CN107125803A - A kind of electronic cigarette tobacco tar and preparation method thereof - Google Patents
A kind of electronic cigarette tobacco tar and preparation method thereof Download PDFInfo
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- CN107125803A CN107125803A CN201710327614.4A CN201710327614A CN107125803A CN 107125803 A CN107125803 A CN 107125803A CN 201710327614 A CN201710327614 A CN 201710327614A CN 107125803 A CN107125803 A CN 107125803A
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- tobacco tar
- cigarette tobacco
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0069—Heterocyclic compounds
- C11B9/0073—Heterocyclic compounds containing only O or S as heteroatoms
- C11B9/0076—Heterocyclic compounds containing only O or S as heteroatoms the hetero rings containing less than six atoms
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- Chemical Kinetics & Catalysis (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Confectionery (AREA)
- Seasonings (AREA)
Abstract
The invention provides a kind of electronic cigarette tobacco tar, include the component of following mass percent：90% 99% atomized liquid, the 1% 10% savory essence of Coca-Cola；Wherein, the savory spermatophore of Coca-Cola includes the component of following parts by weight：0.1 2 parts of first position firpenes, 0.1 2 parts of second position firpenes, 1 30 Fen limonenes, 1 10 parts of orange oils, 1 20 parts of lemon oils, 0.1 0.5 parts of laurenes, 0.1 2 parts of cinnamic aldehydes, 0.1 5 parts of cinnamon oils, 0.1 10 parts of citrals, 0.1 5 parts of geranials, 1 10 parts of geranyl acetates, 0.1 5 parts of sinensals, 1 10 parts of citronellols, 1 10 parts of geranyl propionates, 0.1 5 parts of eugenols, 0.1 2 parts of ethylmaltols, 0.1 3 parts of furanones, 0.1 5 parts of raspberry ketones, 1 25 parts of cinnamic alcohols, 1 10 parts of cinnamyl acetates, 1 15 parts of vanillic aldehydes, 1 15 parts of Ethyl vanillins and 0.1 2 parts of coffee-extracts.The electronic cigarette tobacco tar with Coca-Cola taste that the present invention is provided, fragrance enriches full, can reach similar effect for drinking the pleasant feeling that Coca-Cola is brought.Present invention also offers the preparation method of electronic cigarette tobacco tar, method is simple to operation, is adapted to industrialization production.
Description
Technical field
The present invention relates to electronic cigarette field, and in particular to a kind of electronic cigarette tobacco tar and preparation method thereof.
Background technology
Electronic cigarette controls smog output quantity and working condition by high-tech silicon and airflow sensor device, makes tobacco tar by mist
Change, by the solution atomization containing extract, essence, glycerine and propane diols into particulate, by pulmonary absorption, while the simulation that spues
Smog, but tar and other harmful components in cigarette are but free of, second-hand-cigarette will not be also produced, also will not diffuse or curl up
In confined space.Electronic cigarette provides similar with traditional cigarette disappear as a kind of form in novel tobacco product, on the one hand its
Take custom and satisfaction, the hazard index of another aspect electronic cigarette is substantially reduced than traditional cigarette.Therefore, electronic cigarette presents huge
Market prospects.
Coca-Cola, due to its unique taste, is the popular a beverage liked very much.But there is presently no develop height
Spend the electronic cigarette tobacco tar close to Coca-Cola taste.
The content of the invention
To solve the above problems, the invention provides a kind of electronic cigarette tobacco tar.Electronic cigarette tobacco tar of the present invention have it is tasty can
Happy taste, can not only meet the smoking demand of smoker, and enrich full with fragrance, reach and similar drink Coca-Cola institute band
The effect for the pleasant feeling come.
First aspect present invention provides a kind of electronic cigarette tobacco tar, includes the component of following mass percent：
90%-99% atomized liquid, the 1%-10% savory essence of Coca-Cola；
Wherein, the savory spermatophore of described Coca-Cola includes the component of following parts by weight：
0.1-2 parts of first position firpene, 0.1-2 part second firpenes, 1-30 Fen limonenes, 1-10 parts of orange oil, 1-20 parts of lemon oils,
0.1-0.5 parts of laurenes, 0.1-2 parts of cinnamic aldehydes, 0.1-5 parts of cinnamon oils, 0.1-10 parts of citrals, 0.1-5 parts of geranials, 1-10 parts
Geranyl acetate, 0.1-5 part sinensal, 1-10 parts of citronellols, 1-10 parts of geranyl propionates, 0.1-5 parts of eugenols, 0.1-2 parts
Ethylmaltol, 0.1-3 part furanone, 0.1-5 parts of raspberry ketones, 1-25 parts of cinnamic alcohols, 1-10 parts of cinnamyl acetates, 1-15 parts of chinese cymbidiums
Element, 1-15 parts of Ethyl vanillins and 0.1-2 parts of coffee-extracts.
Wherein, in the electronic cigarette tobacco tar, the savory smart mass percent of Coca-Cola is 5%-10%.
Wherein, the electronic cigarette tobacco tar also includes food additives, and the food additives include caramel, fructose, grape
At least one of sugar, Aspartame and honey element.
Wherein, in the electronic cigarette tobacco tar, the mass percent of the food additives is 1%-15%.
Wherein, in the electronic cigarette tobacco tar, the mass percent of the caramel is 0.5%-5%, the quality of the fructose
Percentage is 0.1%-5%, and the mass percent of the glucose is 0.1%-5%, the mass percent of the Aspartame
For 0.01%-0.5%, the mass percent of the honey element is 0.1%-1%.
Wherein, also include 10-30 parts of organic solvent in the savory essence of described Coca-Cola, the organic solvent includes the third two
Alcohol.
Wherein, the atomized liquid includes propane diols and glycerine.
Wherein, in the electronic cigarette tobacco tar, the mass percent of the propane diols is 45%-80%, the glycerine
Mass percent is 1%-30%.
The invention provides a kind of electronic cigarette tobacco tar with Coca-Cola taste, the smoking need of smoker can not only be met
Ask, and enrich full with fragrance, may also reach up similar effect for drinking the pleasant feeling that Coca-Cola is brought.
Second aspect of the present invention provides a kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
The savory essence mixing of Coca-Cola of atomized liquid and 1%-10% that mass percent is respectively 90%-99%,
Stir at room temperature, the electronic cigarette tobacco tar is made；
Wherein, the savory spermatophore of described Coca-Cola includes the component of following parts by weight：
0.1-2 parts of first position firpene, 0.1-2 part second firpenes, 1-30 Fen limonenes, 1-10 parts of orange oil, 1-20 parts of lemon oils,
0.1-0.5 parts of laurenes, 0.1-2 parts of cinnamic aldehydes, 0.1-5 parts of cinnamon oils, 0.1-10 parts of citrals, 0.1-5 parts of geranials, 1-10 parts
Geranyl acetate, 0.1-5 part sinensal, 1-10 parts of citronellols, 1-10 parts of geranyl propionates, 0.1-5 parts of eugenols, 0.1-2 parts
Ethylmaltol, 0.1-3 part furanone, 0.1-5 parts of raspberry ketones, 1-25 parts of cinnamic alcohols, 1-10 parts of cinnamyl acetates, 1-15 parts of chinese cymbidiums
Element, 1-15 parts of Ethyl vanillins and 0.1-2 parts of coffee-extracts.
Wherein, the electronic cigarette tobacco tar also includes food additives, and the food additives include caramel, fructose, grape
At least one of sugar, Aspartame and honey element.
The preparation method for the electronic cigarette tobacco tar that second aspect of the present invention is provided, by by atomized liquid and the savory essence of Coca-Cola
Be simply mixed, the electronic cigarette tobacco tar for Coca-Cola taste that fragrance is abundant, comfortable taste, satisfaction are good, the preparation side has been made
Method is simple to operation, is adapted to industrialization production.
To sum up, beneficial effect of the present invention includes the following aspects：
1st, the invention provides a kind of electronic cigarette tobacco tar with Coca-Cola taste, the smoking of smoker can not only be met
Demand, and enrich full with fragrance, reach similar effect for drinking the pleasant feeling that Coca-Cola is brought；
2nd, the preparation method of electronic cigarette tobacco tar that the present invention is provided, by the way that atomized liquid and Coca-Cola is savory smart simple
Mixing, has been made the electronic cigarette tobacco tar for Coca-Cola taste that fragrance is abundant, comfortable taste, satisfaction are good, and the preparation method is simple
It is easy to operate, it is adapted to industrialization production.
Embodiment
As described below is the preferred embodiment of the present invention, it is noted that for those skilled in the art
For, under the premise without departing from the principles of the invention, some improvements and modifications can also be made, these improvements and modifications are also considered as
Protection scope of the present invention.
In a first aspect, the invention provides a kind of electronic cigarette tobacco tar, including the component of following mass percent：
90%-99% atomized liquid, the 1%-10% savory essence of Coca-Cola；
Wherein, the savory spermatophore of described Coca-Cola includes the component of following parts by weight：
0.1-2 parts of first position firpene, 0.1-2 part second firpenes, 1-30 Fen limonenes, 1-10 parts of orange oil, 1-20 parts of lemon oils,
0.1-0.5 parts of laurenes, 0.1-2 parts of cinnamic aldehydes, 0.1-5 parts of cinnamon oils, 0.1-10 parts of citrals, 0.1-5 parts of geranials, 1-10 parts
Geranyl acetate, 0.1-5 part sinensal, 1-10 parts of citronellols, 1-10 parts of geranyl propionates, 0.1-5 parts of eugenols, 0.1-2 parts
Ethylmaltol, 0.1-3 part furanone, 0.1-5 parts of raspberry ketones, 1-25 parts of cinnamic alcohols, 1-10 parts of cinnamyl acetates, 1-15 parts of chinese cymbidiums
Element, 1-15 parts of Ethyl vanillins and 0.1-2 parts of coffee-extracts.
Food grade spices is passed through rational allocation by the present invention by the blending means of science, make with it is abundant it is true to nature can
The essence of the laughable fragrance of mouth is used in electronic cigarette tobacco tar, to greatest extent close to Coca-Cola local flavor, obtained Coca-Cola mouthful
Taste electronic cigarette tobacco tar, not only meets the smoking impression of electronic cigarette consumer, while bringing cuisines to enjoy.
In embodiment of the present invention, in the electronic cigarette tobacco tar, the savory smart mass percent of Coca-Cola is
5%-10%.
In embodiment of the present invention, the electronic cigarette tobacco tar also includes food additives, and the food additives include Jiao
At least one of sugar, fructose, glucose, Aspartame and honey element.The present invention adds food addition in electronic cigarette tobacco tar
Agent, can lift the overall mouthfeel of electronic cigarette.
In embodiment of the present invention, in the electronic cigarette tobacco tar, the mass percent of the food additives is 1%-
15%.Alternatively, in the electronic cigarette tobacco tar, the mass percent of the caramel is 0.5%-5%, the quality hundred of the fructose
Divide than being 0.1%-5%, the mass percent of the glucose is 0.1%-5%, and the mass percent of the Aspartame is
0.01%-0.5%, the mass percent of the honey element is 0.1%-1%.
In embodiment of the present invention, in the electronic cigarette tobacco tar, also include 10-30 parts in the savory essence of Coca-Cola
Organic solvent, the organic solvent includes propane diols.The organic solvent is used to dissolve the savory essence of above-mentioned Coca-Cola.
In embodiment of the present invention, the atomized liquid includes propane diols and glycerine.Alternatively, the propane diols, the third three
Alcohol is food grade or pharmaceutical grade product.Alternatively, in the electronic cigarette tobacco tar, the mass percent of the propane diols is
45%-80%, the mass percent of the glycerine is 1%-30%.
In an embodiment of the present invention, the electronic cigarette tobacco tar includes the component of following mass percent：
45%-80% propane diols, 1%-30% glycerine, the 1%-10% savory essence of Coca-Cola, 1%-15%
Food additives.
Alternatively, the electronic cigarette tobacco tar includes the component of following mass percent：
45%-80% propane diols, 1%-30% glycerine, the 1%-10% savory essence of Coca-Cola, 0.5%-5%
Caramel, 0.1%-5% fructose, 0.1%-5% glucose, 0.01%-0.5% Aspartame, 0.1%-1% sweet tea
Sweet element.
In food flavor used in Coca-Cola taste electronics tobacco tar of the present invention：
First position firpene has the breath of pine, needle and resin-like, and fragrance is sent out thoroughly.There is Titian as the fragrant part of the head of essence
Effect.
Second position firpene has distinctive turpentine oil fragrance, desiccated wood and rosin smell.It divides together each other with first position firpene
Isomers, fragrance is also approached with effect purposes with first position firpene.
Limonene has lemon characteristic perfume, and fragrance is clearly sent out thoroughly, can promoting or transferring fragrance.
Orange oil has the fragrance and gentle mouthfeel of fresh and sweet orange, is the aniseed of flavorant.
Lemon oil has Fresh Lemon fruity gas, the same with orange oil, because its fine odor is used extensively with comfortable mouthfeel
In food and drink.
Laurene is colourless to pale yellow oily liquid.With sweet tea tangerine taste and face cream gas, appropriate addition can enrich citrus
Fragrance makes it softer.
Cinnamic aldehyde is called cinnamic acid, is naturally occurring in Chinese cassia tree, cassia bark, wrinkled giant hyssop, in the plant such as hyacinth, with strong cassia bark
The fragrance of oil and cinnamon oil, gentle pungent fragrance breath.
Cinnamon oil has the special osmanthus sweet fragrance of Chinese cassia tree, is the characteristic perfume of Coca-Cola.
Citral is colourless or slightly yellow liquid, in strong citrus scented, is mainly used in preparing lemon, citrus and assorted water
Fruit type essence.
Geranial is the optical isomer of citral, usually colourless and weak yellow liquid.There is strong lemon smell.With
Citral is shared, with natural citris aromas true to nature.
Geranyl acetate is colourless liquid.It is fresh and sweet and soft, seemingly there is the fragrance of rose, bergamot, lavender.
Sinensal is yellow liquid, and with strong sweet orange fruity, aldehyde is fragrant.
Citronellol is colourless oil liquid, has fresh rose like special aroma and lemon flores aurantii fragrance, slightly bitter taste.
Geranyl propionate has fresh and sweet fruity and the fragrance of rose, taste slightly bitter.Citrus water can be lifted
The fruity breath of fruit.
Eugenol has strong cloves fragrance and gentle pungent fragrance.
The ultimate food additive that ethylmaltol is a kind of safety non-toxic, purposes is wide, effect is good, consumption is few, be tobacco,
The good fragrance synergist such as food, beverage, essence, fruit wine, daily cosmetics, improving fragrance and enhancing to food have aobvious
Effect is write, sweetened effect is played to sweet food, and the food storing phase can be extended.
Furanone is micro to be present in food, tobacco, beverage, and fragrance threshold values is that 0.04ppb just there is obvious flavouring to repair
Effect is adornd, thus is widely used as the fumet of food, tobacco, beverage.
Raspberry ketone has sweet raspberry fragrance, and fruit sweet tea, fragrance remaining time is long.
Cinnamic alcohol is mainly used in preparing the flavor essences such as apricot, peach, raspberry, Lee, there is gentle, lasting and comfortable fragrance, fragrance
Gracefulness, also serves as fixastive.
Cinnamyl acetate is naturally occurring in cassia oil.Can as cinnamic alcohol dressing agent, the fixation ability having had can prepare meat
The flavoring essences such as osmanthus, apple, cherry, pineapple, in flavouring and candy.
Chinese cymbidium have the banksia rose, and milk is widely used in the flavouring of food.
Ethyl vanillin is usually used in food flavouring, effect is notable in sweet chocolate and the aroma of vanillic aldehyde.
Coffee-extract is extracted by raw material of Rubiaceae coffee platymiscium coffee, mainly contain volatile ingredient, alkaloid,
Phenols and caffeic acid derivative etc., caffeine have stimulating central nervous system system, aid digestion, diuresis, sober up, relaxing smooth muscle,
Cardiac stimulant, regulation body metabolism, sterilization, resist the pharmacological actions such as disease, antipyretic-antalgic, and in the row such as medicine, food, beverage
Industry is widely used.
Caramel is the thick liquid or powder being boiled into maltose, sucrose etc., and dark brown has bitter taste.It is widely used in various foods
In product.
Fructose is a kind of most commonly seen ketohexose.It is present in honey, fruit, and glucose is bonded daily consumption
Sucrose.Fructose is mainly originated among natural fruit and cereal, with good taste, sugariness is high, glycemic index is low and is difficult
The advantages of causing carious tooth.The sugariness of fructose is 1.8 times of sucrose, is sugariness highest sugar in all natural sugars.
Glucose colourless crystallization or white crystalline or graininess powder.Odorless, taste sweet tea.
Aspartame is a kind of natural function oligosaccharide, will not carious tooth, sweet taste be pure, hygroscopicity is low, it is existing without stickness
As.The significantly raised of blood glucose will not be caused, be adapted to patients with diabetes mellitus.Because Aspartame is than about 200 times general of sugared sweet tea,
Contain less heat than general sucrose again；One gram of Aspartame there are about 4 kilocalories of heat.But make one to feel needed for sweet taste Ah
This Ba Tian amount is considerably less, so that the heat contained by it can be neglected, therefore also by widely as the substitute of sucrose.
Honey element belongs to non-nutritive synthetic sweetener, and its sugariness is 30 times of sucrose, and price is only three points of sucrose
One of, and its consumption unlike saccharin it is slightly many when have bitter taste, thus be used as international food additives.
The present invention selects above-mentioned raw materials and carries out compatibility, and each raw material acts synergistically that the effect of maximum can be played.
The invention provides a kind of electronic cigarette tobacco tar with Coca-Cola taste, the smoking need of smoker can not only be met
Ask, and enrich full with fragrance, may also reach up similar effect for drinking the pleasant feeling that Coca-Cola is brought.
Second aspect, the invention provides a kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
The savory essence mixing of Coca-Cola of atomized liquid and 1%-10% that mass percent is respectively 90%-99%,
Stir at room temperature, the electronic cigarette tobacco tar is made；
Wherein, the savory spermatophore of described Coca-Cola includes the component of following parts by weight：
0.1-2 parts of first position firpene, 0.1-2 part second firpenes, 1-30 Fen limonenes, 1-10 parts of orange oil, 1-20 parts of lemon oils,
0.1-0.5 parts of laurenes, 0.1-2 parts of cinnamic aldehydes, 0.1-5 parts of cinnamon oils, 0.1-10 parts of citrals, 0.1-5 parts of geranials, 1-10 parts
Geranyl acetate, 0.1-5 part sinensal, 1-10 parts of citronellols, 1-10 parts of geranyl propionates, 0.1-5 parts of eugenols, 0.1-2 parts
Ethylmaltol, 0.1-3 part furanone, 0.1-5 parts of raspberry ketones, 1-25 parts of cinnamic alcohols, 1-10 parts of cinnamyl acetates, 1-15 parts of chinese cymbidiums
Element, 1-15 parts of Ethyl vanillins and 0.1-2 parts of coffee-extracts.
In embodiment of the present invention, the electronic cigarette tobacco tar also includes food additives, and the food additives include Jiao
At least one of sugar, fructose, glucose, Aspartame and honey element.Alternatively, the preparation method of the electronic cigarette tobacco tar,
Comprise the following steps：
Atomized liquid, the savory essence of Coca-Cola and food additives are mixed, uniform, the obtained electricity is stirred at room temperature
Sub- cigarette tobacco tar.
In embodiment of the present invention, the preparation method of the electronic cigarette tobacco tar comprises the following steps：
By propane diols, glycerine, the savory essence of Coca-Cola, caramel, fructose, Aspartame, each raw material of honey element by certain
Ratio, which is uniformly mixed to form at normal temperatures, produces the electronic cigarette tobacco tar.
In embodiment of the present invention, 10-30 parts of organic solvent is also included in Coca-Cola essence, it is described organic molten
Agent is propane diols.
In embodiment of the present invention, the savory smart preparation method of Coca-Cola includes：
By 0.1-2 parts of first position firpenes, 0.1-2 portions of second position firpenes, 1-30 Fen limonenes, 1-10 portions of orange oils, 1-20 portions of lemons
Oil, 0.1-0.5 parts of laurenes, 0.1-2 parts of cinnamic aldehydes, 0.1-5 parts of cinnamon oils, 0.1-10 parts of citrals, 0.1-5 parts of geranials, 1-
10 parts of geranyl acetates, 0.1-5 parts of sinensals, 1-10 parts of citronellols, 1-10 parts of geranyl propionates, 0.1-5 parts of eugenols, 0.1-
2 parts of ethylmaltols, 0.1-3 parts of furanones, 0.1-5 parts of raspberry ketones, 1-25 parts of cinnamic alcohols, 1-10 parts of cinnamyl acetates, 1-15 parts
Vanillic aldehyde, 1-15 part Ethyl vanillin and 0.1-2 parts of coffee-extracts are mixed with 10-30 parts of organic solvent, are made after dissolving
The savory essence of Coca-Cola.
The preparation method for the electronic cigarette tobacco tar that second aspect of the present invention is provided, by by atomized liquid and the savory essence of Coca-Cola
Be simply mixed, the electronic cigarette tobacco tar for Coca-Cola taste that fragrance is abundant, comfortable taste, satisfaction are good, the preparation side has been made
Method is simple to operation, is adapted to industrialization production.
Embodiment 1：
A kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
(1) the savory smart preparation of Coca-Cola：Weigh first position firpene (0.01g), second position firpene (0.02g), limonenes (2g),
Orange oil (0.2g), lemon oil (0.3g), laurene (0.01g), cinnamic aldehyde (0.02g), cinnamon oil (0.04g), citral
(0.5g), geranial (0.4g), geranyl acetate (0.1g), sinensal (0.05g) citronellol (0.2g), geranyl propionate
(0.1g), eugenol (0.2g), ethylmaltol (0.05g), furanone (0.2g), raspberry ketone (0.2g), cinnamic alcohol (2g), second
Sour osmanthus ester (0.7g), vanillic aldehyde (0.5g), Ethyl vanillin (0.2g), coffee-extract (0.1g), add propylene glycol solvent extremely
10g, it is standby after dissolving.
(2) preparation of electronic cigarette tobacco tar：In clean reactor, propane diols (75g) and glycerine are separately added into
(15g), add Coca-Cola savory smart (7g) obtained by above-mentioned allotment, caramel (1g), fructose (0.5g), glucose (0.1g) Ah
This Ba Tian (0.3g), honey element (0.1g), it is well mixed to produce Coca-Cola taste type electronic cigarette tobacco tar.
Embodiment 2：
A kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
(1) the savory smart preparation of Coca-Cola：Weigh first position firpene (0.02g), second position firpene (0.03g), limonenes
(2.2g), orange oil (0.3g), lemon oil (0.3g), laurene (0.01g), cinnamic aldehyde (0.01g), cinnamon oil (0.04g), lemon
Aldehyde (0.55g), geranial (0.45g), geranyl acetate (0.15g), sinensal (0.05g) citronellol (0.15g), propionic acid spiceleaf
Ester (0.1g), eugenol (0.15g), ethylmaltol (0.04g), furanone (0.2g), raspberry ketone (0.25g), cinnamic alcohol
(1.8g), cinnamyl acetate (0.6g), vanillic aldehyde (0.3g), Ethyl vanillin (0.4g), coffee-extract (0.1g), add the third two
Alcoholic solvent is standby after dissolving to 10g.
(2) preparation of electronic cigarette tobacco tar：In clean reactor, propane diols (75g) and glycerine are separately added into
(15g), adds Coca-Cola savory smart (7g), caramel (0.8g), fructose (0.6g), the glucose (0.2g) obtained by above-mentioned allotment
Aspartame (0.25g), honey element (0.15g), it is well mixed to produce Coca-Cola taste type electronic cigarette tobacco tar.
Embodiment 3：
A kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
(1) the savory smart preparation of Coca-Cola：Weigh first position firpene (0.02g), second position firpene (0.02g), limonenes
(2.2g), orange oil (0.65g), lemon oil (0.55g), laurene (0.01g), cinnamic aldehyde (0.01g), cinnamon oil (0.03g), lemon
Lemon aldehyde (0.55g), geranial (0.25g), geranyl acetate (0.15g), sinensal (0.05g) citronellol (0.15g), propionic acid are fragrant
Leaf ester (0.1g), eugenol (0.1g), ethylmaltol (0.035g), furanone (0.15g), raspberry ketone (0.25g), cinnamic alcohol
(1.6g), cinnamyl acetate (0.7g), vanillic aldehyde (0.2g), Ethyl vanillin (0.3g), coffee-extract (0.1g), add the third two
Alcoholic solvent is standby after dissolving to 10g.
(2) preparation of electronic cigarette tobacco tar：In clean reactor, propane diols (75g) and glycerine are separately added into
(15g), adds Coca-Cola savory smart (7g), caramel (0.6g), fructose (0.6g), the glucose (0.3g) obtained by above-mentioned allotment
Aspartame (0.25g), honey element (0.25g), it is well mixed to produce Coca-Cola taste type electronic cigarette tobacco tar.
Embodiment 4：
A kind of preparation method of electronic cigarette tobacco tar, comprises the following steps：
(1) the savory smart preparation of Coca-Cola：Weigh first position firpene (0.01g), second position firpene (0.01g), limonenes (2g),
Orange oil (0.75g), lemon oil (0.6g), laurene (0.01g), cinnamic aldehyde (0.01g), cinnamon oil (0.04g), citral
(0.35g), geranial (0.25g), geranyl acetate (0.1g), sinensal (0.05g) citronellol (0.1g), geranyl propionate
(0.1g), eugenol (0.1g), ethylmaltol (0.035g), furanone (0.15g), raspberry ketone (0.25g), cinnamic alcohol
(1.4g), cinnamyl acetate (0.7g), vanillic aldehyde (0.25g), Ethyl vanillin (0.45g), coffee-extract (0.15g), are added
Propylene glycol solvent is standby after dissolving to 10g.
(2) preparation of electronic cigarette tobacco tar：In clean reactor, propane diols (75g) and glycerine are separately added into
(15g), adds Coca-Cola savory smart (7g), caramel (0.65g), fructose (0.65g), the glucose obtained by above-mentioned allotment
(0.2g) Aspartame (0.25g), honey element (0.25g), it is well mixed to produce Coca-Cola taste type electronic cigarette tobacco tar.
Embodiment 5：
Electronic cigarette tobacco tar in above-described embodiment is added in electronic cigarette device and carries out sensory effects evaluation respectively.
Sensory effects evaluation method comprises the following steps：
There is provided 6 evaluation indexes, including excitant, satisfaction, feature style, similarity, fragrance and smoke amount, and root
According to every evaluation index different score values are assigned to the Different Effects degree of electronic cigarette tobacco tar aesthetic quality.
The excitant refers to：Suck flue gas of the electronic cigarette tobacco tar through atomization generation includes oral cavity, throat to sense organ
With nasal cavity produce discomfort by；
The satisfaction refers to：Flue gas strength, concentration and the note that electronic cigarette tobacco tar is produced through atomization are on sense organ
The comprehensive impression of generation；
The feature style refers to：A kind of electronic cigarette tobacco tar is different from the sense of other homogeneous e cigarette tobacco tar in pleasant feeling
Official's Main Differences are showed；
The similarity refers to：During smokeing panel test sensory feel to truly drinking the similar journey that Coca-Cola is experienced
Degree；
The fragrance refers to：The good and bad degree of pleasant breath is felt during smokeing panel test by smell and the sense of taste；
The smoke amount refers to：Electronic cigarette tobacco tar through atomization produce exhaust gas volumn number.
The member of smoking of 9 people is set, everyone a electronic cigarette tobacco tar sensory quality assessment table, using the marking mode secretly commented,
Smoked panel test method using overall circulation, electronic cigarette tobacco tar is aspirated, 6 sensory quality assessment index score values in foundation table 1
Implication, carries out comprehensive grading, every evaluation index presses 15 points using hundred-mark system point system to the aesthetic quality of electronic cigarette tobacco tar
System and twenty point system scoring.
The electronic cigarette tobacco tar sensory quality assessment index of table 1 and score value implication table
Evaluation method：Evaluation index and score value in table 1, member of smoking should carry out aesthetic quality to each evaluation index
Evaluate, and record its evaluation result, the minimum score unit of score value is 0.5.
As a result count：Remove one minimum point and a best result in the sensory quality assessment result of all members of smoking, count
The arithmetic mean of instantaneous value of remaining effective single item evaluation index scoring is calculated, as a result retains two-decimal, the sense of last electronic cigarette tobacco tar
Official's quality evaluation comprehensive grading is the arithmetic mean of instantaneous value sum for calculating each single index scoring, obtains total score, as a result retains one
Decimal.Total score score value is higher, then it represents that the sensory evaluation effect of this electronics tobacco tar is better, the evaluation of above-described embodiment comparative example
It the results are shown in Table 2.
The evaluation result of the embodiment of table 2
Integrated comparative, the effect of embodiment 4 is optimal.Used food flavor species is different to 6 index generations with ratio
Influence.The smoke amount of embodiment 1 foot, but head perfume (or spice) is on the weak side, stimulates, and lacks the refreshing aroma of taste sweet orange lemon before Coca-Cola；It is real
Apply the head portrait of example 2 to pierce partially, whole style is varied from；Embodiment 3 perfume (or spice) it is somewhat stiff some；The whole structure of embodiment 4 compares
Satisfactory, Coca-Cola local flavor relatively enriches true to nature, comfortable taste.
Embodiment described above only expresses the several embodiments of the present invention, and it describes more specific and detailed, but simultaneously
Therefore the limitation to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for one of ordinary skill in the art
For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to the guarantor of the present invention
Protect scope.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.
Claims (10)
1. a kind of electronic cigarette tobacco tar, it is characterised in that include the component of following mass percent：
90%-99% atomized liquid, the 1%-10% savory essence of Coca-Cola；
Wherein, the savory spermatophore of described Coca-Cola includes the component of following parts by weight：
0.1-2 parts of first position firpenes, 0.1-2 parts of second position firpenes, 1-30 Fen limonenes, 1-10 parts of orange oils, 1-20 parts of lemon oils, 0.1-
0.5 part of laurene, 0.1-2 parts of cinnamic aldehydes, 0.1-5 parts of cinnamon oils, 0.1-10 parts of citrals, 0.1-5 parts of geranials, 1-10 parts of acetic acid
Geraniol ester, 0.1-5 part sinensal, 1-10 parts of citronellols, 1-10 parts of geranyl propionates, 0.1-5 parts of eugenols, 0.1-2 parts of ethyls
Maltol, 0.1-3 part furanone, 0.1-5 parts of raspberry ketones, 1-25 parts of cinnamic alcohols, 1-10 parts of cinnamyl acetates, 1-15 parts of vanillic aldehydes,
1-15 parts of Ethyl vanillins and 0.1-2 parts of coffee-extracts.
2. electronic cigarette tobacco tar as claimed in claim 1, it is characterised in that in the electronic cigarette tobacco tar, Coca-Cola taste
The mass percent of essence is 5%-10%.
3. electronic cigarette tobacco tar as claimed in claim 1, it is characterised in that the electronic cigarette tobacco tar also includes food additives,
The food additives include at least one of caramel, fructose, glucose, Aspartame and honey element.
4. electronic cigarette tobacco tar as claimed in claim 3, it is characterised in that in the electronic cigarette tobacco tar, the food additives
Mass percent be 1%-15%.
5. electronic cigarette tobacco tar as claimed in claim 3, it is characterised in that in the electronic cigarette tobacco tar, the quality of the caramel
Percentage is 0.5%-5%, and the mass percent of the fructose is 0.1%-5%, and the mass percent of the glucose is
0.1%-5%, the mass percent of the Aspartame is 0.01%-0.5%, and the mass percent of the honey element is
0.1%-1%.
6. electronic cigarette tobacco tar as claimed in claim 1, it is characterised in that also include 10-30 in the savory essence of Coca-Cola
The organic solvent of part, the organic solvent includes propane diols.
7. electronic cigarette tobacco tar as claimed in claim 1, it is characterised in that the atomized liquid includes propane diols and glycerine.
8. electronic cigarette tobacco tar as claimed in claim 7, it is characterised in that in the electronic cigarette tobacco tar, the matter of the propane diols
Amount percentage is 45%-80%, and the mass percent of the glycerine is 1%-30%.
9. a kind of preparation method of electronic cigarette tobacco tar, it is characterised in that comprise the following steps：
The savory essence mixing of Coca-Cola of atomized liquid and 1%-10% that mass percent is respectively 90%-99%, in room temperature
Under stir, be made the electronic cigarette tobacco tar；
Wherein, the savory spermatophore of described Coca-Cola includes the component of following parts by weight：
0.1-2 parts of first position firpenes, 0.1-2 parts of second position firpenes, 1-30 Fen limonenes, 1-10 parts of orange oils, 1-20 parts of lemon oils, 0.1-
0.5 part of laurene, 0.1-2 parts of cinnamic aldehydes, 0.1-5 parts of cinnamon oils, 0.1-10 parts of citrals, 0.1-5 parts of geranials, 1-10 parts of acetic acid
Geraniol ester, 0.1-5 part sinensal, 1-10 parts of citronellols, 1-10 parts of geranyl propionates, 0.1-5 parts of eugenols, 0.1-2 parts of ethyls
Maltol, 0.1-3 part furanone, 0.1-5 parts of raspberry ketones, 1-25 parts of cinnamic alcohols, 1-10 parts of cinnamyl acetates, 1-15 parts of vanillic aldehydes,
1-15 parts of Ethyl vanillins and 0.1-2 parts of coffee-extracts.
10. electronic cigarette tobacco tar as claimed in claim 9, it is characterised in that the electronic cigarette tobacco tar also includes food additives,
The food additives include at least one of caramel, fructose, glucose, Aspartame and honey element.
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110725156A (en) * | 2019-09-20 | 2020-01-24 | 河南中烟工业有限责任公司 | Milk-flavor essence, milk-flavor gloss oil and application of milk-flavor gloss oil to tipping paper for cigarettes |
| CN110846132A (en) * | 2019-11-27 | 2020-02-28 | 安徽香博士芳香技术研究院有限公司 | Production formula and preparation process of electronic cigarette liquid essence |
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Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1354989A (en) * | 2000-11-28 | 2002-06-26 | 上海家化（集团）有限公司 | White lemon type cole essence |
| CN105124750A (en) * | 2015-07-27 | 2015-12-09 | 浙江中烟工业有限责任公司 | Sweet and fragrant electronic cigarette liquid and preparation method thereof |
| CN105595404A (en) * | 2015-10-20 | 2016-05-25 | 贵州中烟工业有限责任公司 | Tobacco buccal tablet and preparation method thereof |
| KR20160124569A (en) * | 2015-04-20 | 2016-10-28 | 주식회사 비타씨그코리아 | Liquid phase composition for smoking habit helping apparatus |
| CN106174683A (en) * | 2016-07-29 | 2016-12-07 | 福建中烟工业有限责任公司 | A kind of compositions and the tobacco juice for electronic smoke containing said composition |
-
2017
- 2017-05-10 CN CN201710327614.4A patent/CN107125803B/en active Active
Patent Citations (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1354989A (en) * | 2000-11-28 | 2002-06-26 | 上海家化（集团）有限公司 | White lemon type cole essence |
| KR20160124569A (en) * | 2015-04-20 | 2016-10-28 | 주식회사 비타씨그코리아 | Liquid phase composition for smoking habit helping apparatus |
| CN105124750A (en) * | 2015-07-27 | 2015-12-09 | 浙江中烟工业有限责任公司 | Sweet and fragrant electronic cigarette liquid and preparation method thereof |
| CN105595404A (en) * | 2015-10-20 | 2016-05-25 | 贵州中烟工业有限责任公司 | Tobacco buccal tablet and preparation method thereof |
| CN106174683A (en) * | 2016-07-29 | 2016-12-07 | 福建中烟工业有限责任公司 | A kind of compositions and the tobacco juice for electronic smoke containing said composition |
Non-Patent Citations (2)
| Title |
|---|
| 张承曾等: "《日用调香术》", 31 October 1989 * |
| 林翔云: "《香料香精词典》", 31 March 2007 * |
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| CN110846132A (en) * | 2019-11-27 | 2020-02-28 | 安徽香博士芳香技术研究院有限公司 | Production formula and preparation process of electronic cigarette liquid essence |
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