CN1235869C - (甲基)丙烯酸酯的制备方法 - Google Patents
(甲基)丙烯酸酯的制备方法 Download PDFInfo
- Publication number
- CN1235869C CN1235869C CNB028115376A CN02811537A CN1235869C CN 1235869 C CN1235869 C CN 1235869C CN B028115376 A CNB028115376 A CN B028115376A CN 02811537 A CN02811537 A CN 02811537A CN 1235869 C CN1235869 C CN 1235869C
- Authority
- CN
- China
- Prior art keywords
- methyl
- vinylformic acid
- acrylate
- ester
- mixture
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Lifetime
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/06—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton from hydroxy amines by reactions involving the etherification or esterification of hydroxy groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
- C07C213/10—Separation; Purification; Stabilisation; Use of additives
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/20—Power plant
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/22—Accessories
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S203/00—Distillation: processes, separatory
- Y10S203/90—Particular type of heating
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE10127938.8 | 2001-06-08 | ||
| DE10127938A DE10127938A1 (de) | 2001-06-08 | 2001-06-08 | Verfahren zur Herstellung von (Meth)acrylsäureestern |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1592734A CN1592734A (zh) | 2005-03-09 |
| CN1235869C true CN1235869C (zh) | 2006-01-11 |
Family
ID=7687687
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB028115376A Expired - Lifetime CN1235869C (zh) | 2001-06-08 | 2002-05-28 | (甲基)丙烯酸酯的制备方法 |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US7294240B2 (https=) |
| EP (1) | EP1490326B1 (https=) |
| JP (1) | JP2005506958A (https=) |
| CN (1) | CN1235869C (https=) |
| AT (1) | ATE493380T1 (https=) |
| DE (2) | DE10127938A1 (https=) |
| WO (1) | WO2002100817A2 (https=) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI253636B (en) * | 2003-11-19 | 2006-04-21 | Mediatek Inc | Apparatus with switching servo gain and offset for optical disk device and method thereof |
| DE10354652A1 (de) | 2003-11-22 | 2005-07-07 | Clariant Gmbh | Verfahren zur Veresterung von Alkoholen mit olefinisch ungesättigten Carbonsäuren |
| JP2006182606A (ja) * | 2004-12-28 | 2006-07-13 | Miyoshi Oil & Fat Co Ltd | セメント混和剤及びセメント組成物 |
| KR100786945B1 (ko) | 2005-08-11 | 2007-12-17 | 주식회사 엘지화학 | (메타)아크릴 에스테르의 제조 방법 |
| DE102008040221A1 (de) * | 2008-07-07 | 2010-01-14 | Evonik Röhm Gmbh | Verfahren zur Herstellung von (Meth)acrylsäureestern |
| FR2941452B1 (fr) * | 2009-01-27 | 2011-02-11 | Arkema France | Procede de purification de la fraction azeotropique generee lors de la synthese de l'acrylate de n,n-dimethyl aminoethyle |
| CA2811363A1 (en) * | 2010-09-23 | 2012-03-29 | Basf Se | Process for preparing (meth)acrylic esters of n,n-substituted amino alcohols |
| JP5289490B2 (ja) * | 2011-03-18 | 2013-09-11 | 株式会社日本触媒 | エーテル基を有する(メタ)アクリル酸エステルの製造方法 |
| RU2497802C1 (ru) * | 2012-04-24 | 2013-11-10 | Закрытое акционерное общество "Химтэк Инжиниринг" | Способ получения диметиламиноэтилакрилата |
| CN102850155B (zh) * | 2012-09-24 | 2015-07-08 | 上海和创化学股份有限公司 | 甲基丙烯酸酯类产品的制备方法 |
| KR101984280B1 (ko) | 2015-11-27 | 2019-05-30 | 주식회사 엘지화학 | (메트)아크릴산의 제조 방법 |
| FR3050731B1 (fr) | 2016-04-28 | 2018-04-20 | Arkema France | Composition d'acrylate de n,n-dimethyl aminoethyle stabilisee vis-a-vis de la coloration |
| FR3069538B1 (fr) | 2017-07-25 | 2020-05-15 | Arkema France | Procede de purification d'esters (meth)acryliques. |
| FR3086658B1 (fr) | 2018-10-02 | 2021-10-15 | Arkema France | Stabilisation de (meth)acrylates d'aminoalkyle |
| BR102020022314A2 (pt) * | 2020-10-30 | 2022-05-10 | Oxiteno S.A. Indústria E Comércio | Processo para a preparação de poliacrilatos alcoxilados funcionais, poliacrilatos alcoxilados funcionais, e, uso dos mesmos |
Family Cites Families (22)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE1067806B (de) | 1954-09-09 | 1959-10-29 | Roehm & Haas Gmbh | Verfahren zur kontinuierlichen Herstellung von Estern der Acryl- und Methacrylsaeuremit hoehermolekularen Alkoholen |
| US2832800A (en) | 1956-01-23 | 1958-04-29 | Rohm & Haas | Reesterification alcoholysis |
| DE1248943C2 (de) * | 1965-07-20 | 1974-03-07 | Basf Ag | Verfahren und Vorrichtung zur diskontinuierlichen Entfernung von Geruchs-stoffen auswaessrigen Polymerisatdispersionen |
| FR2033441A5 (https=) | 1969-02-25 | 1970-12-04 | Ugilor | |
| BE787750A (fr) * | 1971-08-20 | 1973-02-19 | Union Carbide Corp | Procede pour inhiber la polymerisation d'acrylates et methacrylates pendant leur distillation |
| GB1573071A (en) | 1977-02-10 | 1980-08-13 | Mitsubishi Rayon Co | Process for producing unsaturated carbocylic acid esters |
| US4147721A (en) * | 1978-04-06 | 1979-04-03 | Halcon Research And Development Corporation | Process for recovering methacrylic acid |
| US4260821A (en) * | 1979-03-15 | 1981-04-07 | Halcon Research And Development Corp. | Minimizing polymerization during recovery of methacrylic acid |
| US4698440A (en) * | 1983-09-14 | 1987-10-06 | E. I. Du Pont De Nemours And Company | Process for making n-butyl methacrylate |
| GB8410497D0 (en) | 1984-04-25 | 1984-05-31 | Allied Colloids Ltd | Synthesis of vinyl esters |
| FR2617840B1 (fr) | 1987-07-08 | 1989-09-01 | Charbonnages Ste Chimique | Procede de fabrication de (meth)acrylate de dialkylaminoalkyle |
| DE3843854A1 (de) | 1988-12-24 | 1990-06-28 | Henkel Kgaa | Verfahren zur verbesserten herstellung von (meth)acrylsaeureestern mehrwertiger alkohole (i) |
| JPH0713050B2 (ja) | 1989-09-26 | 1995-02-15 | 東亞合成株式会社 | ジメチルアミノエチルアクリレートの製造方法 |
| DE4019788A1 (de) | 1990-06-21 | 1992-01-02 | Henkel Kgaa | Verfahren zur herstellung von mehrfunktionellen (meth)acrylsaeureestern |
| DE69807406T2 (de) * | 1997-10-01 | 2003-04-24 | Nippon Shokubai Co. Ltd., Osaka | Verfahren zur Herstellung von Alkylamino-(meth)Acrylat und eine Vorrichtung dafür |
| DE19814529A1 (de) * | 1998-04-01 | 1999-10-07 | Basf Ag | Polyalkylenarylate mit hohem Carbonylendgruppengehalt |
| FR2777561B1 (fr) | 1998-04-21 | 2000-06-02 | Atochem Elf Sa | Procede de fabrication en continu de (meth)acrylates de dialkylaminoalkyle |
| EP0965593B2 (en) * | 1998-06-19 | 2008-12-03 | Shin-Etsu Chemical Co., Ltd. | Distillation of (meth)acryloxybearing alkoxysilane |
| US6482976B1 (en) * | 1999-06-17 | 2002-11-19 | Union Carbide Chemicals & Plastics Technology Corporation | Processes for conducting equilibrium-limited reactions |
| DE10063175A1 (de) * | 2000-12-18 | 2002-06-20 | Basf Ag | Verfahren zur Herstellung von höheren (Meth)acrylsäureestern |
| DE10127939A1 (de) | 2001-06-08 | 2002-05-29 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
| DE10127941A1 (de) * | 2001-06-08 | 2002-05-29 | Basf Ag | Verfahren zur Herstellung von (Meth)acrylsäureestern |
-
2001
- 2001-06-08 DE DE10127938A patent/DE10127938A1/de not_active Withdrawn
-
2002
- 2002-05-28 JP JP2003503587A patent/JP2005506958A/ja active Pending
- 2002-05-28 CN CNB028115376A patent/CN1235869C/zh not_active Expired - Lifetime
- 2002-05-28 AT AT02758206T patent/ATE493380T1/de active
- 2002-05-28 WO PCT/EP2002/005818 patent/WO2002100817A2/de not_active Ceased
- 2002-05-28 DE DE50214843T patent/DE50214843D1/de not_active Expired - Lifetime
- 2002-05-28 EP EP02758206A patent/EP1490326B1/de not_active Expired - Lifetime
- 2002-05-28 US US10/479,962 patent/US7294240B2/en not_active Expired - Lifetime
Also Published As
| Publication number | Publication date |
|---|---|
| DE50214843D1 (de) | 2011-02-10 |
| EP1490326A2 (de) | 2004-12-29 |
| CN1592734A (zh) | 2005-03-09 |
| US20040168903A1 (en) | 2004-09-02 |
| WO2002100817A2 (de) | 2002-12-19 |
| EP1490326B1 (de) | 2010-12-29 |
| WO2002100817A3 (de) | 2004-10-21 |
| DE10127938A1 (de) | 2002-07-25 |
| US7294240B2 (en) | 2007-11-13 |
| JP2005506958A (ja) | 2005-03-10 |
| ATE493380T1 (de) | 2011-01-15 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CX01 | Expiry of patent term | ||
| CX01 | Expiry of patent term |
Granted publication date: 20060111 |