CN110742831B - Brightening eye brightening and night-out eye mask essence and preparation method thereof - Google Patents
Brightening eye brightening and night-out eye mask essence and preparation method thereof Download PDFInfo
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Abstract
The invention relates to the technical field of eye masks, and particularly relates to bright eye brightening and night-out eye mask essence and a preparation method thereof. The eye mask essence comprises the following raw materials: deionized water; group A: 1, 3-propylene glycol, allantoin, trehalose, acetyl chitosamine, sclerotium rolfsii gum, EDTA disodium; group B: butanediol, hydrolyzed sodium hyaluronate; group C: niacinamide, magnesium ascorbyl phosphate; group D: olive fruit oil, solubilizer; group E: palmitoyl hexapeptide compound conditioner, acetyl tetrapeptide compound conditioner, carnosine compound conditioner, gentiana lutea root extract conditioner, dogwood fruit extract conditioner, yeast lysate extract conditioner, centella asiatica conditioner, chlorella vulgaris extract conditioner, glyceryl caprylate compound humectant and ethylhexyl glycerin compound humectant. The eye mask essence is prepared by gradient stirring and cooling, so that the raw materials are fully mixed, the biological activity of the raw materials is ensured, and the aging of skin around eyes can be effectively slowed down.
Description
Technical Field
The invention relates to the technical field of eye masks, and particularly relates to bright eye brightening and night-out eye mask essence and a preparation method thereof.
Background
The eye mask is a beauty and skin care product for applying on eyes, is a first-aid wonderful prescription for eye skin problems, and can replenish moisture, eliminate fatigue and quickly reduce edema and eye dark circles in a short time.
The existing eye mask essence for removing eye puffiness, dark eye circles and edema has various types. The Chinese patent with publication number CN102860961B discloses an eye mask essence applying peony root extract and a preparation method thereof, wherein the essence comprises moisture-retaining components: water, 1, 3-butanediol, glycerol, betaine, a thickening stabilizing component and an anti-allergy component: allantoin and dipotassium glycyrrhizinate, and the effective active components are as follows: sodium hyaluronate, oat glucan, witch hazel extract and peony root extract, a neutralizing component and a preserving component. The essence can relieve eye fatigue, and has obvious effects of promoting blood circulation for removing blood stasis, diminishing inflammation, calming, fading dark eye circles, eliminating edema and eye bags and supplementing water.
However, for people staying up for a long time, the product can only temporarily relieve eye fatigue of people using the product, and has small effect on delaying skin aging around eyes. Therefore, the research and development of a novel eye mask essence for staying up at night to achieve the purposes of brightening eyes and slowing down skin aging around eyes are the technical problems which need to be solved urgently at present.
Disclosure of Invention
Aiming at the defects in the prior art, the first purpose of the invention is to provide a bright eye brightening and night-out eye mask essence which can moisten eyes, improve eye wrinkles, delicately repair and brighten skin around the eyes, and has the effects of brightening eyes and slowing down aging of skin around the eyes.
The second purpose of the invention is to provide a preparation method of the bright eye brightening and night-out eye mask essence, which has the advantages of simple process and convenience in operation, ensures the biological activity of raw materials, and enables the essence to effectively slow down the aging of skin around eyes.
In order to achieve the first object, the invention provides the following technical scheme:
the brightening eye mask essence capable of staying up at night is composed of the following raw materials in parts by weight:
40.00-85.00 parts of deionized water;
group A: 1.00-6.00 parts of 1, 3-propylene glycol, 0.02-0.50 part of allantoin, 0.10-4.00 parts of trehalose, 0.10-2.00 parts of acetyl chitosamine, 0.02-0.50 part of sclerotium rolfsii gum and 0.02-0.06 part of EDTA disodium;
group B: 1.00-12.00 parts of butanediol and 0.01-0.40 part of hydrolyzed sodium hyaluronate;
group C: 0.30-5.00 parts of nicotinamide and 0.02-3.00 parts of magnesium ascorbyl phosphate;
group D: 0.10-5.00 parts of olive fruit oil and 0.10-0.50 part of solubilizer;
group E: 0.30-4.00 parts of palmitoyl hexapeptide compound conditioner, 0.10-4.00 parts of acetyl tetrapeptide compound conditioner, 0.10-4.00 parts of carnosine compound conditioner, 0.05-3.00 parts of Gentiana lutea root extract conditioner, 0.05-3.00 parts of dogwood fruit extract conditioner, 0.01-3.00 parts of yeast lysate extract conditioner, 0.01-0.40 parts of centella asiatica conditioner, 0.03-3.00 parts of chlorella vulgaris extract conditioner, 0.50-1.50 parts of glycerol caprylate compound humectant and 0.01-0.20 parts of ethylhexylglycerol compound humectant.
By adopting the technical scheme, in the eye membrane fine whitening, the palmitoyl hexapeptide compound conditioner, the acetyl tetrapeptide compound conditioner and the carnosine compound conditioner in the group D are used in a compound way, wherein the small molecular polypeptide can repair cells at multiple angles, the yeast lysate extract conditioner provides cell respiration energy, and the nicotinamide is used for assisting in the permeation of whitening channels, the gentiana lutea root extract conditioner and the dogwood fruit extract conditioner enhance the adaptability of weak cell self barriers, so that the eye skin can be refreshed.
On the basis, the conditioner of the centella is added, and the strong repairing force and the cell protection mechanism of the conditioner are utilized to enhance the plasticity of cells and the elasticity and extensibility of cell walls, so that the aging of skin around eyes is effectively delayed. In addition, amino acids such as lysine, proline, glycine, alanine and the like contained in the chlorella extract are basic components of the constructed protein and form independent collagen units, so that the chlorella extract is helpful for increasing collagen of skin around eyes and effectively reducing eye marks around the eyes.
On the basis, 1, 3-propylene glycol, trehalose, butanediol, hydrolyzed sodium hyaluronate, glyceryl caprylate compound humectant and ethylhexylglycerin compound humectant are added to improve the moisturizing effect of the eye mask essence. Olive oil is used as an emollient, and can be uniformly dispersed in deionized water in combination with a solubilizer; and allantoin, acetyl chitosamine and sclerotium rolfsii gel are matched to keep the skin moisture, moist and soft, promote the tissue growth and cell metabolism and soften the stratum corneum protein, thereby delaying the skin aging around the eyes. In addition, allantoin can be chelated with EDTA disodium to form double salt, so that the eye mask essence has the effects of shading, sterilization, antisepsis, pain relief and oxidation resistance.
The raw materials supplement each other to form a complete composition, so that the raw materials can fully exert the functions of the composition, and further achieve the purposes of moistening eyes, improving eye wrinkles, delicately repairing and brightening the skin around the eyes, and the effects of brightening eyes and slowing down the aging of the skin around the eyes are achieved.
Further, the weight ratio of the palmitoyl hexapeptide compound conditioner to the acetyl tetrapeptide compound conditioner to the carnosine compound conditioner is 1:1: 1.
By adopting the technical scheme, a large number of experiments prove that when the weight ratio of the palmitoyl hexapeptide compound conditioner to the acetyl tetrapeptide compound conditioner to the carnosine compound conditioner is 1:1:1, the prepared eye mask essence has a particularly remarkable effect of slowing down skin aging around eyes, so that the eye mask essence is preferred.
Further, the palmitoyl hexapeptide compound conditioner consists of the following raw materials in parts by weight: 20.00-25.00 parts of glycerol polymethacrylate, 874.50-79.90 parts of polyethylene glycol-120.10-0.50 part of palmitoyl hexapeptide.
By adopting the technical scheme, the palmitoyl hexapeptide-12 has similar substances capable of inhibiting nerve conduction, blocks the conduction function between neuromuscular, avoids over-contraction of muscle, can prevent fine lines from forming, further slows down the force of muscle contraction, relaxes muscle, reduces the occurrence of dynamic lines and eliminates fine lines. In addition, it can effectively reorganize collagen elasticity, increase elastin activity, relax facial lines, smooth wrinkles and improve laxity. The glycerol polymethacrylate and the polyethylene glycol-8 are prepared according to the weight parts, so that the biological activity of the palmitoyl hexapeptide-12 is ensured, and the effective function of the palmitoyl hexapeptide-12 is further facilitated.
Further, the acetyl tetrapeptide compound conditioner is prepared from the following raw materials in parts by weight: 77.80 parts of deionized water, 2.00 parts of 1, 2-hexanediol, 20.00 parts of glycerol, 0.10 part of ethylhexyl glycerol and 50.10 parts of acetyl tetrapeptide.
By adopting the technical scheme, the acetyl tetrapeptide-5 can improve the microcirculation of eye lymph and capillary vessels, eliminate edema, relieve dark circles and improve the elasticity and smoothness of skin. Meanwhile, acetyl tetrapeptide-5 has the function of inhibiting collagen glycosylation and can prevent collagen from aging and aggregating, thereby further achieving the effects of relieving pouch and resisting wrinkles. Deionized water, 1, 2-hexanediol, glycerol and ethylhexylglycerol as a compatibilizer contributed to the biological activity of acetyl tetrapeptide-5.
Further, the carnosine compound conditioner consists of the following raw materials in parts by weight: 33.80-45.60 parts of deionized water, 50.00-60.00 parts of glycerol, 0.05-0.20 part of ethylhexyl glycerol, 2.00-4.00 parts of 1, 2-hexanediol, 80.10-0.50 part of acetyl hexapeptide, 40.10-0.50 part of palmitoyl pentapeptide, 10.10-0.50 part of palmitoyl tripeptide and 0.10-0.50 part of carnosine.
By adopting the technical scheme, the acetyl hexapeptide-8 is neurotransmitter inhibitory peptide and has the characteristics of high anti-wrinkle activity and small side effect. Palmitoyl pentapeptide-4 is used as messenger peptide to stimulate the synthesis and development of collagen and elastin in the dermis layer of the skin, so as to achieve the effects of resisting wrinkles and aging and improving the quality of the skin. Palmitoyl tripeptide-1 is a matrikine signal peptide that acts on the dermis to promote the synthesis of extracellular matrix (e.g., collagen types I and III, elastin), structural glycoproteins (e.g., laminin and fibronectin), promote wound healing and tissue remodeling, strengthen the dermis, make the skin thicker and more compact, smooth wrinkles, and provide greater resistance to uv radiation. Carnosine has the functions of buffering, regulating human body functions, scavenging free radicals, resisting oxidation, resisting aging and preventing metabolic disorder, can enhance the Haverek limit of human fibroblasts, and plays roles of promoting bridges and protecting safety as a protective peptide in the whole process.
The acetyl hexapeptide-8, the palmitoyl pentapeptide-4, the palmitoyl tripeptide-1 and the carnosine can generate a synergistic effect, and the biological activity of the palmitoyl pentapeptide-1 and the carnosine can be effectively ensured under the compatibility of deionized water, glycerol, ethylhexyl glycerol and 1, 2-hexanediol, so that the anti-aging effect of eye mask essence is provided.
Further, the weight ratio of the gentiana lutea root extract conditioner to the dogwood fruit extract conditioner is 4: 3.
By adopting the technical scheme, a large number of experiments prove that when the weight ratio of the gentiana lutea root extract conditioner to the dogwood fruit extract conditioner is 4:3, the prepared eye mask essence has a particularly remarkable effect of slowing down skin aging around eyes, and therefore the eye mask essence is preferred.
Further, the gentiana lutea root extract conditioner is prepared from the following raw materials in parts by weight: 74.00 parts of deionized water, 25.00 parts of butanediol and 1.00 part of Gentiana lutea root extract;
the dogwood fruit extract conditioner is prepared from the following raw materials in parts by weight: 74.50 parts of deionized water, 25.00 parts of butanediol and 0.50 part of dogwood fruit extract;
the yeast lysate extract conditioner consists of the following raw materials in parts by weight: 74.00-76.00 parts of deionized water and 24.00-26.00 parts of yeast lysate extract;
the centella conditioner is prepared from the following raw materials in parts by weight: asiaticoside 37.00-43.00 parts, asiatic acid 57.00-63.00 parts;
the chlorella extract conditioner is prepared from the following raw materials in parts by weight: 83.50 parts of deionized water, 6.5 parts of chlorella extract, 2.00 parts of pentanediol, 2.00 parts of 1, 2-hexanediol and 6.00 parts of butanediol;
the glyceryl caprylate compound humectant is prepared from the following raw materials in parts by weight: 15-20 parts of glycerol caprylate, 74.00-81.50 parts of 1, 2-pentanediol and 3.50-6.00 parts of caprylyl hydroximic acid;
the ethylhexyl glycerin compound humectant is prepared from the following raw materials in parts by weight: 20.00 parts of ethylhexyl glycerol and 80.00 parts of octyl glycol.
By adopting the technical scheme, the Gentiana lutea root extract conditioner, the dogwood fruit extract conditioner, the yeast lysate extract conditioner, the centella asiatica conditioner, the chlorella vulgaris extract conditioner, the glyceryl caprylate compound humectant and the ethylhexyl glycerin compound humectant which are prepared according to the weight ratio can effectively increase the effects of eye mask essence on moistening eyes, improving eye marks, delicately repairing and brightening skin around the eyes.
Further, the solubilizer comprises the following raw materials in parts by weight: PPG-268.00-12.00 parts, PEG-4088.00-92.00 parts.
By adopting the technical scheme, the solubilizer prepared from the components according to the proportion can promote the olive fruit oil to be more uniformly dispersed in deionized water to form a stable and transparent solution.
In order to achieve the second object, the invention provides the following technical scheme:
a preparation method of a bright eye brightening and night-out eye mask essence comprises the following steps:
pouring deionized water into a stirring tank, adding the group A raw materials, heating to 78 ℃ while stirring, preserving heat for 40min, and cooling to 50 ℃;
secondly, premixing the raw materials in the group B, putting the premixed raw materials into a stirring tank in the step I, uniformly stirring, adding the raw materials in the group C, and continuously cooling while stirring;
thirdly, when the temperature of the feed liquid obtained in the second step is reduced to below 45 ℃, premixing the group D raw materials and then adding the premixed group D raw materials, stirring uniformly, then adding the group E raw materials, and continuously stirring and reducing the temperature to below 37 ℃ to obtain bright eye brightening eye-staying eye mask essence;
and fourthly, sampling and detecting, and discharging and filling the bright eye brightening and night-out eye mask essence after the physicochemical indexes are qualified.
Through adopting above-mentioned technical scheme, the back is put into the deionized water to group A raw materials of this application, keeps warm for 40min at 78 ℃ to do preliminary sterilization, help the raw materials fast dispersion dissolve simultaneously evenly. Although the higher the temperature is, the better the sterilization effect is, the raw material is decomposed at a high temperature to cause a certain loss, so that it is preferable to control the heating temperature to 78 ℃. The rest active raw materials are added at low temperature, so that better biological activity of the active raw materials is ensured. The whole preparation process adopts gradient stirring for cooling, so that the raw materials are fully mixed, the biological activity of the raw materials is ensured, and the preparation method has the characteristics of simple process and convenience in operation, and is suitable for batch production of eye mask essence.
In conclusion, the invention has the following beneficial effects:
1. the eye mask essence is prepared from various small molecular polypeptides, a yeast lysate extract conditioner, nicotinamide, a gentiana lutea root extract conditioner, a dogwood fruit extract conditioner, a centella asiatica conditioner, a chlorella vulgaris extract and other compatible raw materials, can moisten eyes, improve eye wrinkles, delicately repair and brighten skin around the eyes, and has the effects of brightening eyes and slowing down aging of skin around the eyes;
2. this application adopts gradient formula stirring cooling, has both made the abundant mixing of raw materials, has guaranteed the biological activity of raw materials again, has characteristics that the process is simple, convenient operation, is applicable to the batch production of eye mask essence.
Drawings
Fig. 1 is a process flow diagram for preparing bright eye glow overnight eye mask essence.
Detailed Description
The present invention will be described in further detail with reference to the accompanying drawings.
1. Raw materials
The raw materials except the deionized water are self-made, and the rest are all commercial products.
1, 3-propanediol: purchased from ajinomoto.
Allantoin: ALLENTOIN, purchased from the general medicinal industry.
Trehalose: TREHALOSE 100 available from Nagase Personal Care.
Acetyl chitosamine: NAG, available from Ecosol/Youxol.
SCLEROTIUM rolfsii (scleritium rolfsii) gum: chcogum HG, available from Yizhi of Taiwan, China.
Disodium EDTA: DISSOLVINE NA2, available from Acrossobuel.
Butanediol: purchased from japan consortium.
Hydrolysis of sodium hyaluronate: nano HA, purchased from forrad.
Nicotinamide: niacinamide PC, from Longsha.
Magnesium ascorbyl phosphate: VC magnesium phosphate, available from Uighur.
Olive (OLEA EUROPAEA) fruit oil: EVOIL OLEVE P (Olive oil) available from Service Chemical Inc.
Solubilizer: solubilisant LRI, purchased from shin; the composite material is prepared from the following raw materials in parts by weight: 8.00-12.00 parts of PPG-26 (Butanol polyether-26) and 88.00-92.00 parts of PEG-40 (hydrogenated castor oil-40).
Palmitoyl hexapeptide compound conditioner: cornum 8806, available from platinum rich; the composite material is prepared from the following raw materials in parts by weight: 20.00-25.00 parts of glycerol polymethacrylate, 874.50-79.90 parts of polyethylene glycol-120.10-0.50 part of palmitoyl hexapeptide.
Acetyl tetrapeptide compound conditioner: ZPC Eyepep001 purchased from surge peptide; the composite material is prepared from the following raw materials in parts by weight: 77.80 parts of deionized water, 2.00 parts of 1, 2-hexanediol, 20.00 parts of glycerol, 0.10 part of ethylhexyl glycerol and 50.10 parts of acetyl tetrapeptide.
Carnosine compound conditioner: ZPC Wrinklend036 purchased from surge peptide; the composite material is prepared from the following raw materials in parts by weight: 33.80-45.60 parts of deionized water, 50.00-60.00 parts of glycerol, 0.05-0.20 part of ethylhexyl glycerol, 2.00-4.00 parts of 1, 2-hexanediol, 80.10-0.50 part of acetyl hexapeptide, 40.10-0.50 part of palmitoyl pentapeptide, 10.10-0.50 part of palmitoyl tripeptide and 0.10-0.50 part of carnosine.
Gentiana lutea root extract conditioner: PHYTELENE EG 156 Gentianan, available from Greentech; the composite material is prepared from the following raw materials in parts by weight: 74.00 parts of deionized water, 25.00 parts of butanediol and 1.00 part of gentiana lutea root extract.
Dogwood fruit extract conditioner: EVOIL OLEIVE P available from TEXTRON; the composite material is prepared from the following raw materials in parts by weight: 74.50 parts of deionized water, 25.00 parts of butanediol and 0.50 part of dogwood fruit extract.
Yeast lysate extract conditioner: AC Dermal Respiratory Factor, available from Active Concept; the composite material is prepared from the following raw materials in parts by weight: 74.00-76.00 parts of deionized water and 24.00-26.00 parts of yeast lysate extract.
Centella conditioner: TECA, purchased from seppic, france; the composite material is prepared from the following raw materials in parts by weight: asiaticoside 37.00-43.00 parts, asiatic acid 57.00-63.00 parts.
Chlorella extract conditioner: chloressence SK, available from Taiwan Yi Zhi; the composite material is prepared from the following raw materials in parts by weight: 83.50 parts of deionized water, 6.5 parts of CHLORELLA (Chlorella VULGARIS) extract, 2.00 parts of pentanediol, 2.00 parts of 1, 2-hexanediol and 6.00 parts of butanediol.
The glycerin caprylate compound humectant is as follows: innosei GPC, available from Innovative Chemicals; the composite material is prepared from the following raw materials in parts by weight: 15-20 parts of glycerol caprylate, 74.00-81.50 parts of 1, 2-pentanediol and 3.50-6.00 parts of caprylyl hydroximic acid.
And (3) the ethylhexyl glycerin compound humectant: SENSIVA SC 10, available from sumei, germany; the composite material is prepared from the following raw materials in parts by weight: 20.00 parts of ethylhexyl glycerol and 80.00 parts of octyl glycol.
The above raw materials are preferred.
2. Examples of the embodiments
2.1, example 1
The brightening eye mask essence capable of staying up at night is composed of the following raw materials in parts by weight:
75.00kg of deionized water;
group A: 2.00kg of 1, 3-propylene glycol, 0.10kg of allantoin, 0.10kg of trehalose, 0.50kg of acetyl chitosamine, 0.15kg of sclerotium rolfsii gel and 0.05kg of EDTA disodium;
group B: 8.00kg of butanediol and 0.10kg of hydrolyzed sodium hyaluronate;
group C: 2.00kg of nicotinamide and 0.50kg of magnesium ascorbyl phosphate;
group D: 0.20kg of olive fruit oil and 0.80kg of solubilizer;
group E: 0.50kg of palmitoyl hexapeptide compound conditioner, 0.50kg of acetyl tetrapeptide compound conditioner, 0.50kg of carnosine compound conditioner, 2.00kg of Gentiana lutea root extract conditioner, 1.50kg of dogwood fruit extract conditioner, 0.50kg of yeast lysate extract conditioner, 0.15kg of centella asiatica conditioner, 1.00kg of chlorella vulgaris extract conditioner, 0.90kg of glyceryl caprylate compound humectant and 0.05kg of ethylhexyl glycerin compound humectant.
The preparation method of the bright eye brightening overnight eye mask essence is shown in fig. 1, and comprises the following steps:
pouring deionized water into a stirring tank, adding the group A raw materials, controlling the stirring speed to be 300r/min, heating to 78 ℃ while stirring, preserving heat for 40min, and then cooling to 50 ℃;
secondly, premixing the raw materials of the group B, putting the premixed raw materials into a stirring tank in the step I, stirring for 1h until the mixture is uniformly stirred, adding the raw materials of the group C, and continuously cooling while stirring;
thirdly, when the temperature of the feed liquid obtained in the second step is reduced to below 45 ℃, premixing the group D raw materials and then adding the premixed group D raw materials, stirring uniformly, then adding the group E raw materials, and continuously stirring and reducing the temperature to below 37 ℃ to obtain bright eye brightening eye-staying eye mask essence;
and fourthly, sampling and detecting, and discharging and filling the bright eye brightening and night-out eye mask essence after the physicochemical indexes are qualified.
2.2, examples 2 to 5
Examples 2-5 the amounts of the starting materials were adjusted on the basis of the process of example 1, in kg, as shown in table one below.
Table raw material parameters of the eye mask essence of examples 1 to 5
3. Comparative example
3.1, comparative example 1
Comparative example 1 the feed for group E was modified based on the procedure of example 1. Wherein, palmitoyl hexapeptide-120.50 parts, acetyl tetrapeptide-50.50 parts, carnosine 0.50 parts, gentiana lutea root extract 2.00 parts, dogwood fruit extract 1.50 parts, yeast lysate extract 0.50 parts, asiaticoside and asiatic acid mixture 0.15 parts, chlorella extract 1.00 parts, glyceryl caprylate 0.90 parts and ethyl hexyl glycerol 0.05 parts.
3.2, comparative example 2
Comparative example 2 no palmitoyl hexapeptide built conditioner was added based on the method of example 1.
3.3, comparative example 3
Comparative example 3 based on the method of example 1, no acetyl tetrapeptide built conditioner was added.
3.4, comparative example 4
Comparative example 4 based on the method of example 1, no carnosine complex conditioner was added.
3.5, comparative example 5
Comparative example 5 no conditioner of gentiana lutea root extract and no conditioner of dogwood fruit extract were added on the basis of the method of example 1.
3.6, comparative example 6
Comparative example 6 no yeast lysate extract conditioner was added based on the method of example 1.
3.7, comparative example 7
Comparative example 7 no conditioner of centella asiatica and no conditioner of extract of centella asiatica were added on the basis of the method of example 1.
4. Performance testing
600 volunteers staying overnight, aged 20-40 years, were selected and divided into 12 groups of 50 persons each, and 12 groups of volunteers were subjected to the periocular skin improvement test for 6 months for examples 1-5 and comparative examples 1-7, respectively.
The survey was recorded in the following scoring manner: score 0 indicates no significant improvement; score 1 indicates that eye fatigue can be relieved, but the skin around the eyes is not obviously changed; score 2 indicates that eye fatigue can be relieved, and the skin around the eyes is slightly improved; and 3 points show that the eye fatigue can be effectively relieved, the eye skin has obvious hair-changing activity, and the eye wrinkles are obviously reduced.
The specific detection results are shown in the following table II:
TABLE II eye mask essence test results of examples 1 to 5 and comparative examples 1 to 7
Referring to the table above, the effect of the eye mask essences of examples 1 to 5 on improving the skin around the eyes is obvious because of the comparative examples 1 to 7, and thus, the raw materials of the present application supplement each other to form a complete composition, so that each raw material can fully exert its effect, and further, the purposes of moistening the eyes, improving the wrinkles, delicately repairing and brightening the skin around the eyes are achieved, and the effects of brightening the eyes and slowing down the aging of the skin around the eyes are achieved.
Comparing the detection results of the embodiment 1 and the embodiment 4, it can be obtained that when the weight ratio of the palmitoyl hexapeptide compound conditioner, the acetyl tetrapeptide compound conditioner and the carnosine compound conditioner is 1:1:1, the prepared eye mask essence has a particularly prominent effect of slowing down the skin aging around the eyes, and therefore, the eye mask essence is preferred.
Comparing the test results of example 1 and example 5, it can be seen that when the weight ratio of the gentiana lutea root extract conditioner to the dogwood fruit extract conditioner is 4:3, the prepared eye mask essence has a particularly prominent effect of slowing down the aging of skin around eyes, and thus is preferred.
The present embodiment is only for explaining the present invention, and it is not limited to the present invention, and those skilled in the art can make modifications of the present embodiment without inventive contribution as needed after reading the present specification, but all of them are protected by patent law within the scope of the claims of the present invention.
Claims (9)
1. The brightening eye mask essence capable of staying up at night is characterized by comprising the following raw materials in parts by weight:
40.00-85.00 parts of deionized water;
group A: 1.00-6.00 parts of 1, 3-propylene glycol, 0.02-0.50 part of allantoin, 0.10-4.00 parts of trehalose, 0.10-2.00 parts of acetyl chitosamine, 0.02-0.50 part of sclerotium rolfsii gum and 0.02-0.06 part of EDTA disodium;
group B: 1.00-12.00 parts of butanediol and 0.01-0.40 part of hydrolyzed sodium hyaluronate;
group C: 0.30-5.00 parts of nicotinamide and 0.02-3.00 parts of magnesium ascorbyl phosphate;
group D: 0.10-5.00 parts of olive fruit oil and 0.10-0.50 part of solubilizer;
group E: 0.30-4.00 parts of palmitoyl hexapeptide compound conditioner, 0.10-4.00 parts of acetyl tetrapeptide compound conditioner, 0.10-4.00 parts of carnosine compound conditioner, 0.05-3.00 parts of Gentiana lutea root extract conditioner, 0.05-3.00 parts of dogwood fruit extract conditioner, 0.01-3.00 parts of yeast lysate extract conditioner, 0.01-0.40 parts of centella asiatica conditioner, 0.03-3.00 parts of chlorella vulgaris extract conditioner, 0.50-1.50 parts of glycerol caprylate compound humectant and 0.01-0.20 parts of ethylhexylglycerol compound humectant.
2. The bright eye glow overnight eye mask essence according to claim 1, wherein the weight ratio of the palmitoyl hexapeptide compound conditioner, the acetyl tetrapeptide compound conditioner and the carnosine compound conditioner is 1:1: 1.
3. The bright eye glow overnight eye mask essence according to claim 1, characterized in that the palmitoyl hexapeptide compound conditioner consists of the following raw materials in parts by weight: 20.00-25.00 parts of glycerol polymethacrylate, 874.50-79.90 parts of polyethylene glycol-120.10-0.50 part of palmitoyl hexapeptide.
4. The bright eye brightening and night-out eye mask essence according to claim 1, characterized in that the acetyl tetrapeptide compound conditioner consists of the following raw materials in parts by weight: 77.80 parts of deionized water, 2.00 parts of 1, 2-hexanediol, 20.00 parts of glycerol, 0.10 part of ethylhexyl glycerol and 50.10 parts of acetyl tetrapeptide.
5. The bright eye brightening and night-out eye mask essence according to claim 1, characterized in that the carnosine compound conditioner consists of the following raw materials in parts by weight: 33.80-45.60 parts of deionized water, 50.00-60.00 parts of glycerol, 0.05-0.20 part of ethylhexyl glycerol, 2.00-4.00 parts of 1, 2-hexanediol, 80.10-0.50 part of acetyl hexapeptide, 40.10-0.50 part of palmitoyl pentapeptide, 10.10-0.50 part of palmitoyl tripeptide and 0.10-0.50 part of carnosine.
6. The bright eye glow overnight eye mask essence according to claim 1, wherein the weight ratio of gentiana lutea root extract conditioner to dogwood fruit extract conditioner is 4: 3.
7. The bright eye brightening overnight eye mask essence according to claim 1, characterized in that the gentiana lutea root extract conditioner consists of the following raw materials in parts by weight: 74.00 parts of deionized water, 25.00 parts of butanediol and 1.00 part of Gentiana lutea root extract; the dogwood fruit extract conditioner is prepared from the following raw materials in parts by weight: 74.50 parts of deionized water, 25.00 parts of butanediol and 0.50 part of dogwood fruit extract; the yeast lysate extract conditioner consists of the following raw materials in parts by weight: 74.00-76.00 parts of deionized water and 24.00-26.00 parts of yeast lysate extract; the centella conditioner is prepared from the following raw materials in parts by weight: asiaticoside 37.00-43.00 parts, asiatic acid 57.00-63.00 parts; the chlorella extract conditioner is prepared from the following raw materials in parts by weight: 83.50 parts of deionized water, 6.5 parts of chlorella extract, 2.00 parts of pentanediol, 2.00 parts of 1, 2-hexanediol and 6.00 parts of butanediol; the glyceryl caprylate compound humectant is prepared from the following raw materials in parts by weight: 15-20 parts of glycerol caprylate, 74.00-81.50 parts of 1, 2-pentanediol and 3.50-6.00 parts of caprylyl hydroximic acid; the ethylhexyl glycerin compound humectant is prepared from the following raw materials in parts by weight: 20.00 parts of ethylhexyl glycerol and 80.00 parts of octyl glycol.
8. The bright eye brightening overnight eye mask essence according to claim 1, characterized in that the solubilizer consists of the following raw materials in parts by weight: PPG-268.00-12.00 parts, PEG-4088.00-92.00 parts.
9. Method for the preparation of a bright eye glow overnight eye mask essence according to any of claims 1 to 8, characterized in that it comprises the following steps:
pouring deionized water into a stirring tank, adding the group A raw materials, heating to 78 ℃ while stirring, preserving heat for 40min, and cooling to 50 ℃;
secondly, premixing the raw materials in the group B, putting the premixed raw materials into a stirring tank in the step I, uniformly stirring, adding the raw materials in the group C, and continuously cooling while stirring;
thirdly, when the temperature of the feed liquid obtained in the second step is reduced to below 45 ℃, premixing the group D raw materials and then adding the premixed group D raw materials, stirring uniformly, then adding the group E raw materials, and continuously stirring and reducing the temperature to below 37 ℃ to obtain bright eye brightening eye-staying eye mask essence;
and fourthly, sampling and detecting, and discharging and filling the bright eye brightening and night-out eye mask essence after the physicochemical indexes are qualified.
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