CN105147545A - Compound vetiver essential oil and preparation method thereof - Google Patents

Compound vetiver essential oil and preparation method thereof Download PDF

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Publication number
CN105147545A
CN105147545A CN201510546363.XA CN201510546363A CN105147545A CN 105147545 A CN105147545 A CN 105147545A CN 201510546363 A CN201510546363 A CN 201510546363A CN 105147545 A CN105147545 A CN 105147545A
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Prior art keywords
essential oil
oil
caulis miscanthis
miscanthis floriduli
quintessence oil
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CN201510546363.XA
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CN105147545B (en
Inventor
刘金祥
刘锴栋
霍平惠
章武
刘晚苟
肖生鸿
孙余丹
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GUANGDONG JINGCAI INTERNATIONAL BIOTECHNOLOGY Co.,Ltd.
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Lingnan Normal University
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    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
    • A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
    • A61K8/34—Alcohols
    • A61K8/342—Alcohols having more than seven atoms in an unbroken chain
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
    • A61K8/00—Cosmetics or similar toiletry preparations
    • A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
    • A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
    • A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
    • A—HUMAN NECESSITIES
    • A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
    • A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
    • A61Q19/00—Preparations for care of the skin
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/02—Recovery or refining of essential oils from raw materials
    • C11B9/027—Recovery of volatiles by distillation or stripping

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  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Veterinary Medicine (AREA)
  • Public Health (AREA)
  • General Health & Medical Sciences (AREA)
  • Animal Behavior & Ethology (AREA)
  • Birds (AREA)
  • Engineering & Computer Science (AREA)
  • Epidemiology (AREA)
  • Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Organic Chemistry (AREA)
  • Botany (AREA)
  • Microbiology (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Mycology (AREA)
  • Wood Science & Technology (AREA)
  • Biotechnology (AREA)
  • Dermatology (AREA)
  • Emergency Medicine (AREA)
  • Fats And Perfumes (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)
  • Treatments For Attaching Organic Compounds To Fibrous Goods (AREA)
  • Detergent Compositions (AREA)

Abstract

The invention belongs to the technical field of cosmetics and particularly discloses compound vetiver essential oil and a preparation method thereof. The compound vetiver essential oil is composed of, by weight, 77.0%-85.8% of vetiver essential oil, 3-5% of labdanum, 0.2-0.8% of cedar essential oil, 3-5% of geraniol, 3-5% of cananga odorata essential oil and 5-10% of grapefruit essential oil. The compound vetiver essential oil which is mainly made from the vetiver essential oil is a novel essential oil product with addition of the labdanum, the cedar essential oil, the geraniol, the cananga odorata essential oil and the grapefruit essential oil. By means of a great deal of experimental research, adding proportions of components are optimized, and the compound vetiver essential oil is pleasant to smell and capable of calming and soothing the nervous system and has a certain curative effect on insomnia. In addition, the compound vetiver essential oil has an excellent antibacterial function, and stability of the compound vetiver essential oil is greatly improved.

Description

A kind of Caulis Miscanthis floriduli compound essential Oil and preparation method thereof
Technical field
The invention belongs to cosmetic technical field, particularly, relate to a kind of Caulis Miscanthis floriduli compound essential Oil and preparation method thereof.
Background technology
Caulis Miscanthis floriduli is a kind of perennial herb plant of tall and big one-tenth spike, and blade is elongated, and subterraneous root is the lacery of white, multiple-limb, one-tenth complexity.Its Main Cultivation in torrid areas, as India, Tahiti, Java and Haiti.In Calcutta (harbor city of Northeastern India) and Haiti, this grass is used to build banda and do rain cover, parasols; In Java, people weave a mat with its root system and build banda, and it can not only bring graceful fragrance to room, can also repel insects.It is the composition that soap, cosmetics and perfume are conventional, plants this grass and soil can also be prevented to suffer erosion.Caulis Miscanthis floriduli quintessence oil is otherwise known as " quiet oil ", because it has good calm effect, but mostly Caulis Miscanthis floriduli quintessence oil is on the market folk prescription quintessence oil at present, and effect is comparatively single.
Summary of the invention
The present invention is directed to the deficiencies in the prior art, provide a kind of Caulis Miscanthis floriduli compound essential Oil.Described quintessence oil is for main constituent with Caulis Miscanthis floriduli quintessence oil, and be added with a kind of new essential oil product that labdanum, Deodar Cedar (Himalayan Cedar) quintessence oil, geraniol, Cananga odorata quintessence oil and grapefruit essential oil combine, this quintessence oil good smell, energy is calm and console nervous system, relieving stress and buck fever are also beneficial to, have certain curative effect to insomnia; Meanwhile, this quintessence oil also has good antibacterium and fungus effect.
Another object of the present invention is to, the preparation method of above-mentioned Caulis Miscanthis floriduli compound essential Oil is provided.
The present invention is achieved by the following technical programs.
A kind of Caulis Miscanthis floriduli compound essential Oil, is made up of each component of following mass percent: Caulis Miscanthis floriduli quintessence oil 77.0 ~ 85.8%, labdanum 3 ~ 5%, Deodar Cedar (Himalayan Cedar) quintessence oil 0.2 ~ 0.8%, geraniol 3 ~ 5%, Cananga odorata quintessence oil 3 ~ 5%, grapefruit essential oil 5 ~ 10%.
Caulis Miscanthis floriduli quintessence oil is the quintessence oil of a kind of nontoxic, nonirritant and heliosensitivity, is usually applicable to the quintessence oil mixed with Caulis Miscanthis floriduli quintessence oil and comprises grapefruit, jasmine, lavandula angustifolia and Cananga odorata quintessence oil.The present invention not only optimizes the mixed proportion of Caulis Miscanthis floriduli quintessence oil and grapefruit, Cananga odorata quintessence oil, also optimizes and with the addition of labdanum, Deodar Cedar (Himalayan Cedar) quintessence oil and geraniol.
Caulis Miscanthis floriduli quintessence oil has deep Earthy Taste, slightly smoke; Deodar Cedar (Himalayan Cedar) quintessence oil has soft wood breath, implies lighter sandalwood odors, can well in and Caulis Miscanthis floriduli quintessence oil smoke.Meanwhile, in Caulis Miscanthis floriduli quintessence oil, add Deodar Cedar (Himalayan Cedar) quintessence oil, this essential oil product more contributes to alleviating the emotion of angry, abnormal excitement and irritability than folk prescription quintessence oil, is also beneficial to relieving stress and buck fever.Inventor finds after lot of experiments in addition, Caulis Miscanthis floriduli quintessence oil, Deodar Cedar (Himalayan Cedar) quintessence oil and geraniol are mixed according to specific ratio, Synergistic antimicrobial, anti-infectious function can be played, thus the antibiotic effect of the composite essential oil product finally obtained is significantly improved, and substantially prolongs the stability of composite essential oil product, extended shelf-life.
Preferably, described compound essential Oil is made up of each component of following mass percent: Caulis Miscanthis floriduli quintessence oil 77.0 ~ 80.0%, labdanum 5%, Deodar Cedar (Himalayan Cedar) quintessence oil 0.6 ~ 0.8%, geraniol 3 ~ 4%, Cananga odorata quintessence oil 4 ~ 4.2%, grapefruit essential oil 6.4 ~ 10%.
Preferably, described Caulis Miscanthis floriduli quintessence oil is be that raw material obtains through distillation, condensation and separation with Caulis Miscanthis floriduli.
The present invention also provides a kind of preparation method of above-mentioned Caulis Miscanthis floriduli compound essential Oil, comprises the steps:
S1. the preparation of Caulis Miscanthis floriduli quintessence oil: carried out cleaning, pulverize, dry and soaking by Caulis Miscanthis floriduli, is undertaken distilling by the clean Caulis Miscanthis floriduli of immersion, condensation and oil-water separation, obtains Caulis Miscanthis floriduli quintessence oil;
S2. proportionally Caulis Miscanthis floriduli quintessence oil is mixed with labdanum, Deodar Cedar (Himalayan Cedar) quintessence oil, geraniol, Cananga odorata quintessence oil and grapefruit essential oil, obtain the mixed liquor before quintessence oil extraction;
S3. S2 gained mixed liquor is obtained described Caulis Miscanthis floriduli compound essential Oil product after second distillation, condenser condenses, secondary oil-water separation.
Preferably, its preparation method comprises the steps:
S1. Caulis Miscanthis floriduli is carried out cleaning, mince, dry and soaking, will clean Caulis Miscanthis floriduli distillation be soaked; After distillation a period of time, collect the oil-water mixture in condensing tube, recycling oil water separator, separately deposits Caulis Miscanthis floriduli quintessence oil and hydrosol, obtains Caulis Miscanthis floriduli quintessence oil;
S2. proportionally add labdanum, Deodar Cedar (Himalayan Cedar) quintessence oil, geraniol, Cananga odorata quintessence oil, grapefruit essential oil, obtain the mixed liquor before quintessence oil extraction;
S3. mixed liquor is carried out fast-open type second distillation, distill while stirring, by condenser condenses, cooler cooling, then carry out secondary oil-water separation, finally obtain Caulis Miscanthis floriduli compound essential Oil product.
Said method due to heating surface (area) (HS large, firing rate is fast, after mixed liquor is heated, stirring makes thermal response carry out under dynamic situation, do not have influence on the inherent quality of Caulis Miscanthis floriduli, maintain the original character of Caulis Miscanthis floriduli, after adopting secondary oil-water separation, oil is thoroughly separated with water, improves the quality of Caulis Miscanthis floriduli quintessence oil, output and purity.
During use, Caulis Miscanthis floriduli compound essential Oil product of the present invention can be applied on human body skin, and massage gently.
Compared with prior art, beneficial effect of the present invention is: described compound essential Oil is with Caulis Miscanthis floriduli quintessence oil for main constituent, and is added with a kind of new essential oil product that labdanum, Deodar Cedar (Himalayan Cedar) quintessence oil, geraniol, Cananga odorata quintessence oil and grapefruit essential oil combine.Inventor, through lot of experiments, optimizes the adding proportion of each component, this quintessence oil good smell, and energy is calm and console nervous system, is also beneficial to, has certain curative effect to insomnia to relieving stress and buck fever; Meanwhile, this quintessence oil also has good antibacterial action, the stability also significant prolongation of essential oil product.
Detailed description of the invention
Below in conjunction with specific embodiment, the present invention is described in further details, but embodiment does not limit in any form the present invention.Unless stated otherwise, the present invention adopts reagent, method and apparatus are the art conventional reagent, method and apparatus.
embodiment 1
The present embodiment provides a kind of Caulis Miscanthis floriduli compound essential Oil, is made up of: Caulis Miscanthis floriduli quintessence oil 77%, labdanum 5%, Deodar Cedar (Himalayan Cedar) quintessence oil 0.8%, geraniol 3%, Cananga odorata quintessence oil 4.2%, grapefruit essential oil 10% each component of following mass percent.
The preparation method of above-mentioned Caulis Miscanthis floriduli compound essential Oil comprises the steps:
S1. Caulis Miscanthis floriduli is carried out cleaning, mince, dry and soaking, the clean Caulis Miscanthis floriduli of immersion is put into boiler distill, the derived essential oil of Caulis Miscanthis floriduli internal memory evaporates along with steam, and along with steam is by the condensing tube above boiler, finally introduces in condenser; Condenser makes steam cool and is converted into oil-water mixture, then flows into oil water separator; The oil lighter than water can be kept afloat, and the oil heavier than water will sink to the water bottom, and remaining water is exactly hydrosol; Then further Caulis Miscanthis floriduli quintessence oil and hydrosol are separately deposited with separatory funnel, thus obtain Caulis Miscanthis floriduli quintessence oil;
S2. labdanum, Deodar Cedar (Himalayan Cedar) quintessence oil, geraniol, Cananga odorata quintessence oil, grapefruit essential oil added in the Caulis Miscanthis floriduli quintessence oil that S1 obtains by said ratio, obtain the mixed liquor before quintessence oil extraction;
S3. mixed liquor is inserted in fast-open type alembic, then steam is passed in the chuck of fast-open type alembic, heat while stirring in fast-open type alembic with agitating device, the steam produced in fast-open type alembic is after the second distillation of distillation column, by condenser condenses, cooler cooling, carry out secondary oil-water separation again, finally obtain Caulis Miscanthis floriduli compound essential Oil product.
embodiment 2
The present embodiment provides a kind of Caulis Miscanthis floriduli compound essential Oil, is made up of: Caulis Miscanthis floriduli quintessence oil 80%, labdanum 5%, Deodar Cedar (Himalayan Cedar) quintessence oil 0.6%, geraniol 4%, Cananga odorata quintessence oil 4%, grapefruit essential oil 6.4% each component of following mass percent.
The preparation method of above-mentioned Caulis Miscanthis floriduli compound essential Oil is identical with the preparation method of embodiment 1.
embodiment 3
The present embodiment provides a kind of Caulis Miscanthis floriduli compound essential Oil, is made up of: Caulis Miscanthis floriduli quintessence oil 85.8%, labdanum 3%, Deodar Cedar (Himalayan Cedar) quintessence oil 0.2%, geraniol 3%, Cananga odorata quintessence oil 3%, grapefruit essential oil 5% each component of following mass percent.
The preparation method of above-mentioned Caulis Miscanthis floriduli compound essential Oil is identical with the preparation method of embodiment 1.
embodiment 4
The present embodiment provides a kind of Caulis Miscanthis floriduli compound essential Oil, is made up of: Caulis Miscanthis floriduli quintessence oil 77.6%, labdanum 4%, Deodar Cedar (Himalayan Cedar) quintessence oil 0.4%, geraniol 5%, Cananga odorata quintessence oil 5%, grapefruit essential oil 8% each component of following mass percent.
The preparation method of above-mentioned Caulis Miscanthis floriduli compound essential Oil is identical with the preparation method of embodiment 1.
comparative example 1
This comparative example provides a kind of Caulis Miscanthis floriduli compound essential Oil, is made up of: Caulis Miscanthis floriduli quintessence oil 77%, labdanum 5%, geraniol 3.8%, Cananga odorata quintessence oil 4.2%, grapefruit essential oil 10% each component of following mass percent.
Without Deodar Cedar (Himalayan Cedar) essential oil component in above-mentioned Caulis Miscanthis floriduli compound essential Oil, its preparation method is identical with the preparation method of embodiment 1.
comparative example 2
This comparative example provides a kind of Caulis Miscanthis floriduli compound essential Oil, is made up of: Caulis Miscanthis floriduli quintessence oil 77%, labdanum 5%, Deodar Cedar (Himalayan Cedar) quintessence oil 3.8%, Cananga odorata quintessence oil 4.2%, grapefruit essential oil 10% each component of following mass percent.
Without geraniol component in above-mentioned Caulis Miscanthis floriduli compound essential Oil, and the percentage composition of Deodar Cedar (Himalayan Cedar) quintessence oil is higher, and its preparation method is identical with the preparation method of embodiment 1.
comparative example 3
This comparative example provides a kind of Caulis Miscanthis floriduli compound essential Oil, is made up of: Caulis Miscanthis floriduli quintessence oil 70%, labdanum 5%, Deodar Cedar (Himalayan Cedar) quintessence oil 3.3%, geraniol 7.5%, Cananga odorata quintessence oil 4.2%, grapefruit essential oil 10% each component of following mass percent.
Caulis Miscanthis floriduli quintessence oil in above-mentioned Caulis Miscanthis floriduli compound essential Oil, Deodar Cedar (Himalayan Cedar) quintessence oil and geraniol quintessence oil mass percentage be not in the framework of the present definition, and its preparation method is identical with the preparation method of embodiment 1.
application examples 1
By the Caulis Miscanthis floriduli compound essential Oil of the embodiment of the present invention 1 ~ 4 and comparative example 1 ~ 3, carry out fill with dark brown vial, be uncoveredly placed in 30 DEG C, under the environment of relative humidity 85%, continuous observation, concrete outcome sees the following form.
The stability test table of table 1 Caulis Miscanthis floriduli compound essential Oil product
Note: become sour: product becomes sour, gives out unhappy abnormal smells from the patient.Normal: product no abnormality seen, fragrance is pure.
From data in table, the uncork shelf-life of Caulis Miscanthis floriduli compound essential Oil of the present invention is longer; When lack in comparative example Deodar Cedar (Himalayan Cedar) quintessence oil, geraniol or Caulis Miscanthis floriduli quintessence oil, Deodar Cedar (Himalayan Cedar) quintessence oil and geraniol quintessence oil mass percentage not in the framework of the present definition time, not only the fragrance of this essential oil product is not so good as the quintessence oil of embodiment, and product is more easily corrupt.Illustrate between quintessence oil of the present invention and quintessence oil it is mutual coordination, complement each other in addition each other, the effect heightened the effect of a treatment.
application examples 2
Use one month continuously to 100 bit test persons the product of the embodiment of the present invention 1 ~ 4, total effective rate is 80%, and tester uses rear insomnia and nervous there is a change for the better.

Claims (4)

1. a Caulis Miscanthis floriduli compound essential Oil, is characterized in that, is made up of: Caulis Miscanthis floriduli quintessence oil 77.0 ~ 85.8%, labdanum 3 ~ 5%, Deodar Cedar (Himalayan Cedar) quintessence oil 0.2 ~ 0.8%, geraniol 3 ~ 5%, Cananga odorata quintessence oil 3 ~ 5%, grapefruit essential oil 5 ~ 10% each component of following mass percent.
2. Caulis Miscanthis floriduli compound essential Oil according to claim 1, is characterized in that, is made up of: Caulis Miscanthis floriduli quintessence oil 77.0 ~ 80.0% each component of following mass percent, labdanum 5%, Deodar Cedar (Himalayan Cedar) quintessence oil 0.6 ~ 0.8%, geraniol 3 ~ 4%, Cananga odorata quintessence oil 4 ~ 4.2%, grapefruit essential oil 6.4 ~ 10%.
3. Caulis Miscanthis floriduli compound essential Oil according to claim 1, is characterized in that, described Caulis Miscanthis floriduli quintessence oil is be that raw material obtains through distillation, condensation and separation with Caulis Miscanthis floriduli.
4. a preparation method for Caulis Miscanthis floriduli compound essential Oil described in any one of claim 1 ~ 3, is characterized in that, comprise the steps:
S1. the preparation of Caulis Miscanthis floriduli quintessence oil: carried out cleaning, pulverize, dry and soaking by Caulis Miscanthis floriduli, is undertaken distilling by the clean Caulis Miscanthis floriduli of immersion, condensation and oil-water separation, obtains Caulis Miscanthis floriduli quintessence oil;
S2. proportionally Caulis Miscanthis floriduli quintessence oil is mixed with labdanum, Deodar Cedar (Himalayan Cedar) quintessence oil, geraniol, Cananga odorata quintessence oil and grapefruit essential oil, obtain the mixed liquor before quintessence oil extraction;
S3. S2 gained mixed liquor is obtained described Caulis Miscanthis floriduli compound essential Oil product after second distillation, condenser condenses, secondary oil-water separation.
CN201510546363.XA 2015-08-31 2015-08-31 A kind of vetiver compound essential oil and preparation method thereof Active CN105147545B (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107375057A (en) * 2017-06-30 2017-11-24 广州市澳键丰泽生物科技股份有限公司 A kind of skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103418079A (en) * 2013-08-06 2013-12-04 汪辉 Purifier combining aromatic therapy and salt therapy
CN104306248A (en) * 2014-09-30 2015-01-28 青岛康合伟业商贸有限公司 Perfume for men

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103418079A (en) * 2013-08-06 2013-12-04 汪辉 Purifier combining aromatic therapy and salt therapy
CN104306248A (en) * 2014-09-30 2015-01-28 青岛康合伟业商贸有限公司 Perfume for men

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107375057A (en) * 2017-06-30 2017-11-24 广州市澳键丰泽生物科技股份有限公司 A kind of skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction

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