CN105147545B - A kind of vetiver compound essential oil and preparation method thereof - Google Patents
A kind of vetiver compound essential oil and preparation method thereof Download PDFInfo
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- CN105147545B CN105147545B CN201510546363.XA CN201510546363A CN105147545B CN 105147545 B CN105147545 B CN 105147545B CN 201510546363 A CN201510546363 A CN 201510546363A CN 105147545 B CN105147545 B CN 105147545B
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- essential oil
- vetiver
- oil
- compound
- cedarwood
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/30—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds
- A61K8/33—Cosmetics or similar toiletry preparations characterised by the composition containing organic compounds containing oxygen
- A61K8/34—Alcohols
- A61K8/342—Alcohols having more than seven atoms in an unbroken chain
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61K—PREPARATIONS FOR MEDICAL, DENTAL OR TOILETRY PURPOSES
- A61K8/00—Cosmetics or similar toiletry preparations
- A61K8/18—Cosmetics or similar toiletry preparations characterised by the composition
- A61K8/96—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution
- A61K8/97—Cosmetics or similar toiletry preparations characterised by the composition containing materials, or derivatives thereof of undetermined constitution from algae, fungi, lichens or plants; from derivatives thereof
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- A—HUMAN NECESSITIES
- A61—MEDICAL OR VETERINARY SCIENCE; HYGIENE
- A61Q—SPECIFIC USE OF COSMETICS OR SIMILAR TOILETRY PREPARATIONS
- A61Q19/00—Preparations for care of the skin
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
- C11B9/027—Recovery of volatiles by distillation or stripping
Abstract
The invention belongs to cosmetic technical field, specifically discloses a kind of vetiver compound essential oil and preparation method thereof.The vetiver compound essential oil is made up of each component of following mass percent：Vetiver essential oil 77.0% ~ 85.8%, labdanum 3 ~ 5%, cedarwood essential oil 0.2 ~ 0.8%, geraniol 3 ~ 5%, Cananga odorata quintessence oil 3 ~ 5%, grapefruit essential oil 5 ~ 10%.The compound essential oil is and a kind of new essential oil product combined added with labdanum, cedarwood essential oil, geraniol, Cananga odorata quintessence oil and grapefruit essential oil using vetiver essential oil as principal component.Inventor passes through lot of experiments, optimizes the adding proportion of each component, the essential oil good smell, and energy is calm and consoles nervous system, has certain curative effect to insomnia；Meanwhile the essential oil also has good antibacterial action, the stability of essential oil product significantly extends.
Description
Technical field
The invention belongs to cosmetic technical field, in particular it relates to a kind of vetiver compound essential oil and preparation method thereof.
Background technology
Vetiver is a kind of tall and big perennial herb plant into spike, and blade is elongated, and underground root system is white, more points
Branch, the lacery into complexity.Its Main Cultivation is in torrid areas, such as India, Tahiti, Java and Haiti.In Calcutta
（The harbor city of Northeastern India）And Haiti, this grass be used to build banda and do rain cover, parasols；In Java, Ren Menshi
Banda is woven a mat and built with its root system, and it can not only carry out graceful fragrance to interatrial band, moreover it is possible to repellent insect.It is
The conventional composition of soap, cosmetics and perfume, plants this grass and can also prevent soil and suffer erosion.Vetiver essential oil is claimed again
For " quiet oil ", because it has good calm effect, however, vetiver essential oil on the market is mostly folk prescription essential oil at present,
Effect is more single.
The content of the invention
In view of the deficiencies of the prior art, the present invention provides a kind of vetiver compound essential oil.The essential oil is with vetiver
Essential oil is principal component, and one combined added with labdanum, cedarwood essential oil, geraniol, Cananga odorata quintessence oil and grapefruit essential oil
The new essential oil product of kind, the essential oil good smell, energy is calm and consoles nervous system, also has to alleviating pressure and buck fever
Place, there is certain curative effect to insomnia；Meanwhile also there is the essential oil good antibacterium and fungi to act on.
Another object of the present invention is to, there is provided the preparation method of above-mentioned vetiver compound essential oil.
The present invention is achieved by the following technical programs.
A kind of vetiver compound essential oil, is made up of each component of following mass percent：Vetiver essential oil 77.0 ~ 85.8%,
Labdanum 3 ~ 5%, cedarwood essential oil 0.2 ~ 0.8%, geraniol 3 ~ 5%, Cananga odorata quintessence oil 3 ~ 5%, grapefruit essential oil 5 ~ 10%.
Vetiver essential oil is a kind of nontoxic, nonirritant and light sensitivity essential oil, generally is suitable for mixed with vetiver essential oil
Essential oil include grape fruit, jasmine, lavender and Cananga odorata quintessence oil.The present invention not only optimize vetiver essential oil and grape fruit, according to
The mixed proportion of Lenzin oil, also optimization with the addition of labdanum, cedarwood essential oil and geraniol.
Vetiver essential oil has deep Earthy Taste, slightly smoke；Cedarwood essential oil has soft wood breath, implies
Thin sandalwood odors, vetiver essential oil smoke can be neutralized well.Meanwhile add cedarwood into vetiver essential oil
Essential oil, the essential oil product is more conducive to alleviate angry, abnormal excited and irritability mood than folk prescription essential oil, to alleviating pressure
Also it is beneficial to buck fever.Other inventor has found after lot of experiments, by vetiver essential oil, cedarwood essential oil and
Geraniol mixes according to specific ratio, can play Synergistic antimicrobial, anti-infectious function, so that the composite precision finally given
The antibiotic effect of oil product significantly improves, and substantially prolongs the stability of composite essential oil product, extended shelf-life.
Preferably, the compound essential oil is made up of each component of following mass percent：Vetiver essential oil 77.0 ~ 80.0%,
Labdanum 5%, cedarwood essential oil 0.6 ~ 0.8%, geraniol 3 ~ 4%, Cananga odorata quintessence oil 4 ~ 4.2%, grapefruit essential oil 6.4 ~ 10%.
Preferably, the vetiver essential oil is through distilling, condensing and isolated by raw material of vetiver.
The present invention also provides a kind of preparation method of above-mentioned vetiver compound essential oil, comprises the following steps：
S1. the preparation of vetiver essential oil：Vetiver is cleaned, crushed, dried and soaked, clean perfume (or spice) will be soaked
Root grass distilled, is condensed and water-oil separating, obtains vetiver essential oil；
S2. proportionally by vetiver essential oil and labdanum, cedarwood essential oil, geraniol, Cananga odorata quintessence oil and grape fruit essence
Oil mixing, obtain the mixed liquor before essential oil extraction；
S3. mixed liquor obtained by S2 is obtained into the vetiver after second distillation, condenser condensation, two level water-oil separating
Compound essential oil product.
Preferably, its preparation method comprises the following steps：
S1. vetiver cleaned, minced, dried and soaked, clean vetiver will be soaked and distilled；One section of distillation
After time, the oil-water mixture in condenser pipe is collected, oil water separator is recycled, vetiver essential oil and hydrosol is separately deposited,
Obtain vetiver essential oil；
S2. labdanum, cedarwood essential oil, geraniol, Cananga odorata quintessence oil, grapefruit essential oil are proportionally added, obtains essential oil
Mixed liquor before extraction；
S3. by mixed liquor carry out fast-open type second distillation, distill while stirring, condensed by condenser, cooler it is cold
But, then two level water-oil separating is carried out, finally obtains vetiver compound essential oil product.
For the above method because heating surface (area) (HS is big, firing rate is fast, and after mixed liquor is heated, stirring makes thermal response in dynamic situation
Lower progress, without influence on the inherent quality of vetiver, the original property of vetiver is maintained, after two level water-oil separating,
Oil is completely separated with water, improve the quality, yield and purity of vetiver essential oil.
In use, the vetiver compound essential oil product of the present invention can be applied on human body skin, and gently massage.
Compared with prior art, beneficial effect of the present invention is：The compound essential oil be using vetiver essential oil as principal component,
A kind of and new essential oil production combined added with labdanum, cedarwood essential oil, geraniol, Cananga odorata quintessence oil and grapefruit essential oil
Product.Inventor passes through lot of experiments, optimizes the adding proportion of each component, the essential oil good smell, and energy is calm and consoles
Nervous system, is also beneficial to alleviating pressure and buck fever, has certain curative effect to insomnia；Meanwhile the essential oil also has well
Antibacterial action, the stability of essential oil product also significantly extends.
Embodiment
The present invention is described in further details with reference to specific embodiment, but embodiment the present invention is not done it is any
The restriction of form.Unless stated otherwise, the reagent of the invention used, method and apparatus is the art conventional reagent, methods
And equipment.
Embodiment 1
The present embodiment provides a kind of vetiver compound essential oil, is made up of each component of following mass percent：Vetiver essence
Oil 77%, labdanum 5%, cedarwood essential oil 0.8%, geraniol 3%, Cananga odorata quintessence oil 4.2%, grapefruit essential oil 10%.
The preparation method of above-mentioned vetiver compound essential oil comprises the following steps：
S1. vetiver cleaned, minced, dried and soaked, the vetiver for soaking clean is put into boiler and steamed
Evaporating, the derived essential oil of vetiver internal memory evaporates with vapor, and as vapor is by the condenser pipe above boiler, most
Introduce afterwards in condenser；Condenser makes steam cooling be converted into oil-water mixture, then flows into oil water separator；The oil lighter than water
It can keep afloat, the oil than water weight will sink to the water bottom, and remaining water is exactly hydrosol；Then with separatory funnel further perfume (or spice)
Root grass essential oil and hydrosol are separately deposited, so as to obtain vetiver essential oil；
S2. labdanum, cedarwood essential oil, geraniol, Cananga odorata quintessence oil, grapefruit essential oil are added S1 and obtained by said ratio
To vetiver essential oil in, obtain essential oil extraction before mixed liquor；
S3. mixed liquor is inserted in fast-open type alembic, be then passed through steam in the chuck of fast-open type alembic, used
Agitating device is heated while stirring in fast-open type alembic, and caused steam is by distillation column in fast-open type alembic
After second distillation, condensed by condenser, cooler cooling, then carry out two level water-oil separating, finally obtain vetiver compound essence
Oil product.
Embodiment 2
The present embodiment provides a kind of vetiver compound essential oil, is made up of each component of following mass percent：Vetiver essence
Oil 80%, labdanum 5%, cedarwood essential oil 0.6%, geraniol 4%, Cananga odorata quintessence oil 4%, grapefruit essential oil 6.4%.
The preparation method of above-mentioned vetiver compound essential oil is identical with the preparation method of embodiment 1.
Embodiment 3
The present embodiment provides a kind of vetiver compound essential oil, is made up of each component of following mass percent：Vetiver essence
Oil 85.8%, labdanum 3%, cedarwood essential oil 0.2%, geraniol 3%, Cananga odorata quintessence oil 3%, grapefruit essential oil 5%.
The preparation method of above-mentioned vetiver compound essential oil is identical with the preparation method of embodiment 1.
Embodiment 4
The present embodiment provides a kind of vetiver compound essential oil, is made up of each component of following mass percent：Vetiver essence
Oil 77.6%, labdanum 4%, cedarwood essential oil 0.4%, geraniol 5%, Cananga odorata quintessence oil 5%, grapefruit essential oil 8%.
The preparation method of above-mentioned vetiver compound essential oil is identical with the preparation method of embodiment 1.
Comparative example 1
This comparative example provides a kind of vetiver compound essential oil, is made up of each component of following mass percent：Vetiver essence
Oil 77%, labdanum 5%, geraniol 3.8%, Cananga odorata quintessence oil 4.2%, grapefruit essential oil 10%.
Without cedarwood essential oil component, its preparation method and the preparation method phase of embodiment 1 in above-mentioned vetiver compound essential oil
Together.
Comparative example 2
This comparative example provides a kind of vetiver compound essential oil, is made up of each component of following mass percent：Vetiver essence
Oil 77%, labdanum 5%, cedarwood essential oil 3.8%, Cananga odorata quintessence oil 4.2%, grapefruit essential oil 10%.
Without spiceleaf alkoxide component in above-mentioned vetiver compound essential oil, and the percentage composition of cedarwood essential oil is higher, its preparation side
Method is identical with the preparation method of embodiment 1.
Comparative example 3
This comparative example provides a kind of vetiver compound essential oil, is made up of each component of following mass percent：Vetiver essence
Oil 70%, labdanum 5%, cedarwood essential oil 3.3%, geraniol 7.5%, Cananga odorata quintessence oil 4.2%, grapefruit essential oil 10%.
Vetiver essential oil, cedarwood essential oil and spiceleaf ether oil weight/mass percentage composition in above-mentioned vetiver compound essential oil are not
In the framework of the present definition, its preparation method is identical with the preparation method of embodiment 1.
Application examples 1
By the vetiver compound essential oil of the embodiment of the present invention 1 ~ 4 and comparative example 1 ~ 3, carried out with dark brown vial it is filling,
Opening is placed in 30 DEG C, in the environment of relative humidity 85%, and continuous observation, concrete outcome see the table below.
The stability test table of the vetiver compound essential oil product of table 1
Note：Become sour：Product becomes sour, and gives out unhappy smell.Normally：Product no abnormality seen, fragrance are pure.
From data in table, the corkage shelf-life of vetiver compound essential oil of the present invention is longer；When lacking perfume (or spice) in comparative example
Cypress ethereal oil, geraniol or vetiver essential oil, cedarwood essential oil and spiceleaf ether oil weight/mass percentage composition do not limit in the present invention
In the range of when, not only the fragrance of the essential oil product is not so good as the essential oil of embodiment, and product is more easy to corruption.Illustrate essence of the invention
It is mutually coordinated between oil and essential oil, also has complement each other each other, the effect to heighten the effect of a treatment.
Application examples 2
The product of the embodiment of the present invention 1 ~ 4 is used continuously one month to 100 bit test persons, total effective rate 80%, test
Insomnia and nervous there is a change for the better after person's use.
Claims (4)
1. a kind of vetiver compound essential oil, it is characterised in that be made up of each component of following mass percent：Vetiver essential oil
77.0 ~ 85.8%, labdanum 3 ~ 5%, cedarwood essential oil 0.2 ~ 0.8%, geraniol 3 ~ 5%, Cananga odorata quintessence oil 3 ~ 5%, grapefruit essential oil 5 ~
10%。
2. vetiver compound essential oil according to claim 1, it is characterised in that be grouped by each group of following mass percent
Into：Vetiver essential oil 77.0 ~ 80.0%, labdanum 5%, cedarwood essential oil 0.6 ~ 0.8%, geraniol 3 ~ 4%, Cananga odorata quintessence oil 4 ~
4.2%, grapefruit essential oil 6.4 ~ 10%.
3. vetiver compound essential oil according to claim 1, it is characterised in that the vetiver essential oil be using vetiver as
Raw material is through distilling, condensing and isolated.
4. the preparation method of any one of a kind of claim 1 ~ 3 vetiver compound essential oil, it is characterised in that including following step
Suddenly：
S1. the preparation of vetiver essential oil：Vetiver is cleaned, crushed, dried and soaked, clean vetiver will be soaked
Distilled, condensed and water-oil separating, obtain vetiver essential oil；
S2. proportionally vetiver essential oil and labdanum, cedarwood essential oil, geraniol, Cananga odorata quintessence oil and grapefruit essential oil are mixed
Close, obtain the mixed liquor before essential oil extraction；
S3. mixed liquor obtained by S2 is obtained into the vetiver compound after second distillation, condenser condensation, two level water-oil separating
Essential oil product.
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| Application Number | Priority Date | Filing Date | Title |
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| CN201510546363.XA CN105147545B (en) | 2015-08-31 | 2015-08-31 | A kind of vetiver compound essential oil and preparation method thereof |
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| CN201510546363.XA CN105147545B (en) | 2015-08-31 | 2015-08-31 | A kind of vetiver compound essential oil and preparation method thereof |
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| CN105147545A CN105147545A (en) | 2015-12-16 |
| CN105147545B true CN105147545B (en) | 2018-02-16 |
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| CN107375057A (en) * | 2017-06-30 | 2017-11-24 | 广州市澳键丰泽生物科技股份有限公司 | A kind of skin-moisturizing, skin water containing cedarwood essential oil and Uruguay's tea extraction |
Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103418079A (en) * | 2013-08-06 | 2013-12-04 | 汪辉 | Purifier combining aromatic therapy and salt therapy |
| CN104306248A (en) * | 2014-09-30 | 2015-01-28 | 青岛康合伟业商贸有限公司 | Perfume for men |
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Patent Citations (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103418079A (en) * | 2013-08-06 | 2013-12-04 | 汪辉 | Purifier combining aromatic therapy and salt therapy |
| CN104306248A (en) * | 2014-09-30 | 2015-01-28 | 青岛康合伟业商贸有限公司 | Perfume for men |
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Effective date of registration: 20210208 Address after: 516100 Huizhou, Boluo, Guangdong Province Yang Yang Qiao Town, South East Road Patentee after: GUANGDONG JINGCAI INTERNATIONAL BIOTECHNOLOGY Co.,Ltd. Address before: 524048 Guangdong Province, Zhanjiang city Chikan District Road No. 29. Patentee before: LINGNAN NORMAL University |