CN112080834A - 一种超疏水棉麻纺织面料的制备方法 - Google Patents
一种超疏水棉麻纺织面料的制备方法 Download PDFInfo
- Publication number
- CN112080834A CN112080834A CN202010874025.XA CN202010874025A CN112080834A CN 112080834 A CN112080834 A CN 112080834A CN 202010874025 A CN202010874025 A CN 202010874025A CN 112080834 A CN112080834 A CN 112080834A
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- China
- Prior art keywords
- cotton
- solution
- base cloth
- textile fabric
- soaking
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
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- 239000004744 fabric Substances 0.000 title claims abstract description 150
- 239000004753 textile Substances 0.000 title claims abstract description 66
- 230000003075 superhydrophobic effect Effects 0.000 title claims abstract description 19
- 238000002360 preparation method Methods 0.000 title claims abstract description 13
- 229920000742 Cotton Polymers 0.000 claims abstract description 63
- 238000002791 soaking Methods 0.000 claims abstract description 38
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 23
- 238000001035 drying Methods 0.000 claims abstract description 20
- 238000000034 method Methods 0.000 claims abstract description 20
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 claims abstract description 15
- 239000000835 fiber Substances 0.000 claims abstract description 10
- 239000007864 aqueous solution Substances 0.000 claims abstract description 9
- 238000005406 washing Methods 0.000 claims abstract description 9
- 244000025254 Cannabis sativa Species 0.000 claims abstract description 5
- 235000012766 Cannabis sativa ssp. sativa var. sativa Nutrition 0.000 claims abstract description 5
- 235000012765 Cannabis sativa ssp. sativa var. spontanea Nutrition 0.000 claims abstract description 5
- 235000004431 Linum usitatissimum Nutrition 0.000 claims abstract description 5
- 235000009120 camo Nutrition 0.000 claims abstract description 5
- 235000005607 chanvre indien Nutrition 0.000 claims abstract description 5
- 239000011487 hemp Substances 0.000 claims abstract description 5
- 239000000243 solution Substances 0.000 claims description 64
- 230000001153 anti-wrinkle effect Effects 0.000 claims description 34
- 230000000844 anti-bacterial effect Effects 0.000 claims description 28
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 14
- ADCOVFLJGNWWNZ-UHFFFAOYSA-N antimony trioxide Chemical compound O=[Sb]O[Sb]=O ADCOVFLJGNWWNZ-UHFFFAOYSA-N 0.000 claims description 14
- 239000003795 chemical substances by application Substances 0.000 claims description 14
- 230000000149 penetrating effect Effects 0.000 claims description 14
- 239000003054 catalyst Substances 0.000 claims description 13
- 238000010438 heat treatment Methods 0.000 claims description 13
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 claims description 12
- JQWHASGSAFIOCM-UHFFFAOYSA-M sodium periodate Chemical compound [Na+].[O-]I(=O)(=O)=O JQWHASGSAFIOCM-UHFFFAOYSA-M 0.000 claims description 12
- 238000003756 stirring Methods 0.000 claims description 12
- 230000002209 hydrophobic effect Effects 0.000 claims description 10
- 239000002994 raw material Substances 0.000 claims description 9
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 8
- 238000002156 mixing Methods 0.000 claims description 8
- 238000005096 rolling process Methods 0.000 claims description 8
- BJEPYKJPYRNKOW-REOHCLBHSA-N (S)-malic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O BJEPYKJPYRNKOW-REOHCLBHSA-N 0.000 claims description 7
- RSWGJHLUYNHPMX-UHFFFAOYSA-N Abietic-Saeure Natural products C12CCC(C(C)C)=CC2=CCC2C1(C)CCCC2(C)C(O)=O RSWGJHLUYNHPMX-UHFFFAOYSA-N 0.000 claims description 7
- FEWJPZIEWOKRBE-JCYAYHJZSA-N Dextrotartaric acid Chemical compound OC(=O)[C@H](O)[C@@H](O)C(O)=O FEWJPZIEWOKRBE-JCYAYHJZSA-N 0.000 claims description 7
- 108010022355 Fibroins Proteins 0.000 claims description 7
- KHPCPRHQVVSZAH-HUOMCSJISA-N Rosin Natural products O(C/C=C/c1ccccc1)[C@H]1[C@H](O)[C@@H](O)[C@@H](O)[C@@H](CO)O1 KHPCPRHQVVSZAH-HUOMCSJISA-N 0.000 claims description 7
- FEWJPZIEWOKRBE-UHFFFAOYSA-N Tartaric acid Natural products [H+].[H+].[O-]C(=O)C(O)C(O)C([O-])=O FEWJPZIEWOKRBE-UHFFFAOYSA-N 0.000 claims description 7
- 244000269722 Thea sinensis Species 0.000 claims description 7
- BJEPYKJPYRNKOW-UHFFFAOYSA-N alpha-hydroxysuccinic acid Natural products OC(=O)C(O)CC(O)=O BJEPYKJPYRNKOW-UHFFFAOYSA-N 0.000 claims description 7
- 239000008367 deionised water Substances 0.000 claims description 7
- 229910021641 deionized water Inorganic materials 0.000 claims description 7
- 235000011187 glycerol Nutrition 0.000 claims description 7
- 239000001630 malic acid Substances 0.000 claims description 7
- 235000011090 malic acid Nutrition 0.000 claims description 7
- 229920001444 polymaleic acid Polymers 0.000 claims description 7
- 150000008442 polyphenolic compounds Chemical class 0.000 claims description 7
- 235000013824 polyphenols Nutrition 0.000 claims description 7
- 239000003223 protective agent Substances 0.000 claims description 7
- 239000011347 resin Substances 0.000 claims description 7
- 229920005989 resin Polymers 0.000 claims description 7
- 239000011975 tartaric acid Substances 0.000 claims description 7
- 235000002906 tartaric acid Nutrition 0.000 claims description 7
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N titanium dioxide Inorganic materials O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 claims description 7
- KHPCPRHQVVSZAH-UHFFFAOYSA-N trans-cinnamyl beta-D-glucopyranoside Natural products OC1C(O)C(O)C(CO)OC1OCC=CC1=CC=CC=C1 KHPCPRHQVVSZAH-UHFFFAOYSA-N 0.000 claims description 7
- 229920001661 Chitosan Polymers 0.000 claims description 6
- 239000006087 Silane Coupling Agent Substances 0.000 claims description 6
- 125000002057 carboxymethyl group Chemical group [H]OC(=O)C([H])([H])[*] 0.000 claims description 6
- 229910052681 coesite Inorganic materials 0.000 claims description 6
- 229910052906 cristobalite Inorganic materials 0.000 claims description 6
- 239000011859 microparticle Substances 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 239000000377 silicon dioxide Substances 0.000 claims description 6
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N silicon dioxide Inorganic materials O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 claims description 6
- 229910052682 stishovite Inorganic materials 0.000 claims description 6
- 229910052905 tridymite Inorganic materials 0.000 claims description 6
- GNFTZDOKVXKIBK-UHFFFAOYSA-N 3-(2-methoxyethoxy)benzohydrazide Chemical compound COCCOC1=CC=CC(C(=O)NN)=C1 GNFTZDOKVXKIBK-UHFFFAOYSA-N 0.000 claims description 4
- FGUUSXIOTUKUDN-IBGZPJMESA-N C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 Chemical compound C1(=CC=CC=C1)N1C2=C(NC([C@H](C1)NC=1OC(=NN=1)C1=CC=CC=C1)=O)C=CC=C2 FGUUSXIOTUKUDN-IBGZPJMESA-N 0.000 claims description 4
- 238000004140 cleaning Methods 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 238000007493 shaping process Methods 0.000 claims description 4
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 3
- 239000012295 chemical reaction liquid Substances 0.000 claims 2
- 240000006240 Linum usitatissimum Species 0.000 claims 1
- 230000014759 maintenance of location Effects 0.000 abstract description 7
- 241000208202 Linaceae Species 0.000 abstract description 4
- 238000006243 chemical reaction Methods 0.000 description 6
- 230000007547 defect Effects 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 description 3
- 230000037303 wrinkles Effects 0.000 description 3
- 235000013305 food Nutrition 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 208000034656 Contusions Diseases 0.000 description 1
- 239000000987 azo dye Substances 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000009519 contusion Effects 0.000 description 1
- 239000000975 dye Substances 0.000 description 1
- -1 formaldehyde and azo Chemical class 0.000 description 1
- 229910001385 heavy metal Inorganic materials 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 230000035699 permeability Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 210000004243 sweat Anatomy 0.000 description 1
- 238000009941 weaving Methods 0.000 description 1
Classifications
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- D—TEXTILES; PAPER
- D03—WEAVING
- D03D—WOVEN FABRICS; METHODS OF WEAVING; LOOMS
- D03D13/00—Woven fabrics characterised by the special disposition of the warp or weft threads, e.g. with curved weft threads, with discontinuous warp threads, with diagonal warp or weft
- D03D13/002—With diagonal warps or wefts
-
- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B15/00—Removing liquids, gases or vapours from textile materials in association with treatment of the materials by liquids, gases or vapours
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- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B21/00—Successive treatments of textile materials by liquids, gases or vapours
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- D—TEXTILES; PAPER
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- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/10—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
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- D—TEXTILES; PAPER
- D06—TREATMENT OF TEXTILES OR THE LIKE; LAUNDERING; FLEXIBLE MATERIALS NOT OTHERWISE PROVIDED FOR
- D06B—TREATING TEXTILE MATERIALS USING LIQUIDS, GASES OR VAPOURS
- D06B3/00—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating
- D06B3/10—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics
- D06B3/18—Passing of textile materials through liquids, gases or vapours to effect treatment, e.g. washing, dyeing, bleaching, sizing, impregnating of fabrics combined with squeezing, e.g. in padding machines
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- D06M—TREATMENT, NOT PROVIDED FOR ELSEWHERE IN CLASS D06, OF FIBRES, THREADS, YARNS, FABRICS, FEATHERS OR FIBROUS GOODS MADE FROM SUCH MATERIALS
- D06M10/00—Physical treatment of fibres, threads, yarns, fabrics, or fibrous goods made from such materials, e.g. ultrasonic, corona discharge, irradiation, electric currents, or magnetic fields; Physical treatment combined with treatment with chemical compounds or elements
- D06M10/001—Treatment with visible light, infrared or ultraviolet, X-rays
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- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/07—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof
- D06M11/30—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with halogens; with halogen acids or salts thereof; with oxides or oxyacids of halogens or salts thereof with oxides of halogens, oxyacids of halogens or their salts, e.g. with perchlorates
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- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
- D06M11/32—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond
- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/44—Oxides or hydroxides of elements of Groups 2 or 12 of the Periodic Table; Zincates; Cadmates
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- D06M11/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising
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- D06M11/46—Oxides or hydroxides of elements of Groups 4 or 14 of the Periodic Table; Titanates; Zirconates; Stannates; Plumbates
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- D06M11/36—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with oxygen, ozone, ozonides, oxides, hydroxides or percompounds; Salts derived from anions with an amphoteric element-oxygen bond with oxides, hydroxides or mixed oxides; with salts derived from anions with an amphoteric element-oxygen bond
- D06M11/47—Oxides or hydroxides of elements of Groups 5 or 15 of the Periodic Table; Vanadates; Niobates; Tantalates; Arsenates; Antimonates; Bismuthates
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- D06M11/51—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof
- D06M11/55—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with sulfur, selenium, tellurium, polonium or compounds thereof with sulfur trioxide; with sulfuric acid or thiosulfuric acid or their salts
- D06M11/56—Sulfates or thiosulfates other than of elements of Groups 3 or 13 of the Periodic Table
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- D06M11/77—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof
- D06M11/79—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with inorganic substances or complexes thereof; Such treatment combined with mechanical treatment, e.g. mercerising with silicon or compounds thereof with silicon dioxide, silicic acids or their salts
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- D06M13/00—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment
- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/192—Polycarboxylic acids; Anhydrides, halides or salts thereof
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- D06M13/184—Carboxylic acids; Anhydrides, halides or salts thereof
- D06M13/207—Substituted carboxylic acids, e.g. by hydroxy or keto groups; Anhydrides, halides or salts thereof
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- D06M13/10—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with compounds containing oxygen
- D06M13/224—Esters of carboxylic acids; Esters of carbonic acid
- D06M13/238—Tannins, e.g. gallotannic acids
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- D06M13/50—Treating fibres, threads, yarns, fabrics or fibrous goods made from such materials, with non-macromolecular organic compounds; Such treatment combined with mechanical treatment with organometallic compounds; with organic compounds containing boron, silicon, selenium or tellurium atoms
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- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
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- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
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- D06M15/01—Treating fibres, threads, yarns, fabrics, or fibrous goods made from such materials, with macromolecular compounds; Such treatment combined with mechanical treatment with natural macromolecular compounds or derivatives thereof
- D06M15/17—Natural resins, resinous alcohols, resinous acids, or derivatives thereof
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- D06M2101/04—Vegetal fibres
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Abstract
本发明公开了一种超疏水棉麻纺织面料的制备方法，制备步骤如下：a.首先将天然棉纤维和汉麻纤维经加捻工艺制作成经丝，接着将棉纤维和亚麻纤维经加捻工艺制作成纬丝，并在喷气织机上采用经纬交织的斜纹组织法织造成基布；b.待步骤a完成后，再将织造好的基布在质量分数为13％的NaOH水溶液中浸泡7‑14min，待捞出后用清水洗涤数次后甩干；c.待步骤b完成后。本发明具有多孔性、保湿性和弹性高等优点，棉麻纺织面料之间能积存较多的空气，如果棉麻纺织面料湿度较大，周围温度较高时，棉麻纺织面料中含的多余水分会蒸发散去，会使棉麻纺织面料纺织品保持水平衡状态，提高了棉麻纺织面料穿在身上时的舒适性。
Description
技术领域
本发明涉及棉麻纺织面料技术领域，具体为一种超疏水棉麻纺织面料的制备方法。
背景技术
棉麻纺织面料是由棉和麻交织的布料，具有较多的优点，例如棉麻面料透气性好，身体出汗后，能够及时随着空气散发到面料的外部；质地柔软，冬暖夏凉，舒适性好，适合贴身穿着；抗静电、不起球、不挫起、不卷边，棉麻布是用纯棉缝制，不带自由电荷，棉纤维不易变形，不起球；自然环保，从种植到手织成布，不使用农药和化学染剂，纺织品不含甲醛、偶氮等化学重金属离子，完全符合欧共体纺织品生化标准规定的“禁用致癌-偶氮染料”的要求，真正的绿色生态纺织珍品。
目前，现有的超疏水棉麻纺织面料还存在着一些不足的地方，例如；现有的棉麻纺织面料在湿度较大，周围温度较高时，棉麻纺织面料中含的多余水分不容易蒸发散去，不会使棉麻纺织面料纺织品保持水平衡状态，降低了棉麻纺织面料穿在身上时的舒适性，而且现有的棉麻纺织面料具有经过常规抗皱整理后手感偏硬的缺陷，同时不具有抗皱性和抗菌性能，不适于各种场合穿着。
发明内容
本发明的目的在于提供一种超疏水棉麻纺织面料的制备方法，解决了背景技术中所提出的问题。
为实现上述目的，本发明提供如下技术方案：一种超疏水棉麻纺织面料的制备方法，制备步骤如下：
a.首先将天然棉纤维和汉麻纤维经加捻工艺制作成经丝，接着将棉纤维和亚麻纤维经加捻工艺制作成纬丝，并在喷气织机上采用经纬交织的斜纹组织法织造成基布；
b.待步骤a完成后，再将织造好的基布在质量分数为13％的NaOH水溶液中浸泡7-14min，待捞出后用清水洗涤数次后甩干；
c.待步骤b完成后，再将经步骤b处理后的基布放入到抗菌溶液和抗皱溶液中进行处理；
d.待步骤c完成后，再将处理好的基布放入到疏水溶液中进行处理，在基布处理好后，再放入到紫外线下辐照处理15—25min，然后再室温条件下干燥；
e.待步骤d完成后，再将干燥后的基布在-8—-3℃环境中放3—7min，再在35—45℃环境中放置12—17min，如此高低温交替进行5—7次，再将高低温处理后的基布浸入去离子水清洗5—10min，经干燥、定型得到超疏水棉麻纺织面料。
作为本发明的一种优选实施方式，所述步骤b中待捞出后用清水洗涤数次后甩干，清洗的次数为3—5次，基布甩干采用的是离心脱水机。
作为本发明的一种优选实施方式，所述步骤c中的基布放入到抗菌溶液和抗皱溶液中进行处理，抗菌溶液包括以下原料：茶多酚、苹果酸、酒石酸、三聚马来酸、纳米TiO2、三氧化二锑、渗透剂、丝素和乙醇水溶液，所述抗皱溶液包括以下原料：甘油松香树脂、强力保护剂、催化剂和渗透剂。
作为本发明的一种优选实施方式，所述步骤c中基布放入到抗菌溶液和抗皱溶液中进行处理，处理步骤如下：
f.首先将茶多酚、苹果酸、酒石酸、三聚马来酸、纳米TiO2、三氧化二锑、渗透剂、丝素和乙醇水溶液添加到混合器中混合，制得抗菌溶液，再将甘油松香树脂、强力保护剂、催化剂和渗透剂添加到混合器中混合，制得抗皱溶液；
g.待步骤f完成后，再将甩干后的基布以浸渍浴比1:40进行浸渍，浸渍温度为50-65℃，二浸二轧，每次浸35-60min，轧余率为75-95％，再将浸渍好的基布在80℃的温度下预烘5min；
h.待步骤g完成后，再将预烘后的基布放入到抗皱溶液中浸渍，浸渍温度为45-55℃，二浸二轧，浸渍时间为2-3h；
i.待步骤h完成后，再将处理后的基布送入烘箱，采用90℃进行加热处理，控制基布带液率降至5％-10％。
作为本发明的一种优选实施方式，所述步骤d中疏水溶液包括以下原料：羧甲基壳聚糖、高碘酸钠、盐酸催化剂、SiO2微米颗粒、ZnO微米颗粒、Ti(SO4)2和硅烷偶联剂。
作为本发明的一种优选实施方式，所述步骤d中基布放入到疏水溶液中进行处理步骤如下：先将羧甲基壳聚糖加入80—110mL去离子水中，搅拌溶解，然后加入0.5—0.8g高碘酸钠，升温至55—70℃，搅拌反应1.5—3h，得到反应液，再将基布浸入反应液中，然后加入0.03—0.06mol盐酸催化剂，加热至60—70℃，反应2—4h，中反应完毕后，加入3—5gSiO2微米颗粒和2—3gZnO微米颗粒，在40—45℃的条件下超声搅拌15—30min，升温至45—55℃，加入2—4gTi(SO4)2和0.3—0.5g硅烷偶联剂，超声搅拌15—25min，静置10—15h。
与现有技术相比，本发明的有益效果如下：
本发明具有多孔性、保湿性和弹性高等优点，棉麻纺织面料之间能积存较多的空气，如果棉麻纺织面料湿度较大，周围温度较高时，棉麻纺织面料中含的多余水分会蒸发散去，会使棉麻纺织面料纺织品保持水平衡状态，提高了棉麻纺织面料穿在身上时的舒适性，而且本发明经过抗菌溶液和抗皱溶液处理后的棉麻纺织面料可克服棉麻织物经过常规抗皱整理后手感偏硬的缺陷，同时使棉麻纺织面料具有抗皱性和抗菌性能，适于各种场合穿着。
具体实施方式
本发明实施例中的技术方案进行清楚、完整地描述，显然，所描述的实施例仅仅是本发明一部分实施例，而不是全部的实施例。
本发明提供一种技术方案：一种超疏水棉麻纺织面料的制备方法，制备步骤如下：
a.首先将天然棉纤维和汉麻纤维经加捻工艺制作成经丝，接着将棉纤维和亚麻纤维经加捻工艺制作成纬丝，并在喷气织机上采用经纬交织的斜纹组织法织造成基布；
b.待步骤a完成后，再将织造好的基布在质量分数为13％的NaOH水溶液中浸泡7-14min，待捞出后用清水洗涤数次后甩干；
c.待步骤b完成后，再将经步骤b处理后的基布放入到抗菌溶液和抗皱溶液中进行处理；
d.待步骤c完成后，再将处理好的基布放入到疏水溶液中进行处理，在基布处理好后，再放入到紫外线下辐照处理15—25min，然后再室温条件下干燥；
e.待步骤d完成后，再将干燥后的基布在-8—-3℃环境中放3—7min，再在35—45℃环境中放置12—17min，如此高低温交替进行5—7次，再将高低温处理后的基布浸入去离子水清洗5—10min，经干燥、定型得到超疏水棉麻纺织面料。
进一步，所述步骤b中待捞出后用清水洗涤数次后甩干，清洗的次数为3—5次，基布甩干采用的是离心脱水机。
进一步，所述步骤c中的基布放入到抗菌溶液和抗皱溶液中进行处理，抗菌溶液包括以下原料：茶多酚、苹果酸、酒石酸、三聚马来酸、纳米TiO2、三氧化二锑、渗透剂、丝素和乙醇水溶液，所述抗皱溶液包括以下原料：甘油松香树脂、强力保护剂、催化剂和渗透剂。
进一步，所述步骤c中基布放入到抗菌溶液和抗皱溶液中进行处理，处理步骤如下：
f.首先将茶多酚、苹果酸、酒石酸、三聚马来酸、纳米TiO2、三氧化二锑、渗透剂、丝素和乙醇水溶液添加到混合器中混合，制得抗菌溶液，再将甘油松香树脂、强力保护剂、催化剂和渗透剂添加到混合器中混合，制得抗皱溶液；
g.待步骤f完成后，再将甩干后的基布以浸渍浴比1:40进行浸渍，浸渍温度为50-65℃，二浸二轧，每次浸35-60min，轧余率为75-95％，再将浸渍好的基布在80℃的温度下预烘5min；
h.待步骤g完成后，再将预烘后的基布放入到抗皱溶液中浸渍，浸渍温度为45-55℃，二浸二轧，浸渍时间为2-3h；
i.待步骤h完成后，再将处理后的基布送入烘箱，采用90℃进行加热处理，控制基布带液率降至5％-10％。
进一步，所述步骤d中疏水溶液包括以下原料：羧甲基壳聚糖、高碘酸钠、盐酸催化剂、SiO2微米颗粒、ZnO微米颗粒、Ti(SO4)2和硅烷偶联剂。
进一步，所述步骤d中基布放入到疏水溶液中进行处理步骤如下：先将羧甲基壳聚糖加入80—110mL去离子水中，搅拌溶解，然后加入0.5—0.8g高碘酸钠，升温至55—70℃，搅拌反应1.5—3h，得到反应液，再将基布浸入反应液中，然后加入0.03—0.06mol盐酸催化剂，加热至60—70℃，反应2—4h，中反应完毕后，加入3—5gSiO2微米颗粒和2—3gZnO微米颗粒，在40—45℃的条件下超声搅拌15—30min，升温至45—55℃，加入2—4gTi(SO4)2和0.3—0.5g硅烷偶联剂，超声搅拌15—25min，静置10—15h。
实施例一
一种超疏水棉麻纺织面料的制备方法，制备步骤如下：
a.首先将天然棉纤维和汉麻纤维经加捻工艺制作成经丝，接着将棉纤维和亚麻纤维经加捻工艺制作成纬丝，并在喷气织机上采用经纬交织的斜纹组织法织造成基布；
b.待步骤a完成后，再将织造好的基布在质量分数为13％的NaOH水溶液中浸泡7-14min，待捞出后用清水洗涤数次后甩干；
c.待步骤b完成后，再将经步骤b处理后的基布放入到抗菌溶液和抗皱溶液中进行处理；
d.待步骤c完成后，再将处理好的基布放入到疏水溶液中进行处理，在基布处理好后，再放入到紫外线下辐照处理15—25min，然后再室温条件下干燥；
e.待步骤d完成后，再将干燥后的基布在-8—-3℃环境中放3—7min，再在35—45℃环境中放置12—17min，如此高低温交替进行5—7次，再将高低温处理后的基布浸入去离子水清洗5—10min，经干燥、定型得到超疏水棉麻纺织面料。
综上所述，本发明具有多孔性、保湿性和弹性高等优点，棉麻纺织面料之间能积存较多的空气，如果棉麻纺织面料湿度较大，周围温度较高时，棉麻纺织面料中含的多余水分会蒸发散去，会使棉麻纺织面料纺织品保持水平衡状态，提高了棉麻纺织面料穿在身上时的舒适性。
实施例二
所述步骤c中基布放入到抗菌溶液和抗皱溶液中进行处理，处理步骤如下：
f.首先将茶多酚、苹果酸、酒石酸、三聚马来酸、纳米TiO2、三氧化二锑、渗透剂、丝素和乙醇水溶液添加到混合器中混合，制得抗菌溶液，再将甘油松香树脂、强力保护剂、催化剂和渗透剂添加到混合器中混合，制得抗皱溶液；
g.待步骤f完成后，再将甩干后的基布以浸渍浴比1:40进行浸渍，浸渍温度为50-65℃，二浸二轧，每次浸35-60min，轧余率为75-95％，再将浸渍好的基布在80℃的温度下预烘5min；
h.待步骤g完成后，再将预烘后的基布放入到抗皱溶液中浸渍，浸渍温度为45-55℃，二浸二轧，浸渍时间为2-3h；
i.待步骤h完成后，再将处理后的基布送入烘箱，采用90℃进行加热处理，控制基布带液率降至5％-10％。
综上所述，本发明经过抗菌溶液和抗皱溶液处理后的棉麻纺织面料可克服棉麻织物经过常规抗皱整理后手感偏硬的缺陷，同时使棉麻纺织面料具有抗皱性和抗菌性能，适于各种场合穿着。
传统棉麻纺织面料数据参数表1如下：
| 测试项目 | 保湿性 | 弹性 | 抗皱性 | 抗菌性 |
| 参数指标 | 较差 | 一般 | 较弱 | 一般 |
实施例一棉麻纺织面料数据参数表2如下：
| 测试项目 | 保湿性 | 弹性 | 抗皱性 | 抗菌性 |
| 参数指标 | 一般 | 良好 | 一般 | 良好 |
实施例二棉麻纺织面料数据参数表3如下：
| 测试项目 | 保湿性 | 弹性 | 抗皱性 | 抗菌性 |
| 参数指标 | 良好 | 优 | 良好 | 优 |
综上述，参照表1、表2和表3的数据对比得到，本发明具有多孔性、保湿性和弹性高等优点，棉麻纺织面料之间能积存较多的空气，如果棉麻纺织面料湿度较大，周围温度较高时，棉麻纺织面料中含的多余水分会蒸发散去，会使棉麻纺织面料纺织品保持水平衡状态，提高了棉麻纺织面料穿在身上时的舒适性，而且本发明经过抗菌溶液和抗皱溶液处理后的棉麻纺织面料可克服棉麻织物经过常规抗皱整理后手感偏硬的缺陷，同时使棉麻纺织面料具有抗皱性和抗菌性能，适于各种场合穿着。
以上显示和描述了本发明的基本原理和主要特征和本发明的优点，对于本领域技术人员而言，显然本发明不限于上述示范性实施例的细节，而且在不背离本发明的精神或基本特征的情况下，能够以其他的具体形式实现本发明。因此，无论从哪一点来看，均应将实施例看作是示范性的，而且是非限制性的，本发明的范围由所附权利要求而不是上述说明限定，因此旨在将落在权利要求的等同要件的含义和范围内的所有变化囊括在本发明内。
此外，应当理解，虽然本说明书按照实施方式加以描述，但并非每个实施方式仅包含一个独立的技术方案，说明书的这种叙述方式仅仅是为清楚起见，本领域技术人员应当将说明书作为一个整体，各实施例中的技术方案也可以经适当组合，形成本领域技术人员可以理解的其他实施方式。
Claims (6)
1.一种超疏水棉麻纺织面料的制备方法，其特征在于：制备步骤如下：
a.首先将天然棉纤维和汉麻纤维经加捻工艺制作成经丝，接着将棉纤维和亚麻纤维经加捻工艺制作成纬丝，并在喷气织机上采用经纬交织的斜纹组织法织造成基布；
b.待步骤a完成后，再将织造好的基布在质量分数为13％的NaOH水溶液中浸泡7-14min，待捞出后用清水洗涤数次后甩干；
c.待步骤b完成后，再将经步骤b处理后的基布放入到抗菌溶液和抗皱溶液中进行处理；
d.待步骤c完成后，再将处理好的基布放入到疏水溶液中进行处理，在基布处理好后，再放入到紫外线下辐照处理15—25min，然后再室温条件下干燥；
e.待步骤d完成后，再将干燥后的基布在-8—-3℃环境中放3—7min，再在35—45℃环境中放置12—17min，如此高低温交替进行5—7次，再将高低温处理后的基布浸入去离子水清洗5—10min，经干燥、定型得到超疏水棉麻纺织面料。
2.根据权利要求1所述的一种超疏水棉麻纺织面料的制备方法，其特征在于：所述步骤b中待捞出后用清水洗涤数次后甩干，清洗的次数为3—5次，基布甩干采用的是离心脱水机。
3.根据权利要求1所述的一种超疏水棉麻纺织面料的制备方法，其特征在于：所述步骤c中的基布放入到抗菌溶液和抗皱溶液中进行处理，抗菌溶液包括以下原料：茶多酚、苹果酸、酒石酸、三聚马来酸、纳米TiO2、三氧化二锑、渗透剂、丝素和乙醇水溶液，所述抗皱溶液包括以下原料：甘油松香树脂、强力保护剂、催化剂和渗透剂。
4.根据权利要求1所述的一种超疏水棉麻纺织面料的制备方法，其特征在于：所述步骤c中基布放入到抗菌溶液和抗皱溶液中进行处理，处理步骤如下：
f.首先将茶多酚、苹果酸、酒石酸、三聚马来酸、纳米TiO2、三氧化二锑、渗透剂、丝素和乙醇水溶液添加到混合器中混合，制得抗菌溶液，再将甘油松香树脂、强力保护剂、催化剂和渗透剂添加到混合器中混合，制得抗皱溶液；
g.待步骤f完成后，再将甩干后的基布以浸渍浴比1:40进行浸渍，浸渍温度为50-65℃，二浸二轧，每次浸35-60min，轧余率为75-95％，再将浸渍好的基布在80℃的温度下预烘5min；
h.待步骤g完成后，再将预烘后的基布放入到抗皱溶液中浸渍，浸渍温度为45-55℃，二浸二轧，浸渍时间为2-3h；
i.待步骤h完成后，再将处理后的基布送入烘箱，采用90℃进行加热处理，控制基布带液率降至5％-10％。
5.根据权利要求1所述的一种超疏水棉麻纺织面料的制备方法，其特征在于：所述步骤d中疏水溶液包括以下原料：羧甲基壳聚糖、高碘酸钠、盐酸催化剂、SiO2微米颗粒、ZnO微米颗粒、Ti(SO4)2和硅烷偶联剂。
6.根据权利要求1所述的一种超疏水棉麻纺织面料的制备方法，其特征在于：所述步骤d中基布放入到疏水溶液中进行处理步骤如下：先将羧甲基壳聚糖加入80—110mL去离子水中，搅拌溶解，然后加入0.5—0.8g高碘酸钠，升温至55—70℃，搅拌反应1.5—3h，得到反应液，再将基布浸入反应液中，然后加入0.03—0.06mol盐酸催化剂，加热至60—70℃，反应2—4h，中反应完毕后，加入3—5gSiO2微米颗粒和2—3gZnO微米颗粒，在40—45℃的条件下超声搅拌15—30min，升温至45—55℃，加入2—4gTi(SO4)2和0.3—0.5g硅烷偶联剂，超声搅拌15—25min，静置10—15h。
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