CN115990130A - Face-cleaning porcelain Bai Xuefu mask - Google Patents

Face-cleaning porcelain Bai Xuefu mask Download PDF

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CN115990130A
CN115990130A CN202310299589.9A CN202310299589A CN115990130A CN 115990130 A CN115990130 A CN 115990130A CN 202310299589 A CN202310299589 A CN 202310299589A CN 115990130 A CN115990130 A CN 115990130A
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facial mask
ascorbic acid
mask
ethyl ascorbic
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CN115990130B (en
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黄志渊
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Guangzhou Huaxia Biopharmaceutical Co ltd
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Guangzhou Huaxia Biopharmaceutical Co ltd
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    • YGENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02ATECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
    • Y02A50/00TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
    • Y02A50/30Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change

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Abstract

The invention relates to the technical field of cosmetics, and in particular provides a face-cleaning porcelain Bai Xuefu mask, which comprises the following components in parts by weight: 2-4 parts of methyl propylene glycol, 1-3 parts of PEG/PPG-17/6 copolymer, 1-3 parts of nicotinamide, 0.2-0.6 part of p-hydroxyacetophenone, 0.2-0.8 part of hydroxyethyl piperazine ethane sulfonic acid, 70-80 parts of water, 1.5-3.5 parts of skin conditioner, 1.2-1.6 parts of carbomer, 1-3 parts of modified 3-ethyl ascorbic acid, 1-3 parts of arginine and 1-3 parts of methyl hydroxybenzoate; the added modified 3-ethyl ascorbic acid has the advantages of enhanced oxidation resistance, mild effect, effective free radical elimination, and capability of improving skin activity, and whitening and brightening skin from inside to outside by being compounded with a skin conditioner.

Description

Face-cleaning porcelain Bai Xuefu mask
Technical Field
The invention relates to the technical field of cosmetics, in particular to a face mask for cleaning, whitening and whitening skin.
Background
The asian women mostly pursue fair skin color, colloquially say: the white-shading clown and the white-temporary and flawless skin are more similar to the main aesthetic of Asia, the whitening wind has a certain history, people want to achieve the whitening purpose through various means, such as all-round sunscreening, eating food with whitening efficacy, medical whitening and the like, more and more whitening products are popular in recent years, but most products have no real and mild and effective whitening effect through market research, wherein the added whitening powder plays a role in surface coverage, and the substances accumulated on the skin face influence physiological activities such as metabolism of the skin to cause burden to the skin after long-term use of the product; also, whitening effects are obtained by promoting exfoliation of the horny layer by bleaching effects such as a very popular fruit acid component and various whitening scrub for the face and body; even lead mercury and other toxic components are added to achieve the whitening effect.
Disclosure of Invention
Based on the technical scheme, the invention has the following technical effects:
the paeoniflorin extract prepared by the invention contains abundant paeoniflorin and other active components, has strong free radical removal capability, has the effects of resisting inflammation and repairing skin injury, and can effectively condition skin together with a compound solvent.
The modified 3-ethyl ascorbic acid prepared by the invention has milder effect on skin, does not generate stimulation while improving the permeability of the skin, and can effectively resist oxidation.
The invention provides a face-cleaning porcelain Bai Xuefu facial mask which is characterized by comprising the following components in parts by weight
The method comprises the following steps: 2-4 parts of methyl propylene glycol, 1-3 parts of PEG/PPG-17/6 copolymer, 1-3 parts of nicotinamide, 0.2-0.6 part of p-hydroxyacetophenone, 0.2-0.8 part of hydroxyethyl piperazine ethane sulfonic acid, 70-80 parts of water, 1.5-3.5 parts of skin conditioner, 1.2-1.6 parts of carbomer, 1-3 parts of modified 3-ethyl ascorbic acid, 1-3 parts of arginine and 1-3 parts of methyl hydroxybenzoate.
Further researched, the face cleaning porcelain Bai Xuefu mask comprises the following components in parts by weight:
3 parts of methyl propylene glycol, 2 parts of PEG/PPG-17/6 copolymer, 2 parts of nicotinamide, 0.4 part of p-hydroxyacetophenone, 0.6 part of hydroxyethyl piperazine ethane sulfonic acid, 75 parts of water, 2.5 parts of skin conditioner, 1.4 parts of carbomer, 2 parts of modified 3-ethyl ascorbic acid, 2 parts of arginine and 2 parts of methyl hydroxybenzoate.
In a further study, the preparation method of the modified 3-ethyl ascorbic acid comprises the following steps: phospholipid is prepared
Adding the compound into a homogenizing pot for homogenizing and emulsifying, adding 3-ethyl ascorbic acid and panthenol, homogenizing and stirring, and shearing and emulsifying to obtain modified 3-ethyl ascorbic acid; the weight ratio of the phospholipid complex to the 3-ethyl ascorbic acid to the panthenol is 7-9:7-9:1-3.
Further studied, the phospholipid complex is soybean phosphate and egg yolk lecithin, soybean
The weight ratio of the phosphate to the egg yolk lecithin is 1:1-3.
Further researched, the skin conditioner consists of paeonia lactiflora root extract and a compound solvent,
the mass ratio of the paeonia lactiflora extract to the composite solvent is 8-10:28-32.
Further researched, the preparation method of the paeonia lactiflora extract comprises the following steps:
step 1: pretreatment: pulverizing radix Paeoniae, reflux-extracting with 6-8 times of water under heating,
cooling, adding 3-5% Trichoderma harzianum for fermentation for 12-16 hr at 30-37deg.C;
step 2: adding ethanol solution with mass fraction of 60-75% into the fermented product obtained in step 1, leaching for 3-5 times, filtering, leaching residue with mannitol with mass fraction of 3-5 times for 1-2 times, mixing the leaching solutions, and rotary steaming to obtain radix Paeoniae extract.
Further researched, the extraction temperature of the reflux extraction is 60-70 ℃, and the reflux extraction time is 1-3h.
Further researched, the composite solvent is 1, 2-hexanediol and butanediol with the mass ratio of 1-3:1.
Further researched, the preparation method of the face-cleansing porcelain white snow skin mask provided by the invention comprises the following steps: all the components are backed up according to the weight parts, and then are uniformly stirred in a homogenizing pot to obtain a facial mask liquid, and then the facial mask liquid is coated on facial mask cloth to obtain the face-cleaning porcelain white snow skin facial mask.
Further studied, the homogenizing temperature of the homogenizing stirring is 60-70 ℃.
The beneficial effects are that: the added modified 3-ethyl ascorbic acid has the advantages of enhanced oxidation resistance, mild effect, effective free radical removal, and capability of improving skin activity, and whitening and brightening skin from inside to outside by being compounded with a skin conditioner.
Detailed Description
The invention is illustrated below by way of specific examples, which are chosen to illustrate and explain the invention only and are not intended to limit the invention.
Example 1
The embodiment provides a face-cleaning porcelain Bai Xuefu mask which comprises the following components in parts by weight: methylpropyl
3 parts of glycol, 2 parts of PEG/PPG-17/6 copolymer, 2 parts of nicotinamide, 0.4 part of p-hydroxyacetophenone, 0.6 part of hydroxyethyl piperazine ethane sulfonic acid, 75 parts of water, 2.5 parts of skin conditioner, 1.4 parts of carbomer, 2 parts of modified 3-ethyl ascorbic acid, 2 parts of arginine and 2 parts of methylparaben.
Example 2
The embodiment provides a face-cleaning porcelain Bai Xuefu mask which comprises the following components in parts by weight: methylpropyl
2 parts of glycol, 1 part of PEG/PPG-17/6 copolymer, 1 part of nicotinamide, 0.2 part of p-hydroxyacetophenone, 0.2 part of hydroxyethyl piperazine ethane sulfonic acid, 70 parts of water, 1.5 parts of skin conditioner, 1.2 parts of carbomer, 1 part of modified 3-ethyl ascorbic acid, 1 part of arginine and 1 part of hydroxybenzoate.
Example 3
The embodiment provides a face-cleaning porcelain Bai Xuefu mask which comprises the following components in parts by weight: methylpropyl
4 parts of glycol, 3 parts of PEG/PPG-17/6 copolymer, 3 parts of nicotinamide, 0.6 part of p-hydroxyacetophenone, 0.8 part of hydroxyethyl piperazine ethane sulfonic acid, 80 parts of water, 3.5 parts of skin conditioner, 1.6 parts of carbomer, 3 parts of modified 3-ethyl ascorbic acid, 3 parts of arginine and 3 parts of methyl hydroxybenzoate.
Example 4
The preparation method of the modified 3-ethyl ascorbic acid comprises the following steps: adding phospholipid complex into homogenizing pot
Homogenizing and emulsifying, adding 3-ethyl ascorbic acid and panthenol, homogenizing and stirring, and shearing and emulsifying to obtain modified 3-ethyl ascorbic acid; the weight ratio of the phospholipid complex to the 3-ethyl ascorbic acid to the panthenol is 8:8:2.
The phospholipid complex is soybean phosphate and egg yolk lecithin, and soybean phosphate and egg yolk lecithin
The weight ratio of the phospholipids is 1:2.
The skin conditioner comprises radix Paeoniae extract and complex solvent
The mass ratio of the cosolvent is 9:30.
The preparation method of the paeonia lactiflora extract comprises the following steps:
step 1: pretreatment: pulverizing radix Paeoniae, reflux-extracting with 7 times of water under heating,
cooling, adding 4% Trichoderma harzianum by mass fraction for fermentation for 14h at 33 ℃;
step 2: adding ethanol solution with mass fraction of 65% and mass multiple of 11 times into the fermented product obtained in step 1, leaching for 4 times, filtering, leaching residue with mannitol with mass multiple of 4 times for 2 times, mixing the leaching solutions, and performing rotary steaming to obtain radix Paeoniae extract.
The extraction temperature of the reflux extraction is 65 ℃, and the reflux extraction time is 2 hours.
The composite solvent is 1, 2-hexanediol and butanediol with a mass ratio of 2:1.
The preparation method of the face-cleaning porcelain white skin-cleansing facial mask comprises the following steps: and backing up all the components according to parts by weight, homogenizing and stirring uniformly in a homogenizing pot at the homogenizing temperature of 60 ℃ to obtain a facial mask liquid, and coating the facial mask liquid on facial mask cloth to obtain the face-cleaning porcelain white snow skin facial mask.
Comparative example 1
Comparative example 1 differs from example 1 in that comparative example 1 does not add modified 3-ethyl ascorbic acid.
Comparative example 2
Comparative example 2 differs from example 1 in that comparative example 2 was added with unmodified 3-ethyl ascorbic acid.
Comparative example 3
Comparative example 3 differs from example 1 in that comparative example 3 does not add skin conditioning agent.
Comparative example 4
Comparative example 4 differs from example 1 in that the skin conditioner of comparative example 4 does not add paeonia lactiflora extract.
Comparative example 5
Comparative example 5 is different from example 1 in that the paeonia lactiflora root extract of comparative example 5 is prepared
The preparation method is different, and the preparation method comprises the following steps: pulverizing radix Paeoniae, reflux-extracting with 7 times of water under heating, adding 11 times of 65% ethanol solution, extracting for 4 times, and rotary steaming to obtain radix Paeoniae extract.
The extraction temperature of the reflux extraction is 65 ℃, and the reflux extraction time is 2 hours.
Comparative example 6
Comparative example 6 differs from example 1 in that the skin conditioner of comparative example 6 does not add a complex solvent.
And (5) verifying efficacy.
Preparing 2mg/ml solutions of the mask solutions prepared in the examples and the comparative examples respectively, dissolving 3.5g of 1, 1-diphenyl-2-picrylhydrazine in absolute ethyl alcohol to prepare 10ml of DPPH solution, diluting the solution to 0.0178mmol/L of DPPH solution, adding 4ml of DPPH solution and test solution into a 10ml colorimetric tube, adding absolute ethyl alcohol to a scale, mixing uniformly, and immediately obtaining a visible light spectrometer
(UV-2001 Spectrophotometer, available from HITACHI Co.) for measuring absorbance at 517nm, storing in dark for 30min, and measuring absorbance to obtain free radical scavenging rate. The test results are shown in Table 1.
Table 1.
Figure SMS_1
As shown in the results of Table 1, the mask prepared by the invention has a radical scavenging rate of more than 90%, and has excellent whitening effect, and example 1 is the best example of the invention.
As is clear from comparative examples 1 to 2, the invention has more remarkable whitening effect by adding the modified 3-ethyl ascorbic acid and adopting the modification method to modify the 3-ethyl ascorbic acid than not modifying and not adding the 3-ethyl ascorbic acid.
Furthermore, as is clear from comparative example 3, the skin conditioner of the present invention has a synergistic whitening effect by being added together with the modified 3-ethyl ascorbic acid.
As can be seen from comparative examples 4-6, the skin conditioner provided by the invention has remarkable whitening effect when the paeonia lactiflora root extract prepared by the invention is added, and has more remarkable whitening effect when the skin conditioner is compounded with a compound solvent than when the paeonia lactiflora root extract is not added or extracted by water and ethanol.
Finally, it should be noted that the above-mentioned embodiments are only for illustrating the technical solution of the present invention and not for limiting the scope of the present invention, and although the present invention has been described in detail with reference to the preferred embodiments, it should be understood by those skilled in the art that the technical solution of the present invention may be modified or substituted equally without departing from the spirit and scope of the technical solution of the present invention.

Claims (10)

1. The face cleaning porcelain Bai Xuefu mask is characterized by comprising the following components in parts by weight: 2-4 parts of methyl propylene glycol, 1-3 parts of PEG/PPG-17/6 copolymer, 1-3 parts of nicotinamide, 0.2-0.6 part of p-hydroxyacetophenone, 0.2-0.8 part of hydroxyethyl piperazine ethane sulfonic acid, 70-80 parts of water, 1.5-3.5 parts of skin conditioner, 1.2-1.6 parts of carbomer, 1-3 parts of modified 3-ethyl ascorbic acid, 1-3 parts of arginine and 1-3 parts of methyl hydroxybenzoate.
2. The face cleaning porcelain Bai Xuefu mask according to claim 1, which is characterized by comprising the following components in parts by weight: 2-4 parts of methyl propylene glycol, 1-3 parts of PEG/PPG-17/6 copolymer, 1-3 parts of nicotinamide, 0.2-0.6 part of p-hydroxyacetophenone, 0.2-0.8 part of hydroxyethyl piperazine ethane sulfonic acid, 70-80 parts of water, 1.5-3.5 parts of skin conditioner, 1.2-1.6 parts of carbomer, 1-3 parts of modified 3-ethyl ascorbic acid, 1-3 parts of arginine and 1-3 parts of methyl hydroxybenzoate.
3. The facial mask of claim 1, wherein the preparation method of the modified 3-ethyl ascorbic acid is as follows: adding the phospholipid complex into a homogenizing pot for homogenizing and emulsifying, adding 3-ethyl ascorbic acid and panthenol for homogenizing and stirring, and shearing and emulsifying to obtain modified 3-ethyl ascorbic acid; the weight ratio of the phospholipid complex to the 3-ethyl ascorbic acid to the panthenol is 7-9:7-9:1-3.
4. The face cleansing porcelain Bai Xuefu mask according to claim 1, wherein the phospholipid complex is soybean phosphate and egg yolk lecithin, and the weight ratio of the soybean phosphate to the egg yolk lecithin is 1:1-3.
5. The facial mask of claim 1, wherein the skin conditioner comprises paeonia lactiflora extract and a compound solvent, wherein the mass ratio of paeonia lactiflora extract to compound solvent is 8-10:28-32.
6. The facial mask of claim 5, wherein the composite solvent is 1, 2-hexanediol and butanediol with a mass ratio of 1-3:1.
7. The facial mask of claim 1, wherein the peony extract is prepared by the following steps:
step 1: pretreatment: pulverizing radix Paeoniae, reflux-extracting with 6-8 times of water, cooling, adding 3-5% Trichoderma harzianum, fermenting for 12-16 hr at 30-37deg.C;
step 2: adding ethanol solution with mass fraction of 60-75% into the fermented product obtained in step 1, leaching for 3-5 times, filtering, leaching residue with mannitol with mass fraction of 3-5 times for 1-2 times, mixing the leaching solutions, and rotary steaming to obtain radix Paeoniae extract.
8. The facial mask of claim 7, wherein the reflux extraction temperature is 60-70 ℃ and the reflux extraction time is 1-3h.
9. The facial mask of any one of claims 1-8, wherein the preparation method comprises the following steps: all the components are backed up according to the weight parts, and then are uniformly stirred in a homogenizing pot to obtain a facial mask liquid, and then the facial mask liquid is coated on facial mask cloth to obtain the face-cleaning porcelain white snow skin facial mask.
10. The facial mask of claim 9, wherein the homogenized temperature of the homogenized mixture is 60-70 ℃.
CN202310299589.9A 2023-03-25 2023-03-25 Face-cleaning porcelain Bai Xuefu mask Active CN115990130B (en)

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CN114522109A (en) * 2022-03-14 2022-05-24 广州科妙生物科技有限公司 Whitening and skin-refreshing ampoule essence microemulsion and preparation method thereof
CN114532096A (en) * 2022-01-24 2022-05-27 菏泽学院 Method for improving content of peony red pigment by exogenous inoculation of strain
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CN103655434A (en) * 2013-04-28 2014-03-26 钱臻 Biological fermentation bath cream and preparation method thereof
CN103655437A (en) * 2013-05-24 2014-03-26 钱臻 Biological fermentation day cream and preparation method thereof
CN106635824A (en) * 2016-11-01 2017-05-10 东北林业大学 Trichoderma harzianum solid-state fermentation method
CN106966806A (en) * 2017-04-17 2017-07-21 山东省农业科学院农产品研究所 A kind of edible fungi residue living soil fertility regulation compound and preparation method thereof
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