CN117046513A - 酸处理以使包含具有mww骨架类型的含钛沸石材料的组合物的可塑性降低的用途 - Google Patents

酸处理以使包含具有mww骨架类型的含钛沸石材料的组合物的可塑性降低的用途 Download PDF

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Publication number
CN117046513A
CN117046513A CN202311004026.9A CN202311004026A CN117046513A CN 117046513 A CN117046513 A CN 117046513A CN 202311004026 A CN202311004026 A CN 202311004026A CN 117046513 A CN117046513 A CN 117046513A
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CN
China
Prior art keywords
framework type
titanium
mww framework
acid
zeolite material
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Pending
Application number
CN202311004026.9A
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English (en)
Chinese (zh)
Inventor
A-N·帕乌莱斯库
U·穆勒
H-J·卢茨伊勒
G·尤尔
J·H·泰勒斯
D·里德尔
D·乌尔班奇克
U·韦格利
M·韦伯
N·T·沃兹
C·穆勒
R·施密特
X·罗马尼费尔南德斯
H·维尔茨
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BASF SE
Original Assignee
BASF SE
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Publication date
Application filed by BASF SE filed Critical BASF SE
Publication of CN117046513A publication Critical patent/CN117046513A/zh
Pending legal-status Critical Current

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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7049—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65 containing rare earth elements, titanium, zirconium, hafnium, zinc, cadmium, mercury, gallium, indium, thallium, tin or lead
    • B01J29/7088—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J29/00—Catalysts comprising molecular sieves
    • B01J29/04—Catalysts comprising molecular sieves having base-exchange properties, e.g. crystalline zeolites
    • B01J29/06—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof
    • B01J29/70—Crystalline aluminosilicate zeolites; Isomorphous compounds thereof of types characterised by their specific structure not provided for in groups B01J29/08 - B01J29/65
    • B01J29/7038—MWW-type, e.g. MCM-22, ERB-1, ITQ-1, PSH-3 or SSZ-25
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28002—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their physical properties
    • B01J20/28004—Sorbent size or size distribution, e.g. particle size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/02—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material
    • B01J20/10—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising inorganic material comprising silica or silicate
    • B01J20/16—Alumino-silicates
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/223—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material containing metals, e.g. organo-metallic compounds, coordination complexes
    • B01J20/226—Coordination polymers, e.g. metal-organic frameworks [MOF], zeolitic imidazolate frameworks [ZIF]
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28016—Particle form
    • B01J20/28021—Hollow particles, e.g. hollow spheres, microspheres or cenospheres
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/30—Processes for preparing, regenerating, or reactivating
    • B01J20/3071—Washing or leaching
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J35/00—Catalysts, in general, characterised by their form or physical properties
    • B01J35/40—Catalysts, in general, characterised by their form or physical properties characterised by dimensions, e.g. grain size
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/0009—Use of binding agents; Moulding; Pressing; Powdering; Granulating; Addition of materials ameliorating the mechanical properties of the product catalyst
    • B01J37/0018—Addition of a binding agent or of material, later completely removed among others as result of heat treatment, leaching or washing,(e.g. forming of pores; protective layer, desintegrating by heat)
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/02—Impregnation, coating or precipitation
    • B01J37/0236—Drying, e.g. preparing a suspension, adding a soluble salt and drying
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J37/00—Processes, in general, for preparing catalysts; Processes, in general, for activation of catalysts
    • B01J37/08—Heat treatment
    • B01J37/10—Heat treatment in the presence of water, e.g. steam
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/10—After treatment, characterised by the effect to be obtained
    • B01J2229/18—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself
    • B01J2229/186—After treatment, characterised by the effect to be obtained to introduce other elements into or onto the molecular sieve itself not in framework positions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2229/00—Aspects of molecular sieve catalysts not covered by B01J29/00
    • B01J2229/30—After treatment, characterised by the means used
    • B01J2229/37—Acid treatment

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Analytical Chemistry (AREA)
  • Inorganic Chemistry (AREA)
  • Thermal Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Catalysts (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Compositions Of Macromolecular Compounds (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
CN202311004026.9A 2016-12-20 2017-12-20 酸处理以使包含具有mww骨架类型的含钛沸石材料的组合物的可塑性降低的用途 Pending CN117046513A (zh)

Applications Claiming Priority (4)

Application Number Priority Date Filing Date Title
EP16205266.6 2016-12-20
EP16205266 2016-12-20
CN201780078886.3A CN110087768B (zh) 2016-12-20 2017-12-20 酸处理以使包含具有mww骨架类型的含钛沸石材料的组合物的可塑性降低的用途
PCT/EP2017/083810 WO2018115118A1 (en) 2016-12-20 2017-12-20 Use of an acid treatment to decrease the plasticity of a composition comprising a titanium-containing zeolitic material having framework type mww

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
CN201780078886.3A Division CN110087768B (zh) 2016-12-20 2017-12-20 酸处理以使包含具有mww骨架类型的含钛沸石材料的组合物的可塑性降低的用途

Publications (1)

Publication Number Publication Date
CN117046513A true CN117046513A (zh) 2023-11-14

Family

ID=57838133

Family Applications (2)

Application Number Title Priority Date Filing Date
CN202311004026.9A Pending CN117046513A (zh) 2016-12-20 2017-12-20 酸处理以使包含具有mww骨架类型的含钛沸石材料的组合物的可塑性降低的用途
CN201780078886.3A Active CN110087768B (zh) 2016-12-20 2017-12-20 酸处理以使包含具有mww骨架类型的含钛沸石材料的组合物的可塑性降低的用途

Family Applications After (1)

Application Number Title Priority Date Filing Date
CN201780078886.3A Active CN110087768B (zh) 2016-12-20 2017-12-20 酸处理以使包含具有mww骨架类型的含钛沸石材料的组合物的可塑性降低的用途

Country Status (10)

Country Link
US (1) US11351525B2 (enExample)
EP (1) EP3558517A1 (enExample)
JP (1) JP7296880B2 (enExample)
KR (1) KR102555075B1 (enExample)
CN (2) CN117046513A (enExample)
BR (1) BR112019011059B1 (enExample)
MY (1) MY199977A (enExample)
RU (1) RU2761301C2 (enExample)
WO (1) WO2018115118A1 (enExample)
ZA (1) ZA201903192B (enExample)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ES2867052T3 (es) 2016-06-29 2021-10-20 Basf Se Procedimiento de preparación de aldehídos alfa, beta insaturados por oxidación de alcoholes en presencia de una fase líquida
EP3619190B1 (en) 2017-05-03 2021-08-04 Basf Se Process for the conversion of ethylene oxide to monoethanolamine and ethylenediamine employing a zeolite
CN115477310B (zh) * 2021-06-16 2023-11-28 中国石油化工股份有限公司 P-Ti-MWW分子筛及其制备方法与应用

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0689170B2 (ja) * 1985-09-24 1994-11-09 日本化学工業株式会社 樹脂組成物
JP3706457B2 (ja) * 1997-02-28 2005-10-12 帝人化成株式会社 熱可塑性樹脂組成物
DE10320635A1 (de) 2003-05-08 2004-11-18 Basf Ag Verfahren zur Herstellung von Propylenoxid
US8124555B2 (en) * 2010-02-01 2012-02-28 Lyondell Chemical Technology L.P. Process for making titanium-MWW zeolite
BR122019019074B1 (pt) * 2012-02-07 2020-11-24 Basf Se molde e uso do molde
WO2014060261A1 (en) * 2012-10-18 2014-04-24 Basf Se Post-treatment of deboronated mww zeolite
CN103934039A (zh) * 2013-01-23 2014-07-23 中国石油化工股份有限公司 提高分子筛催化剂强度的方法
SG10201705892RA (en) * 2013-02-05 2017-08-30 Basf Se Process for preparing a titanium-containing zeolitic material having an mww framework structure
BR112016007918B1 (pt) * 2013-10-23 2020-12-29 Basf Se processo para a produção de um corpo de moldagem, corpo de moldagem e uso de um corpo de moldagem
CN104437616B (zh) * 2014-11-21 2017-10-10 武汉工程大学 层状含介孔钛硅分子筛催化剂及其制备方法和应用

Also Published As

Publication number Publication date
ZA201903192B (en) 2024-09-25
KR20190089913A (ko) 2019-07-31
CN110087768A (zh) 2019-08-02
JP2020502304A (ja) 2020-01-23
EP3558517A1 (en) 2019-10-30
KR102555075B1 (ko) 2023-07-12
WO2018115118A1 (en) 2018-06-28
US11351525B2 (en) 2022-06-07
RU2761301C2 (ru) 2021-12-07
CN110087768B (zh) 2023-09-01
RU2019122860A (ru) 2021-01-25
RU2019122860A3 (enExample) 2021-04-21
BR112019011059A2 (pt) 2019-10-08
JP7296880B2 (ja) 2023-06-23
US20190321811A1 (en) 2019-10-24
MY199977A (en) 2023-12-01
BR112019011059B1 (pt) 2022-08-09

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