=CC=C2NC(NC(=O)OC)=NC2=C1.C=1C=C(F)C=CC=1[Si](C=1C=CC(F)=CC=1)(C)CN1C=NC=N1 VQLYBLABXAHUDN-UHFFFAOYSA-N 0.000 description 1
- TXTCTCUXLQYGLA-UHFFFAOYSA-L calcium;prop-2-enoate Chemical compound [Ca+2].[O-]C(=O)C=C.[O-]C(=O)C=C TXTCTCUXLQYGLA-UHFFFAOYSA-L 0.000 description 1
- BVKZGUZCCUSVTD-UHFFFAOYSA-N carbonic acid Chemical compound OC(O)=O BVKZGUZCCUSVTD-UHFFFAOYSA-N 0.000 description 1
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- 239000013078 crystal Substances 0.000 description 1
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- FPAFDBFIGPHWGO-UHFFFAOYSA-N dioxosilane;oxomagnesium;hydrate Chemical compound O.[Mg]=O.[Mg]=O.[Mg]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O.O=[Si]=O FPAFDBFIGPHWGO-UHFFFAOYSA-N 0.000 description 1
- 229920001971 elastomer Polymers 0.000 description 1
- 238000007429 general method Methods 0.000 description 1
- 239000011229 interlayer Substances 0.000 description 1
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- QSHDDOUJBYECFT-UHFFFAOYSA-N mercury Chemical compound [Hg] QSHDDOUJBYECFT-UHFFFAOYSA-N 0.000 description 1
- 229910052753 mercury Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 235000020636 oyster Nutrition 0.000 description 1
- 239000000123 paper Substances 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920003023 plastic Polymers 0.000 description 1
- 229920005749 polyurethane resin Polymers 0.000 description 1
- KCTAWXVAICEBSD-UHFFFAOYSA-N prop-2-enoyloxy prop-2-eneperoxoate Chemical compound C=CC(=O)OOOC(=O)C=C KCTAWXVAICEBSD-UHFFFAOYSA-N 0.000 description 1
- 239000005060 rubber Substances 0.000 description 1
- 150000005846 sugar alcohols Polymers 0.000 description 1
- 239000012974 tin catalyst Substances 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Landscapes
- Macromonomer-Based Addition Polymer (AREA)
- Polyurethanes Or Polyureas (AREA)
Abstract
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Priority Applications (1)
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CNB031168825A CN100556970C (zh) | 2003-05-13 | 2003-05-13 | 自消光树脂的合成工艺和紫外光固化漆膜坚韧的亚光面漆 |
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CNB031168825A CN100556970C (zh) | 2003-05-13 | 2003-05-13 | 自消光树脂的合成工艺和紫外光固化漆膜坚韧的亚光面漆 |
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CN1548491A true CN1548491A (zh) | 2004-11-24 |
CN100556970C CN100556970C (zh) | 2009-11-04 |
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Cited By (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100382898C (zh) * | 2006-04-29 | 2008-04-23 | 江苏海陆装饰有限公司 | 亚光凹凸花纹彩色钢板的连续化生产方法 |
CN103113554A (zh) * | 2013-03-19 | 2013-05-22 | 中国科学院长春应用化学研究所 | 紫外光固化消光树脂及其制备方法 |
CN103665767A (zh) * | 2013-11-25 | 2014-03-26 | 苏州宏泉高压电容器有限公司 | 环氧树脂及其制备方法 |
CN104974324A (zh) * | 2015-06-30 | 2015-10-14 | 中科院广州化学有限公司南雄材料生产基地 | 一种反应自消光型水性聚氨酯树脂及其制备方法与应用 |
CN108623782A (zh) * | 2017-03-22 | 2018-10-09 | 万华化学(北京)有限公司 | 一种自消光性光固化树脂、制备方法及其用途 |
CN109762421A (zh) * | 2018-12-26 | 2019-05-17 | 宁波惠之星新材料科技有限公司 | 一种曲面盖板用硬化涂液以及利用该涂液制备曲面盖板硬化涂层的方法 |
CN110204684A (zh) * | 2019-05-20 | 2019-09-06 | 佳化化学科技发展(上海)有限公司 | 一种聚氨酯丙烯酸树脂及其制备方法和应用 |
CN110330936A (zh) * | 2019-06-10 | 2019-10-15 | 佳化化学科技发展(上海)有限公司 | 一种烷氧化双酚f在uv固化胶粘剂树脂制备中的应用及其胶粘剂 |
CN114806388A (zh) * | 2022-04-13 | 2022-07-29 | 佳化化学科技发展(上海)有限公司 | 一种紫外光固化哑光涂料及其制备方法和制品 |
-
2003
- 2003-05-13 CN CNB031168825A patent/CN100556970C/zh not_active Expired - Fee Related
Cited By (12)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100382898C (zh) * | 2006-04-29 | 2008-04-23 | 江苏海陆装饰有限公司 | 亚光凹凸花纹彩色钢板的连续化生产方法 |
CN103113554A (zh) * | 2013-03-19 | 2013-05-22 | 中国科学院长春应用化学研究所 | 紫外光固化消光树脂及其制备方法 |
CN103113554B (zh) * | 2013-03-19 | 2014-10-22 | 中国科学院长春应用化学研究所 | 紫外光固化消光树脂及其制备方法 |
CN103665767A (zh) * | 2013-11-25 | 2014-03-26 | 苏州宏泉高压电容器有限公司 | 环氧树脂及其制备方法 |
CN104974324A (zh) * | 2015-06-30 | 2015-10-14 | 中科院广州化学有限公司南雄材料生产基地 | 一种反应自消光型水性聚氨酯树脂及其制备方法与应用 |
CN108623782A (zh) * | 2017-03-22 | 2018-10-09 | 万华化学(北京)有限公司 | 一种自消光性光固化树脂、制备方法及其用途 |
CN108623782B (zh) * | 2017-03-22 | 2020-11-24 | 万华化学(北京)有限公司 | 一种自消光性光固化树脂、制备方法及其用途 |
CN109762421A (zh) * | 2018-12-26 | 2019-05-17 | 宁波惠之星新材料科技有限公司 | 一种曲面盖板用硬化涂液以及利用该涂液制备曲面盖板硬化涂层的方法 |
CN110204684A (zh) * | 2019-05-20 | 2019-09-06 | 佳化化学科技发展(上海)有限公司 | 一种聚氨酯丙烯酸树脂及其制备方法和应用 |
CN110330936A (zh) * | 2019-06-10 | 2019-10-15 | 佳化化学科技发展(上海)有限公司 | 一种烷氧化双酚f在uv固化胶粘剂树脂制备中的应用及其胶粘剂 |
CN110330936B (zh) * | 2019-06-10 | 2021-06-29 | 佳化化学科技发展(上海)有限公司 | 一种烷氧化双酚f在uv固化胶粘剂树脂制备中的应用及其胶粘剂 |
CN114806388A (zh) * | 2022-04-13 | 2022-07-29 | 佳化化学科技发展(上海)有限公司 | 一种紫外光固化哑光涂料及其制备方法和制品 |
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