CN106174683A - A kind of compositions and the tobacco juice for electronic smoke containing said composition - Google Patents
A kind of compositions and the tobacco juice for electronic smoke containing said composition Download PDFInfo
- Publication number
- CN106174683A CN106174683A CN201610609456.7A CN201610609456A CN106174683A CN 106174683 A CN106174683 A CN 106174683A CN 201610609456 A CN201610609456 A CN 201610609456A CN 106174683 A CN106174683 A CN 106174683A
- Authority
- CN
- China
- Prior art keywords
- percent
- tea
- wuyi
- extract
- rock tea
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000000203 mixture Substances 0.000 title claims abstract description 46
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 9
- 235000011389 fruit/vegetable juice Nutrition 0.000 title claims abstract description 7
- 239000000779 smoke Substances 0.000 title abstract description 4
- 241000208125 Nicotiana Species 0.000 title abstract 3
- 239000000284 extract Substances 0.000 claims abstract description 78
- 239000003571 electronic cigarette Substances 0.000 claims abstract description 75
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 43
- 239000000469 ethanolic extract Substances 0.000 claims abstract description 6
- 241001122767 Theaceae Species 0.000 claims description 159
- 239000011435 rock Substances 0.000 claims description 99
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 63
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims description 48
- 239000007788 liquid Substances 0.000 claims description 44
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 claims description 33
- 238000000605 extraction Methods 0.000 claims description 27
- 239000000243 solution Substances 0.000 claims description 24
- 238000004821 distillation Methods 0.000 claims description 23
- 239000000341 volatile oil Substances 0.000 claims description 20
- 238000002156 mixing Methods 0.000 claims description 17
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims description 15
- 235000019504 cigarettes Nutrition 0.000 claims description 13
- 235000020230 cinnamon extract Nutrition 0.000 claims description 12
- 238000001914 filtration Methods 0.000 claims description 12
- OOCCDEMITAIZTP-QPJJXVBHSA-N (E)-cinnamyl alcohol Chemical compound OC\C=C\C1=CC=CC=C1 OOCCDEMITAIZTP-QPJJXVBHSA-N 0.000 claims description 10
- LCZUOKDVTBMCMX-UHFFFAOYSA-N 2,5-Dimethylpyrazine Chemical compound CC1=CN=C(C)C=N1 LCZUOKDVTBMCMX-UHFFFAOYSA-N 0.000 claims description 10
- DBZAKQWXICEWNW-UHFFFAOYSA-N 2-acetylpyrazine Chemical compound CC(=O)C1=CN=CC=N1 DBZAKQWXICEWNW-UHFFFAOYSA-N 0.000 claims description 10
- XPCTZQVDEJYUGT-UHFFFAOYSA-N 3-hydroxy-2-methyl-4-pyrone Chemical compound CC=1OC=CC(=O)C=1O XPCTZQVDEJYUGT-UHFFFAOYSA-N 0.000 claims description 10
- ISAOCJYIOMOJEB-UHFFFAOYSA-N benzoin Chemical compound C=1C=CC=CC=1C(O)C(=O)C1=CC=CC=C1 ISAOCJYIOMOJEB-UHFFFAOYSA-N 0.000 claims description 10
- JOZKFWLRHCDGJA-UHFFFAOYSA-N citronellol acetate Chemical compound CC(=O)OCCC(C)CCC=C(C)C JOZKFWLRHCDGJA-UHFFFAOYSA-N 0.000 claims description 10
- IDGUHHHQCWSQLU-UHFFFAOYSA-N ethanol;hydrate Chemical compound O.CCO IDGUHHHQCWSQLU-UHFFFAOYSA-N 0.000 claims description 10
- MMXKVMNBHPAILY-UHFFFAOYSA-N ethyl laurate Chemical compound CCCCCCCCCCCC(=O)OCC MMXKVMNBHPAILY-UHFFFAOYSA-N 0.000 claims description 10
- CDOSHBSSFJOMGT-UHFFFAOYSA-N linalool Chemical compound CC(C)=CCCC(C)(O)C=C CDOSHBSSFJOMGT-UHFFFAOYSA-N 0.000 claims description 10
- 238000001256 steam distillation Methods 0.000 claims description 10
- IAEGWXHKWJGQAZ-UHFFFAOYSA-N trimethylpyrazine Chemical compound CC1=CN=C(C)C(C)=N1 IAEGWXHKWJGQAZ-UHFFFAOYSA-N 0.000 claims description 10
- 239000000796 flavoring agent Substances 0.000 claims description 9
- 235000019634 flavors Nutrition 0.000 claims description 9
- 235000017803 cinnamon Nutrition 0.000 claims description 8
- 238000000034 method Methods 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 8
- 235000015197 apple juice Nutrition 0.000 claims description 7
- 239000000463 material Substances 0.000 claims description 7
- 238000002360 preparation method Methods 0.000 claims description 7
- 239000000126 substance Substances 0.000 claims description 7
- 244000061176 Nicotiana tabacum Species 0.000 claims description 6
- MTHSVFCYNBDYFN-UHFFFAOYSA-N diethylene glycol Chemical compound OCCOCCO MTHSVFCYNBDYFN-UHFFFAOYSA-N 0.000 claims description 6
- 239000010502 orange oil Substances 0.000 claims description 6
- 238000010992 reflux Methods 0.000 claims description 6
- CRDAMVZIKSXKFV-FBXUGWQNSA-N (2-cis,6-cis)-farnesol Chemical compound CC(C)=CCC\C(C)=C/CC\C(C)=C/CO CRDAMVZIKSXKFV-FBXUGWQNSA-N 0.000 claims description 5
- 239000000260 (2E,6E)-3,7,11-trimethyldodeca-2,6,10-trien-1-ol Substances 0.000 claims description 5
- 239000001490 (3R)-3,7-dimethylocta-1,6-dien-3-ol Substances 0.000 claims description 5
- CDOSHBSSFJOMGT-JTQLQIEISA-N (R)-linalool Natural products CC(C)=CCC[C@@](C)(O)C=C CDOSHBSSFJOMGT-JTQLQIEISA-N 0.000 claims description 5
- 239000001934 2,5-dimethylpyrazine Substances 0.000 claims description 5
- WLJVXDMOQOGPHL-PPJXEINESA-N 2-phenylacetic acid Chemical compound O[14C](=O)CC1=CC=CC=C1 WLJVXDMOQOGPHL-PPJXEINESA-N 0.000 claims description 5
- JOZKFWLRHCDGJA-LLVKDONJSA-N Citronellyl acetate Natural products CC(=O)OCC[C@H](C)CCC=C(C)C JOZKFWLRHCDGJA-LLVKDONJSA-N 0.000 claims description 5
- 235000005976 Citrus sinensis Nutrition 0.000 claims description 5
- 240000002319 Citrus sinensis Species 0.000 claims description 5
- YIKYNHJUKRTCJL-UHFFFAOYSA-N Ethyl maltol Chemical compound CCC=1OC=CC(=O)C=1O YIKYNHJUKRTCJL-UHFFFAOYSA-N 0.000 claims description 5
- 244000303040 Glycyrrhiza glabra Species 0.000 claims description 5
- 235000006200 Glycyrrhiza glabra Nutrition 0.000 claims description 5
- 235000019501 Lemon oil Nutrition 0.000 claims description 5
- HYMLWHLQFGRFIY-UHFFFAOYSA-N Maltol Natural products CC1OC=CC(=O)C1=O HYMLWHLQFGRFIY-UHFFFAOYSA-N 0.000 claims description 5
- YKVWPZJHENXDAJ-VOTSOKGWSA-N Megastigmatrienone Chemical compound CC1=CC(=O)CC(C)(C)C1\C=C\C=C YKVWPZJHENXDAJ-VOTSOKGWSA-N 0.000 claims description 5
- 241000234479 Narcissus Species 0.000 claims description 5
- 244000028419 Styrax benzoin Species 0.000 claims description 5
- 235000000126 Styrax benzoin Nutrition 0.000 claims description 5
- 235000008411 Sumatra benzointree Nutrition 0.000 claims description 5
- OOCCDEMITAIZTP-UHFFFAOYSA-N allylic benzylic alcohol Natural products OCC=CC1=CC=CC=C1 OOCCDEMITAIZTP-UHFFFAOYSA-N 0.000 claims description 5
- 229960002130 benzoin Drugs 0.000 claims description 5
- RHDGNLCLDBVESU-UHFFFAOYSA-N but-3-en-4-olide Chemical compound O=C1CC=CO1 RHDGNLCLDBVESU-UHFFFAOYSA-N 0.000 claims description 5
- 229940093503 ethyl maltol Drugs 0.000 claims description 5
- 229940043259 farnesol Drugs 0.000 claims description 5
- 229930002886 farnesol Natural products 0.000 claims description 5
- HIGQPQRQIQDZMP-UHFFFAOYSA-N geranil acetate Natural products CC(C)=CCCC(C)=CCOC(C)=O HIGQPQRQIQDZMP-UHFFFAOYSA-N 0.000 claims description 5
- HIGQPQRQIQDZMP-DHZHZOJOSA-N geranyl acetate Chemical compound CC(C)=CCC\C(C)=C\COC(C)=O HIGQPQRQIQDZMP-DHZHZOJOSA-N 0.000 claims description 5
- LPLVUJXQOOQHMX-QWBHMCJMSA-N glycyrrhizinic acid Chemical compound O([C@@H]1[C@@H](O)[C@H](O)[C@H](O[C@@H]1O[C@@H]1C([C@H]2[C@]([C@@H]3[C@@]([C@@]4(CC[C@@]5(C)CC[C@@](C)(C[C@H]5C4=CC3=O)C(O)=O)C)(C)CC2)(C)CC1)(C)C)C(O)=O)[C@@H]1O[C@H](C(O)=O)[C@@H](O)[C@H](O)[C@H]1O LPLVUJXQOOQHMX-QWBHMCJMSA-N 0.000 claims description 5
- 235000019382 gum benzoic Nutrition 0.000 claims description 5
- 239000010501 lemon oil Substances 0.000 claims description 5
- 229930007744 linalool Natural products 0.000 claims description 5
- 235000011477 liquorice Nutrition 0.000 claims description 5
- 229940043353 maltol Drugs 0.000 claims description 5
- SATCULPHIDQDRE-UHFFFAOYSA-N piperonal Chemical compound O=CC1=CC=C2OCOC2=C1 SATCULPHIDQDRE-UHFFFAOYSA-N 0.000 claims description 5
- CRDAMVZIKSXKFV-UHFFFAOYSA-N trans-Farnesol Natural products CC(C)=CCCC(C)=CCCC(C)=CCO CRDAMVZIKSXKFV-UHFFFAOYSA-N 0.000 claims description 5
- NQBWNECTZUOWID-UHFFFAOYSA-N (E)-cinnamyl (E)-cinnamate Natural products C=1C=CC=CC=1C=CC(=O)OCC=CC1=CC=CC=C1 NQBWNECTZUOWID-UHFFFAOYSA-N 0.000 claims description 4
- 239000001636 3-phenylprop-2-enyl 3-phenylprop-2-enoate Substances 0.000 claims description 4
- NQBWNECTZUOWID-MZXMXVKLSA-N Cinnamyl cinnamate Chemical compound C=1C=CC=CC=1/C=C/C(=O)OC\C=C\C1=CC=CC=C1 NQBWNECTZUOWID-MZXMXVKLSA-N 0.000 claims description 4
- 239000003921 oil Substances 0.000 claims description 4
- 235000019198 oils Nutrition 0.000 claims description 4
- 238000000926 separation method Methods 0.000 claims description 4
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 claims description 3
- 239000006286 aqueous extract Substances 0.000 claims description 3
- 229960002715 nicotine Drugs 0.000 claims description 3
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 claims description 3
- FBPFZTCFMRRESA-FSIIMWSLSA-N D-Glucitol Natural products OC[C@H](O)[C@H](O)[C@@H](O)[C@H](O)CO FBPFZTCFMRRESA-FSIIMWSLSA-N 0.000 claims description 2
- 235000007612 Peruvian apple Nutrition 0.000 claims description 2
- 244000136787 Peruvian apple Species 0.000 claims description 2
- 239000007864 aqueous solution Substances 0.000 claims description 2
- 239000000600 sorbitol Substances 0.000 claims description 2
- ZIBGPFATKBEMQZ-UHFFFAOYSA-N triethylene glycol Chemical compound OCCOCCOCCO ZIBGPFATKBEMQZ-UHFFFAOYSA-N 0.000 claims description 2
- 244000223760 Cinnamomum zeylanicum Species 0.000 claims 3
- 240000001238 Gaultheria procumbens Species 0.000 claims 1
- 235000007297 Gaultheria procumbens Nutrition 0.000 claims 1
- 235000010394 Solidago odora Nutrition 0.000 claims 1
- 239000003205 fragrance Substances 0.000 abstract description 22
- 244000269722 Thea sinensis Species 0.000 abstract 4
- 230000001953 sensory effect Effects 0.000 description 14
- 230000000391 smoking effect Effects 0.000 description 11
- 230000005923 long-lasting effect Effects 0.000 description 6
- 238000013441 quality evaluation Methods 0.000 description 6
- 241000723347 Cinnamomum Species 0.000 description 5
- 230000000052 comparative effect Effects 0.000 description 5
- 238000011156 evaluation Methods 0.000 description 5
- PUPZLCDOIYMWBV-UHFFFAOYSA-N (+/-)-1,3-Butanediol Chemical compound CC(O)CCO PUPZLCDOIYMWBV-UHFFFAOYSA-N 0.000 description 4
- 235000009754 Vitis X bourquina Nutrition 0.000 description 3
- 235000012333 Vitis X labruscana Nutrition 0.000 description 3
- 240000006365 Vitis vinifera Species 0.000 description 3
- 235000014787 Vitis vinifera Nutrition 0.000 description 3
- 235000019674 grape juice Nutrition 0.000 description 3
- 206010013911 Dysgeusia Diseases 0.000 description 2
- 235000012377 Salvia columbariae var. columbariae Nutrition 0.000 description 2
- 240000005481 Salvia hispanica Species 0.000 description 2
- 235000001498 Salvia hispanica Nutrition 0.000 description 2
- TVXBFESIOXBWNM-UHFFFAOYSA-N Xylitol Natural products OCCC(O)C(O)C(O)CCO TVXBFESIOXBWNM-UHFFFAOYSA-N 0.000 description 2
- 235000019437 butane-1,3-diol Nutrition 0.000 description 2
- 235000014167 chia Nutrition 0.000 description 2
- 238000009472 formulation Methods 0.000 description 2
- 230000007794 irritation Effects 0.000 description 2
- HEBKCHPVOIAQTA-UHFFFAOYSA-N meso ribitol Natural products OCC(O)C(O)C(O)CO HEBKCHPVOIAQTA-UHFFFAOYSA-N 0.000 description 2
- 239000000811 xylitol Substances 0.000 description 2
- HEBKCHPVOIAQTA-SCDXWVJYSA-N xylitol Chemical compound OC[C@H](O)[C@@H](O)[C@H](O)CO HEBKCHPVOIAQTA-SCDXWVJYSA-N 0.000 description 2
- 229960002675 xylitol Drugs 0.000 description 2
- 235000010447 xylitol Nutrition 0.000 description 2
- 244000037364 Cinnamomum aromaticum Species 0.000 description 1
- 235000014489 Cinnamomum aromaticum Nutrition 0.000 description 1
- 235000021511 Cinnamomum cassia Nutrition 0.000 description 1
- 235000009917 Crataegus X brevipes Nutrition 0.000 description 1
- 235000013204 Crataegus X haemacarpa Nutrition 0.000 description 1
- 235000009685 Crataegus X maligna Nutrition 0.000 description 1
- 235000009444 Crataegus X rubrocarnea Nutrition 0.000 description 1
- 235000009486 Crataegus bullatus Nutrition 0.000 description 1
- 235000017181 Crataegus chrysocarpa Nutrition 0.000 description 1
- 235000009682 Crataegus limnophila Nutrition 0.000 description 1
- 240000000171 Crataegus monogyna Species 0.000 description 1
- 235000004423 Crataegus monogyna Nutrition 0.000 description 1
- 235000002313 Crataegus paludosa Nutrition 0.000 description 1
- 235000009840 Crataegus x incaedua Nutrition 0.000 description 1
- 235000019502 Orange oil Nutrition 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- 230000005540 biological transmission Effects 0.000 description 1
- 229940114081 cinnamate Drugs 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 235000011187 glycerol Nutrition 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- -1 lauryl cinnamate Chemical compound 0.000 description 1
- 229940069445 licorice extract Drugs 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 235000013772 propylene glycol Nutrition 0.000 description 1
- 210000002345 respiratory system Anatomy 0.000 description 1
- 238000002390 rotary evaporation Methods 0.000 description 1
- 238000006467 substitution reaction Methods 0.000 description 1
- 229940098465 tincture Drugs 0.000 description 1
- 238000003809 water extraction Methods 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/02—Recovery or refining of essential oils from raw materials
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Cosmetics (AREA)
- Medicines Containing Plant Substances (AREA)
- Tea And Coffee (AREA)
Abstract
The present invention provides a kind of compositions and the tobacco juice for electronic smoke containing said composition, and described compositions includes: Wuyi cliff tea quintessence oil 1～4 parts, such as 2～3 parts；Wuyi cliff tea ethanol extract 5～10 parts；Such as 7～8 parts；Wuyi cliff tea water extract 5～12 parts；Such as 8～10 parts.With the tobacco juice for electronic smoke of said composition configuration for electronic cigarette, make electronic cigarette not only have clear and upright long ago, the Wuyi cliff tea odor characteristic of mellow fragrance, and fragrance is abundant coordinates, fine and smooth soft, there is preferably plumpness and abundant property.
Description
Technical Field
The invention belongs to the technical field of electronic cigarettes, and particularly relates to a composition and electronic cigarette liquid containing the same.
Background
An electronic cigarette is an electronic transmission device that transmits fragrance, nicotine, and the like to the respiratory system by an electronic heating means. As a substitute for the conventional cigarette, the electronic cigarette is very similar to the conventional cigarette in appearance. It simulates the taste of cigarette, but has no ash, no tip, no burning, no open fire and very low harmful matter content.
The electronic cigarette mainly comprises a smoking set and a cartridge, wherein the cartridge is loaded with tobacco juice, and the smoking set atomizes the tobacco juice to generate smoking effect. The electronic cigarette liquid is mainly a product prepared by blending various flavors and fragrances, although the smoke generated by the electronic cigarette liquid has a gap with the real smoking feeling of cigarettes in the aspects of fragrance, taste and the like.
CN104087415A discloses an electronic cigarette liquid with grape flavor and a preparation method thereof. The grape-flavored electronic cigarette liquid is prepared by uniformly mixing propylene glycol, glycerol, 1, 3-butanediol, xylitol liquid, grape juice concentrated solution, edible grape formula essence and the like according to a proportion; wherein the grape juice concentrated solution is obtained by squeezing, extracting, and concentrating by rotary evaporation under reduced pressure; the grape-flavored electronic cigarette liquid comprises the following components in parts by weight: 1-80 parts of propylene glycol, 1-60 parts of glycerol, 1-50 parts of 1, 3-butanediol, 1-30 parts of xylitol solution, 5-10 parts of grape juice concentrated solution and 0.1-2 parts of edible grape formula essence.
Disclosure of Invention
The invention creatively adopts the processes of distillation, alcohol extraction, water extraction and the like to obtain the Wuyi rock tea extract from the Wuyi rock tea, and further prepares the Wuyi rock tea extract into a composition containing the Wuyi rock tea extract by the technologies of compounding, flavor blending, flavor imitation and the like, and further prepares the Wuyi rock tea essence. The composition containing the Wuyi rock tea extract and the Wuyi rock tea essence are applied to electronic cigarette liquid, and the aroma style and the aroma characteristics of the Wuyi rock tea can be integrated into the electronic cigarette liquid, so that the electronic cigarette is endowed with the Wuyi rock tea aroma characteristics of being clear, long-lasting, mellow and fragrant.
An object of the present invention is to obtain a composition, and another object of the present invention is to obtain a Wuyi rock tea essence having the characteristic of Wuyi rock tea aroma. Still another object of the present invention is to obtain an electronic cigarette liquid with the characteristic of wuyi rock tea aroma.
The present invention provides in a first aspect a composition comprising, by weight:
1-4 parts, such as 2-3 parts, of Wuyi rock tea essential oil;
5-10 parts of Wuyi cliff tea alcohol extract; for example, 7 to 8 parts;
5-12 parts of Wuyi rock tea water extract; for example, 8 to 10 parts; wherein,
the Wuyi rock tea essential oil is prepared by the following steps a1) to a 2):
a1) distilling Wuyi rock tea with water vapor, collecting distillate,
a2) performing oil-water separation on the distillate to obtain an oil phase which is the Wuyi rock tea essential oil;
the Wuyi cliff tea alcohol extract is prepared by the following steps b1) to b 2):
b1) mixing the residue of WUYIYAN tea and/or WUYIYAN tea with ethanol or ethanol water solution, extracting under reflux at 60-70 deg.C for 1-2 hr, filtering to obtain ethanol extractive solution,
optionally, repeating the above extraction steps once for the residue after filtration, then combining the ethanol extractive solutions obtained by two extractions,
b2) distilling the ethanol extract under reduced pressure, wherein the vacuum degree of the reduced pressure distillation is 40-60 mbar, the temperature of the reduced pressure distillation is 45-55 ℃, and the obtained distillation residue is the Wuyi rock tea alcohol extract;
the Wuyi rock tea aqueous extract is prepared by the following steps c1) to c 2):
c1) mixing the Wuyi rock tea leaves and/or residues left after extraction of the Wuyi rock tea with water according to the weight ratio of 1: 8-10, carrying out hot reflux extraction at the extraction temperature of 80-90 ℃ for 1-2h, then filtering to obtain a water extract,
optionally, repeating the extraction step once for the residue remaining after filtration, and then combining the water extracts obtained twice,
c2) and distilling the water extract under reduced pressure, wherein the vacuum degree of the reduced pressure distillation is 40-60 mbar, the temperature of the reduced pressure distillation is 50-60 ℃, and the obtained distillation residue is the water extract of the Wuyi rock tea.
In one embodiment, the composition of any of the present invention, wherein step a1) or a2) has one or more of the following characteristics:
in step a1), steam distillation is water distillation;
in the step a1), the temperature of steam is 102-110 ℃ in the steam distillation process;
in the step a1), the time of steam distillation is 2-3 h;
in the step a1), the output speed of distillate is 20-40 parts by weight per hour for every 100-200 parts by weight of Wuyi rock tea;
in the step a2), performing oil-water separation on the distillate through an oil-water separator;
in the step a2), the yield of the Wuyi rock tea essential oil is 0.005-0.01 wt%.
In one embodiment, the composition of any of the present invention, wherein step b1) or b2) has one or more of the following characteristics:
in the step b1), mixing the Wuyi rock tea leaves and/or residues left after extraction of the Wuyi rock tea with ethanol or ethanol water solution according to the weight ratio of 1: 8-10;
the concentration of the ethanol aqueous solution in the step b1) is 90-99 wt%;
in the step b2), the density of the alcohol extract of the Wuyi rock tea is 1.05-1.10 g/cm3；
In the step b2), the yield of the alcohol extract of the Wuyi rock tea is 10-15 wt%.
In one embodiment, the composition of any of the present invention, wherein step c1) or c2) has one or more of the following characteristics:
in the step c1), mixing the Wuyi rock tea leaves and/or residues left after extraction of the Wuyi rock tea with water according to the weight ratio of 1: 8-10;
in the step c2), the density of the Wuyi rock tea aqueous extract is 1.00-1.10g/cm 3;
in the step c2), the yield of the Wuyi rock tea water extract is 10-15 wt%.
In one embodiment, the composition of any one of the present invention, wherein the residue after extraction of wuyiyan tea is: preparing the solid residue of Wuyi cliff tea left after Wuyi cliff tea essential oil preparation, the solid residue of Wuyi cliff tea left after Wuyi cliff tea alcohol extract preparation or the solid residue of Wuyi cliff tea left after Wuyi cliff tea water extract preparation.
In one embodiment, the composition of any one of the present invention, wherein the wuyi yan tea is one or more varieties of tea selected from dahongpao, mingxia, cinnamon, narcissus, chia;
preferably, the Wuyi Yancha includes tea of cinnamon variety and tea of at least one of dahongpao, Mingxiang, narcissus and Qizhong;
preferably, the Wuyi rock tea is a cinnamon variety tea.
The second aspect of the invention provides a Wuyi rock tea essence which comprises the composition and formula essence of any one of the invention;
the formula essence consists of the following substances in percentage by weight: 0.3 to 0.7 percent of acetic acid, 0.5 to 1.5 percent of phenylacetic acid, 0.3 to 0.7 percent of ethyl laurate, 0.1 to 0.3 percent of cinnamyl cinnamate, 0.03 to 0.07 percent of geranyl acetate, 0.3 to 0.7 percent of citronellyl acetate, 0.05 to 0.15 percent of linalool, 0.03 to 0.07 percent of heliotropin, 0.1 to 0.3 percent of cinnamyl alcohol, 0.3 to 0.7 percent of farnesol, 0.01 to 0.02 percent of maltol, 0.03 to 0.07 percent of ethyl maltol, 0.03 to 0.07 percent of furanone, 0.03 to 0.07 percent of megastigmatrienone, 0.01 to 0.02 percent of 2, 5-dimethyl pyrazine, 0.01 to 0.03 percent of 2-acetyl pyrazine, 2,3, 5-trimethyl pyrazine, 0.03 to 0.07 percent of lemon oil, 0.01 to 0.03 percent of sweet orange oil, 0.7 percent of peruvian apple juice, 2.3 to 2 percent of apple juice extract, 3 to 2 percent of cinnamon extract, 3 to 0.07 percent of cinnamon extract, 2 to 2 percent of liquorice extract, 3 percent of cinnamon extract, 2 to 0.3 percent of cinnamon extract, 2, 0.3 to 0.7 percent of benzoin paste, 20 to 30 percent of propylene glycol and the balance of ethanol water solution (such as ethanol water solution with the ethanol concentration of 50 to 95 percent by weight);
preferably, the weight ratio of the composition to the formula essence is 10-25: 6-8, preferably 15-20: 6-8.
In one embodiment, the wuyiyan tea flavor of any one of the present inventions, wherein the formula flavor consists of the following materials in weight percentage: 0.4 to 0.6 percent of acetic acid, 0.8 to 1.2 percent of phenylacetic acid, 0.4 to 0.6 percent of ethyl laurate, 0.1 to 0.3 percent of cinnamyl cinnamate, 0.04 to 0.06 percent of geranyl acetate, 0.4 to 0.6 percent of citronellyl acetate, 0.08 to 0.12 percent of linalool, 0.04 to 0.06 percent of heliotropin, 0.1 to 0.3 percent of cinnamyl alcohol, 0.4 to 0.6 percent of farnesol, 0.01 to 0.02 percent of maltol, 0.04 to 0.06 percent of ethyl maltol, 0.04 to 0.06 percent of furanone, 0.04 to 0.06 percent of megastigmatrienone, 0.01 to 0.03 percent of 2, 5-dimethyl pyrazine, 0.01 to 0.03 percent of 2-acetyl pyrazine, 2,3, 5-trimethyl pyrazine, 0.04 to 0.06 percent of lemon oil, 0.01 to 0.03 percent of sweet orange oil, 0.6 percent of secret orange oil, 1 to 2 percent of apple juice, 1 to 3 percent of apple juice extract, 1 to 1 percent of 1 to 0.6 percent of cinnamon extract, 1 to 0.06 percent of liquorice extract, 1 to 0.4 percent of cinnamon extract, 1 to 0.06 percent, 0.4-0.6% of benzoin paste, 20-30% of propylene glycol and the balance of ethanol (for example, ethanol solution with the ethanol concentration of 50-99 wt%).
In a third aspect, the invention provides a composition according to any one of the invention, or a wuyiyan tea flavor according to any one of the invention, for use in flavoring a cigarette or an electronic cigarette.
The fourth aspect of the invention provides an electronic cigarette liquid containing the composition of any one of the invention or the wuyiyan tea essence of any one of the invention.
In one embodiment, the electronic cigarette liquid of any of the present inventions further comprises an electronic cigarette liquid adjuvant;
preferably, the electronic cigarette liquid auxiliary material is one or more selected from the following substances: glycerol, propylene glycol, ethanol water solution (the concentration is preferably 60-80 weight percent), diethylene glycol, triethylene glycol, sorbitol, tobacco extract and nicotine;
preferably, each 100 parts of the electronic cigarette liquid contains 20-50 parts of Wuyi rock tea essence, 5-10 parts of glycerol and the balance of propylene glycol.
The fifth aspect of the invention provides an electronic cigarette, or an electronic cigarette cartridge, containing the electronic cigarette liquid according to any one of the invention.
In the present invention, unless otherwise specified, the ethanol solution is an aqueous ethanol solution, and the concentration thereof is a weight% concentration.
In one embodiment, the wuyi rock tea is the wuyi rock tea specified in GBT 18745-.
In one embodiment, the Wuyi cliff tea is one or more selected from the group consisting of clovershrub, Minabies, cinnamon, narcissus, chia, preferably cinnamon.
In one embodiment, the wuyiyan tea is finished wuyiyan tea (tea subjected to the whole tea making process) or a tea process processed in one or more steps during the tea making process, such as a green-making or green-removing product of wuyiyan tea green.
In one embodiment, the wuyiyan tea extract is wuyiyan tea essential oil, wuyiyan tea alcohol extract, and/or wuyiyan tea water extract.
Accordingly, the present invention may provide one or more of the following advantages:
(1) the composition containing the Wuyi rock tea extract has the fragrance characteristics of Wuyi rock tea, has pure and long fragrance, is mellow and fragrant, and is particularly suitable for flavoring cigarettes/electronic cigarettes;
(2) the composition containing the Wuyi rock tea extract is reasonably compounded with the formula essence, so that the Wuyi rock tea essence has pure and long-lasting fragrance and is mellow and fragrant, and is particularly suitable for flavoring cigarettes/electronic cigarettes;
(3) the composition containing the Wuyi rock tea extract or the Wuyi rock tea essence is used for flavoring the electronic cigarette, not only endows the electronic cigarette with the characteristics of pure and long-lasting and mellow and fragrant Wuyi rock tea fragrance, but also enriches and coordinates the fragrance of the electronic cigarette, ensures that the cigarette fragrance is fine and soft during smoking, has better fullness and thickness, and obviously improves the smoking quality and the sensory comfort of the electronic cigarette.
Detailed Description
The technical solution of the present invention is further described in detail by the following examples. The exemplary embodiments of the present invention and the description thereof are provided for the purpose of explanation and are not to be construed as limiting the invention.
The formulations/fragrances used in the following examples and comparative examples are supplied by Huabao formulation fragrance (Shanghai) Co., Ltd.
The wuyiyan tea extracts (wuyiyan tea essential oil, wuyiyan tea alcohol extract and wuyiyan tea water extract) in the following examples and comparative examples were prepared by the following methods:
a) preparing Wuyi rock tea essential oil:
steam distilling Wuyi rock tea (Cinnamomum cassia) with steam distilling kettle. The lower part of the steam distillation kettle is provided with a steam inlet, the upper part of the steam distillation kettle is provided with a steam outlet, and perforated sieve plates for placing the to-be-distilled substance and penetrating steam are arranged in the steam distillation kettle and between the steam inlet and the steam outlet. 200kg of Wuyi rock tea is placed on a sieve plate of a steam distillation kettle, steam (with the temperature of about 102-110 ℃) enters the distillation kettle from the lower part of the distillation kettle, fully contacts with the Wuyi rock tea through the sieve plate, is led out from a steam outlet at the upper part, is condensed by a condenser and is collected, and the collected distillate is obtained. The temperature of the condenser is-5-10 ℃, the distilling speed of the distillate is 20-40 Kg/h, and the distilling time is 2-3 h. And (3) separating oil and water of the distillate from an oil-water separator to obtain an oil phase, namely the Wuyi rock tea essential oil. The yield of the essential oil is 0.005-0.01 wt%.
b) Preparing alcohol extract of Wuyi cliff tea:
b1) mixing the solid residue of Wuyi cliff tea left after preparing Wuyi cliff tea essential oil with 95 wt% ethanol according to the weight ratio of 1:10, carrying out hot reflux extraction at the extraction temperature of 60-70 ℃ for 1-2h, and then filtering to obtain an ethanol extract; repeating the above extraction steps once for the residue after filtration, and then combining the ethanol extract obtained by the two extractions;
b2) and distilling the ethanol extract under reduced pressure, wherein the vacuum degree (absolute pressure) of the reduced pressure distillation is 40-60 mbar, the temperature of the reduced pressure distillation is 45-55 ℃, and the obtained distillation residue is the Wuyi rock tea alcohol extract. The yield of the Wuyi rock tea alcohol extract is 10-15 wt%.
c) Preparing the Wuyi rock tea water extract:
c1) mixing the solid residue of Wuyi cliff tea left after preparing the Wuyi cliff tea alcohol extract with water according to the weight ratio of 1:10, carrying out hot reflux extraction at the extraction temperature of 80-90 ℃ for 1-2h, and then filtering to obtain a water extract; repeating the above extraction steps once for the residue after filtration, and then combining the water extract obtained by the two extractions;
c2) and distilling the water extract under reduced pressure, wherein the vacuum degree of the reduced pressure distillation is 40-60 mbar, the temperature of the reduced pressure distillation is 50-60 ℃, and the obtained distillation residue is the water extract of the Wuyi rock tea. The yield of Wuyi rock tea water extract is 10-15 wt%.
(II) the formula essence in the following examples consists of the following substances in percentage by weight: 0.50% of acetic acid, 1.00% of phenylacetic acid, 0.50% of ethyl laurate, 0.20% of lauryl cinnamate, 0.05% of geranyl acetate, 0.50% of citronellyl acetate, 0.10% of linalool, 0.05% of heliotropin, 0.20% of cinnamyl alcohol, 0.50% of farnesol, 0.01% of maltol, 0.05% of ethyl maltol, 0.05% of furanone, 0.05% of megastigmatrienone, 0.01% of 2, 5-dimethylpyrazine, 0.02% of 2-acetylpyrazine, 0.05% of 2,3, 5-trimethylpyrazine, 0.02% of lemon oil, 0.50% of sweet orange oil, 1.50% of apple juice, 2.50% of hawthorn tincture, 1.50% of Yunyan extract, 3.50% of Zimbabwe extract, 1.50% of licorice extract, 0.50% of Peru extract, 0.50% of benzoin extract, 25.00% of propylene glycol, and the balance of an aqueous. The substances are mixed according to a certain proportion and stirred for 30min at normal temperature, so that the components are fully and uniformly mixed to obtain the formula essence.
(III) examples 1 to 6 and comparative examples 1 to 3
Examples 1 to 6 include:
1. the proportion of the composition containing the Wuyi rock tea extract is as follows: the Wuyi cliff tea essential oil, the Wuyi cliff tea alcohol extract and the Wuyi cliff tea water extract are mixed and proportioned to obtain the composition alpha 1-alpha 5.
2. The proportion of the Wuyi rock tea essence is as follows: the composition is compounded with the essence according to the formula to obtain Wuyi rock tea essence beta 1-beta 5 with the characteristics of Wuyi rock tea essence.
3. The ratio of the electronic cigarette liquid is as follows: mixing the Wuyi rock tea essence beta 1-beta 5 with electronic cigarette liquid auxiliary materials (propylene glycol and glycerol) to obtain electronic cigarette liquid A1-A5; the composition beta 5 is also separately mixed with electronic cigarette liquid accessories (propylene glycol and glycerol) to obtain the electronic cigarette liquid A6.
Comparative examples 1 to 4 include:
1. mixing the Wuyi rock tea essence formula, the formula essence and electronic cigarette liquid auxiliary materials (propylene glycol and glycerol) to obtain the electronic cigarette liquid B1.
2. Mixing the Wuyi rock tea essential oil with electronic cigarette auxiliary materials (propylene glycol and glycerol) to obtain electronic cigarette liquid B2.
3. And mixing the formula essence with the electronic cigarette auxiliary materials (propylene glycol and glycerol) to obtain the electronic cigarette liquid B3.
The composition, the Wuyi rock tea essence and the electronic cigarette liquid contained in the embodiment are sequentially shown in the following tables 1-3:
TABLE 1 composition containing extract of WUYIYANCHA
| Containing a composition | Wuyi rock tea essential oil | Wuyi rock tea alcohol extract | Wuyi rock tea water extract |
| α1 | 1.5 | 5.5 | 7.1 |
| α2 | 2.5 | 8.5 | 11.0 |
| α3 | 1.0 | 4.5 | 5.5 |
| α4 | 2.0 | 7.0 | 9.5 |
| α5 | 2.0 | 7.5 | 9.0 |
Unit: parts by weight
TABLE 2 Wuyi rock tea essence
Unit: parts by weight
TABLE 3 electronic cigarette liquid
Unit: by weight%
(IV) evaluation of sensory quality
The electronic cigarette tobacco liquids A1-A6 of examples 1-6 and the electronic cigarette tobacco liquids B1-B3 of comparative examples 1-3 were added to electronic cigarettes for sensory quality evaluation. The sensory quality evaluation method of the electronic cigarette adopts GB 5606.4-2005 part IV of cigarettes: the evaluation method of sensory technical requirements was found to have an evaluation index of "gloss" of 11 persons, and the specific evaluation results are shown in table 4.
TABLE 4 sensory quality evaluation results
As can be seen from table 4, the electronic cigarette liquids a 1-a 6 have significantly improved aroma, coordination, miscellaneous odor, irritation, and aftertaste, higher sensory quality scores, and improved smoking quality and sensory comfort, as compared with the electronic cigarette liquids B1-B3.
The sensory quality evaluation result of the electronic cigarette liquid shows that: the electronic cigarette liquid A1-A6 is used for electronic cigarettes, so that the electronic cigarettes are endowed with the characteristics of being clear, long-lasting, mellow and fragrant Wuyi rock tea fragrance, and the electronic cigarettes have good fragrance, coordination, miscellaneous gas, irritation and aftertaste during smoking, and good smoking quality and sensory comfort. Particularly, the electronic cigarette liquid A5 has the most abundant, coordinated, fine and soft aroma, better fullness and thickness, more comfortable mouthfeel and highest sensory evaluation score.
In contrast, the formula of the wuyiyan tea extract of the electronic cigarette liquid B1 is different from the formula of the electronic cigarette liquid B1, and the sensory quality evaluation score is low; the electronic cigarette liquid B2 and B3 only contain Wuyi rock tea essential oil and formula essence respectively, the fragrance is slightly thin, the miscellaneous gas is slightly high, and the sensory quality evaluation score is low.
Accordingly, the above-described embodiments of the present invention may have one or more of the following advantages:
(1) the composition containing the Wuyi rock tea extract has the fragrance characteristics of Wuyi rock tea, has pure and long fragrance, is mellow and fragrant, and is particularly suitable for flavoring cigarettes/electronic cigarettes;
(2) the composition containing the Wuyi rock tea extract is reasonably compounded with the formula essence, so that the Wuyi rock tea essence has pure and long-lasting fragrance and is mellow and fragrant, and is particularly suitable for flavoring cigarettes/electronic cigarettes;
(3) the composition containing the Wuyi rock tea extract or the Wuyi rock tea essence is used for flavoring the electronic cigarette, not only endows the electronic cigarette with the characteristics of pure and long-lasting and mellow and fragrant Wuyi rock tea fragrance, but also enriches and coordinates the fragrance of the electronic cigarette, ensures that the cigarette fragrance is fine and soft during smoking, has better fullness and thickness, and obviously improves the smoking quality and the sensory comfort of the electronic cigarette.
Finally, it should be noted that: the above examples are only intended to illustrate the technical solution of the present invention and not to limit it; although the present invention has been described in detail with reference to preferred embodiments, those skilled in the art will understand that: modifications to the specific embodiments of the invention or equivalent substitutions for parts of the technical features may be made; without departing from the spirit of the present invention, it is intended to cover all aspects of the invention as defined by the appended claims.
Claims (12)
1. A composition, comprising, by weight:
1-4 parts, such as 2-3 parts, of Wuyi rock tea essential oil;
5-10 parts of Wuyi cliff tea alcohol extract; for example, 7 to 8 parts;
5-12 parts of Wuyi rock tea water extract; for example, 8 to 10 parts; wherein,
the Wuyi rock tea essential oil is prepared by the following steps a1) to a 2):
a1) distilling Wuyi rock tea with water vapor, collecting distillate,
a2) performing oil-water separation on the distillate to obtain an oil phase which is the Wuyi rock tea essential oil;
the Wuyi cliff tea alcohol extract is prepared by the following steps b1) to b 2):
b1) mixing the residue of WUYIYAN tea and/or WUYIYAN tea with ethanol or ethanol water solution, extracting under reflux at 60-70 deg.C for 1-2 hr, filtering to obtain ethanol extractive solution,
optionally, repeating the above extraction steps once for the residue after filtration, then combining the ethanol extractive solutions obtained by two extractions,
b2) distilling the ethanol extract under reduced pressure, wherein the vacuum degree of the reduced pressure distillation is 40-60 mbar, the temperature of the reduced pressure distillation is 45-55 ℃, and the obtained distillation residue is the Wuyi rock tea alcohol extract;
the Wuyi rock tea aqueous extract is prepared by the following steps c1) to c 2):
c1) mixing the Wuyi rock tea leaves and/or residues left after extraction of the Wuyi rock tea with water according to the weight ratio of 1: 8-10, carrying out hot reflux extraction at the extraction temperature of 80-90 ℃ for 1-2h, then filtering to obtain a water extract,
optionally, repeating the extraction step once for the residue remaining after filtration, and then combining the water extracts obtained twice,
c2) and distilling the water extract under reduced pressure, wherein the vacuum degree of the reduced pressure distillation is 40-60 mbar, the temperature of the reduced pressure distillation is 50-60 ℃, and the obtained distillation residue is the water extract of the Wuyi rock tea.
2. The composition of claim 1, wherein step a1) or a2) has one or more of the following characteristics:
in step a1), steam distillation is water distillation;
in the step a1), the temperature of steam is 102-110 ℃ in the steam distillation process;
in the step a1), the time of steam distillation is 2-3 h;
in the step a1), the output speed of distillate is 20-40 parts by weight per hour for every 100-200 parts by weight of Wuyi rock tea;
in the step a2), performing oil-water separation on the distillate through an oil-water separator;
in the step a2), the yield of the Wuyi rock tea essential oil is 0.005-0.01 wt%.
3. The composition of claim 1, wherein step b1) or b2) has one or more of the following characteristics:
in the step b1), mixing the Wuyi rock tea leaves and/or residues left after extraction of the Wuyi rock tea with ethanol or ethanol water solution according to the weight ratio of 1: 8-10;
the concentration of the ethanol aqueous solution in the step b1) is 90-99 wt%;
in the step b2), the density of the alcohol extract of the Wuyi rock tea is 1.05-1.10 g/cm3；
In the step b2), the yield of the alcohol extract of the Wuyi rock tea is 10-15 wt%.
4. The composition of claim 1, wherein step c1) or c2) has one or more of the following characteristics:
in the step c1), mixing the Wuyi rock tea leaves and/or residues left after extraction of the Wuyi rock tea with water according to the weight ratio of 1: 8-10;
in the step c2), the density of the Wuyi rock tea water extract is 1.00-1.10g/cm3；
In the step c2), the yield of the Wuyi rock tea water extract is 10-15 wt%.
5. The composition according to any one of claims 1 to 5, wherein the residue after extraction of Wuyi mountain tea is: preparing the solid residue of Wuyi cliff tea left after Wuyi cliff tea essential oil preparation, the solid residue of Wuyi cliff tea left after Wuyi cliff tea alcohol extract preparation or the solid residue of Wuyi cliff tea left after Wuyi cliff tea water extract preparation.
6. The composition of any one of claims 1 to 5, wherein the Wuyi Yancha is one or more selected from Dahongpao, Ming Chung, cinnamon, narcissus and Qizhong tea;
preferably, the Wuyi Yancha includes tea of cinnamon variety and tea of at least one of dahongpao, Mingxiang, narcissus and Qizhong;
preferably, the Wuyi rock tea is a cinnamon variety tea.
7. A Wuyi rock tea essence comprising the composition of any one of claims 1 to 6 and a formula essence;
the formula essence consists of the following substances in percentage by weight: 0.3 to 0.7 percent of acetic acid, 0.5 to 1.5 percent of phenylacetic acid, 0.3 to 0.7 percent of ethyl laurate, 0.1 to 0.3 percent of cinnamyl cinnamate, 0.03 to 0.07 percent of geranyl acetate, 0.3 to 0.7 percent of citronellyl acetate, 0.05 to 0.15 percent of linalool, 0.03 to 0.07 percent of heliotropin, 0.1 to 0.3 percent of cinnamyl alcohol, 0.3 to 0.7 percent of farnesol, 0.01 to 0.02 percent of maltol, 0.03 to 0.07 percent of ethyl maltol, 0.03 to 0.07 percent of furanone, 0.03 to 0.07 percent of megastigmatrienone, 0.01 to 0.02 percent of 2, 5-dimethyl pyrazine, 0.01 to 0.03 percent of 2-acetyl pyrazine, 2,3, 5-trimethyl pyrazine, 0.03 to 0.07 percent of lemon oil, 0.01 to 0.03 percent of sweet orange oil, 0.7 percent of peruvian apple juice, 2.3 to 2 percent of apple juice extract, 3 to 2 percent of cinnamon extract, 3 to 0.07 percent of cinnamon extract, 2 to 2 percent of liquorice extract, 3 percent of cinnamon extract, 2 to 0.3 percent of cinnamon extract, 2, 0.3 to 0.7 percent of benzoin paste, 20 to 30 percent of propylene glycol and the balance of ethanol water solution (such as ethanol water solution with the ethanol concentration of 50 to 95 percent by weight);
preferably, the weight ratio of the composition to the formula essence is 10-25: 6-8, preferably 15-20: 6-8.
8. The wuyiyan tea flavor of claim 7, wherein the formula is comprised of, by weight: 0.4 to 0.6 percent of acetic acid, 0.8 to 1.2 percent of phenylacetic acid, 0.4 to 0.6 percent of ethyl laurate, 0.1 to 0.3 percent of cinnamyl cinnamate, 0.04 to 0.06 percent of geranyl acetate, 0.4 to 0.6 percent of citronellyl acetate, 0.08 to 0.12 percent of linalool, 0.04 to 0.06 percent of heliotropin, 0.1 to 0.3 percent of cinnamyl alcohol, 0.4 to 0.6 percent of farnesol, 0.01 to 0.02 percent of maltol, 0.04 to 0.06 percent of ethyl maltol, 0.04 to 0.06 percent of furanone, 0.04 to 0.06 percent of megastigmatrienone, 0.01 to 0.02 percent of 2, 5-dimethyl pyrazine, 0.01 to 0.03 percent of 2-acetyl pyrazine, 2,3, 5-trimethyl pyrazine, 0.04 to 0.06 percent of lemon oil, 0.01 to 0.03 percent of sweet orange oil, 1 to 0.6 percent of apple juice, 1 to 3 percent of apple juice extract, 1 to 1 percent of 1 to 0.06 percent of cinnamon extract, 1 to 0.06 percent of liquorice extract, 1 percent of 3 percent of cinnamon extract, 3 percent of liquorice extract, Peru extract 0.4-0.6%, benzoin extract 0.4-0.6%, propylene glycol 20-30%, and the balance ethanol (for example, ethanol solution with ethanol concentration of 50-99 wt%).
9. The composition of any one of claims 1 to 6, or the Wuyi rock tea essence of claim 7 or 8, for use in perfuming a cigarette or an electronic cigarette.
10. An electronic cigarette liquid containing the composition of any one of claims 1 to 6 or the wuyiyan tea flavor of claim 7 or 8.
11. The e-cigarette liquid of claim 10, further comprising an e-cigarette liquid adjunct;
preferably, the electronic cigarette liquid auxiliary material is one or more selected from the following substances: glycerol, propylene glycol, ethanol water solution (the concentration is preferably 60-80 weight percent), diethylene glycol, triethylene glycol, sorbitol, tobacco extract and nicotine;
preferably, each 100 parts of the electronic cigarette liquid contains 20-50 parts of Wuyi rock tea essence, 5-10 parts of glycerol and the balance of propylene glycol.
12. An electronic cigarette, or an electronic cigarette cartridge, containing the electronic cigarette liquid of claim 10 or 11.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610609456.7A CN106174683B (en) | 2016-07-29 | 2016-07-29 | A kind of composition and the tobacco juice for electronic smoke containing said composition |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201610609456.7A CN106174683B (en) | 2016-07-29 | 2016-07-29 | A kind of composition and the tobacco juice for electronic smoke containing said composition |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN106174683A true CN106174683A (en) | 2016-12-07 |
| CN106174683B CN106174683B (en) | 2018-05-15 |
Family
ID=57496777
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201610609456.7A Active CN106174683B (en) | 2016-07-29 | 2016-07-29 | A kind of composition and the tobacco juice for electronic smoke containing said composition |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN106174683B (en) |
Cited By (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106723300A (en) * | 2016-12-08 | 2017-05-31 | 深圳市华加生物科技有限公司 | Electronics tobacco tar perfume base and electronics tobacco tar |
| CN107125803A (en) * | 2017-05-10 | 2017-09-05 | 深圳瀚星翔科技有限公司 | A kind of electronic cigarette tobacco tar and preparation method thereof |
| CN107467719A (en) * | 2017-08-29 | 2017-12-15 | 贵州普定印象朵贝农业开发有限公司 | A kind of Chinese yew electronic cigarette |
| CN107586616A (en) * | 2017-11-01 | 2018-01-16 | 湖北中烟工业有限责任公司 | One grows tobacco with tea perfume essence |
| CN108125277A (en) * | 2018-03-21 | 2018-06-08 | 福建中烟工业有限责任公司 | A kind of electronic cigarette and preparation method thereof |
| CN109329503A (en) * | 2018-12-10 | 2019-02-15 | 青岛三味香道文化传播有限公司 | Tea perfume cream, green tea balm and preparation method thereof |
| CN110506982A (en) * | 2019-09-12 | 2019-11-29 | 深圳雾芯科技有限公司 | Flavour compositions and electronic cigarette liquid comprising the flavour compositions |
| CN111004679A (en) * | 2019-11-25 | 2020-04-14 | 福建中烟工业有限责任公司 | Lysimachia capillipes extract and essence |
| CN111254013A (en) * | 2020-02-21 | 2020-06-09 | 福建中烟工业有限责任公司 | Perfume composition containing Lysimachia capillipes extract |
| CN111671133A (en) * | 2020-06-22 | 2020-09-18 | 福建中烟工业有限责任公司 | Tea-flavored flue-cured tobacco type tobacco flavor electronic cigarette atomized liquid |
| CN112094692A (en) * | 2020-09-17 | 2020-12-18 | 湖北中烟工业有限责任公司 | Amber-flavor cigarette essence and application thereof |
Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH11225731A (en) * | 1998-02-12 | 1999-08-24 | Japan Tobacco Inc | Improving agent for aroma and smoking taste of tobacco and improvement of the same |
| WO2002091866A1 (en) * | 2001-05-11 | 2002-11-21 | Thione International, Inc. | Glutathione, green tea, grape seed extract to neutralize tobacco free radicals |
| CN103468410A (en) * | 2013-09-27 | 2013-12-25 | 福建中烟工业有限责任公司 | Tea flower extract composition and its use in cigarette |
| CN103484248A (en) * | 2013-09-27 | 2014-01-01 | 福建中烟工业有限责任公司 | Tea flower essence with fresh and sweet characteristics, and application of essence in cigarettes |
| CN104544552A (en) * | 2014-12-31 | 2015-04-29 | 贵州中烟工业有限责任公司 | Electronic cigarette smoke solution prepared through oolong leaf extract |
-
2016
- 2016-07-29 CN CN201610609456.7A patent/CN106174683B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPH11225731A (en) * | 1998-02-12 | 1999-08-24 | Japan Tobacco Inc | Improving agent for aroma and smoking taste of tobacco and improvement of the same |
| WO2002091866A1 (en) * | 2001-05-11 | 2002-11-21 | Thione International, Inc. | Glutathione, green tea, grape seed extract to neutralize tobacco free radicals |
| CN103468410A (en) * | 2013-09-27 | 2013-12-25 | 福建中烟工业有限责任公司 | Tea flower extract composition and its use in cigarette |
| CN103484248A (en) * | 2013-09-27 | 2014-01-01 | 福建中烟工业有限责任公司 | Tea flower essence with fresh and sweet characteristics, and application of essence in cigarettes |
| CN104544552A (en) * | 2014-12-31 | 2015-04-29 | 贵州中烟工业有限责任公司 | Electronic cigarette smoke solution prepared through oolong leaf extract |
Cited By (17)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106723300A (en) * | 2016-12-08 | 2017-05-31 | 深圳市华加生物科技有限公司 | Electronics tobacco tar perfume base and electronics tobacco tar |
| CN107125803A (en) * | 2017-05-10 | 2017-09-05 | 深圳瀚星翔科技有限公司 | A kind of electronic cigarette tobacco tar and preparation method thereof |
| CN107467719A (en) * | 2017-08-29 | 2017-12-15 | 贵州普定印象朵贝农业开发有限公司 | A kind of Chinese yew electronic cigarette |
| CN107586616A (en) * | 2017-11-01 | 2018-01-16 | 湖北中烟工业有限责任公司 | One grows tobacco with tea perfume essence |
| CN108125277A (en) * | 2018-03-21 | 2018-06-08 | 福建中烟工业有限责任公司 | A kind of electronic cigarette and preparation method thereof |
| CN109329503A (en) * | 2018-12-10 | 2019-02-15 | 青岛三味香道文化传播有限公司 | Tea perfume cream, green tea balm and preparation method thereof |
| CN109329503B (en) * | 2018-12-10 | 2021-09-24 | 青岛三味香道文化传播有限公司 | Tea balm, green tea balm and preparation method thereof |
| WO2021046899A1 (en) * | 2019-09-12 | 2021-03-18 | 深圳雾芯科技有限公司 | Flavor composition and electronic cigarette liquid comprising said flavor composition |
| CN110506982B (en) * | 2019-09-12 | 2021-01-26 | 深圳雾芯科技有限公司 | Flavor composition and electronic cigarette liquid containing same |
| CN110506982A (en) * | 2019-09-12 | 2019-11-29 | 深圳雾芯科技有限公司 | Flavour compositions and electronic cigarette liquid comprising the flavour compositions |
| CN111004679A (en) * | 2019-11-25 | 2020-04-14 | 福建中烟工业有限责任公司 | Lysimachia capillipes extract and essence |
| CN111004679B (en) * | 2019-11-25 | 2023-04-07 | 福建中烟工业有限责任公司 | Lysimachia capillipes extract and essence |
| CN111254013A (en) * | 2020-02-21 | 2020-06-09 | 福建中烟工业有限责任公司 | Perfume composition containing Lysimachia capillipes extract |
| CN111254013B (en) * | 2020-02-21 | 2023-07-21 | 福建中烟工业有限责任公司 | Perfume composition containing extract of lysimachia capillipes |
| CN111671133A (en) * | 2020-06-22 | 2020-09-18 | 福建中烟工业有限责任公司 | Tea-flavored flue-cured tobacco type tobacco flavor electronic cigarette atomized liquid |
| CN112094692A (en) * | 2020-09-17 | 2020-12-18 | 湖北中烟工业有限责任公司 | Amber-flavor cigarette essence and application thereof |
| CN112094692B (en) * | 2020-09-17 | 2023-01-06 | 湖北中烟工业有限责任公司 | Amber-flavor cigarette essence and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN106174683B (en) | 2018-05-15 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN106174683B (en) | A kind of composition and the tobacco juice for electronic smoke containing said composition | |
| CN104770863B (en) | Electronic cigarette liquid with herbal tea flavor and application thereof | |
| CN104839885B (en) | A kind of electronic cigarette liquid and preparation method thereof of improvement | |
| CN106263013B (en) | A kind of high fragrance tobacco extract, preparation method and applications | |
| CN104839883A (en) | Electronic cigarette liquid with characteristics of tobaccos for tobacco pipes | |
| CN105533793B (en) | A kind of preparation method of Dark sun-cured tobacco extract | |
| CN111671134A (en) | Mint flue-cured tobacco type tobacco flavor electronic cigarette atomized liquid | |
| CN108060014A (en) | For the preparation method of the Flos Caryophylli extract of quick-fried pearl base oil | |
| CN102907760A (en) | Method for regulating chemical components of tobacco material | |
| CN104082853B (en) | A kind of electronic cigarette liquid containing tomato extract and preparation method thereof | |
| CN104544552A (en) | Electronic cigarette smoke solution prepared through oolong leaf extract | |
| CN104544549A (en) | Electronic cigarette smoke solution prepared through green tea leaf extract | |
| CN108203623B (en) | Composition, preparation method thereof and application of composition as tobacco flavor | |
| CN104544543A (en) | Electronic cigarette smoke solution prepared through black tea leaf extract | |
| CN104939305A (en) | Tobacco extract and electronic cigarette liquid | |
| CN113243550B (en) | Bergamot spice for electronic atomized liquid | |
| CN104544544A (en) | Electronic cigarette smoke solution prepared through white tea leaf extract | |
| CN104082855A (en) | Double-apple-aroma electronic cigarette liquid and preparation method thereof | |
| CN104544548A (en) | Electronic cigarette smoke solution prepared through yellow tea leaf extract | |
| CN110295088A (en) | A kind of gold Orange-flavored essence and application thereof | |
| CN112369651B (en) | Tobacco-flavored electronic lampblack and preparation method thereof | |
| CN109234011A (en) | A kind of fragrance-enhancing tobacco agent containing sage clary oil | |
| CN110331043B (en) | Essence for buccal cigarettes as well as preparation method and application thereof | |
| EP2888951A1 (en) | Product comprising kratom | |
| CN113995159A (en) | Electronic cigarette liquid containing plant fragrance |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| GR01 | Patent grant | ||
| GR01 | Patent grant |