CN1207746A - 统一连续制备聚酰胺的方法和设备 - Google Patents
统一连续制备聚酰胺的方法和设备 Download PDFInfo
- Publication number
- CN1207746A CN1207746A CN96199638A CN96199638A CN1207746A CN 1207746 A CN1207746 A CN 1207746A CN 96199638 A CN96199638 A CN 96199638A CN 96199638 A CN96199638 A CN 96199638A CN 1207746 A CN1207746 A CN 1207746A
- Authority
- CN
- China
- Prior art keywords
- pressure
- reactor
- polyamide
- melt
- water
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/08—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino-carboxylic acids
- C08G69/14—Lactams
- C08G69/16—Preparatory processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/04—Preparatory processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/26—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from polyamines and polycarboxylic acids
- C08G69/28—Preparatory processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G69/00—Macromolecular compounds obtained by reactions forming a carboxylic amide link in the main chain of the macromolecule
- C08G69/02—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids
- C08G69/36—Polyamides derived from amino-carboxylic acids or from polyamines and polycarboxylic acids derived from amino acids, polyamines and polycarboxylic acids
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P20/00—Technologies relating to chemical industry
- Y02P20/50—Improvements relating to the production of bulk chemicals
- Y02P20/582—Recycling of unreacted starting or intermediate materials
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Proteomics, Peptides & Aminoacids (AREA)
- Polyamides (AREA)
Abstract
Description
Claims (10)
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE19546417A DE19546417B4 (de) | 1995-12-12 | 1995-12-12 | Verfahren und Vorrichtung zur vereinheitlichten, kontinuierlichen Herstellung von Polyamiden |
DE19546417.6 | 1995-12-12 |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1207746A true CN1207746A (zh) | 1999-02-10 |
CN1108330C CN1108330C (zh) | 2003-05-14 |
Family
ID=7779923
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN96199638A Expired - Fee Related CN1108330C (zh) | 1995-12-12 | 1996-12-10 | 统一连续制备聚酰胺的方法和设备 |
Country Status (5)
Country | Link |
---|---|
US (1) | US6136947A (zh) |
EP (1) | EP0866826B1 (zh) |
CN (1) | CN1108330C (zh) |
DE (2) | DE19546417B4 (zh) |
WO (1) | WO1997021758A2 (zh) |
Cited By (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100378142C (zh) * | 1999-05-03 | 2008-04-02 | L.布鲁克曼酒精化学工厂两合公司 | 聚酰胺的缩合工艺 |
CN101050279B (zh) * | 2007-05-09 | 2010-05-19 | 武汉森大科技研究发展中心 | 聚酰胺聚合生产工艺及设备 |
CN102585216A (zh) * | 2012-01-20 | 2012-07-18 | 北京伊克希德化工技术有限公司 | 尼龙66短流程连续聚合的方法及设备 |
WO2013107425A1 (zh) * | 2012-01-20 | 2013-07-25 | 北京伊克希德化工技术有限公司 | 尼龙66等以双组分单体为原料的尼龙连续聚合方法及设备 |
CN104910375A (zh) * | 2015-06-25 | 2015-09-16 | 安庆市虹泰新材料有限责任公司 | 一种聚酰胺缩聚反应装置 |
CN105722891A (zh) * | 2013-06-12 | 2016-06-29 | 巴斯夫欧洲公司 | 用于制备脂族或部分芳族聚酰胺的方法,所述方法包含固相聚合过程 |
CN106866956A (zh) * | 2017-03-27 | 2017-06-20 | 万华化学集团股份有限公司 | 聚十二内酰胺及其改性树脂的多级串联聚合方法 |
WO2018153048A1 (en) * | 2017-02-24 | 2018-08-30 | Advansix Resins & Chemicals Llc | Enhanced polyamide base resin for engineering plastics formulations |
CN108586731A (zh) * | 2018-06-12 | 2018-09-28 | 江苏海阳锦纶新材料有限公司 | 一种pa6/66生产用新型前聚合器 |
CN110684192A (zh) * | 2019-11-07 | 2020-01-14 | 蓝星(成都)新材料有限公司 | 一种用于芳纶1414连续聚合的对苯二胺溶解系统及方法 |
CN110818892A (zh) * | 2019-12-13 | 2020-02-21 | 万华化学集团股份有限公司 | 尼龙的制备方法及装置 |
CN111100287A (zh) * | 2018-10-26 | 2020-05-05 | 中国石油化工股份有限公司 | 一种生产高粘度聚酰胺的方法 |
CN113861410A (zh) * | 2021-10-28 | 2021-12-31 | 湖南世博瑞高分子新材料有限公司 | 一种pa6树脂连续聚合工艺 |
CN114874434A (zh) * | 2021-02-05 | 2022-08-09 | 天津科技大学 | 一种在中低压和常压下两段式聚合制备共聚酰胺pa6/66的方法 |
CN114949901A (zh) * | 2022-04-01 | 2022-08-30 | 宿迁联盛亚克力有限公司 | 一种适用于己二胺哌啶的连续化精馏工艺以及精馏设备 |
Families Citing this family (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
NL1010161C2 (nl) * | 1998-09-23 | 2000-03-24 | Dsm Nv | Proces voor de productie van polyamide-6 uitgaande èpsilon-caprolactam. |
DE10213263B4 (de) * | 2002-03-25 | 2013-03-14 | Karl-Heinz Wiltzer | Verfahren und Vorrichtung zur kontinuierlichen Herstellung von Copolyamid oder Polyamid |
CN1480479B (zh) * | 2002-09-05 | 2010-04-28 | 中蓝晨光化工研究院有限公司 | 一种制备高粘度芳纶ⅲ树脂母液的工艺方法及生产装置 |
US7199126B2 (en) * | 2004-04-29 | 2007-04-03 | Pharmix Corporation | Compositions and treatments for inhibiting kinase and/or HMG-CoA reductase |
CN102167816B (zh) * | 2011-01-24 | 2012-09-05 | 北京国能新兴化工科技发展有限公司 | 一种制备聚对苯二甲酰对苯二胺聚合物的方法 |
FR3029923B1 (fr) * | 2014-12-12 | 2018-04-27 | Arkema France | Procede de preparation d'un polyamide semi-aromatique |
CN110998004A (zh) | 2017-06-08 | 2020-04-10 | 奥升德功能材料运营有限公司 | 聚酰胺纳米纤维非织造物 |
US11376534B2 (en) | 2017-06-08 | 2022-07-05 | Ascend Performance Materials Operations Llc | Polyamide nanofiber nonwovens for filters |
CA3102787A1 (en) | 2018-06-08 | 2019-12-12 | Ascend Performance Materials Operations Llc | Tunable nanofiber nonwoven products |
EP3814400A1 (en) | 2018-06-27 | 2021-05-05 | Ascend Performance Materials Operations LLC | Processes for removing residual caprolactam via ssp water addition |
DE102018120988C5 (de) | 2018-08-28 | 2023-01-12 | Technip Zimmer Gmbh | Verfahren und Vorrichtung zur Herstellung von extraktarmem Polyamid 6 |
AU2019404016B2 (en) | 2018-12-18 | 2022-12-08 | Ascend Performance Materials Operations Llc | Antimicrobial nonwoven polyamides with zinc content |
MX2021008214A (es) | 2019-01-07 | 2021-08-11 | Ascend Performance Mat Operations Llc | Composiciones de poliamida retardadoras de llama no halogenadas. |
MX2021009284A (es) | 2019-01-31 | 2021-11-12 | Ascend Performance Mat Operations Llc | Poliamida moldeada por inyeccion modificada por impacto. |
KR20210126672A (ko) | 2019-02-12 | 2021-10-20 | 어센드 퍼포먼스 머티리얼즈 오퍼레이션즈 엘엘씨 | 내가수분해성 폴리아미드 |
EP3947563A1 (en) | 2019-04-01 | 2022-02-09 | Ascend Performance Materials Operations LLC | Non-halogenated flame retardant polyamide compositions |
WO2020223638A1 (en) | 2019-05-01 | 2020-11-05 | Ascend Performance Materials Operations Llc | Filter media comprising polyamide nanofiber layer |
US20210186025A1 (en) | 2019-12-18 | 2021-06-24 | Ascend Performance Materials Operations Llc | Processes for producing fiber and fabrics with zinc content |
CN116056874A (zh) | 2020-08-13 | 2023-05-02 | 奥升德功能材料运营有限公司 | 具有二聚酸和二聚胺的脂族和半芳族聚酰胺 |
WO2022094321A1 (en) | 2020-10-30 | 2022-05-05 | Ascend Performance Materials Operations Llc | Polyamide nonwovens in sound absorbing multi-layer composites |
Family Cites Families (9)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2689839A (en) * | 1951-08-22 | 1954-09-21 | Du Pont | Dispersion of delusterants in polyamides |
DE2501348B2 (de) * | 1975-01-15 | 1981-04-09 | Basf Ag, 6700 Ludwigshafen | Kontinuierliches Verfahren zur Herstellung von Polyamiden aus epsilon-Caprolactam |
DD133681B1 (de) * | 1977-08-15 | 1983-09-21 | Baldur Ebert | Verfahren zur herstellung von polyamid 6 in mehreren verfahrensstufen |
US4246395A (en) * | 1979-07-25 | 1981-01-20 | Monsanto Company | 6T/6I Terpolyamide |
DE3223823A1 (de) * | 1982-06-25 | 1983-12-29 | Bayer Ag, 5090 Leverkusen | Verfahren zur kontinuierlichen herstellung von polyamiden |
DE3321581A1 (de) * | 1983-06-15 | 1984-12-20 | Basf Ag, 6700 Ludwigshafen | Verfahren zur kontinuierlichen herstellung von polyamiden |
US4892927A (en) * | 1987-05-01 | 1990-01-09 | Bayer Aktiengesellschaft | α-amino-ε-caprolactam-modified polyamide of dicarboxylic acids/diamines |
DE3912768A1 (de) * | 1989-04-19 | 1990-10-25 | Basf Ag | Verfahren zur kontinuierlichen herstellung von copolyamiden aus caprolactam und salzen aus diaminen und dicarbonsaeuren |
DE59307118D1 (de) * | 1993-01-28 | 1997-09-18 | Polymer Eng Gmbh | Verfahren und Vorrichtung zur Herstellung von Polyamid 6 aus Polyamid-Abfällen |
-
1995
- 1995-12-12 DE DE19546417A patent/DE19546417B4/de not_active Expired - Fee Related
-
1996
- 1996-12-10 WO PCT/EP1996/005514 patent/WO1997021758A2/de active IP Right Grant
- 1996-12-10 DE DE59606677T patent/DE59606677D1/de not_active Expired - Lifetime
- 1996-12-10 US US09/077,737 patent/US6136947A/en not_active Expired - Lifetime
- 1996-12-10 CN CN96199638A patent/CN1108330C/zh not_active Expired - Fee Related
- 1996-12-10 EP EP96943074A patent/EP0866826B1/de not_active Expired - Lifetime
Cited By (20)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100378142C (zh) * | 1999-05-03 | 2008-04-02 | L.布鲁克曼酒精化学工厂两合公司 | 聚酰胺的缩合工艺 |
CN101050279B (zh) * | 2007-05-09 | 2010-05-19 | 武汉森大科技研究发展中心 | 聚酰胺聚合生产工艺及设备 |
CN102585216A (zh) * | 2012-01-20 | 2012-07-18 | 北京伊克希德化工技术有限公司 | 尼龙66短流程连续聚合的方法及设备 |
WO2013107425A1 (zh) * | 2012-01-20 | 2013-07-25 | 北京伊克希德化工技术有限公司 | 尼龙66等以双组分单体为原料的尼龙连续聚合方法及设备 |
CN105722891A (zh) * | 2013-06-12 | 2016-06-29 | 巴斯夫欧洲公司 | 用于制备脂族或部分芳族聚酰胺的方法,所述方法包含固相聚合过程 |
US9701790B2 (en) | 2013-06-12 | 2017-07-11 | Basf Se | Method for producing aliphatic or partially aromatic polyamides, said method comprising a solid-phase polymerization process |
CN105722891B (zh) * | 2013-06-12 | 2018-08-24 | 巴斯夫欧洲公司 | 用于制备脂族或部分芳族聚酰胺的方法,所述方法包含固相聚合过程 |
CN104910375A (zh) * | 2015-06-25 | 2015-09-16 | 安庆市虹泰新材料有限责任公司 | 一种聚酰胺缩聚反应装置 |
WO2018153048A1 (en) * | 2017-02-24 | 2018-08-30 | Advansix Resins & Chemicals Llc | Enhanced polyamide base resin for engineering plastics formulations |
CN106866956A (zh) * | 2017-03-27 | 2017-06-20 | 万华化学集团股份有限公司 | 聚十二内酰胺及其改性树脂的多级串联聚合方法 |
CN108586731A (zh) * | 2018-06-12 | 2018-09-28 | 江苏海阳锦纶新材料有限公司 | 一种pa6/66生产用新型前聚合器 |
CN111100287A (zh) * | 2018-10-26 | 2020-05-05 | 中国石油化工股份有限公司 | 一种生产高粘度聚酰胺的方法 |
CN111100287B (zh) * | 2018-10-26 | 2023-01-20 | 中国石油化工股份有限公司 | 一种生产高粘度聚酰胺的方法 |
CN110684192A (zh) * | 2019-11-07 | 2020-01-14 | 蓝星(成都)新材料有限公司 | 一种用于芳纶1414连续聚合的对苯二胺溶解系统及方法 |
CN110818892A (zh) * | 2019-12-13 | 2020-02-21 | 万华化学集团股份有限公司 | 尼龙的制备方法及装置 |
CN110818892B (zh) * | 2019-12-13 | 2022-07-12 | 万华化学集团股份有限公司 | 尼龙的制备方法及装置 |
CN114874434A (zh) * | 2021-02-05 | 2022-08-09 | 天津科技大学 | 一种在中低压和常压下两段式聚合制备共聚酰胺pa6/66的方法 |
CN113861410A (zh) * | 2021-10-28 | 2021-12-31 | 湖南世博瑞高分子新材料有限公司 | 一种pa6树脂连续聚合工艺 |
CN113861410B (zh) * | 2021-10-28 | 2024-04-05 | 湖南世博瑞高分子新材料有限公司 | 一种pa6树脂连续聚合工艺 |
CN114949901A (zh) * | 2022-04-01 | 2022-08-30 | 宿迁联盛亚克力有限公司 | 一种适用于己二胺哌啶的连续化精馏工艺以及精馏设备 |
Also Published As
Publication number | Publication date |
---|---|
DE19546417A1 (de) | 1997-06-19 |
DE59606677D1 (de) | 2001-05-03 |
US6136947A (en) | 2000-10-24 |
WO1997021758A3 (de) | 1997-08-21 |
DE19546417B4 (de) | 2005-12-22 |
CN1108330C (zh) | 2003-05-14 |
WO1997021758A2 (de) | 1997-06-19 |
EP0866826A2 (de) | 1998-09-30 |
EP0866826B1 (de) | 2001-03-28 |
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Owner name: KARL FROM HUNTSVILLE POLICY; TANYA N BULASILA Free format text: FORMER OWNER: POLYMER ENGINEERING GMBH Effective date: 20061124 |
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