CN114272185A - A method for preparing facial cream containing multiple plant extracts - Google Patents
A method for preparing facial cream containing multiple plant extracts Download PDFInfo
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- CN114272185A CN114272185A CN202111469586.2A CN202111469586A CN114272185A CN 114272185 A CN114272185 A CN 114272185A CN 202111469586 A CN202111469586 A CN 202111469586A CN 114272185 A CN114272185 A CN 114272185A
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Images
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- Cosmetics (AREA)
Abstract
A method for preparing facial cream containing multiple plant extracts comprises preparing vegetable oil from avocado fruit, peel of fructus Citri Tangerinae and sweet almond kernel, respectively, and preparing plant extracts from stem of herba Dendrobii, folium Aloe Barbadensis, radix Sophorae Flavescentis, fructus Lycii, flos Echinacea purpurea and flos Citri sinensis; then mixing vegetable oil and fat, plant extract, glycerol, acryloyl dimethyl ammonium taurate/VP copolymer, xanthan gum, butanediol, arginine, trehalose, tocopheryl acetate and other materials, and blending to obtain the cream. The facial cream prepared by the method contains various plant extracts, and has the effects of keeping skin moisture, whitening, removing freckles and the like.
Description
Technical Field
The invention belongs to the technical field of cosmetic preparation, and relates to a method for preparing a facial cream containing various plant extracts.
Background
With the social development and the improvement of living standard, cosmetics are luxury goods for a small number of people and become an indispensable component in daily life of people. The cream is an indispensable product in cosmetics, has almost the same efficacy as the lotion, can cover the surface layer of the skin to form a protective film, can achieve the effects of moisturizing and locking water, can block harmful substances in the air, repair fine lines of the skin, deeply activate the skin and the like; generally has the effects of moisturizing, whitening, resisting aging and the like.
Under the promotion of continuous progress of science and technology, green and functional cosmetics are more and more favored by people, the application of plant extracts in the cosmetics is more and more extensive, and the variety of the application is more and more. Cosmetics formulated with plant extracts as active ingredients have many advantages over conventional cosmetics, such as: overcomes the defect that the traditional cosmetics depend on chemical synthetic products, and ensures that the safety performance of the product is higher; the natural components are easier to be absorbed by the skin, so that the effect of the product is more obvious; more outstanding functionality, etc.
The root, stem, leaf, flower, fruit and seed of the plant are the functions of six major organs of the plant, and as the organs of the plant, the root, stem, leaf, flower, fruit and seed are rich in nutrient substances and functional components with different characteristics.
The stem of herba Dendrobii is the main medicinal part of whole plant of herba Dendrobii, contains active substances such as polysaccharide and active enzyme, and can be added into cosmetics for dilating capillary vessel, improving blood flow, and resisting aging.
Aloe leaves, especially Aloe barbadensis leaves, are rich in fat and succulent, contain active substances such as nicotinic acid, vitamin B6, aloin, etc., and can be used in cosmetics, and has antibacterial, antiinflammatory, skin moisture protecting, and acne and comedo preventing and treating effects.
The kuh-seng root contains a large amount of alkaloid, volatile oil and various mineral compounds, can help to dispel skin toxin, promote the growth and repair of damaged vascular nerve cells, has the effects of beautifying and protecting skin, and is beneficial to the skin health of human bodies.
The fructus Lycii is fructus Lycii, contains betaine, polysaccharide, crude fat, crude protein, carotene, vitamin A, vitamin C, vitamin B1, vitamin B2, and nutritional components such as calcium, phosphorus, iron, zinc, manganese, and linoleic acid, has effects of promoting hematopoietic function, and has antiaging effect when used in cosmetics.
The bitter orange flower and the purple coneflower contain rich alcohol, terpene and ester compounds, can eliminate free radicals, and have the effects of resisting oxidation and relieving aging; can inhibit melanin precipitation in vivo, and can remove sunburn, mottle, senile plaque, and chloasma, and has effects of whitening skin and removing speckle.
The avocado, the tangerine peel and the sweet almond are fruits of avocado, tangerine peel and almond, respectively, the fruits, the peels and the nuts of the avocado, the tangerine peel and the sweet almond contain rich polyunsaturated fatty acid, and the avocado, the tangerine peel and the sweet almond are mainly used as moisturizers in cosmetics, can enhance the moisturizing capability of skin and moisturize dry skin, namely skin with damaged cutin.
Disclosure of Invention
The invention aims to provide a method for preparing a facial cream containing various plant extracts.
In order to achieve the above objects and other related objects, the present invention provides the following technical solutions: a method for preparing facial cream containing multiple plant extracts comprises the following steps:
step 1: drying 30-40 parts by weight of avocado fruits, 30-40 parts by weight of tangerines peels and 30-40 parts by weight of sweet almond kernels until the water content is lower than 5% to obtain a dried material; putting the dried material into an oil press, pressing at normal temperature and 1.30-1.35Mpa, and collecting the oil material; filtering the oil obtained by squeezing by adopting a ceramic membrane, and collecting filtrate to obtain refined vegetable oil;
step 2: mixing and crushing 10-20 parts by weight of dendrobium stem, 10-20 parts by weight of aloe barbadensis leaf, 10-20 parts by weight of sophora flavescens root, 10-20 parts by weight of fructus lycii, 10-20 parts by weight of echinacea purpurea and 15-40 parts by weight of neroli, to 80-100 meshes to obtain mixed powder; mixing the mixed powder with deionized water at a mass ratio of 1:40-60, and extracting at 50-60 deg.C and stirring speed of 30-60r/min for 90-120min to obtain extractive solution; filtering the extractive solution with filter paper or filter screen with aperture of 30-50 μm to obtain receipt filtrate; placing the filtrate into vacuum decompression concentration equipment, and boiling and concentrating under the condition of vacuum gauge pressure of-0.09 to-0.10 MPa to 5-10% of the original volume to obtain concentrated plant extract;
and step 3: the following materials were prepared according to the recipe: 70-90 parts by weight of deionized water, 0.1-0.3 part by weight of ammonium acryloyldimethyltaurate/VP copolymer, 0.01-0.02 part by weight of xanthan gum, 0.2-0.8 part by weight of butanediol, 3-5 parts by weight of glycerol, 0.01-0.05 part by weight of arginine, 0.1-0.5 part by weight of cetyl ethylhexanoate, 0.1-0.5 part by weight of caprylic/capric triglyceride, 0.1-0.25 part by weight of white beeswax, 0.1-0.25 part by weight of isononyl isononanoate, 0.05-0.15 part by weight of sucrose stearate, 0.05-0.15 part by weight of cetostearyl glucoside, 0.05-0.15 part by weight of cetyl alcohol, 0.05-0.15 part by weight of glyceryl stearate, 0.05-0.15 part by weight of PEG-100 stearate, 0.1-0.5 part by weight of cetostearyl alcohol, 0.1 to 0.5 part by weight of pentaerythritol tetrakis (bis-tert-butylhydroxyhydrocinnamate), 1.0 to 7.5 parts by weight of (1) vegetable fat, 0.2 to 1.0 part by weight of tocopherol acetate, 0.05 to 0.25 part by weight of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.05 to 0.25 part by weight of isohexadecane, 0.05 to 0.25 part by weight of polysorbate-80, 0.05 to 0.25 part by weight of sorbitan oleate, 0.5 to 5.0 parts by weight of hydrogenated vegetable oil, 0.1 to 0.5 part by weight of glyceryl acrylate/acrylic acid copolymer, 0.1 to 0.5 part by weight of propylene glycol, 0.1 to 0.5 part by weight of methyl hydroxybenzoate, 0.1 to 0.5 part by weight of propyl hydroxybenzoate, 0.5 to 0.25 part by weight of fermentation lysate of bifidus yeast, 0.05 to 0.15 part by weight of 1.05 to 0.25 part by weight of sodium dihydrohydrocinnamate, 2-pentanediol, 0.05-0.15 part by weight of 1, 2-hexanediol, 0.05-0.25 part by weight of acetyl hexapeptide-8, 0.1-0.5 part by weight of trehalose, 1.0-10 parts by weight of (2) medium concentrated plant extract, 0.05-0.25 part by weight of phenoxyethanol, 0.05-0.25 part by weight of ethylhexyl glycerol, 0.05-0.15 part by weight of xanthan gum, 0.1-0.5 part by weight of p-hydroxyacetophenone, 0.1-0.5 part by weight of 1, 2-hexanediol;
and 4, step 4:
firstly, mixing p-hydroxyacetophenone, 1, 2-hexanediol and butanediol, and heating to 50-55 ℃ under the condition of stirring;
secondly, keeping the rotating speed of 50-100r/min and the heating state of deionized water, and adding the acryloyl dimethyl ammonium taurate/VP copolymer, xanthan gum and glycerol into the deionized water; heating to 82-85 deg.C, stirring at 3000-; keeping the solution at 82-85 deg.C and rotation speed of 50-100r/min, adding arginine, stirring, and keeping the temperature for 20-30 min;
thirdly, mixing cetyl ethyl hexanoate, caprylic/capric triglyceride, white beeswax, isononyl isononanoate, sucrose stearate, cetearyl glucoside, cetyl alcohol, glyceryl stearate, PEG-100 stearate, cetearyl alcohol and pentaerythritol tetrakis (di-tert-butyl hydroxy hydrocinnamate) ester, heating to 82-85 ℃, stirring until the mixture is melted into liquid, and keeping the temperature for standby, wherein the temperature is not longer than 30 min; adding tocopherol acetate into the heat preservation solution, and stirring until the tocopherol acetate is completely dissolved for later use;
fourthly, mixing the solution obtained in the second step with the solution obtained in the third step, putting the mixture into vacuum high-shear stirring equipment, and performing high-shear stirring for 5-10min at the rotation speed of 4000 plus materials 6000r/min under the vacuum condition of the vacuum gauge pressure of-0.09 to-0.10 MPa until the materials are completely and uniformly emulsified;
fifthly, cooling the material obtained in the fourth step to 70-75 ℃, adding vegetable oil, sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80, sorbitan oleate and hydrogenated vegetable oil, putting into a vacuum high-shear stirring device, and stirring for 1-2min at a high shear of 6000r/min at a rotation speed of 4000-;
sixthly, cooling the materials obtained in the fifth step to 55-60 ℃, adding the glycerin acrylate/acrylic acid copolymer, propylene glycol, methyl hydroxybenzoate and propyl hydroxybenzoate, putting the mixture into vacuum stirring equipment, and stirring for 5-15min at a rotating speed of 50-200r/min under the vacuum condition of vacuum gauge pressure of-0.09 to-0.10 MPa until the materials are uniformly mixed;
seventhly, cooling the materials obtained in the sixth step to 25-45 ℃, adding the concentrated plant extract, the lysate of the yeast fermentation product of the second cracking, 1, 2-pentanediol, 1, 2-hexanediol, acetyl hexapeptide-8, trehalose, phenoxyethanol, ethylhexyl glycerol and xanthan gum, putting into a vacuum stirring device, and stirring for 5-15min at the rotating speed of 50-200r/min under the vacuum condition of the vacuum gauge pressure of-0.09 to-0.10 MPa until the materials are uniformly mixed;
eighthly, mixing the material obtained in the first step with the material obtained in the seventh step, putting the mixture into vacuum stirring equipment, and stirring the mixture for 5 to 15 minutes at a rotating speed of 50 to 200r/min under the vacuum condition of vacuum gauge pressure of-0.09 to-0.10 MPa until the materials are uniformly mixed;
and ninthly, filtering the material obtained in the eighth step by a filtering device with the fineness of 200 and 400 meshes to obtain a receipt filtrate, namely the face cream.
The preferable technical scheme is as follows: in the step 1, the material is placed into vacuum drying equipment during drying, and is dried under the conditions of vacuum gauge pressure of-0.09 to-0.1 MPa and temperature of 50 to 55 ℃ until the water content is lower than 5 percent, so that the dried material is obtained.
The preferable technical scheme is as follows: the oil press is a screw oil press, the pressing frequency is 5-6 times, and the rotating speed of a pressing shaft is 40-50 r/min.
The preferable technical scheme is as follows: the membrane aperture is 50-100nm and the filtering pressure is 0.25-0.50MPa when the ceramic membrane is used for filtering.
The preferable technical scheme is as follows: the fourth step is carried out by adopting a vacuum homogenizing emulsifying machine, and the rotating speed is 4000-.
The preferable technical scheme is as follows: the fifth step is carried out by adopting a vacuum homogenizing emulsifying machine, and the rotating speed is 4000-.
Drawings
Fig. 1 is a package overwrap for the product of the present invention.
FIG. 2 is a diagram of a product prepared by the present invention.
Detailed Description
The following description of the embodiments of the present invention is provided for illustrative purposes, and other advantages and effects of the present invention will become apparent to those skilled in the art from the present disclosure.
Please refer to fig. 1-2. It should be understood that the structures, ratios, sizes, and the like shown in the drawings and described in the specification are for illustrative purposes only and are not intended to limit the scope of the present invention. The following examples are provided for a better understanding of the present invention, and are not intended to limit the invention. The experimental procedures in the following examples are conventional unless otherwise specified. The experimental materials used in the following examples were all purchased from a conventional biochemical reagent store unless otherwise specified.
Example 1: a method for preparing facial cream containing multiple plant extracts
A method for preparing a face cream containing a plurality of plant extracts is characterized by comprising the following technical steps.
(1) Preparation of vegetable oil and fat
Collecting fresh avocado fruit, scarlet orange peel and sweet almond, cleaning, and draining.
Drying in vacuum at low temperature. Putting 35 parts by weight of avocado fruit, 35 parts by weight of tangerines peel and 35 parts by weight of sweet almond into vacuum drying equipment, and drying under the conditions of vacuum gauge pressure of-0.09 to-0.1 MPa and temperature of 52 ℃ until the water content is lower than 5% to obtain a dry material for later use.
Squeezing to obtain oil. Treating the dried material by an oil press at normal temperature and 1.2MPa, and collecting the oil obtained by pressing for later use. Preferably, the oil press is a screw oil press, the pressing frequency is 5 times, and the rotating speed of a pressing shaft is 45 r/min.
And (5) filtering and refining by a ceramic membrane. Filtering the oil material obtained by squeezing at normal temperature by ceramic membrane with filtering aperture of 50-100nm and filtering pressure of 0.25-0.50Mpa, and collecting filtrate to obtain refined vegetable oil for use.
(2) Preparation of plant extracts
The stem of dendrobium nobile, the leaves of aloe barbadensis, the roots of the sophora flavescens ait, the fruits of the fructus lycii, the chrysanthemum of the echinacea purpurea and the flowers of the bitter orange are dry products, have no mildew or insect damage, and meet the production and sanitation requirements of cosmetics.
Mixing and pulverizing. Mixing 15 parts by weight of dendrobium stem, 15 parts by weight of aloe barbadensis leaf, 15 parts by weight of sophora flavescens root, 15 parts by weight of fructus lycii ningxia, 15 parts by weight of echinacea purpurea flower and 25 parts by weight of neroli amara flower, and crushing to 80-100 meshes to obtain mixed powder for later use. Preferably, the mixed stem of dendrobium nobile, aloe barbadensis leaf, root of sophora flavescens ait, fructus lycii, echinacea purpurea and neroli in the dendrobium nobile are pulverized to 80-100 meshes by air flow.
And (4) leaching. Mixing the mixed powder with deionized water according to the mass ratio of 1:50, then placing the mixture into stirring extraction equipment with an ultrasonic generator, and keeping the temperature at 55 ℃ and the stirring speed at 45 r/min; every 9min, starting ultrasonic treatment for 4min, with ultrasonic frequency of 30KHz and power density of 0.4w/cm2(ii) a Extracting for 100min to obtain extractive solution.
And (5) filtering. Filtering the extractive solution with filter paper or filter screen with aperture of 40 μm to obtain receipt filtrate;
vacuum concentrating under reduced pressure. Placing the filtrate into vacuum reduced pressure concentration equipment, boiling and concentrating under the condition of vacuum gauge pressure of-0.09 to-0.10 MPa to 8 percent of the original volume to obtain concentrated plant extract for later use.
(3) Stock preparation
The following materials were prepared according to the recipe: 80 parts by weight of deionized water, 0.2 part by weight of ammonium acryloyldimethyltaurate/VP copolymer, 0.015 part by weight of xanthan gum, 0.5 part by weight of butanediol, 4 parts by weight of glycerol, 0.03 part by weight of arginine, 0.3 part by weight of cetyl ethylhexanoate, 0.3 part by weight of caprylic/capric triglyceride, 0.15 part by weight of white beeswax, 0.5 part by weight of isononyl isononanoate, 0.1 part by weight of sucrose stearate, 0.1 part by weight of cetearyl glucoside, 0.1 part by weight of cetyl alcohol, 0.1 part by weight of glyceryl stearate, 0.1 part by weight of PEG-100 stearate, 0.3 part by weight of cetearyl alcohol, 0.3 part by weight of pentaerythritol tetrakis (di-t-butylhydroxyhydro-) acrylate, 3.5 parts by weight of vegetable fat in (1), 0.6 part by weight of tocopheryl acetate, 0.15 part by weight of sodium acrylate/dimethylacryloyl taurate copolymer, 0.15 parts by weight of isohexadecane, 0.15 parts by weight of polysorbate-80, 0.15 parts by weight of sorbitan oleate, 2.5 parts by weight of hydrogenated vegetable oil, 0.3 parts by weight of glycerin acrylate/acrylic acid copolymer, 0.3 parts by weight of propylene glycol, 0.3 parts by weight of methylparaben, 0.3 parts by weight of propylparaben, 15 parts by weight of yeast schizolysis lysate, 0.1 parts by weight of 1, 2-pentanediol, 0.1 parts by weight of 1, 2-hexanediol, 0.15 parts by weight of acetyl hexapeptide-8, 0.3 parts by weight of trehalose, 5 parts by weight of (2) medium concentrated plant extract, 0.15 parts by weight of phenoxyethanol, 0.15 parts by weight of ethylhexylglycerol, 0.1 parts by weight of xanthan gum, 0.3 parts by weight of p-hydroxyacetophenone, 0.3 parts by weight of 1, 2-hexanediol.
(4) Blending
Step one, preparing the materials according to the step (3), mixing the p-hydroxyacetophenone, the 1, 2-hexanediol and the butanediol, stirring and heating to about 53 ℃, and completely dissolving the materials into transparent liquid for later use.
Secondly, deionized water keeps the rotating speed of 80r/min and the heating state, and acryloyl dimethyl ammonium taurate/VP copolymer, xanthan gum and glycerol are added into water; heating the solution to 83 ℃, and stirring for 6min at a high shear speed of 4000r/min until the solution is completely and uniformly dispersed; keeping the temperature of the solution at 84 ℃ and the rotating speed at 80r/min, adding arginine, stirring until the arginine is completely dissolved uniformly, and keeping the temperature for 20-30 min.
Thirdly, mixing cetyl ethyl hexanoate, caprylic/capric triglyceride, white beeswax, isononyl isononanoate, sucrose stearate, cetearyl glucoside, cetyl alcohol, glyceryl stearate, PEG-100 stearate, cetearyl alcohol and pentaerythritol tetra (di-tert-butyl hydroxy hydrocinnamic acid) ester, heating to 83 ℃, stirring until the mixture is completely melted into liquid, and keeping the temperature for standby, wherein the temperature is kept for no more than 30 min; adding the tocopherol acetate into the heat preservation solution, and stirring until the tocopherol acetate is completely dissolved for later use.
And fourthly, mixing the solution obtained in the second step and the solution obtained in the third step, putting the mixture into vacuum high-shear stirring equipment, and performing high-shear stirring for 8min at the rotating speed of 5000r/min under the vacuum of the vacuum gauge pressure of-0.095 MPa until the materials are completely and uniformly emulsified. Preferably, the processing of the step is carried out by adopting a vacuum homogenizing emulsifying machine, the rotating speed can reach 5000r/min, and the high shearing fineness can reach 0.5 mu m.
And fifthly, cooling the material obtained in the fourth step to 72 ℃, adding the vegetable oil and fat, the sodium acrylate/sodium acryloyldimethyl taurate copolymer, the isohexadecane, the polysorbate-80, the sorbitan oleate and the hydrogenated vegetable oil in the step (1), putting into a vacuum high-shear stirring device, and stirring for 1.5min at a high shear of a rotating speed of 5000r/min under the vacuum of a vacuum gauge pressure of-0.09 to-0.10 MPa until the material is completely and uniformly emulsified. Preferably, the processing of the step is carried out by adopting a vacuum homogenizing emulsifying machine, the rotating speed can reach 5000r/min, and the high shearing fineness can reach 0.5 mu m.
And sixthly, cooling the materials obtained in the fifth step to 58 ℃, adding the glycerin acrylate/acrylic acid copolymer, propylene glycol, methyl hydroxybenzoate and propyl hydroxybenzoate, putting the mixture into a vacuum stirring device, and stirring for 10min at a rotating speed of 100r/min under the vacuum condition of vacuum gauge pressure of-0.09 to-0.10 MPa until the materials are uniformly mixed.
And seventhly, cooling the materials in the sixth step to 35 ℃, adding the concentrated plant extracting solution, the schizosaccharomyces cerevisiae fermentation product lysate, 1, 2-pentanediol, 1, 2-hexanediol, acetyl hexapeptide-8, trehalose, phenoxyethanol, ethylhexyl glycerol and xanthan gum in the step (2), putting the mixture into a vacuum stirring device, and stirring the mixture for 10min at the rotating speed of 100r/min under the vacuum of-0.09 to-0.10 MPa of vacuum gauge pressure until the materials are uniformly mixed.
And eighthly, mixing the material obtained in the first step and the material obtained in the sixth step, putting the mixture into vacuum stirring equipment, and stirring for 10min at the rotating speed of 100r/min under the vacuum of vacuum gauge pressure of-0.09 to-0.10 MPa until the materials are uniformly mixed.
And ninthly, filtering the material obtained in the eighth step by using a filtering device with the fineness of 300 meshes to obtain a receipt filtrate, namely the face cream.
The skin cream product is prepared, and the physical and chemical indexes and stability are tested as follows:
pH value: 6.0-7.0;
viscosity (25 ℃, mpa.s): 50000- -80000 (rotor # 4, 6rpm, ref);
centrifugation (3000 rpm/min; 30 min): there was no abnormality.
Example 2: a method for preparing facial cream containing multiple plant extracts
A method for preparing facial cream containing multiple plant extracts comprises the following steps:
step 1: drying 30 parts by weight of avocado fruits, 30 parts by weight of tangerines peel and 30 parts by weight of sweet almond kernels until the water content is lower than 5% to obtain a dried material; putting the dried material into an oil press, pressing oil at normal temperature and 1.30Mpa, and collecting the oil material obtained by pressing; filtering the oil obtained by squeezing by adopting a ceramic membrane, and collecting filtrate to obtain refined vegetable oil;
step 2: mixing 10 parts by weight of dendrobium stem, 10 parts by weight of aloe barbadensis leaf, 10 parts by weight of sophora flavescens root, 10 parts by weight of fructus lycii ninghami, 10 parts by weight of echinacea purpurea flower and 15 parts by weight of neroli amara flower, and crushing to 80 meshes to obtain mixed powder; mixing the mixed powder with deionized water according to a mass ratio of 1:40, and extracting for 90min at a temperature of 50 ℃ and a stirring speed of 30r/min to obtain an extracting solution; filtering the extractive solution with filter paper or filter screen with aperture of 30 μm to obtain receipt filtrate; placing the filtrate in vacuum decompression concentration equipment, and boiling and concentrating under the condition of vacuum gauge pressure of-0.09 MPa to 5-10% of the original volume to obtain concentrated plant extract;
and step 3: the following materials were prepared according to the recipe: 70 parts by weight of deionized water, 0.1 part by weight of ammonium acryloyldimethyltaurate/VP copolymer, 0.01 part by weight of xanthan gum, 0.2 part by weight of butylene glycol, 3 parts by weight of glycerol, 0.015 part by weight of arginine, 0.1 part by weight of cetyl ethylhexanoate, 0.1 part by weight of caprylic/capric triglyceride, 0.1 part by weight of white beeswax, 0.1 part by weight of isononyl isononanoate, 0.05 part by weight of sucrose stearate, 0.05 part by weight of cetearyl glucoside, 0.05 part by weight of cetyl alcohol, 0.05 part by weight of glyceryl stearate, 0.05 part by weight of PEG-100 stearate, 0.1 part by weight of cetearyl alcohol, 0.1 part by weight of pentaerythritol tetrakis (di-t-butylhydroxyhydro-) acrylate, 1.0 part by weight of vegetable oil and fat in (1), 0.2 part by weight of tocopherol acetate, 0.05 part by weight of sodium acrylate/dimethylacryloyl taurate copolymer, 0.05 parts by weight of isohexadecane, 0.05 parts by weight of polysorbate-80, 0.05 parts by weight of sorbitan oleate, 0.5 parts by weight of hydrogenated vegetable oil, 0.1 parts by weight of a glycerin acrylate/acrylic acid copolymer, 0.1 parts by weight of propylene glycol, 0.1 parts by weight of methylparaben, 0.1 parts by weight of propylparaben, 0.5 parts by weight of a yeast schizophragmatis fermentation product lysate, 0.05 parts by weight of 1, 2-pentanediol, 0.05 parts by weight of 1, 2-hexanediol, 0.05 parts by weight of acetyl hexapeptide-8, 0.1 parts by weight of trehalose, 1.0 parts by weight of concentrated plant extract in (2), 0.05 parts by weight of phenoxyethanol, 0.05 parts by weight of ethylhexylglycerin, 0.05 parts by weight of xanthan gum, 0.1 parts by weight of p-hydroxyacetophenone, 0.1 parts by weight of 1, 2-hexanediol;
and 4, step 4:
firstly, mixing p-hydroxyacetophenone, 1, 2-hexanediol and butanediol, and heating to 50 ℃ under the condition of stirring;
secondly, keeping the rotating speed of 50r/min and the heating state of deionized water, and adding the acryloyl dimethyl ammonium taurate/VP copolymer, xanthan gum and glycerol into the deionized water; heating to 82 ℃, and stirring for 5min by high shear at a rotating speed of 3000r/min until the dispersion is uniform; keeping the temperature of the solution at 82 ℃ and the rotating speed at 50r/min, adding arginine, stirring uniformly, and keeping the temperature for 20 min;
thirdly, mixing cetyl ethyl hexanoate, caprylic/capric triglyceride, white beeswax, isononyl isononanoate, sucrose stearate, cetearyl glucoside, cetyl alcohol, glyceryl stearate, PEG-100 stearate, cetearyl alcohol and pentaerythritol tetrakis (di-tert-butyl hydroxy hydrocinnamate) ester, heating to 82 ℃, stirring until the mixture is melted into liquid, and keeping the temperature for standby, wherein the temperature is not longer than 30 min; adding tocopherol acetate into the heat preservation solution, and stirring until the tocopherol acetate is completely dissolved for later use;
fourthly, mixing the solution obtained in the second step with the solution obtained in the third step, putting the mixture into vacuum high-shear stirring equipment, and performing high-shear stirring for 5min at the rotating speed of 4000r/min under the vacuum of vacuum gauge pressure of-0.09 MPa until the materials are completely and uniformly emulsified;
fifthly, cooling the material obtained in the fourth step to 70 ℃, adding vegetable oil, sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80, sorbitan oleate and hydrogenated vegetable oil, putting into a vacuum high-shear stirring device, and stirring for 1min at a high shear of 4000r/min under the vacuum of-0.09 MPa of vacuum gauge pressure until the material is completely emulsified and uniform;
sixthly, cooling the materials obtained in the fifth step to 55 ℃, adding the glycerin acrylate/acrylic acid copolymer, propylene glycol, methyl hydroxybenzoate and propyl hydroxybenzoate, putting the mixture into a vacuum stirring device, and stirring for 5min at a rotating speed of 50r/min under the vacuum condition of vacuum gauge pressure of-0.09 MPa until the materials are uniformly mixed;
seventhly, cooling the materials obtained in the sixth step to 25 ℃, adding the concentrated plant extract, the lysate of the yeast fermentation product, 1, 2-pentanediol, 1, 2-hexanediol, acetyl hexapeptide-8, trehalose, phenoxyethanol, ethylhexyl glycerol and xanthan gum, putting the mixture into a vacuum stirring device, and stirring the mixture for 5 minutes at the rotating speed of 50r/min under the vacuum of the vacuum gauge pressure of-0.09 MPa until the materials are uniformly mixed;
eighthly, mixing the material obtained in the first step with the material obtained in the seventh step, putting the mixture into vacuum stirring equipment, and stirring for 5min at the rotating speed of 50r/min under the vacuum of-0.09 MPa of vacuum gauge pressure until the materials are uniformly mixed;
and ninthly, filtering the material obtained in the eighth step by using a filtering device with the fineness of 200 meshes to obtain a receipt filtrate, namely the face cream.
The preferred embodiment is: in the step 1, the material is placed into vacuum drying equipment during drying, and is dried under the conditions of vacuum gauge pressure of-0.09 MPa and temperature of 50 ℃ until the water content is lower than 5 percent, so that the dried material is obtained.
The preferred embodiment is: the screw oil press is selected for oil pressing, the pressing frequency is 5 times, and the rotating speed of a pressing shaft is 40 r/min.
The preferred embodiment is: the membrane aperture is 50nm and the filtration pressure is 0.25Mpa when the ceramic membrane is used for filtration.
The preferred embodiment is: the fourth step is carried out by adopting a vacuum homogenizing emulsifying machine, and the rotating speed is 40000 r/min.
The preferred embodiment is: the fifth step is carried out by adopting a vacuum homogenizing emulsifying machine, and the rotating speed is 4000 r/min.
Example 3: a method for preparing facial cream containing multiple plant extracts
A method for preparing facial cream containing multiple plant extracts comprises the following steps:
step 1: drying 40 parts by weight of avocado fruits, 40 parts by weight of tangerines pericarp and 40 parts by weight of sweet almond kernels until the water content is lower than 5% to obtain a dried material; putting the dried material into an oil press, pressing oil at normal temperature and 1.35Mpa, and collecting the oil material obtained by pressing; filtering the oil obtained by squeezing by adopting a ceramic membrane, and collecting filtrate to obtain refined vegetable oil;
step 2: mixing and crushing 20 parts by weight of dendrobium stem, 20 parts by weight of aloe barbadensis leaf, 20 parts by weight of sophora flavescens root, 20 parts by weight of fructus lycii ninghamii, 20 parts by weight of echinacea purpurea flower and 40 parts by weight of neroli amara flower to 100 meshes to obtain mixed powder; mixing the mixed powder with deionized water according to a mass ratio of 1:60, and then extracting for 120min at a temperature of 60 ℃ and a stirring speed of 60r/min to obtain an extracting solution; filtering the extractive solution with filter paper or filter screen with pore diameter of 50 μm to obtain receipt filtrate; placing the filtrate into vacuum decompression concentration equipment, and boiling and concentrating under the condition of vacuum gauge pressure of-0.10 MPa to 10% of the original volume to obtain concentrated plant extract;
and step 3: the following materials were prepared according to the recipe: 90 parts by weight of deionized water, 0.3 part by weight of ammonium acryloyldimethyltaurate/VP copolymer, 0.02 part by weight of xanthan gum, 0.8 part by weight of butylene glycol, 5 parts by weight of glycerol, 0.05 part by weight of arginine, 0.5 part by weight of cetyl ethylhexanoate, 0.5 part by weight of caprylic/capric triglyceride, 0.25 part by weight of white beeswax, 0.25 part by weight of isononyl isononanoate, 0.15 part by weight of sucrose stearate, 0.15 part by weight of cetearyl glucoside, 0.15 part by weight of cetyl alcohol, -0.15 part by weight of glyceryl stearate, 0.15 part by weight of PEG-100 stearate, 0.5 part by weight of cetearyl alcohol, 0.5 part by weight of pentaerythritol tetrakis (di-t-butylhydroxyhydro-) acrylate, 7.5 parts by weight of (1) vegetable oil and fat, 1.0 part by weight of tocopheryl acetate, 0.25 part by weight of sodium acrylate/dimethylacryloyl taurate copolymer, 0.25 parts by weight of isohexadecane, 0.25 parts by weight of polysorbate-80, 0.25 parts by weight of sorbitan oleate, 5.0 parts by weight of hydrogenated vegetable oil, 0.5 parts by weight of a glycerol acrylate/acrylic acid copolymer, 0.5 parts by weight of propylene glycol, 0.5 parts by weight of methylparaben, 0.5 parts by weight of propylparaben, 0.25 parts by weight of a yeast schizophragmatis fermentation product lysate, 0.15 parts by weight of 1, 2-pentanediol, 0.15 parts by weight of 1, 2-hexanediol, 0.25 parts by weight of acetyl hexapeptide-8, 0.5 parts by weight of trehalose, 10 parts by weight of the concentrated plant extract of (2), 0.25 parts by weight of phenoxyethanol, 0.25 parts by weight of ethylhexylglycerin, 0.15 parts by weight of xanthan gum, 0.5 parts by weight of p-hydroxyacetophenone, 0.5 parts by weight of 1, 2-hexanediol;
and 4, step 4:
firstly, mixing p-hydroxyacetophenone, 1, 2-hexanediol and butanediol, and heating to 55 ℃ under the condition of stirring;
secondly, keeping the rotating speed of 100r/min and the heating state of deionized water, and adding the acryloyl dimethyl ammonium taurate/VP copolymer, xanthan gum and glycerol into the deionized water; heating to 85 deg.C, and high-shear stirring at 5000r/min for 10min to disperse uniformly; keeping the temperature of the solution at 85 ℃ and the rotating speed of 100r/min, adding arginine, stirring uniformly, and keeping the temperature for 30 min;
thirdly, mixing cetyl ethyl hexanoate, caprylic/capric triglyceride, white beeswax, isononyl isononanoate, sucrose stearate, cetearyl glucoside, cetyl alcohol, glyceryl stearate, PEG-100 stearate, cetearyl alcohol and pentaerythritol tetrakis (di-tert-butyl hydroxy hydrocinnamate) ester, heating to 85 ℃, stirring until the mixture is melted into liquid, and keeping the temperature for standby, wherein the temperature is not longer than 30 min; adding tocopherol acetate into the heat preservation solution, and stirring until the tocopherol acetate is completely dissolved for later use;
fourthly, mixing the solution obtained in the second step with the solution obtained in the third step, putting the mixture into vacuum high-shear stirring equipment, and performing high-shear stirring for 10min at the rotating speed of 6000r/min under the vacuum condition of vacuum gauge pressure of-0.10 MPa until the materials are completely and uniformly emulsified;
fifthly, cooling the material obtained in the fourth step to 75 ℃, adding vegetable oil, sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80, sorbitan oleate and hydrogenated vegetable oil, putting into a vacuum high-shear stirring device, and stirring for 2min at a high shear of 6000r/min under the vacuum of-0.10 MPa of vacuum gauge pressure until the material is completely emulsified uniformly;
sixthly, cooling the materials obtained in the fifth step to 60 ℃, adding the glycerin acrylate/acrylic acid copolymer, propylene glycol, methyl hydroxybenzoate and propyl hydroxybenzoate, putting the mixture into a vacuum stirring device, and stirring for 15min at a rotating speed of 200r/min under the vacuum condition of vacuum gauge pressure of-0.10 MPa until the materials are uniformly mixed;
seventhly, cooling the materials obtained in the sixth step to 45 ℃, adding the concentrated plant extract, the lysate of the yeast fermentation product, 1, 2-pentanediol, 1, 2-hexanediol, acetyl hexapeptide-8, trehalose, phenoxyethanol, ethylhexyl glycerol and xanthan gum, putting the mixture into a vacuum stirring device, and stirring the mixture for 15min at the rotating speed of 200r/min under the vacuum of-0.10 MPa of vacuum gauge pressure until the materials are uniformly mixed;
eighthly, mixing the material obtained in the first step with the material obtained in the seventh step, putting the mixture into vacuum stirring equipment, and stirring for 15min at the rotating speed of 200r/min under the vacuum of-0.10 MPa of vacuum gauge pressure until the materials are uniformly mixed;
and ninthly, filtering the material obtained in the eighth step by a filtering device with the fineness of 400 meshes to obtain a receipt filtrate, namely the face cream.
The preferred embodiment is: in the step 1, the material is placed into vacuum drying equipment during drying, and is dried under the conditions of vacuum gauge pressure of-0.1 MPa and temperature of 55 ℃ until the water content is lower than 5 percent, so that the dried material is obtained.
The preferred embodiment is: the screw oil press is selected for oil pressing, the pressing frequency is 6 times, and the rotating speed of a pressing shaft is 50 r/min.
The preferred embodiment is: the membrane aperture is 100nm and the filtration pressure is 0.50Mpa when the ceramic membrane is used for filtration.
The preferred embodiment is: the fourth step is carried out by adopting a vacuum homogenizing emulsifying machine at the rotating speed of 6000 r/min.
The preferred embodiment is: the fifth step is carried out by adopting a vacuum homogenizing emulsifying machine at the rotating speed of 6000 r/min.
The foregoing is illustrative of the preferred embodiment of the present invention and is not to be construed as limiting thereof in any way, and any modifications or variations thereof that fall within the spirit of the invention are intended to be included within the scope thereof.
Claims (6)
1. A method for preparing a face cream containing various plant extracts is characterized by comprising the following steps: comprises the following steps:
step 1: drying 30-40 parts by weight of avocado fruits, 30-40 parts by weight of tangerines peels and 30-40 parts by weight of sweet almond kernels until the water content is lower than 5% to obtain a dried material; putting the dried material into an oil press, pressing at normal temperature and 1.30-1.35Mpa, and collecting the oil material; filtering the oil obtained by squeezing by adopting a ceramic membrane, and collecting filtrate to obtain refined vegetable oil;
step 2: mixing and crushing 10-20 parts by weight of dendrobium stem, 10-20 parts by weight of aloe barbadensis leaf, 10-20 parts by weight of sophora flavescens root, 10-20 parts by weight of fructus lycii, 10-20 parts by weight of echinacea purpurea and 15-40 parts by weight of neroli, to 80-100 meshes to obtain mixed powder; mixing the mixed powder with deionized water at a mass ratio of 1:40-60, and extracting at 50-60 deg.C and stirring speed of 30-60r/min for 90-120min to obtain extractive solution; filtering the extractive solution with filter paper or filter screen with aperture of 30-50 μm to obtain receipt filtrate; placing the filtrate into vacuum decompression concentration equipment, and boiling and concentrating under the condition of vacuum gauge pressure of-0.09 to-0.10 MPa to 5-10% of the original volume to obtain concentrated plant extract;
and step 3: the following materials were prepared according to the recipe: 70-90 parts by weight of deionized water, 0.1-0.3 part by weight of ammonium acryloyldimethyltaurate/VP copolymer, 0.01-0.02 part by weight of xanthan gum, 0.2-0.8 part by weight of butanediol, 3-5 parts by weight of glycerol, 0.01-0.05 part by weight of arginine, 0.1-0.5 part by weight of cetyl ethylhexanoate, 0.1-0.5 part by weight of caprylic/capric triglyceride, 0.1-0.25 part by weight of white beeswax, 0.1-0.25 part by weight of isononyl isononanoate, 0.05-0.15 part by weight of sucrose stearate, 0.05-0.15 part by weight of cetostearyl glucoside, 0.05-0.15 part by weight of cetyl alcohol, 0.05-0.15 part by weight of glyceryl stearate, 0.05-0.15 part by weight of PEG-100 stearate, 0.1-0.5 part by weight of cetostearyl alcohol, 0.1 to 0.5 part by weight of pentaerythritol tetrakis (bis-tert-butylhydroxyhydrocinnamate), 1.0 to 7.5 parts by weight of (1) vegetable fat, 0.2 to 1.0 part by weight of tocopherol acetate, 0.05 to 0.25 part by weight of sodium acrylate/sodium acryloyldimethyl taurate copolymer, 0.05 to 0.25 part by weight of isohexadecane, 0.05 to 0.25 part by weight of polysorbate-80, 0.05 to 0.25 part by weight of sorbitan oleate, 0.5 to 5.0 parts by weight of hydrogenated vegetable oil, 0.1 to 0.5 part by weight of glyceryl acrylate/acrylic acid copolymer, 0.1 to 0.5 part by weight of propylene glycol, 0.1 to 0.5 part by weight of methyl hydroxybenzoate, 0.1 to 0.5 part by weight of propyl hydroxybenzoate, 0.5 to 0.25 part by weight of fermentation lysate of bifidus yeast, 0.05 to 0.15 part by weight of 1.05 to 0.25 part by weight of sodium dihydrohydrocinnamate, 2-pentanediol, 0.05-0.15 part by weight of 1, 2-hexanediol, 0.05-0.25 part by weight of acetyl hexapeptide-8, 0.1-0.5 part by weight of trehalose, 1.0-10 parts by weight of (2) medium concentrated plant extract, 0.05-0.25 part by weight of phenoxyethanol, 0.05-0.25 part by weight of ethylhexyl glycerol, 0.05-0.15 part by weight of xanthan gum, 0.1-0.5 part by weight of p-hydroxyacetophenone, 0.1-0.5 part by weight of 1, 2-hexanediol;
and 4, step 4:
firstly, mixing p-hydroxyacetophenone, 1, 2-hexanediol and butanediol, and heating to 50-55 ℃ under the condition of stirring;
secondly, keeping the rotating speed of 50-100r/min and the heating state of deionized water, and adding the acryloyl dimethyl ammonium taurate/VP copolymer, xanthan gum and glycerol into the deionized water; heating to 82-85 deg.C, stirring at 3000-; keeping the solution at 82-85 deg.C and rotation speed of 50-100r/min, adding arginine, stirring, and keeping the temperature for 20-30 min;
thirdly, mixing cetyl ethyl hexanoate, caprylic/capric triglyceride, white beeswax, isononyl isononanoate, sucrose stearate, cetearyl glucoside, cetyl alcohol, glyceryl stearate, PEG-100 stearate, cetearyl alcohol and pentaerythritol tetrakis (di-tert-butyl hydroxy hydrocinnamate) ester, heating to 82-85 ℃, stirring until the mixture is melted into liquid, and keeping the temperature for standby, wherein the temperature is not longer than 30 min; adding tocopherol acetate into the heat preservation solution, and stirring until the tocopherol acetate is completely dissolved for later use;
fourthly, mixing the solution obtained in the second step with the solution obtained in the third step, putting the mixture into vacuum high-shear stirring equipment, and performing high-shear stirring for 5-10min at the rotation speed of 4000 plus materials 6000r/min under the vacuum condition of the vacuum gauge pressure of-0.09 to-0.10 MPa until the materials are completely and uniformly emulsified;
fifthly, cooling the material obtained in the fourth step to 70-75 ℃, adding vegetable oil, sodium acrylate/sodium acryloyldimethyl taurate copolymer, isohexadecane, polysorbate-80, sorbitan oleate and hydrogenated vegetable oil, putting into a vacuum high-shear stirring device, and stirring for 1-2min at a high shear of 6000r/min at a rotation speed of 4000-;
sixthly, cooling the materials obtained in the fifth step to 55-60 ℃, adding the glycerin acrylate/acrylic acid copolymer, propylene glycol, methyl hydroxybenzoate and propyl hydroxybenzoate, putting the mixture into vacuum stirring equipment, and stirring for 5-15min at a rotating speed of 50-200r/min under the vacuum condition of vacuum gauge pressure of-0.09 to-0.10 MPa until the materials are uniformly mixed;
seventhly, cooling the materials obtained in the sixth step to 25-45 ℃, adding the concentrated plant extract, the lysate of the yeast fermentation product of the second cracking, 1, 2-pentanediol, 1, 2-hexanediol, acetyl hexapeptide-8, trehalose, phenoxyethanol, ethylhexyl glycerol and xanthan gum, putting into a vacuum stirring device, and stirring for 5-15min at the rotating speed of 50-200r/min under the vacuum condition of the vacuum gauge pressure of-0.09 to-0.10 MPa until the materials are uniformly mixed;
eighthly, mixing the material obtained in the first step with the material obtained in the seventh step, putting the mixture into vacuum stirring equipment, and stirring the mixture for 5 to 15 minutes at a rotating speed of 50 to 200r/min under the vacuum condition of vacuum gauge pressure of-0.09 to-0.10 MPa until the materials are uniformly mixed;
and ninthly, filtering the material obtained in the eighth step by a filtering device with the fineness of 200 and 400 meshes to obtain a receipt filtrate, namely the face cream.
2. The method for preparing a cream containing a plurality of plant extracts according to claim 1, wherein: in the step 1, the material is placed into vacuum drying equipment during drying, and is dried under the conditions of vacuum gauge pressure of-0.09 to-0.1 MPa and temperature of 50 to 55 ℃ until the water content is lower than 5 percent, so that the dried material is obtained.
3. The method for preparing a cream containing a plurality of plant extracts according to claim 1, wherein: the oil press is a screw oil press, the pressing frequency is 5-6 times, and the rotating speed of a pressing shaft is 40-50 r/min.
4. The method for preparing a cream containing a plurality of plant extracts according to claim 1, wherein: the membrane aperture is 50-100nm and the filtering pressure is 0.25-0.50MPa when the ceramic membrane is used for filtering.
5. The method for preparing a cream containing a plurality of plant extracts according to claim 1, wherein: the fourth step is carried out by adopting a vacuum homogenizing emulsifying machine, and the rotating speed is 4000-.
6. The method for preparing a cream containing a plurality of plant extracts according to claim 1, wherein: the fifth step is carried out by adopting a vacuum homogenizing emulsifying machine, and the rotating speed is 4000-.
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| CN111920721A (en) * | 2020-09-03 | 2020-11-13 | 深圳市花纪元日用科技有限公司 | Small cherry face cream and preparation method thereof |
| WO2021088399A1 (en) * | 2019-11-05 | 2021-05-14 | 湖北创界生物科技有限公司 | Moisturizing and hydrating facial mask composition, facial mask, and preparation method for facial mask composition |
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| WO2021088399A1 (en) * | 2019-11-05 | 2021-05-14 | 湖北创界生物科技有限公司 | Moisturizing and hydrating facial mask composition, facial mask, and preparation method for facial mask composition |
| CN111920721A (en) * | 2020-09-03 | 2020-11-13 | 深圳市花纪元日用科技有限公司 | Small cherry face cream and preparation method thereof |
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