CN108623773B - 多硫醇组合物、光学材料用聚合性组合物及其用途 - Google Patents

多硫醇组合物、光学材料用聚合性组合物及其用途 Download PDF

Info

Publication number
CN108623773B
CN108623773B CN201810335752.1A CN201810335752A CN108623773B CN 108623773 B CN108623773 B CN 108623773B CN 201810335752 A CN201810335752 A CN 201810335752A CN 108623773 B CN108623773 B CN 108623773B
Authority
CN
China
Prior art keywords
compound
polythiol
minutes
peak area
polythiol composition
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
CN201810335752.1A
Other languages
English (en)
Chinese (zh)
Other versions
CN108623773A (zh
Inventor
川口胜
西村雄
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Mitsui Chemicals Inc
Original Assignee
Mitsui Chemicals Inc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=49954940&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=CN108623773(B) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Mitsui Chemicals Inc filed Critical Mitsui Chemicals Inc
Publication of CN108623773A publication Critical patent/CN108623773A/zh
Application granted granted Critical
Publication of CN108623773B publication Critical patent/CN108623773B/zh
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/38—Low-molecular-weight compounds having heteroatoms other than oxygen
    • C08G18/3855—Low-molecular-weight compounds having heteroatoms other than oxygen having sulfur
    • C08G18/3876—Low-molecular-weight compounds having heteroatoms other than oxygen having sulfur containing mercapto groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/70—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the isocyanates or isothiocyanates used
    • C08G18/72—Polyisocyanates or polyisothiocyanates
    • C08G18/74—Polyisocyanates or polyisothiocyanates cyclic
    • C08G18/76—Polyisocyanates or polyisothiocyanates cyclic aromatic
    • C08G18/7614—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring
    • C08G18/7628—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring containing at least one isocyanate or isothiocyanate group linked to the aromatic ring by means of an aliphatic group
    • C08G18/7642—Polyisocyanates or polyisothiocyanates cyclic aromatic containing only one aromatic ring containing at least one isocyanate or isothiocyanate group linked to the aromatic ring by means of an aliphatic group containing at least two isocyanate or isothiocyanate groups linked to the aromatic ring by means of an aliphatic group having a primary carbon atom next to the isocyanate or isothiocyanate groups, e.g. xylylene diisocyanate or homologues substituted on the aromatic ring
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C321/00—Thiols, sulfides, hydropolysulfides or polysulfides
    • C07C321/02—Thiols having mercapto groups bound to acyclic carbon atoms
    • C07C321/04—Thiols having mercapto groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C321/00—Thiols, sulfides, hydropolysulfides or polysulfides
    • C07C321/12—Sulfides, hydropolysulfides, or polysulfides having thio groups bound to acyclic carbon atoms
    • C07C321/14—Sulfides, hydropolysulfides, or polysulfides having thio groups bound to acyclic carbon atoms of an acyclic saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C323/00—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups
    • C07C323/10—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and singly-bound oxygen atoms bound to the same carbon skeleton
    • C07C323/11—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and singly-bound oxygen atoms bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton
    • C07C323/12—Thiols, sulfides, hydropolysulfides or polysulfides substituted by halogen, oxygen or nitrogen atoms, or by sulfur atoms not being part of thio groups containing thio groups and singly-bound oxygen atoms bound to the same carbon skeleton having the sulfur atoms of the thio groups bound to acyclic carbon atoms of the carbon skeleton the carbon skeleton being acyclic and saturated
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C335/00—Thioureas, i.e. compounds containing any of the groups, the nitrogen atoms not being part of nitro or nitroso groups
    • C07C335/30—Isothioureas
    • G—PHYSICS
    • G02—OPTICS
    • G02B—OPTICAL ELEMENTS, SYSTEMS OR APPARATUS
    • G02B1/00—Optical elements characterised by the material of which they are made; Optical coatings for optical elements
    • G02B1/04—Optical elements characterised by the material of which they are made; Optical coatings for optical elements made of organic materials, e.g. plastics
    • G02B1/041—Lenses

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Physics & Mathematics (AREA)
  • General Physics & Mathematics (AREA)
  • Optics & Photonics (AREA)
  • Polyurethanes Or Polyureas (AREA)
CN201810335752.1A 2012-08-14 2013-08-13 多硫醇组合物、光学材料用聚合性组合物及其用途 Active CN108623773B (zh)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
JP2012179899 2012-08-14
JP2012-179899 2012-08-14
JP2013001201 2013-02-28
JPPCT/JP2013/001201 2013-02-28
CN201380023522.7A CN104271629B (zh) 2012-08-14 2013-08-13 多硫醇组合物、光学材料用聚合性组合物及其用途

Related Parent Applications (1)

Application Number Title Priority Date Filing Date
CN201380023522.7A Division CN104271629B (zh) 2012-08-14 2013-08-13 多硫醇组合物、光学材料用聚合性组合物及其用途

Publications (2)

Publication Number Publication Date
CN108623773A CN108623773A (zh) 2018-10-09
CN108623773B true CN108623773B (zh) 2021-04-16

Family

ID=49954940

Family Applications (4)

Application Number Title Priority Date Filing Date
CN201810335752.1A Active CN108623773B (zh) 2012-08-14 2013-08-13 多硫醇组合物、光学材料用聚合性组合物及其用途
CN201380023522.7A Active CN104271629B (zh) 2012-08-14 2013-08-13 多硫醇组合物、光学材料用聚合性组合物及其用途
CN201810336442.1A Active CN108727559B (zh) 2012-08-14 2013-08-13 多硫醇组合物、光学材料用聚合性组合物及其用途
CN201810336616.4A Active CN108559043B (zh) 2012-08-14 2013-08-13 多硫醇组合物、光学材料用聚合性组合物及其用途

Family Applications After (3)

Application Number Title Priority Date Filing Date
CN201380023522.7A Active CN104271629B (zh) 2012-08-14 2013-08-13 多硫醇组合物、光学材料用聚合性组合物及其用途
CN201810336442.1A Active CN108727559B (zh) 2012-08-14 2013-08-13 多硫醇组合物、光学材料用聚合性组合物及其用途
CN201810336616.4A Active CN108559043B (zh) 2012-08-14 2013-08-13 多硫醇组合物、光学材料用聚合性组合物及其用途

Country Status (8)

Country Link
US (4) US9777103B2 (enExample)
EP (2) EP2960266B1 (enExample)
JP (2) JP5373226B1 (enExample)
KR (3) KR101533207B1 (enExample)
CN (4) CN108623773B (enExample)
BR (1) BR112014025570B1 (enExample)
IN (1) IN2014DN08100A (enExample)
WO (1) WO2014027665A1 (enExample)

Families Citing this family (35)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP5373226B1 (ja) 2012-08-14 2013-12-18 三井化学株式会社 ポリチオール組成物、光学材料用重合性組成物およびその用途
TW201506083A (zh) * 2013-06-18 2015-02-16 Mitsubishi Gas Chemical Co 光學材料用組成物
TWI699389B (zh) 2014-07-18 2020-07-21 日商三菱瓦斯化學股份有限公司 聚硫醇組成物及其製造方法
US10132961B2 (en) 2015-03-31 2018-11-20 Mitsubishi Gas Chemical Company, Inc. Episulfide compound and optical material composition including same
KR101831892B1 (ko) * 2016-06-30 2018-02-26 에스케이씨 주식회사 폴리티오우레탄계 광학 재료용 중합성 조성물
CN108884204A (zh) * 2016-06-30 2018-11-23 豪雅镜片泰国有限公司 固化物的制造方法、固化物及眼镜镜片基材
CN108884028B (zh) * 2016-06-30 2020-10-09 豪雅镜片泰国有限公司 多硫醇化合物的制造方法、固化性组合物的制造方法、及固化物的制造方法
JPWO2018003058A1 (ja) * 2016-06-30 2019-01-17 ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ 硬化物の製造方法、硬化物および眼鏡レンズ基材
WO2018012803A1 (ko) 2016-07-14 2018-01-18 에스케이씨 주식회사 광학 재료용 방향족 폴리티올 화합물
JP6306102B2 (ja) 2016-07-29 2018-04-04 ホヤ レンズ タイランド リミテッドＨＯＹＡ Ｌｅｎｓ Ｔｈａｉｌａｎｄ Ｌｔｄ 樹脂組成物
KR101971110B1 (ko) * 2016-08-30 2019-04-22 에스케이씨 주식회사 광학 재료용 폴리티올 화합물
CN113372250B (zh) 2017-02-15 2023-12-08 Ks试验研究株式会社 多硫醇化合物、其制备方法、由其制备的透明氨基甲酸酯类树脂以及光学体
CN110446696A (zh) * 2017-03-24 2019-11-12 三井化学株式会社 多元硫醇化合物的制造方法、聚合性组合物及其用途
KR101894921B1 (ko) * 2018-01-19 2018-09-04 에스케이씨 주식회사 플라스틱 광학 렌즈용 폴리티올 조성물
CN111868025B (zh) * 2018-03-30 2023-12-12 三井化学株式会社 有机巯基化合物或其中间体的制造方法、（多）硫醇成分、光学材料用聚合性组合物、成型体、光学材料及透镜
KR20190138145A (ko) 2018-06-04 2019-12-12 에스케이씨 주식회사 폴리티올 조성물 및 이의 제조방법
EP3841134A1 (en) * 2018-08-20 2021-06-30 PPG Industries Ohio Inc. Polythiol composition
CN109651214A (zh) * 2018-12-17 2019-04-19 锦西化工研究院有限公司 一种去除二巯乙基硫醚中絮状物，提高产品纯度、收率的方法
JP7296754B2 (ja) * 2019-03-28 2023-06-23 ホヤ レンズ タイランド リミテッド 光学部材用重合性組成物、光学部材、及び眼鏡レンズ
JP7296755B2 (ja) * 2019-03-28 2023-06-23 ホヤ レンズ タイランド リミテッド 光学部材用樹脂組成物、光学部材、及び眼鏡レンズ
JP7273156B2 (ja) * 2019-07-17 2023-05-12 三井化学株式会社 ポリチオール組成物及びその応用
JP7437932B2 (ja) * 2019-12-27 2024-02-26 三井化学株式会社 廃水処理方法
EP3916470B1 (en) 2020-01-27 2023-12-27 Mitsui Chemicals, Inc. Polymerizable composition for optical material, polymerizable prepolymer composition for optical material, cured product, and method of producing optical material
MX2021013149A (es) 2020-01-27 2021-12-10 Mitsui Chemicals Inc Composicion polimerizable para material optico, composicion polimerizable de prepolimero para material optico, producto curado y metodo para producir el material optico.
KR20200026853A (ko) 2020-02-28 2020-03-11 에스케이씨 주식회사 폴리티올 조성물 및 이의 제조방법
JP7434526B2 (ja) 2020-03-10 2024-02-20 三井化学株式会社 光学材料用重合性組成物、光学材料用重合性プレポリマー組成物、硬化物及び光学材料の製造方法
MX2022012244A (es) 2020-03-30 2022-10-27 Ppg Ind Ohio Inc Metodo para preparar composiciones de polimeros de baja turbidez para su uso en materiales opticos con indice de refraccion alto.
KR20210121873A (ko) 2020-03-31 2021-10-08 주식회사 엠엘텍 티오우레탄계 광학재료용 수지 조성물과 티오우레탄계 광학재료용 수지의 제조방법
KR20220033890A (ko) * 2020-09-10 2022-03-17 에스케이씨 주식회사 폴리티올 조성물 및 이를 포함하는 광학용 중합성 조성물
KR102448166B1 (ko) * 2020-09-22 2022-09-27 에스케이씨 주식회사 폴리티올 조성물 및 이를 포함하는 광학용 중합성 조성물
CN114765982B (zh) * 2020-11-13 2024-06-28 三井化学株式会社 多硫醇组合物、聚合性组合物、树脂、成型体、光学材料及透镜
CN116601200A (zh) * 2020-11-27 2023-08-15 Skc株式会社 多硫醇组合物、光学组合物和光学产品
CN116457385A (zh) * 2020-11-27 2023-07-18 Skc株式会社 多硫醇组合物、光学组合物和光学产品
EP4455740A1 (en) 2021-12-24 2024-10-30 Mitsui Chemicals, Inc. Method for manufacturing optical member and cured product
JPWO2024080383A1 (enExample) * 2022-10-14 2024-04-18

Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0952931A (ja) * 1995-08-14 1997-02-25 Mitsui Toatsu Chem Inc 新規なポリチオールを用いた含硫ウレタン系プラスチックレンズ
JPH09194558A (ja) * 1996-01-23 1997-07-29 Mitsui Toatsu Chem Inc 含硫ウレタン系プラスチックレンズ
CN101421232A (zh) * 2006-04-19 2009-04-29 三井化学株式会社 光学材料用（多）硫醇化合物的制造方法及含有该化合物的聚合性组合物

Family Cites Families (21)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US5087758A (en) 1988-12-22 1992-02-11 Mitsui Toatsu Chemicals, Inc. Mercapto compound, a high refractive index resin and lens and a process for preparing them
JP2621991B2 (ja) * 1988-12-22 1997-06-18 三井東圧化学株式会社 メルカプト化合物及びその製造方法
JP2989787B2 (ja) * 1991-08-08 1999-12-13 三井化学株式会社 含硫ウレタン系樹脂及びレンズ
JP2740714B2 (ja) * 1991-08-08 1998-04-15 三井東圧化学株式会社 メルカプト化合物及びその製造方法
AU634932B1 (en) 1991-08-08 1993-03-04 Mitsui Chemicals, Inc. Mercapto compound, its preparation process, and sulfur- containing urethane resins and lenses using the same
US5608115A (en) * 1994-01-26 1997-03-04 Mitsui Toatsu Chemicals, Inc. Polythiol useful for preparing sulfur-containing urethane-based resin and process for producing the same
US5736609A (en) * 1995-06-30 1998-04-07 Mitsui Toatsu Chemicals, Inc. Sulfur-containing urethane-based resin composition, its resin, and optical element and lens comprising resin
JP3794651B2 (ja) * 1996-03-28 2006-07-05 住友精化株式会社 メルカプト化合物、メルカプト化合物の製造方法、テトラオール化合物およびテトラオール化合物の製造方法
JP3910232B2 (ja) * 1996-04-19 2007-04-25 住友精化株式会社 メルカプト化合物、トリオール化合物、およびそれらの製造方法
US5932681A (en) * 1998-03-09 1999-08-03 Ppg Industries Ohio, Inc. Method of preparing an optical polymerizate
JP4426017B2 (ja) * 1999-07-27 2010-03-03 三井化学株式会社 有機メルカプト化合物の製造方法
JP2002270859A (ja) * 2000-11-27 2002-09-20 Mitsui Chemicals Inc 光電素子用パッケージおよびその製造方法
JP2007129450A (ja) 2005-11-02 2007-05-24 Canon Inc 画像処理装置
JP2007129449A (ja) 2005-11-02 2007-05-24 Canon Inc 画像処理装置
WO2007129449A1 (ja) 2006-04-20 2007-11-15 Mitsui Chemicals, Inc. 光学材料用ポリチオール化合物の製造方法およびそれを含む重合性組成物
JP5026432B2 (ja) 2006-10-16 2012-09-12 三井化学株式会社 光学材料用樹脂の製造方法
CN101614831B (zh) * 2009-08-11 2010-10-27 杭州新顺化工有限公司 高折射率树脂镜片及其制备方法
IT1400108B1 (it) 2010-05-20 2013-05-17 Acomon Ag Catalizzatore di polimerizzazione per politiouretani, composizione liquida polimerizzabile e procedimento per la produzione di vetri organici politiouretanici ad alto indice di rifrazione
KR20120058635A (ko) * 2010-08-13 2012-06-08 주식회사 케이오씨솔루션 광학렌즈용 폴리티올 화합물의 제조법 및 이를 포함하는 수지 조성물
CN104321306B (zh) * 2012-08-14 2016-10-19 三井化学株式会社 多硫醇化合物的制造方法、光学材料用聚合性组合物及其用途
JP5373226B1 (ja) 2012-08-14 2013-12-18 三井化学株式会社 ポリチオール組成物、光学材料用重合性組成物およびその用途

Patent Citations (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JPH0952931A (ja) * 1995-08-14 1997-02-25 Mitsui Toatsu Chem Inc 新規なポリチオールを用いた含硫ウレタン系プラスチックレンズ
JPH09194558A (ja) * 1996-01-23 1997-07-29 Mitsui Toatsu Chem Inc 含硫ウレタン系プラスチックレンズ
CN101421232A (zh) * 2006-04-19 2009-04-29 三井化学株式会社 光学材料用（多）硫醇化合物的制造方法及含有该化合物的聚合性组合物

Also Published As

Publication number Publication date
CN104271629B (zh) 2018-05-11
EP2824126B1 (en) 2015-09-30
US10858473B2 (en) 2020-12-08
US10858472B2 (en) 2020-12-08
WO2014027665A1 (ja) 2014-02-20
KR20140125457A (ko) 2014-10-28
CN108727559B (zh) 2021-07-23
US20170349692A1 (en) 2017-12-07
CN108559043B (zh) 2021-11-02
US20150094443A1 (en) 2015-04-02
BR112014025570B1 (pt) 2020-12-22
KR20180090898A (ko) 2018-08-13
CN108559043A (zh) 2018-09-21
US20180334527A1 (en) 2018-11-22
CN108727559A (zh) 2018-11-02
US9777103B2 (en) 2017-10-03
EP2824126A1 (en) 2015-01-14
US20180334528A1 (en) 2018-11-22
JPWO2014027665A1 (ja) 2016-07-28
IN2014DN08100A (enExample) 2015-05-01
EP2960266A1 (en) 2015-12-30
KR20150032250A (ko) 2015-03-25
KR101533207B1 (ko) 2015-07-01
EP2824126A4 (en) 2015-03-04
EP2960266B1 (en) 2017-04-19
CN108623773A (zh) 2018-10-09
JP5373226B1 (ja) 2013-12-18
CN104271629A (zh) 2015-01-07
JP5613847B2 (ja) 2014-10-29
KR102074091B1 (ko) 2020-02-05
KR102047571B1 (ko) 2019-11-21

Similar Documents

Publication Publication Date Title
CN108623773B (zh) 多硫醇组合物、光学材料用聚合性组合物及其用途
US9605105B2 (en) Method for producing polythiol compound, polymerizable composition for optical material, and uses thereof
JP5319037B1 (ja) ポリチオール化合物の製造方法
JP5319036B1 (ja) ポリチオール化合物の製造方法

Legal Events

Date Code Title Description
PB01 Publication
PB01 Publication
SE01 Entry into force of request for substantive examination
SE01 Entry into force of request for substantive examination
GR01 Patent grant
GR01 Patent grant