CN113633584A - Asparagus polyphenol moisturizing skin care product and preparation method thereof - Google Patents
Asparagus polyphenol moisturizing skin care product and preparation method thereof Download PDFInfo
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
- A61K8/9706—Algae
- A61K8/9717—Rhodophycota or Rhodophyta [red algae], e.g. Porphyra
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/347—Phenols
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/26—Optical properties
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/74—Biological properties of particular ingredients
- A61K2800/78—Enzyme modulators, e.g. Enzyme agonists
- A61K2800/782—Enzyme inhibitors; Enzyme antagonists
Abstract
The asparagus polyphenol moisturizing skin care product is asparagus polyphenol-containing moisturizing skin care lotion or moisturizing skin care milk or moisturizing skin care cream, wherein the asparagus polyphenol-containing moisturizing skin care lotion comprises the following components in percentage by mass: 1-10% of asparagus polyphenol; humectant 3-6%; 1-6% of a conditioner; 0.03 to 0.06 percent of chelating agent; 0.6 to 4 percent of functional auxiliary agent; water and the balance. The asparagus polyphenol moisturizing skin care product disclosed by the invention has a remarkable moisturizing effect and is mild and non-irritant to skin.
Description
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a asparagus polyphenol moisturizing skin care product and a preparation method thereof.
Background
The skin separates the internal environment of the human body from the external environment, and is similar to a protective wall constructed between the internal environment of the human body and the external environment, so that the stability and the balance of the internal environment of the human body are kept. The skin can be divided into epidermis, dermis, subcutaneous tissue and skin appendage, wherein the epidermis is located at the outermost layer of the skin and sequentially comprises a basal layer, a spinous layer, a granular layer, a transparent layer and a cuticle from inside to outside.
Skin moisturizing is a basic nursing work, and the skin moisturizing is well done, so that the skin aging can be delayed, and the occurrence of skin diseases can be reduced and prevented. Skin moisturization depends primarily on the water content of the stratum corneum, which should be maintained at 10% to 20% for healthy skin, and when the water content of the stratum corneum is sufficient, the skin is soft, smooth, tender and elastic, and less than 10% of the skin is dry, rough and even chapped. The protection and maintenance of stratum corneum moisture relies on the barrier and hydration of the epidermis. The barrier function of the skin relies primarily on the "brick wall structure" of the stratum corneum. The 'brick wall structure' of the horny layer is composed of 'brick walls' (keratinocytes) and 'mortar' (lipid in the gaps between the keratinocytes), and the compact and firm structure can block the invasion of external harmful factors and the loss of water and nutrient substances in the body and maintain the important barrier function of the epidermis. In addition, the lipid (ceramide, squalene, linoleic acid, linolenic acid, etc.) in the sebum membrane on the skin surface can lock water, prevent loss of nutrients, moisturizing factors and water, maintain the water content of the stratum corneum, and play a role in moistening and moisturizing the skin. Hydration of the skin epidermis is mainly dependent on Natural Moisturizing Factors (NMF) in the keratinocyte matrix. NMF is a small molecular compound with water absorption property existing in skin, is formed by amino acid assembly formed by degradation of filaggrin, can effectively absorb and lock water, and mainly comprises amino acid, lactate, urea and other unknown substances. The natural moisturizing factor and the compact keratin cellulose increase the strength of the inside of the cell, and simultaneously combine a large amount of water to ensure that the stratum corneum keeps a certain water content, which is an essential condition for stabilizing the hydration state of the skin and maintaining the normal physiological function of the stratum corneum. The inherent hydration ability of skin depends on hyaluronic acid and moisture transport within the skin, in addition to the presence of NMF in keratinocytes. The proteins in the epidermis of human skin, which play a role in water transport, are mainly Aquaporin 3 (AQP 3), AQP3 can transport water and substances such as urea and glycerol into and out of the skin, and is a key factor for maintaining skin hydration.
In the related art, the cosmetics can achieve the effects of moisturizing water and moisture by adding the moisture-keeping wetting agent. The moisturizing humectant is similar to NMF, human protein, polysaccharide and the like in the epidermis, and when the moisture of the skin is lost, the moisturizing humectant enters the skin through pores, or carries water, or wraps up the water which is not lost in the skin to prevent the water from being lost, so that the water in the skin is retained.
The plant components are natural in source and rich in effect, and are widely used in food and medicines. In cosmetics, plant ingredients can be used in place of various functional materials or as auxiliary materials. The addition of plant components in the product can conform to the idea that consumers adopt nature, so more and more merchants begin to develop products with the center of gravity which is inclined to plant skin care.
Gracilaria lemaneiformis is temperate red algae and is mainly distributed in coastal areas such as Shandong, Fujian and Guangdong. In recent years, researches on asparagus are mostly focused on saccharides, such as asparagus polysaccharide, asparagus oligosaccharide, agar prepared by using asparagus, and the like, while related researches on asparagus polyphenol are few and mainly focused on the antioxidant capacity, and at present, researches or reports on the moisture absorption and retention performance of asparagus polyphenol are not found.
The above-mentioned contents are only the techniques known by the inventor, and are only used for assisting understanding of the technical scheme of the invention, and do not represent an admission that the above-mentioned contents are the prior art.
Disclosure of Invention
The invention mainly aims to provide a asparagus polyphenol moisturizing skin care product which has an obvious moisturizing effect and is mild and non-irritant to skin.
In order to achieve the purpose, the invention provides a asparagus polyphenol moisturizing skin care product, which is a moisturizing skin care lotion containing asparagus polyphenol, and the moisturizing skin care lotion comprises the following components in percentage by mass:
1-10% of asparagus polyphenol;
humectant 3-6%;
1-6% of a conditioner;
0.03 to 0.06 percent of chelating agent;
0.6 to 4 percent of functional auxiliary agent;
water and the balance.
Further, the functional auxiliary agent comprises the following components in percentage by mass:
0.01 to 0.6 percent of aromatic;
0.1 to 0.8 percent of preservative;
0.4 to 2 percent of surfactant;
0.1 to 0.6 percent of acid-base regulator.
Further, the moisturizer includes glycerin, sodium pyrrolidone carboxylate, and sodium hyaluronic acid.
Further, the conditioning agent is D-panthenol.
Further, the chelating agent is disodium ethylene diamine tetraacetate.
Further, the aromatic is essence.
Further, the surfactant is polyglycerol-10 laurate.
Further, the pH regulator is citric acid.
In order to achieve the purpose, the invention also provides a asparagus polyphenol moisturizing skin care product, which is a moisturizing skin care emulsion containing asparagus polyphenol, and the moisturizing skin care emulsion comprises the following components in percentage by mass:
1-10% of asparagus polyphenol;
4% -6% of humectant;
4 to 6 percent of conditioner;
0.06-0.12% of chelating agent;
4 to 6 percent of thickening agent;
2% -4% of a lubricant;
2% -4% of functional auxiliary agent;
water and the balance.
Further, the moisturizer comprises glycerin, cupuacu fruit oil, and vitamin E acetate.
Further, the conditioning agent comprises D-panthenol, caprylic capric triglyceride and allantoin.
Further, the chelating agent is disodium ethylene diamine tetraacetate.
Further, the thickening agent includes cetostearyl alcohol, synthetic squalane, and xanthan gum.
Further, the lubricant is simethicone with the viscosity of 100 cs.
Further, the functional auxiliary agent comprises the following components in percentage by mass:
0.01 to 0.5 percent of aromatic;
0.3 to 1 percent of preservative;
1.6 to 2.5 percent of surfactant.
Further, the aromatic is essence.
Further, the surfactant is C16-C18 alkyl glycoside.
In order to achieve the purpose, the invention also provides a asparagus polyphenol moisturizing skin care product, which is a asparagus polyphenol moisturizing skin care cream, and the asparagus polyphenol moisturizing skin care product comprises the following components in percentage by mass:
1-10% of asparagus polyphenol;
6 to 12 percent of humectant;
4 to 6 percent of conditioner;
5% -8% of thickening agent;
0.5 to 1.5 percent of lubricant;
2.6 to 4.8 percent of functional auxiliary agent;
water and the balance.
Further, the moisturizer comprises glycerin, isopropyl palmitate, shea butter, propylene glycol, and sodium hyaluronate.
Further, the conditioner is caprylic capric triglyceride
Further, the thickener comprises cetostearyl alcohol, synthetic squalane, monoglyceride, carbomer 940, polyacrylamide, C13-C14 isoparaffin, and laureth-7
Further, the lubricant is dimethyl silicone oil with the viscosity of 100cs
Further, the functional auxiliary agent comprises the following components in percentage by mass:
0.01 to 0.5 percent of aromatic;
0.3 to 1 percent of preservative;
0.1 to 0.3 percent of acid-base blender;
1.6 to 3 percent of surfactant.
Further, the aromatic is essence.
Further, the acid-base blender is aminomethyl propanol.
Further, the surfactant includes glyceryl stearate and PEG-100 stearate.
In order to achieve the above object, the present invention also provides a method for preparing the moisturizing skin care lotion containing asparagus polyphenol, which comprises the following steps:
uniformly stirring the phase A component under the heating condition that the heating temperature is 80-85 ℃, and preserving heat for 18-22 min when the phase A component is uniformly stirred until no insoluble substances exist, so as to obtain an aqueous solution of the phase A component; wherein, the phase A component comprises water, glycerol, sodium pyrrolidone carboxylate, sodium hyaluronic acid and disodium ethylene diamine tetraacetate;
mixing a B-phase component with the aqueous solution of the A-phase component under the heating condition that the heating temperature is 40-45 ℃, and uniformly stirring until no insoluble substances exist to obtain a mixed solution of the B-phase component and the A-phase component; wherein the phase B component comprises asparagus polyphenol, D-panthenol, citric acid and a preservative;
premixing all raw materials in the phase C component, and uniformly stirring until the raw materials are transparent to obtain transparent liquid of the phase C component; wherein, the phase C component comprises polyglycerol-10 laurate and essence;
mixing the transparent liquid and the mixed solution under the heating condition that the heating temperature is 40-45 ℃, and stirring uniformly to obtain a mixture of the transparent liquid and the mixed solution;
and cooling the mixture to normal temperature, filtering the mixture by using filter cloth at normal temperature, and filtering to obtain the asparagus polyphenol-containing moisturizing skin-care lotion.
In order to achieve the above object, the present invention also provides a method for preparing the moisturizing skin care milk containing asparagus polyphenol, which comprises the following steps:
heating and dissolving the phase A component at a heating temperature of 75-85 ℃ for later use; wherein the phase A component comprises C16-C18 alkyl glycoside, cetearyl alcohol, synthetic squalane, caprylic capric triglyceride, Cupuacu seed oil, vitamin E acetate and simethicone with the viscosity of 100 cs;
heating and dissolving the phase B component under the heating condition that the heating temperature is 85-95 ℃, adding the dissolved phase A component into the dissolved phase B component, and homogenizing for 2-4 min to obtain a mixture of the phase A component and the phase B component; the phase B component comprises disodium ethylene diamine tetraacetate, glycerol, xanthan gum, D-panthenol, allantoin, asparagus polyphenol and water, wherein the xanthan gum is pre-dispersed by the glycerol;
stirring the mixture, cooling, adding a C-phase component into the mixture after the mixture is cooled to 43-46 ℃, continuously stirring, cooling, and cooling to room temperature to obtain the asparagus polyphenol-containing moisturizing skin care milk; wherein, the phase C component comprises essence and preservative.
In order to achieve the above object, the present invention also provides a method for preparing the above moisturizer containing asparagus polyphenol, which comprises the following steps:
heating and dissolving the phase A component at a heating temperature of 75-85 ℃ for later use; wherein the phase A component comprises caprylic capric triglyceride, synthetic squalane, glyceryl stearate, PEG-100 stearate, monoglyceride, isopropyl palmitate, cetostearyl alcohol, shea butter and dimethicone with viscosity of 100 cs;
heating and dissolving the phase B component under the heating condition that the heating temperature is 85-95 ℃, adding the dissolved phase A component into the dissolved phase B component, and homogenizing for 2-4 min to obtain a mixture of the phase A component and the phase B component; the phase B component comprises propylene glycol, glycerol, carbomer 940, sodium hyaluronate, polyacrylamide, C13-C14 isoparaffin, laureth-7, asparagus polyphenol and water, wherein the sodium hyaluronate and carbomer 940 are pre-dispersed by the glycerol and the propylene glycol;
adding the C-phase component into the mixture, and homogenizing for 2-4 min to obtain a mixed material; wherein the C phase component is aminomethyl propanol;
stirring the mixed material, cooling, adding a phase D component into the mixed material after the mixed material is cooled to 44-46 ℃, homogenizing for 2-4 min, continuing stirring, cooling, and cooling to room temperature to obtain the asparagus polyphenol-containing moisturizing skin cream; wherein, the phase D component comprises essence and preservative.
Compared with the prior art, the invention has the beneficial effects that:
the asparagus polyphenol moisturizing skin care product provided by the invention takes asparagus polyphenol with a plurality of phenolic groups as a main component, and can be moisturizing skin care lotion, moisturizing skin care milk or moisturizing skin care cream through the change of a formula and a production process, and the asparagus polyphenol has better moisture absorption and moisturizing performances both inside and outside the body (specifically, the asparagus polyphenol not only can absorb moisture in the air, but also can be combined with protein, polysaccharide, phospholipid and the like in the skin, so that the moisturizing capability of the skin can be effectively improved, in addition, the asparagus polyphenol can also inhibit the activity of hyaluronidase in the skin, so that the real deep physiological moisturizing effect can be achieved), so the asparagus polyphenol with a specific proportion is compounded with other acceptable auxiliary materials in the skin care product to prepare the moisturizing skin care lotion, the skin care milk or the moisturizing skin care cream, so that the moisture-preserving agent can have a remarkable moisture-preserving effect; and because the asparagus polyphenol is derived from asparagus which can be used as food and is a safe and nontoxic natural plant component, the asparagus polyphenol moisturizing skin care product provided by the invention not only has an obvious moisturizing effect, but also is mild and non-irritant to skin, and is suitable for most people to use.
Drawings
In order to more clearly illustrate the embodiments of the present invention or the technical solutions in the prior art, the drawings used in the description of the embodiments or the prior art will be briefly described below, it is obvious that the drawings in the following description are only some embodiments of the present invention, and for those skilled in the art, other drawings can be obtained according to the structures shown in the drawings without creative efforts.
FIG. 1 is a graph showing the comparison of moisture absorption capacity between Gracilaria lemaneiformis polyphenol and glycerol in an environment of high relative humidity (81%) according to an embodiment of the present invention;
FIG. 2 is a graph showing the comparison of the moisturizing ability of Gracilaria lemaneiformis polyphenol and glycerol in a dry environment according to an embodiment of the present invention;
FIG. 3 is a graph comparing the effect of different proportions of Gracilaria lemaneiformis polyphenol water solution and blank control water on the rate of change of skin moisture in an embodiment of the present invention.
The implementation, functional features and advantages of the objects of the present invention will be further explained with reference to the accompanying drawings.
Detailed Description
The technical solutions in the embodiments of the present invention will be clearly and completely described below with reference to the drawings in the embodiments of the present invention, and it is obvious that the described embodiments are only a part of the embodiments of the present invention, and not all of the embodiments. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
Firstly, extracting asparagus polyphenol in asparagus by an ethanol reflux method:
(1) weighing appropriate amount of thallus Gracilariae dry powder, and placing into a container (such as round bottom flask);
(2) adding 70% ethanol into a container, wherein the liquid-solid ratio of the ethanol to the dry powder of the asparagus is 50 mL/g;
(3) heating the container to 80 ℃, and refluxing for 2h for extraction; wherein the average extraction rate of asparagus polyphenol is 2.20 +/-0.04 mg/g of dry asparagus.
Next, preferred examples of the present invention will be described in detail, and experimental methods in which specific conditions are not specified in the examples are generally conventional conditions.
Example 1
Determination of asparagus polyphenol in vitro moisture absorption capacity:
accurately weighing 0.5g of each of the asparagus polyphenol and glycerol which are dried to constant weight at room temperature of about 20 ℃, respectively putting the asparagus polyphenol and glycerol into a culture dish, putting the culture dish into a constant-temperature and constant-humidity environment with the temperature of 20 ℃ and the Relative Humidity (RH) of 81%, standing for a period of time (1, 2, 4, 8, 12, 24 and 48 hours), accurately weighing the mass of each sample, and calculating the moisture absorption rate. Wherein the moisture absorption rate is (m)1－m0)×100％/m0In the formula, m0To weigh the mass of the sample before moisture absorption, m1For the quality of the sample after moisture absorption, data analysis is carried out by using SPSS 12.0 statistical software, and if the moisture absorption rate P is less than 0.05, the difference is considered to be significant.
As can be seen from fig. 1, in both the asparagus polyphenol and the humectant glycerin commonly used in skin care products, the moisture absorption rate gradually increases with time under a high relative humidity (81%) environment. The moisture absorption rates of asparagus polyphenol and glycerol are similar at 1h, and the moisture absorption capacity of asparagus polyphenol is obviously higher than that of glycerol (P is less than 0.05) at 2h and 4 h. After 8h, the moisture absorption capacity of the glycerol is higher than that of asparagus polyphenol. In real life, the frequency of face cleaning is often several hours, so that the moisture absorption capacity of asparagus polyphenol is stronger than that of glycerin at 2h and 4h, thereby showing the feasibility of the asparagus polyphenol as a skin care product moisture absorbent.
Example 2
Testing the in-vitro moisturizing capability of asparagus polyphenol:
weighing 0.5g each of the asparagus polyphenol and glycerol which are dried to constant weight at room temperature of about 20 ℃, adding the asparagus polyphenol and glycerol into a weighing bottle with the diameter of 3cm, adding 0.2g of deionized water, and placing the weighing bottle in a dryer filled with silica gel. The standing time is 1, 2, 4, 8, 12, 24 and 48 hours, the mass of each sample is accurately weighed, and the moisture retention rate is calculated. WhereinMoisture retention rate ═ m1×100％/m0In the formula, m0To add the amount of water, m1The data analysis is carried out by SPSS 12.0 statistical software for the moisture content after the sample is placed, and the difference is considered to be significant if the moisture retention rate P is less than 0.05.
As can be seen from fig. 2, both the asparagus polyphenol and the glycerin gradually decreased the moisture retention rate with time. The moisturizing rates of asparagus polyphenol and glycerol are similar at 1h and 2h, and after 4h, the moisturizing rate of asparagus polyphenol is higher than that of glycerol (P is less than 0.05).
Example 3
Influence of asparagus polyphenol on human skin moisture change rate (detection of asparagus polyphenol in vivo moisture retention capacity):
the influence of the asparagus polyphenol water solution with the mass fraction of 1% and 3% on the change rate of the skin moisture of a human body is measured by a human body method, and water is used as a negative control. 26 healthy female volunteers without skin diseases are selected, aged between 18 and 25 years, and tested by a CM825 type skin moisture tester under the conditions that the ambient temperature is 22 ℃ and the relative humidity is 60 percent. Any cosmetics or external medicines can not be used for 2 to 3 days before the test of the tested part, and water can not be contacted for 1 to 3 hours before the test. Before the test, the testee needs to clean the inner sides of the forearms of the hands uniformly, and the cleaning method is to wipe the forearms clean by using dry facial tissue. The inner sides of the forearms of both hands of the testee are marked with measuring areas, the area of the testing area is 4cm multiplied by 4cm, the same arm can simultaneously mark a plurality of areas, and each testing area is at least 1cm apart. Before formal test, people should sit still in a room meeting the standard for more than 20min without drinking water and beverages. The forearms were exposed and left in the test condition to remain relaxed. The test sample was evenly spread over the test area using a latex finger cuff at a rate of 2.0mg/cm 2. The skin moisture content was measured before and 30, 60, 90, 120, 150, 180, 210, 240min after sample application, and the skin moisture change rate was calculated. The skin moisture content testing operation is completed by the same person, and the skin moisture change rate calculation formula is as follows:
rate of change of skin moisture ═ mn－m0)×100％/m0。
In the formula: m isnRepresents the measurement value at the n hour after the sample is coated; m is0The measured values before coating the sample are shown. Data analysis was performed using SPSS 12.0 statistical software, and differences were considered significant if the skin moisture change rate P < 0.05.
As can be seen from FIG. 3, the rate of change of skin moisture caused by the application of the aqueous solution of Gracilaria lemaneiformis polyphenol, whether the aqueous solution is a 1% or 3% solution, is significantly higher than that of the application of blank control water (P < 0.05), thereby indicating that the Gracilaria lemaneiformis polyphenol has better moisturizing performance.
Example 4
The moisturizing skin care lotion containing asparagus polyphenol comprises the following components in percentage by mass (see table 1).
TABLE 1 moisturizing lotion formulations
The preparation method of the moisturizing skin care lotion containing asparagus polyphenol comprises the following steps:
step S11, uniformly stirring the phase A component under the heating condition that the heating temperature is 80-85 ℃, and preserving heat for 18-22 min when the phase A component is uniformly stirred until no insoluble substances exist, so as to obtain an aqueous solution of the phase A component; wherein, the phase A component comprises water, glycerol, pyrrolidone sodium carboxylate, hyaluronic acid sodium and ethylene diamine tetraacetic acid disodium;
step S12, mixing the aqueous solution of the B-phase component and the aqueous solution of the A-phase component under the heating condition that the heating temperature is 40-45 ℃, and uniformly stirring until no insoluble substances exist to obtain a mixed solution of the B-phase component and the A-phase component; wherein, the phase B component comprises asparagus polyphenol, D-panthenol, citric acid and preservative;
step S13, premixing raw materials in the C phase component, and uniformly stirring until the mixture is transparent to obtain transparent liquid of the C phase component; wherein, the phase C component comprises polyglycerol-10 laurate and essence;
step S14, mixing the transparent liquid and the mixed solution under the heating condition that the heating temperature is 40-45 ℃, and stirring the mixture uniformly to obtain a mixture of the transparent liquid and the mixed solution;
cooling the mixture to normal temperature, filtering the mixture at normal temperature by using a filter cloth (preferably a filter cloth with a mesh size of more than 400), and filtering to obtain the asparagus polyphenol-containing moisturizing skin-care lotion.
Example 5
The moisturizing and skin-care milk containing asparagus polyphenol in the embodiment comprises the following components in percentage by mass (see table 2).
TABLE 2 moisturizing skin care lotion formula
The preparation method of the moisturizing and skin-care milk containing asparagus polyphenol comprises the following steps:
step S21, heating and dissolving the phase A component under the heating condition that the heating temperature is 75-85 ℃ for later use; wherein, the phase A component comprises C16-C18 alkyl glycoside, cetostearyl alcohol, synthetic squalane, caprylic capric triglyceride, Cupuacu seed oil, vitamin E acetate and simethicone with the viscosity of 100 cs;
step S22, heating and dissolving the phase B component under the heating condition that the heating temperature is 85-95 ℃, adding the dissolved phase A component into the dissolved phase B component, and homogenizing for 2-4 min to obtain a mixture of the phase A component and the phase B component; the phase B component comprises disodium ethylene diamine tetraacetate, glycerol, xanthan gum, D-panthenol, allantoin, asparagus polyphenol and water, wherein the xanthan gum is pre-dispersed with glycerol;
step S23, stirring and cooling the mixture, adding the C-phase component into the mixture after the mixture is cooled to 43-46 ℃, continuing stirring and cooling, and cooling to room temperature to obtain the asparagus polyphenol-containing moisturizing skin care milk; wherein, the phase C component comprises essence and preservative.
Example 6
The moisturizing skin cream containing asparagus polyphenol in the embodiment comprises the following components in percentage by mass (see table 3).
TABLE 3 moisturizing skin cream formulations
The preparation method of the moisturizing and skin-care cream containing asparagus polyphenol comprises the following steps:
step S31, heating and dissolving the phase A component under the heating condition that the heating temperature is 75-85 ℃ for later use; wherein, the phase A component comprises caprylic capric triglyceride, synthetic squalane, glyceryl stearate, PEG-100 stearate, monoglyceride, isopropyl palmitate, cetostearyl alcohol, shea butter and dimethicone with viscosity of 100 cs;
step S32, heating and dissolving the phase B component under the heating condition that the heating temperature is 85-95 ℃, adding the dissolved phase A component into the dissolved phase B component, and homogenizing for 2-4 min to obtain a mixture of the phase A component and the phase B component; the phase B component comprises propylene glycol, glycerol, carbomer 940, sodium hyaluronate, polyacrylamide, C13-C14 isoparaffin, laureth-7, asparagus polyphenol and water, wherein the sodium hyaluronate and carbomer 940 are pre-dispersed by the glycerol and the propylene glycol;
step S33, adding the phase C component into the mixture, and homogenizing for 2-4 min to obtain a mixed material; wherein, the phase C component is aminomethyl propanol;
step S34, stirring and cooling the mixed material, adding the phase D component into the mixed material after the mixed material is cooled to 44-46 ℃, homogenizing for 2-4 min, continuing stirring and cooling, and cooling to room temperature to obtain the asparagus polyphenol-containing moisturizing skin cream; wherein, the phase D component comprises essence and preservative.
It should be noted that other contents of the asparagus polyphenol moisturizing skin care product and the preparation method thereof disclosed by the invention can be found in the prior art, and are not described herein again.
In addition, it should be noted that the technical solutions in the embodiments may be combined with each other, but must be based on the realization of the technical solutions by those skilled in the art, and when the technical solutions are contradictory or cannot be realized, such a combination of the technical solutions should be considered to be absent and not to be within the protection scope of the present invention.
The above description is only an alternative embodiment of the present invention, and not intended to limit the scope of the present invention, and all modifications and equivalents of the present invention, which are made by the contents of the present specification and the accompanying drawings, or directly/indirectly applied to other related technical fields, are included in the scope of the present invention.
Claims (10)
1. The asparagus polyphenol moisturizing skin care product is asparagus polyphenol-containing moisturizing skin care lotion, and the moisturizing skin care lotion comprises the following components in percentage by mass:
1-10% of asparagus polyphenol;
humectant 3-6%;
1-6% of a conditioner;
0.03 to 0.06 percent of chelating agent;
0.6 to 4 percent of functional auxiliary agent;
water and the balance.
2. The asparagus polyphenol moisturizing skin care product as claimed in claim 1, wherein the functional auxiliary comprises the following components in percentage by mass:
0.01 to 0.6 percent of aromatic;
0.1 to 0.8 percent of preservative;
0.4 to 2 percent of surfactant;
0.1 to 0.6 percent of acid-base regulator.
3. The asparagus polyphenol moisturizing skin care product of claim 2, wherein the moisturizers comprise glycerin, sodium pyrrolidone carboxylate, and sodium hyaluronic acid;
and/or, the conditioning agent is D-panthenol;
and/or the chelating agent is disodium ethylene diamine tetraacetate;
and/or the aromatic is essence;
and/or, the surfactant is polyglycerol-10 laurate;
and/or the pH regulator is citric acid.
4. The asparagus polyphenol moisturizing skin care product is characterized by being a moisturizing skin care emulsion containing asparagus polyphenol, and the moisturizing skin care emulsion comprises the following components in percentage by mass:
1-10% of asparagus polyphenol;
4% -6% of humectant;
4 to 6 percent of conditioner;
0.06-0.12% of chelating agent;
4 to 6 percent of thickening agent;
2% -4% of a lubricant;
2% -4% of functional auxiliary agent;
water and the balance.
5. The asparagus polyphenol moisturizing skin care product of claim 4, wherein the moisturizer comprises glycerin, cupuasu fruit oil, and vitamin E acetate;
and/or, the conditioning agent comprises D-panthenol, caprylic capric triglyceride, and allantoin;
and/or the chelating agent is disodium ethylene diamine tetraacetate;
and/or, the thickening agent comprises cetostearyl alcohol, synthetic squalane and xanthan gum;
and/or the lubricant is dimethyl silicone oil with the viscosity of 100 cs;
and/or the functional auxiliary agent comprises the following components in percentage by mass:
0.01 to 0.5 percent of aromatic;
0.3 to 1 percent of preservative;
1.6 to 2.5 percent of surfactant.
6. The asparagus polyphenol moisturizing skin care product is characterized by being asparagus polyphenol moisturizing skin care cream containing asparagus polyphenol, wherein the asparagus polyphenol moisturizing skin care cream comprises the following components in percentage by mass:
1-10% of asparagus polyphenol;
6 to 12 percent of humectant;
4 to 6 percent of conditioner;
5% -8% of thickening agent;
0.5 to 1.5 percent of lubricant;
2.6 to 4.8 percent of functional auxiliary agent;
water and the balance.
7. The asparagus polyphenol moisturizing skin care product of claim 6, wherein the moisturizer comprises glycerin, isopropyl palmitate, shea butter, propylene glycol, and sodium hyaluronate;
and/or the conditioning agent is caprylic capric triglyceride;
and/or, the thickening agent comprises cetostearyl alcohol, synthetic squalane, monoglyceride, carbomer 940, polyacrylamide, C13-C14 isoparaffin, and laureth-7;
and/or the lubricant is dimethyl silicone oil with the viscosity of 100 cs;
and/or the functional auxiliary agent comprises the following components in percentage by mass:
0.01 to 0.5 percent of aromatic;
0.3 to 1 percent of preservative;
0.1 to 0.3 percent of acid-base blender;
1.6 to 3 percent of surfactant.
8. A method of preparing the asparagus polyphenol moisturizing skin care product of any one of claims 1 to 3, comprising the steps of:
uniformly stirring the phase A component under the heating condition that the heating temperature is 80-85 ℃, and preserving heat for 18-22 min when the phase A component is uniformly stirred until no insoluble substances exist, so as to obtain an aqueous solution of the phase A component; wherein, the phase A component comprises water, glycerol, sodium pyrrolidone carboxylate, sodium hyaluronic acid and disodium ethylene diamine tetraacetate;
mixing a B-phase component with the aqueous solution of the A-phase component under the heating condition that the heating temperature is 40-45 ℃, and uniformly stirring until no insoluble substances exist to obtain a mixed solution of the B-phase component and the A-phase component; wherein the phase B component comprises asparagus polyphenol, D-panthenol, citric acid and a preservative;
premixing all raw materials in the phase C component, and uniformly stirring until the raw materials are transparent to obtain transparent liquid of the phase C component; wherein, the phase C component comprises polyglycerol-10 laurate and essence;
mixing the transparent liquid and the mixed solution under the heating condition that the heating temperature is 40-45 ℃, and stirring uniformly to obtain a mixture of the transparent liquid and the mixed solution;
and cooling the mixture to normal temperature, filtering the mixture by using filter cloth at normal temperature, and filtering to obtain the asparagus polyphenol-containing moisturizing skin-care lotion.
9. A method for preparing the asparagus polyphenol moisturizing skin care product as claimed in any one of claims 4 to 5, wherein the method comprises the following steps:
heating and dissolving the phase A component at a heating temperature of 75-85 ℃ for later use; wherein the phase A component comprises C16-C18 alkyl glycoside, cetearyl alcohol, synthetic squalane, caprylic capric triglyceride, Cupuacu seed oil, vitamin E acetate and simethicone with the viscosity of 100 cs;
heating and dissolving the phase B component under the heating condition that the heating temperature is 85-95 ℃, adding the dissolved phase A component into the dissolved phase B component, and homogenizing for 2-4 min to obtain a mixture of the phase A component and the phase B component; the phase B component comprises disodium ethylene diamine tetraacetate, glycerol, xanthan gum, D-panthenol, allantoin, asparagus polyphenol and water, wherein the xanthan gum is pre-dispersed by the glycerol;
stirring the mixture, cooling, adding a C-phase component into the mixture after the mixture is cooled to 43-46 ℃, continuously stirring, cooling, and cooling to room temperature to obtain the asparagus polyphenol-containing moisturizing skin care milk; wherein, the phase C component comprises essence and preservative.
10. A method for preparing the asparagus polyphenol moisturizing skin care product as claimed in any one of claims 6 to 7, wherein the method comprises the following steps:
heating and dissolving the phase A component at a heating temperature of 75-85 ℃ for later use; wherein the phase A component comprises caprylic capric triglyceride, synthetic squalane, glyceryl stearate, PEG-100 stearate, monoglyceride, isopropyl palmitate, cetostearyl alcohol, shea butter and dimethicone with viscosity of 100 cs;
heating and dissolving the phase B component under the heating condition that the heating temperature is 85-95 ℃, adding the dissolved phase A component into the dissolved phase B component, and homogenizing for 2-4 min to obtain a mixture of the phase A component and the phase B component; the phase B component comprises propylene glycol, glycerol, carbomer 940, sodium hyaluronate, polyacrylamide, C13-C14 isoparaffin, laureth-7, asparagus polyphenol and water, wherein the sodium hyaluronate and carbomer 940 are pre-dispersed by the glycerol and the propylene glycol;
adding the C-phase component into the mixture, and homogenizing for 2-4 min to obtain a mixed material; wherein the C phase component is aminomethyl propanol;
stirring the mixed material, cooling, adding a phase D component into the mixed material after the mixed material is cooled to 44-46 ℃, homogenizing for 2-4 min, continuing stirring, cooling, and cooling to room temperature to obtain the asparagus polyphenol-containing moisturizing skin cream; wherein, the phase D component comprises essence and preservative.
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Citations (4)
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| JPH07101871A (en) * | 1992-12-24 | 1995-04-18 | Lion Corp | Promoter for synthesis of hyaluronic acid in living body |
| US20160000697A1 (en) * | 2013-03-14 | 2016-01-07 | Avon Products, Inc. | Gracilaria textorii extracts and methods of use |
| CN106420471A (en) * | 2016-10-31 | 2017-02-22 | 广东科玮生物技术股份有限公司 | Skin care product with sunscreen and sun repair functions and preparation method thereof |
| CN108324651A (en) * | 2018-04-18 | 2018-07-27 | 佛山汇沐化学科技有限公司 | A kind of composition with skin anti-oxidation efficacy |
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2021
- 2021-08-23 CN CN202110965590.1A patent/CN113633584A/en active Pending
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH07101871A (en) * | 1992-12-24 | 1995-04-18 | Lion Corp | Promoter for synthesis of hyaluronic acid in living body |
| US20160000697A1 (en) * | 2013-03-14 | 2016-01-07 | Avon Products, Inc. | Gracilaria textorii extracts and methods of use |
| CN106420471A (en) * | 2016-10-31 | 2017-02-22 | 广东科玮生物技术股份有限公司 | Skin care product with sunscreen and sun repair functions and preparation method thereof |
| CN108324651A (en) * | 2018-04-18 | 2018-07-27 | 佛山汇沐化学科技有限公司 | A kind of composition with skin anti-oxidation efficacy |
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