CN110042503A - 一种MoSe2@C电纺中空纳米纤维及其制备方法和应用 - Google Patents
一种MoSe2@C电纺中空纳米纤维及其制备方法和应用 Download PDFInfo
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- CN110042503A CN110042503A CN201910378336.4A CN201910378336A CN110042503A CN 110042503 A CN110042503 A CN 110042503A CN 201910378336 A CN201910378336 A CN 201910378336A CN 110042503 A CN110042503 A CN 110042503A
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- nano fiber
- mose
- hollow nano
- preparation
- electrospinning
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- 239000002121 nanofiber Substances 0.000 title claims abstract description 77
- 238000001523 electrospinning Methods 0.000 title claims abstract description 32
- 238000002360 preparation method Methods 0.000 title claims abstract description 32
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 35
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 32
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 27
- 239000011248 coating agent Substances 0.000 claims abstract description 25
- 238000000576 coating method Methods 0.000 claims abstract description 25
- QXYJCZRRLLQGCR-UHFFFAOYSA-N molybdenum(IV) oxide Inorganic materials O=[Mo]=O QXYJCZRRLLQGCR-UHFFFAOYSA-N 0.000 claims abstract description 25
- 239000008367 deionised water Substances 0.000 claims abstract description 22
- 229910021641 deionized water Inorganic materials 0.000 claims abstract description 22
- 238000010041 electrostatic spinning Methods 0.000 claims abstract description 18
- NWZSZGALRFJKBT-KNIFDHDWSA-N (2s)-2,6-diaminohexanoic acid;(2s)-2-hydroxybutanedioic acid Chemical compound OC(=O)[C@@H](O)CC(O)=O.NCCCC[C@H](N)C(O)=O NWZSZGALRFJKBT-KNIFDHDWSA-N 0.000 claims abstract description 15
- IKDUDTNKRLTJSI-UHFFFAOYSA-N hydrazine monohydrate Substances O.NN IKDUDTNKRLTJSI-UHFFFAOYSA-N 0.000 claims abstract description 15
- 238000001027 hydrothermal synthesis Methods 0.000 claims abstract description 15
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 claims abstract description 13
- 238000013019 agitation Methods 0.000 claims abstract description 13
- 239000004372 Polyvinyl alcohol Substances 0.000 claims abstract description 10
- 229920002451 polyvinyl alcohol Polymers 0.000 claims abstract description 10
- 229910052750 molybdenum Inorganic materials 0.000 claims abstract description 9
- 239000011733 molybdenum Substances 0.000 claims abstract description 9
- ZOKXTWBITQBERF-UHFFFAOYSA-N Molybdenum Chemical compound [Mo] ZOKXTWBITQBERF-UHFFFAOYSA-N 0.000 claims abstract description 8
- 238000003756 stirring Methods 0.000 claims abstract description 8
- 239000000908 ammonium hydroxide Substances 0.000 claims abstract description 4
- 150000002751 molybdenum Chemical class 0.000 claims abstract description 4
- 239000012378 ammonium molybdate tetrahydrate Substances 0.000 claims abstract description 3
- FIXLYHHVMHXSCP-UHFFFAOYSA-H azane;dihydroxy(dioxo)molybdenum;trioxomolybdenum;tetrahydrate Chemical compound N.N.N.N.N.N.O.O.O.O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O=[Mo](=O)=O.O[Mo](O)(=O)=O.O[Mo](O)(=O)=O.O[Mo](O)(=O)=O FIXLYHHVMHXSCP-UHFFFAOYSA-H 0.000 claims abstract description 3
- 238000005530 etching Methods 0.000 claims abstract description 3
- 125000003748 selenium group Chemical class *[Se]* 0.000 claims abstract 3
- 239000000243 solution Substances 0.000 claims description 28
- 239000012298 atmosphere Substances 0.000 claims description 20
- 238000009987 spinning Methods 0.000 claims description 19
- 238000004140 cleaning Methods 0.000 claims description 18
- 239000007864 aqueous solution Substances 0.000 claims description 15
- BVTBRVFYZUCAKH-UHFFFAOYSA-L disodium selenite Chemical group [Na+].[Na+].[O-][Se]([O-])=O BVTBRVFYZUCAKH-UHFFFAOYSA-L 0.000 claims description 15
- 239000011781 sodium selenite Substances 0.000 claims description 15
- 229960001471 sodium selenite Drugs 0.000 claims description 14
- 235000015921 sodium selenite Nutrition 0.000 claims description 14
- 229910016001 MoSe Inorganic materials 0.000 claims description 13
- 235000018660 ammonium molybdate Nutrition 0.000 claims description 13
- 239000011609 ammonium molybdate Substances 0.000 claims description 13
- APUPEJJSWDHEBO-UHFFFAOYSA-P ammonium molybdate Chemical group [NH4+].[NH4+].[O-][Mo]([O-])(=O)=O APUPEJJSWDHEBO-UHFFFAOYSA-P 0.000 claims description 13
- 229940010552 ammonium molybdate Drugs 0.000 claims description 13
- 229910003208 (NH4)6Mo7O24·4H2O Inorganic materials 0.000 claims description 11
- -1 ethyl carbonate ester Chemical class 0.000 claims description 9
- 239000000835 fiber Substances 0.000 claims description 8
- 239000002033 PVDF binder Substances 0.000 claims description 6
- 229920002981 polyvinylidene fluoride Polymers 0.000 claims description 6
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 5
- 239000006230 acetylene black Substances 0.000 claims description 5
- 229910052700 potassium Inorganic materials 0.000 claims description 5
- 239000011591 potassium Substances 0.000 claims description 5
- 239000002002 slurry Substances 0.000 claims description 4
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims description 3
- 229910021135 KPF6 Inorganic materials 0.000 claims description 3
- 235000007164 Oryza sativa Nutrition 0.000 claims description 3
- 239000012300 argon atmosphere Substances 0.000 claims description 3
- 238000003763 carbonization Methods 0.000 claims description 3
- 239000011889 copper foil Substances 0.000 claims description 3
- 238000007599 discharging Methods 0.000 claims description 3
- 239000003792 electrolyte Substances 0.000 claims description 3
- 239000002070 nanowire Substances 0.000 claims description 3
- 235000009566 rice Nutrition 0.000 claims description 3
- 229910052786 argon Inorganic materials 0.000 claims description 2
- 238000001291 vacuum drying Methods 0.000 claims description 2
- 240000007594 Oryza sativa Species 0.000 claims 1
- 239000003292 glue Substances 0.000 claims 1
- 238000006243 chemical reaction Methods 0.000 abstract description 22
- 239000002994 raw material Substances 0.000 abstract description 3
- 238000000034 method Methods 0.000 description 11
- 239000000463 material Substances 0.000 description 8
- 238000003760 magnetic stirring Methods 0.000 description 7
- 239000002202 Polyethylene glycol Substances 0.000 description 6
- 238000001816 cooling Methods 0.000 description 6
- 238000010438 heat treatment Methods 0.000 description 6
- 239000012456 homogeneous solution Substances 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- 229920001223 polyethylene glycol Polymers 0.000 description 6
- 238000001035 drying Methods 0.000 description 5
- 150000003342 selenium Chemical class 0.000 description 5
- HBBGRARXTFLTSG-UHFFFAOYSA-N Lithium ion Chemical compound [Li+] HBBGRARXTFLTSG-UHFFFAOYSA-N 0.000 description 4
- 230000008901 benefit Effects 0.000 description 4
- 230000005611 electricity Effects 0.000 description 4
- 229910001416 lithium ion Inorganic materials 0.000 description 4
- NPYPAHLBTDXSSS-UHFFFAOYSA-N Potassium ion Chemical compound [K+] NPYPAHLBTDXSSS-UHFFFAOYSA-N 0.000 description 3
- 229910001414 potassium ion Inorganic materials 0.000 description 3
- 230000008569 process Effects 0.000 description 3
- 238000003860 storage Methods 0.000 description 3
- WHXSMMKQMYFTQS-UHFFFAOYSA-N Lithium Chemical compound [Li] WHXSMMKQMYFTQS-UHFFFAOYSA-N 0.000 description 2
- 241000209094 Oryza Species 0.000 description 2
- 239000011149 active material Substances 0.000 description 2
- 230000005540 biological transmission Effects 0.000 description 2
- 239000003575 carbonaceous material Substances 0.000 description 2
- 238000011161 development Methods 0.000 description 2
- 238000002474 experimental method Methods 0.000 description 2
- 239000011796 hollow space material Substances 0.000 description 2
- 238000003780 insertion Methods 0.000 description 2
- 230000037431 insertion Effects 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 239000007788 liquid Substances 0.000 description 2
- 229910052744 lithium Inorganic materials 0.000 description 2
- 239000007773 negative electrode material Substances 0.000 description 2
- 239000002243 precursor Substances 0.000 description 2
- 239000002904 solvent Substances 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 239000006173 Good's buffer Substances 0.000 description 1
- 229910003424 Na2SeO3 Inorganic materials 0.000 description 1
- BUGBHKTXTAQXES-UHFFFAOYSA-N Selenium Chemical compound [Se] BUGBHKTXTAQXES-UHFFFAOYSA-N 0.000 description 1
- 230000009471 action Effects 0.000 description 1
- 229910003481 amorphous carbon Inorganic materials 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 239000003638 chemical reducing agent Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000009831 deintercalation Methods 0.000 description 1
- 238000002242 deionisation method Methods 0.000 description 1
- 238000004090 dissolution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000004146 energy storage Methods 0.000 description 1
- 230000003628 erosive effect Effects 0.000 description 1
- 150000002148 esters Chemical class 0.000 description 1
- 230000007062 hydrolysis Effects 0.000 description 1
- 238000006460 hydrolysis reaction Methods 0.000 description 1
- 238000011835 investigation Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 230000007246 mechanism Effects 0.000 description 1
- 229910052976 metal sulfide Inorganic materials 0.000 description 1
- MHWZQNGIEIYAQJ-UHFFFAOYSA-N molybdenum diselenide Chemical compound [Se]=[Mo]=[Se] MHWZQNGIEIYAQJ-UHFFFAOYSA-N 0.000 description 1
- CQDGTJPVBWZJAZ-UHFFFAOYSA-N monoethyl carbonate Chemical compound CCOC(O)=O CQDGTJPVBWZJAZ-UHFFFAOYSA-N 0.000 description 1
- 239000002086 nanomaterial Substances 0.000 description 1
- 239000002071 nanotube Substances 0.000 description 1
- 239000005416 organic matter Substances 0.000 description 1
- 239000002245 particle Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000011160 research Methods 0.000 description 1
- 150000003839 salts Chemical class 0.000 description 1
- SCWQRZHMKQEINE-UHFFFAOYSA-N selenous acid;sodium Chemical compound [Na].O[Se](O)=O SCWQRZHMKQEINE-UHFFFAOYSA-N 0.000 description 1
- 238000005245 sintering Methods 0.000 description 1
- 230000005476 size effect Effects 0.000 description 1
- 235000015393 sodium molybdate Nutrition 0.000 description 1
- 239000011684 sodium molybdate Substances 0.000 description 1
- TVXXNOYZHKPKGW-UHFFFAOYSA-N sodium molybdate (anhydrous) Chemical compound [Na+].[Na+].[O-][Mo]([O-])(=O)=O TVXXNOYZHKPKGW-UHFFFAOYSA-N 0.000 description 1
- 230000001052 transient effect Effects 0.000 description 1
- 229910052723 transition metal Inorganic materials 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B82—NANOTECHNOLOGY
- B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
- B82Y40/00—Manufacture or treatment of nanostructures
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F1/00—General methods for the manufacture of artificial filaments or the like
- D01F1/02—Addition of substances to the spinning solution or to the melt
- D01F1/08—Addition of substances to the spinning solution or to the melt for forming hollow filaments
-
- D—TEXTILES; PAPER
- D01—NATURAL OR MAN-MADE THREADS OR FIBRES; SPINNING
- D01F—CHEMICAL FEATURES IN THE MANUFACTURE OF ARTIFICIAL FILAMENTS, THREADS, FIBRES, BRISTLES OR RIBBONS; APPARATUS SPECIALLY ADAPTED FOR THE MANUFACTURE OF CARBON FILAMENTS
- D01F9/00—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments
- D01F9/08—Artificial filaments or the like of other substances; Manufacture thereof; Apparatus specially adapted for the manufacture of carbon filaments of inorganic material
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/04—Construction or manufacture in general
- H01M10/0422—Cells or battery with cylindrical casing
- H01M10/0427—Button cells
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/13—Electrodes for accumulators with non-aqueous electrolyte, e.g. for lithium-accumulators; Processes of manufacture thereof
- H01M4/136—Electrodes based on inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/362—Composites
- H01M4/366—Composites as layered products
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/36—Selection of substances as active materials, active masses, active liquids
- H01M4/58—Selection of substances as active materials, active masses, active liquids of inorganic compounds other than oxides or hydroxides, e.g. sulfides, selenides, tellurides, halogenides or LiCoFy; of polyanionic structures, e.g. phosphates, silicates or borates
- H01M4/581—Chalcogenides or intercalation compounds thereof
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
- H01M4/624—Electric conductive fillers
- H01M4/625—Carbon or graphite
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M4/00—Electrodes
- H01M4/02—Electrodes composed of, or comprising, active material
- H01M4/62—Selection of inactive substances as ingredients for active masses, e.g. binders, fillers
- H01M4/628—Inhibitors, e.g. gassing inhibitors, corrosion inhibitors
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P70/00—Climate change mitigation technologies in the production process for final industrial or consumer products
- Y02P70/50—Manufacturing or production processes characterised by the final manufactured product
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Electrochemistry (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Materials Engineering (AREA)
- Textile Engineering (AREA)
- Nanotechnology (AREA)
- Composite Materials (AREA)
- Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- General Physics & Mathematics (AREA)
- Crystallography & Structural Chemistry (AREA)
- Inorganic Compounds Of Heavy Metals (AREA)
- Inorganic Fibers (AREA)
- Carbon And Carbon Compounds (AREA)
- Nonwoven Fabrics (AREA)
Abstract
Description
Claims (10)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
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CN201910378336.4A CN110042503B (zh) | 2019-05-08 | 2019-05-08 | 一种MoSe2@C电纺中空纳米纤维及其制备方法和应用 |
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CN201910378336.4A CN110042503B (zh) | 2019-05-08 | 2019-05-08 | 一种MoSe2@C电纺中空纳米纤维及其制备方法和应用 |
Publications (2)
Publication Number | Publication Date |
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CN110042503A true CN110042503A (zh) | 2019-07-23 |
CN110042503B CN110042503B (zh) | 2021-06-22 |
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CN201910378336.4A Active CN110042503B (zh) | 2019-05-08 | 2019-05-08 | 一种MoSe2@C电纺中空纳米纤维及其制备方法和应用 |
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Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110783568A (zh) * | 2019-11-04 | 2020-02-11 | 陕西科技大学 | 一种中空碳包覆硒化钼纳米结构的制备方法及应用 |
CN111036095A (zh) * | 2019-12-31 | 2020-04-21 | 济南大学 | 一种柔性自支撑MoO2@C纳米纤维薄膜材料及其制备方法和应用 |
CN111293297A (zh) * | 2020-02-26 | 2020-06-16 | 上海电力大学 | 一种碳包覆MoSe2/黑磷复合材料及其制备方法 |
CN113817450A (zh) * | 2021-09-30 | 2021-12-21 | 国网河北省电力有限公司电力科学研究院 | 一种供暖用相变储热材料及其制备方法 |
CN114105107A (zh) * | 2021-12-31 | 2022-03-01 | 西安工业大学 | 具有不同形貌的高度单分散MoSe2纳米材料的制备方法 |
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JP2008159418A (ja) * | 2006-12-25 | 2008-07-10 | Sanyo Electric Co Ltd | 非水電解質二次電池 |
CN102623687A (zh) * | 2012-04-09 | 2012-08-01 | 华中科技大学 | 一种高容量二氧化钼负极材料的制备方法及其应用 |
KR20160042799A (ko) * | 2014-10-10 | 2016-04-20 | 주식회사 아모그린텍 | 플렉서블 배터리용 분리막, 이의 제조방법 및 이를 포함하는 플렉서블 배터리 |
CN105887132A (zh) * | 2016-06-24 | 2016-08-24 | 复旦大学 | 一种二硒化钼纳米片/碳纳米纤维杂化材料及其制备方法 |
CN107170974A (zh) * | 2017-05-26 | 2017-09-15 | 中南大学 | 一种碳包覆MoSe2/石墨烯电纺纳米纤维及其制备方法 |
CN109411721A (zh) * | 2018-10-10 | 2019-03-01 | 陕西科技大学 | 一种片状二硒化钼/碳纤维布复合材料的制备方法 |
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2019
- 2019-05-08 CN CN201910378336.4A patent/CN110042503B/zh active Active
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JP2008159418A (ja) * | 2006-12-25 | 2008-07-10 | Sanyo Electric Co Ltd | 非水電解質二次電池 |
CN102623687A (zh) * | 2012-04-09 | 2012-08-01 | 华中科技大学 | 一种高容量二氧化钼负极材料的制备方法及其应用 |
KR20160042799A (ko) * | 2014-10-10 | 2016-04-20 | 주식회사 아모그린텍 | 플렉서블 배터리용 분리막, 이의 제조방법 및 이를 포함하는 플렉서블 배터리 |
CN105887132A (zh) * | 2016-06-24 | 2016-08-24 | 复旦大学 | 一种二硒化钼纳米片/碳纳米纤维杂化材料及其制备方法 |
CN107170974A (zh) * | 2017-05-26 | 2017-09-15 | 中南大学 | 一种碳包覆MoSe2/石墨烯电纺纳米纤维及其制备方法 |
CN109411721A (zh) * | 2018-10-10 | 2019-03-01 | 陕西科技大学 | 一种片状二硒化钼/碳纤维布复合材料的制备方法 |
Cited By (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN110783568A (zh) * | 2019-11-04 | 2020-02-11 | 陕西科技大学 | 一种中空碳包覆硒化钼纳米结构的制备方法及应用 |
CN110783568B (zh) * | 2019-11-04 | 2021-05-04 | 陕西科技大学 | 一种中空碳包覆硒化钼纳米结构的制备方法及应用 |
CN111036095A (zh) * | 2019-12-31 | 2020-04-21 | 济南大学 | 一种柔性自支撑MoO2@C纳米纤维薄膜材料及其制备方法和应用 |
CN111293297A (zh) * | 2020-02-26 | 2020-06-16 | 上海电力大学 | 一种碳包覆MoSe2/黑磷复合材料及其制备方法 |
CN113817450A (zh) * | 2021-09-30 | 2021-12-21 | 国网河北省电力有限公司电力科学研究院 | 一种供暖用相变储热材料及其制备方法 |
CN114105107A (zh) * | 2021-12-31 | 2022-03-01 | 西安工业大学 | 具有不同形貌的高度单分散MoSe2纳米材料的制备方法 |
CN114105107B (zh) * | 2021-12-31 | 2023-11-07 | 西安工业大学 | 具有不同形貌的高度单分散MoSe2纳米材料的制备方法 |
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