CN107375057A - A kind of skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction - Google Patents
A kind of skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction Download PDFInfo
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- CN107375057A CN107375057A CN201710520221.5A CN201710520221A CN107375057A CN 107375057 A CN107375057 A CN 107375057A CN 201710520221 A CN201710520221 A CN 201710520221A CN 107375057 A CN107375057 A CN 107375057A
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/92—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof
- A61K8/922—Oils, fats or waxes; Derivatives thereof, e.g. hydrogenation products thereof of vegetable origin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/345—Alcohols containing more than one hydroxy group
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/36—Carboxylic acids; Salts or anhydrides thereof
- A61K8/365—Hydroxycarboxylic acids; Ketocarboxylic acids
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/40—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing nitrogen
- A61K8/44—Aminocarboxylic acids or derivatives thereof, e.g. aminocarboxylic acids containing sulfur; Salts; Esters or N-acylated derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/72—Cosmetics or similar toiletry preparations characterised by the composition containing organic macromolecular compounds
- A61K8/73—Polysaccharides
- A61K8/735—Mucopolysaccharides, e.g. hyaluronic acid; Derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/02—Preparations for care of the skin for chemically bleaching or whitening the skin
-
- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
- A61Q19/08—Anti-ageing preparations
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/20—Chemical, physico-chemical or functional or structural properties of the composition as a whole
- A61K2800/26—Optical properties
- A61K2800/262—Transparent; Translucent
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K2800/00—Properties of cosmetic compositions or active ingredients thereof or formulation aids used therein and process related aspects
- A61K2800/80—Process related aspects concerning the preparation of the cosmetic composition or the storage or application thereof
- A61K2800/85—Products or compounds obtained by fermentation, e.g. yoghurt, beer, wine
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Abstract
The invention discloses a kind of skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction.Skin-moisturizing, skin water of the present invention is included as follows according to the component of mass percentage:Concentration is 1wt% cedarwood essential oil 0.5%, and propane diols 2%, glycerine 2%, sodium hyaluronate 0.1%, sodium hydroxy methyl glycinate 0.5%, concentration is 0.1wt% Uruguay's tea extraction 2%, lactic acid 0.25% and water 92.65%.Skin-moisturizing, skin water of the present invention has the function that delaying skin aging, removes skin Huang gas, highlights the obscure colour of skin and desalinate microgroove by adding cedarwood essential oil and Uruguay's tea extraction.Skin-moisturizing, skin water of the present invention is without compositions such as heavy metal, alcohol, hormone, mineral oil, pigments, and formula is soft, and skin, which will not be produced, stimulates and bear.
Description
Technical field
The present invention relates to cosmetic field, and in particular to a kind of moisturizing containing cedarwood essential oil and Uruguay's tea extraction
Lotion.
Background technology
Lotion is a kind of low viscosity, the extremely runny liquid skin care cosmetics as water, by it after facial cleansing
Add on skin, moisturizing, moisturizing, skin care, a kind of beauty and skin care of the effect of promotion skin physiology function can be played
Product.
Essential oil, person " liquid golden ", due to its distinctive natural characteristic and efficacy effect, in cosmetics field,
Obtain the favor of numerous consumers.Cedarwood essential oil, have convergence pore, promote scar healing, nurse one's health aged skin the effect of;
Uruguay's tea enjoys the good reputation of " South America celestial grass ", it is considered to be " the mysterious present that God vouchsafes ", it contains up to 196 kinds of activity
Nutriment and bioactive substance.There has been no the lotion for combining cedarwood essential oil and Uruguay's tea, such market at present
Urgently develop.
The content of the invention
It is an object of the invention to the heavy metal of the lotion generally existing according to current market, hormone, alcohol, pigment etc.
Addition and caused by skin easy allergy the problems such as, and there has been no the lotion for combining cedarwood essential oil and Uruguay's tea, carry
For a kind of skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction, the moisturizing water constituent is pure natural raw material, no
Containing heavy metal, alcohol, hormone, pigment, mineral oil etc., formula is soft, non-stimulated to skin.
Above-mentioned purpose of the present invention is achieved by the following technical programs:
A kind of skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction, it is included as follows according to quality percentage
The component of number meter:Concentration be 1wt% cedarwood essential oil 0.5%, propane diols 2%, glycerine 2%, sodium hyaluronate 0.1%, methylol
Sodium Glycinate 0.5%, concentration are 0.1wt% Uruguay's tea extraction 2%, lactic acid 0.25% and water 92.65%.
Wherein, the preparation method of the cedarwood essential oil comprises the following steps:
(1) take dry cedarwood 500g to crush, be transferred in the 5L fermentation tanks for having added 1500~2500g distilled water, add
0.5% beef extract, 1% peptone and 0.5% sodium chloride, and pH to 4.5~6.0 is adjusted with 1mol/L phosphate buffers, from
So ferment 36h, then high-temperature inactivation strain;
(2) step (1) products therefrom and 1.5~5.0g complex enzyme hydrolysis liquid are sufficiently mixed, 30 is digested at 42~60 DEG C
~50min;The complex enzyme hydrolysis liquid is cellulase, hemicellulase and pectase according to 3:1:1~5:1:2 mass ratio mixes
The mixture of conjunction, adds water to be configured to the complex enzyme hydrolysis liquid that mass percent is 0.3~0.9%, and pH is 4.5~6.0;
(3) step (2) products therefrom is isolated and purified using wiped-film still, obtains cedarwood essential oil;
The preparation method of Uruguay's tea extraction comprises the following steps:
(a) take fresh Uruguay's tea 500g to crush, add 500~1500g distilled water, the complex enzyme hydrolysis with 1.5~5.0g
Liquid is sufficiently mixed, and 30~50min is digested at 42~60 DEG C, and centrifugation obtains digesting head product;The complex enzyme hydrolysis liquid is fiber
Plain enzyme, hemicellulase and pectase are according to 3:1:1~5:1:The mixture of 2 mass ratio mixing, adds water to be configured to quality hundred
Divide than the complex enzyme hydrolysis liquid for 0.3~0.9%, pH is 4.5~6.0;
(b) product filtering will be digested obtained by step (a), filter residue is placed in water-bath and extracted, the volume ratio of filter residue and water
For 1:8~15, leaching liquor filter cleaner;It is repeated twice, merges leaching liquor;
(c) leaching liquor obtained by step (b) is subjected to constant flow filtering in sheet frame, then the rotary evaporation under 0.1MPa pressure
Concentration, is finally settled to 50g, obtains Uruguay's tea extraction.
The complex enzyme hydrolysis liquid that the present invention uses include cellulase (including endoglucanase, exoglucanase and β-
Glucan glycosides enzyme), hemicellulase and pectase, can to the main component cellulose of cedarwood and Uruguay's tea, hemicellulose,
The macromolecular substances such as pectin are acted on, and realize its structural collapse, so that fragrance and functional component discharge more complete, fragrance
It is stronger.
The present invention is mainly entered using molecular distillation technique extraction cedarwood essential oil, molecular distillation under conditions of high vacuum
The technology of row Liquid liquid Separation, its advantage are that the temperature of distillation is low, and the heated time of material is short and separation degree is high, particularly suitable for
Higher boiling, thermal sensitivity and readily oxidizable substance isolate and purify.Cedarwood essential oil is heat-sensitive substance, using molecular distillation to its
Fragrance component retains preferably, while also can remove miscellaneous gas, makes the fragrance of cedarwood essential oil purer, strong.
The preparation method of skin-moisturizing, skin water of the invention containing cedarwood essential oil and Uruguay's tea extraction includes following step
Suddenly:
(1) the cedarwood essential oil that concentration is 1wt% and Uruguay's tea extraction that concentration is 0.1wt% are weighed, stirring is equal
It is even, obtain the mixture of cedarwood essential oil and Uruguay's tea extraction;
(2) propane diols is weighed, adds the mixture of cedarwood essential oil and Uruguay's tea extraction obtained by step (1), stirring
To clear, mixed material is obtained;
(3) other components are weighed, add mixed material obtained by step (2) after being dissolved with water while stirring, be again stirring for
Clear, obtain the skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction.
Skin-moisturizing, skin water of the invention containing cedarwood essential oil and Uruguay's tea extraction can make as daily lotion
With, be additionally operable to improve and prevent skin aging and improve the colour of skin.
Compared with prior art, the present invention has the advantages that:
(1) the skin-moisturizing, skin water of the invention containing cedarwood essential oil and Uruguay's tea extraction is homogeneous, gently, to skin
Skin has no stimulation, and rich in active components of plants, the raw material for being formulated selection is food grade materials and its extract, the pure day of product
Right, without materials such as heavy metal, alcohol, hormone, mineral oil and pigments;
(2) present invention uses cedarwood essential oil to have convergence pore as one of raw material, promote scar to heal, conditioning is old
The effect of changing skin;
(3) present invention uses Uruguay's tea extraction to contain abundant polyphenols as one of raw material, Uruguay's tea,
Polyphenols is a kind of potent antioxidant, can effectively damage to caused by skin for free radical, delay so as to reach
Skin aging, skin Huang gas is removed, highlight the obscure colour of skin and desalinates the effect of microgroove.
Brief description of the drawings
Inhibiting rates pair of the Fig. 1 for the lotion that Uruguay's tea extraction of Different adding amount is prepared to DPPH free radicals
Than.
Fig. 2 is to be tested using the skin moisture content of lotion of the present invention.
Embodiment
The invention will be further described with reference to embodiments, but embodiment the present invention is not done it is any type of
Limit.
In following examples, unless otherwise instructed, used raw material is raw material on sale on the market, used side
Method is method well known to those skilled in the art.
Embodiment 1
Prepare the skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction:
It is made up of the component as follows according to mass percentage:Concentration be 1wt% cedarwood essential oil 0.5%, propane diols
2%, glycerine 2%, sodium hyaluronate 0.1%, sodium hydroxy methyl glycinate 0.5%, concentration is 0.1wt% Uruguay's tea extraction 2%,
Lactic acid 0.25% and water 92.65%.
Wherein, the preparation method of cedarwood essential oil comprises the following steps:
(1) take dry cedarwood 500g to crush, be transferred in the 5L fermentation tanks for having added 1500g distilled water, add 0.5% N
Meat extract, 1% peptone and 0.5% sodium chloride, and pH to 4.5, spontaneous fermentation 36h are adjusted with 1mol/L phosphate buffers, so
High-temperature inactivation strain afterwards;
(2) step (1) products therefrom and 1.5g complex enzyme hydrolysis liquid are sufficiently mixed, 30min is digested at 42 DEG C;Complex enzyme
Solution liquid is cellulase, hemicellulase and pectase according to 5:1:The mixture of 2 mass ratio mixing, adds water to be configured to quality
Percentage be 0.3% complex enzyme hydrolysis liquid, pH 4.5;
(3) step (2) products therefrom is isolated and purified using wiped-film still, purification condition is:
Vapo(u)rizing temperature is 60~70 DEG C, and distillation pressure is 18~25Pa, and feed rate is 1.0~2.0ml/min, scrapes diaphragm plate rotating speed as 25
~40r/min, obtain cedarwood essential oil;
The preparation method of Uruguay's tea extraction comprises the following steps:
(a) take fresh Uruguay's tea 500g to crush, add 1000g distilled water, be sufficiently mixed with 3.0g complex enzyme hydrolysis liquid,
30min is digested at 50 DEG C, centrifugation obtains digesting head product;Complex enzyme hydrolysis liquid is cellulase, hemicellulase and pectase
According to 5:1:The mixture of 2 mass ratio mixing, adds water to be configured to the complex enzyme hydrolysis liquid that mass percent is 0.6%, and pH is
4.5;
(b) product filtering will be digested obtained by step (a), filter residue is placed in water-bath and extracted, the volume ratio of filter residue and water
For 1:8~15, leaching liquor filter cleaner;It is repeated twice, merges leaching liquor;
(c) leaching liquor obtained by step (b) is subjected to constant flow filtering in sheet frame, then the rotary evaporation under 0.1MPa pressure
Concentration, is finally settled to 50g, obtains Uruguay's tea extraction.
Preparation process:
(1) the cedarwood essential oil that concentration is 1wt% and Uruguay's tea extraction that concentration is 0.1wt% are weighed, stirring is equal
It is even, obtain the mixture of cedarwood essential oil and Uruguay's tea extraction;
(2) propane diols is weighed, adds the mixture of cedarwood essential oil and Uruguay's tea extraction obtained by step (1), stirring
To clear, mixed material is obtained;
(3) other components are weighed, add mixed material obtained by step (2) after being dissolved with water while stirring, be again stirring for
Clear, obtain the skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction.
Experimental example 1
Experiment is divided into four groups, and first group is to add lotion made from VC as positive control;Second group is present invention profit
Skin water formula removes lotion made from Uruguay's tea extraction, total amount is reached 100% wherein changing the dosage of water;3rd
Group removes lotion made from cedarwood essential oil for lotion formula of the present invention, reaches total amount wherein changing the dosage of water
100%;4th group is lotion made from lotion of the present invention formula.Four groups change the addition of additive, prepare
Journey determines the inhibiting rate of lotion that the different extracts of Different adding amount are prepared into DPPH free radicals, as a result with embodiment 1
Refer to Fig. 1.
DPPH inhibiting rates (%)=[1- (A-B)/C] × 100%.A:The absorbance of DPPH+ additives;B:Additive
Absorbance;C:The absorbance of positive controls.
As shown in Figure 1, it is prepared by the cedarwood blend of essential oils of the Uruguay's tea extraction and 1wt% that with the addition of 0.1wt%
When the addition of lotion reaches 2%, for DPPH inhibiting rate up to 83%, inhibiting rate is significantly higher than individually addition 1wt% arborvitaes
Another name for oil lotion and individually addition 0.1wt% Uruguay's tea extraction lotion and its positive controls.Therefore, it is of the invention
Lotion can effectively prevent the damage that free radical is brought.
Experimental example 2
20 subjects are chosen, are divided into two groups of A, B, A groups are blank control group, and common profit purchased in market is used in right side eye tail region
Skin water, B groups are experimental group, and lotion made from the embodiment of the present invention 1 is used in right side eye tail region, use 2 times, continuously make daily
With 90 days, the moisture change of subject is observed.As a result such as Fig. 2.
As shown in Figure 2, lotion made from the embodiment of the present invention 1 is remarkably improved the moisture of skin.
The results show, lotion made from the embodiment of the present invention 1 can significantly remove wrinkle of skin, and skin has substantially
Highlight effect, there is the effect of good crease-resistant, de-etiolation, bright color.
The announcement and teaching of book according to the above description, those skilled in the art in the invention can also be to above-mentioned embodiment party
Formula carries out appropriate change and modification.Therefore, the invention is not limited in embodiment disclosed and described above, to this
Some modifications and changes of invention should also be as falling into the scope of the claims of the present invention.In addition, although this specification
In used some specific terms, but these terms are merely for convenience of description, do not form any restrictions to the present invention.
Claims (3)
- A kind of 1. skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction, it is characterised in that including as follows according to The component of mass percentage:Concentration be 1wt% cedarwood essential oil 0.5%, propane diols 2%, glycerine 2%, sodium hyaluronate 0.1%, sodium hydroxy methyl glycinate 0.5%, concentration is 0.1wt% Uruguay's tea extraction 2%, lactic acid 0.25% and water 92.65%;Wherein, the preparation method of the cedarwood essential oil comprises the following steps:(1) take dry cedarwood 500g to crush, be transferred in the 5L fermentation tanks for having added 1500~2500g distilled water, add 0.5% Beef extract, 1% peptone and 0.5% sodium chloride, and adjust pH to 4.5~6.0, spontaneous fermentation with 1mol/L phosphate buffers 36h, then high-temperature inactivation strain;(2) step (1) products therefrom and 1.5~5.0g complex enzyme hydrolysis liquid are sufficiently mixed, at 42~60 DEG C digest 30~ 50min;The complex enzyme hydrolysis liquid is cellulase, hemicellulase and pectase according to 3:1:1~5:1:2 mass ratio mixing Mixture, add water be configured to mass percent be 0.3~0.9% complex enzyme hydrolysis liquid, pH be 4.5~6.0;(3) step (2) products therefrom is isolated and purified using wiped-film still, obtains cedarwood essential oil;The preparation method of Uruguay's tea extraction comprises the following steps:(a) take fresh Uruguay's tea 500g to crush, add 500~1500g distilled water, filled with 1.5~5.0g complex enzyme hydrolysis liquid Divide mixing, 30~50min is digested at 42~60 DEG C, centrifugation obtains digesting head product;The complex enzyme hydrolysis liquid be cellulase, Hemicellulase and pectase are according to 3:1:1~5:1:The mixture of 2 mass ratio mixing, adds water to be configured to mass percent to be 0.3~0.9% complex enzyme hydrolysis liquid, pH are 4.5~6.0;(b) product filtering will be digested obtained by step (a), filter residue is placed in water-bath and extracted, and the volume ratio of filter residue and water is 1:8 ~15, leaching liquor filter cleaner;It is repeated twice, merges leaching liquor;(c) leaching liquor obtained by step (b) is subjected to constant flow filtering in sheet frame, then rotary evaporation is dense under 0.1MPa pressure Contracting, is finally settled to 50g, obtains Uruguay's tea extraction.
- 2. the preparation method of the skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction described in claim 1, it is special Sign is, comprises the following steps:(1) the Uruguay's tea extraction for being 0.1wt% with concentration that concentration is 1wt% is weighed, stirs, obtains arborvitae another name for The mixture of oil and Uruguay's tea extraction;(2) propane diols is weighed, the mixture of cedarwood essential oil and Uruguay's tea extraction obtained by step (1) is added, stirs to clear It is clear bright, obtain mixed material;(3) other components are weighed, step (2) gained mixed material is added after being dissolved with water while stirring, is again stirring for clarification It is transparent, obtain the skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction.
- 3. the skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction described in claim 1 in skin anti-aging and changes Application in the kind colour of skin.
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2017
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CN102258546A (en) * | 2011-04-29 | 2011-11-30 | 李光武 | Aromatic essential oil type medicament for preventing and treating depression and neurosis, boosting mood and improving brain function and composition thereof |
CN104188868A (en) * | 2014-09-09 | 2014-12-10 | 青岛润鑫伟业科贸有限公司 | Compound essential oil capable of increasing energy |
CN104257519A (en) * | 2014-10-10 | 2015-01-07 | 中国热带农业科学院农产品加工研究所 | Pineapple leaf nanocellulose moisturizing skin-whitening washing gel mask and preparation method thereof |
CN105147545A (en) * | 2015-08-31 | 2015-12-16 | 岭南师范学院 | Compound vetiver essential oil and preparation method thereof |
CN105769667A (en) * | 2016-03-18 | 2016-07-20 | 无限极(中国)有限公司 | Lucid ganoderma fermentation liquor preparation method and application of lucid ganoderma fermentation liquor |
CN106389175A (en) * | 2016-09-07 | 2017-02-15 | 广州市澳键丰泽生物科技股份有限公司 | Nourishing and moisturizing lotion containing rose essential oil |
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