CN106858703A - Tobacco juice for electronic smoke and electronic cigarette with milk odor type - Google Patents

Tobacco juice for electronic smoke and electronic cigarette with milk odor type Download PDF

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Publication number
CN106858703A
CN106858703A CN201710082028.8A CN201710082028A CN106858703A CN 106858703 A CN106858703 A CN 106858703A CN 201710082028 A CN201710082028 A CN 201710082028A CN 106858703 A CN106858703 A CN 106858703A
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China
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parts
ethyl
acid
essence
milk
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CN201710082028.8A
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Chinese (zh)
Inventor
姚继德
潘松
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Shenzhen Hangsen Star Technology Co Ltd
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Shenzhen Hangsen Star Technology Co Ltd
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Priority to CN201710082028.8A priority Critical patent/CN106858703A/en
Publication of CN106858703A publication Critical patent/CN106858703A/en
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    • AHUMAN NECESSITIES
    • A24TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24BMANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10Chemical features of tobacco products or tobacco substitutes
    • A24B15/16Chemical features of tobacco products or tobacco substitutes of tobacco substitutes

Abstract

The invention discloses a kind of tobacco juice for electronic smoke and electronic cigarette with milk odor type, the tobacco juice for electronic smoke includes basal liquid, essence and cream enzymatic hydrolyzed extract.The quality parts ratio of basal liquid, essence and cream enzymatic hydrolyzed extract is 90 parts~99 parts:1 part~10 parts:1 part~10 parts.By the blending means of science by spices by rational allocation, make the essence with abundant milk fragrance, and the essence of allotment is provided commonly in tobacco juice for electronic smoke using cream enzymatic hydrolyzed extract, it is successfully prepared out a kind of milk odor type tobacco juice for electronic smoke of odor type stabilization.

Description

Tobacco juice for electronic smoke and electronic cigarette with milk odor type
Technical field
The present invention relates to tobacco juice technical field, more particularly, to a kind of tobacco juice for electronic smoke and electronics with milk odor type Cigarette.
Background technology
Electronic cigarette controls smog output quantity and working condition by high-tech silicon and airflow sensor device, will contain extraction The tobacco tar solution atomization of thing, essence etc. into particulate, by pulmonary absorption, while discharge simulation smoke.It is fragrant without tradition in smog Tar and other harmful components in cigarette, will not also produce and diffuse or curl up the second-hand-cigarette in confined space.Electronic cigarette can be made Be the good substitute of traditional cigarette, but for a long time, electronic cigarette market present production at home, market lattice abroad Office.Taken a stand in the related meeting of State-level, to have paid much attention to the research and development of the novel tobacco such as electronic cigarette product, with middle cigarette pair Electronic cigarette attitude changes, and electronic cigarette policy risk is substantially reduced.Under the increasingly serious background of Tobacco Control, electronic cigarette is in China's demand Startup is Great possibility, and China possesses smoker more than 300,000,000, and the market space is huge.
Popularization of the absorption taste port sense of electronic cigarette to product has important effect, and plain chocolate not only has very to health Big help, while the material with milk class fragrance can excite the appetite of people.However, because pure natural milk is guaranteed the quality Phase is short, apt to deteriorate in addition tobacco juice.Although therefore in the market has the tobacco juice of various suction tastes, do not occur still The tobacco juice for electronic smoke of the milk odor type with odor type stabilization.
The content of the invention
Based on this, it is necessary to provide a kind of tobacco juice for electronic smoke and electronic cigarette of the milk odor type of odor type stabilization.
A kind of tobacco juice for electronic smoke with milk odor type, including basal liquid, essence and cream enzymatic hydrolyzed extract, the base The quality parts ratio of plinth liquid, the essence and the cream enzymatic hydrolyzed extract is 90 parts~99 parts:1 part~10 parts:1 part~10 Part, the essence is selected from vanillic aldehyde, Ethyl vanillin, capric acid, lauric acid/dodecanoic acid, tetradecylic acid, hexadecylic acid, ethyl caprate, lauric acid/dodecanoic acid second Ester, ethyl myristate, ethyl palmitate, gamma decalactone, milk lactone, third dodecalactone, delta-decalactone and fourth position At least one in dodecalactone.
In one embodiment, the essence includes 5 parts~30 parts of vanillic aldehyde, Ethyl vanillin 5 according to the mass fraction Part~30 parts, 0.1 part~10 parts of capric acid, 0.1 part~20 parts of lauric acid/dodecanoic acid, 0.1 part~20 parts of tetradecylic acid, hexadecylic acid 0.1 part~10 Part, 0.1 part~5 parts of ethyl caprate, 0.1 part~10 parts of ethyl laurate, 0.5 part~20 parts of ethyl myristate, ethyl palmitate 0.5 part~30 parts, 0.5 part~10 parts of gamma decalactone, 1 part~20 parts, third 0.1 part~10 parts of dodecalactone of milk lactone, 1 part~20 parts of delta-decalactone and 1 part~20 parts of the dodecalactone in fourth position.
In one embodiment, the essence includes 10 parts~15 parts of vanillic aldehyde, Ethyl vanillin according to the mass fraction 15 parts~20 parts, 0.1 part~1 part of capric acid, 0.1 part~0.2 part of lauric acid/dodecanoic acid, 0.4 part~0.5 part of tetradecylic acid, 0.4 part of hexadecylic acid~ 0.5 part, 0.1 part~0.2 part of ethyl caprate, 0.2 part~0.5 part of ethyl laurate, 1 part~6 parts of ethyl myristate, hexadecylic acid second In 3 parts~8 parts of ester, 1 part~2 parts of gamma decalactone, 5 parts~6 parts, third 2 parts~4 parts of dodecalactone of milk lactone, fourth a last of the ten Heavenly stems 8 parts~10 parts of ester and 1 part~20 parts of the dodecalactone in fourth position.
In one embodiment, also including essence auxiliary element, the essence auxiliary element is selected from ethyl butyrate, lactic acid In ethyl ester, ethyl 2-methylbutyrate, raspberry ketone, isobutyric acid chinese cymbidium ester, anisic aldehyde, lactic acid and benzyl carbinol at least one Kind.
In one embodiment, the essence auxiliary element and the quality parts ratio of the essence are 1 part~3 parts:4 parts ~9 parts.
In one embodiment, the essence auxiliary element includes 1 part~10 parts of ethyl butyrate, breast according to the mass fraction 1 part~20 parts of acetoacetic ester, 0.5 part~10 parts of ethyl 2-methylbutyrate, 0.1 part~10 parts of raspberry ketone, isobutyric acid chinese cymbidium ester 0.5 0.1 part~10 parts of part~10 parts, 0.1 part~5 parts of anisic aldehyde, 0.1 part~20 parts of lactic acid and benzyl carbinol.
In one embodiment, the essence auxiliary element includes 3 parts~5 parts of ethyl butyrate, breast according to the mass fraction 4 parts~6 parts of acetoacetic ester, 2 parts~3 parts of ethyl 2-methylbutyrate, 2 parts~6 parts of raspberry ketone, 5 parts~6 parts of isobutyric acid chinese cymbidium ester, 0.1 part~2 parts of 0.1 part~0.2 part of anisic aldehyde, 0.5 part~2 parts of lactic acid and benzyl carbinol.
In one embodiment, the basal liquid is selected from least one in propane diols, glycerine and ethanol.
In one embodiment, the basal liquid includes that quality parts ratio is 10 parts~80 parts:The third of 10 parts~80 parts Glycol and glycerine.
A kind of electronic cigarette, is mounted with the tobacco juice for electronic smoke with milk odor type in the electronic cigarette.
The above-mentioned tobacco juice for electronic smoke with milk odor type, does not use pure natural milk, but by blending mode by perfume (or spice) Material makes the essence with abundant milk fragrance by rational allocation, and the essence that will be allocated using cream enzymatic hydrolyzed extract It is provided commonly in tobacco juice for electronic smoke.The wherein mass fraction of the basal liquid of tobacco juice for electronic smoke, essence and cream enzymatic hydrolyzed extract Than being 90 parts~99 parts:1 part~10 parts:1 part~10 parts, close to crude milk local flavor and its cost is reduced to greatest extent, success The milk odor type tobacco juice for electronic smoke for preparing a kind of odor type stabilization.
Specific embodiment
To enable the above objects, features and advantages of the present invention more obvious understandable, with reference to of the invention specific Implementation method is described in detail.Elaborate many details in order to fully understand the present invention in the following description.But It is that the present invention can be implemented with being much different from other manner described here, those skilled in the art can be without prejudice to originally Similar improvement is done in the case of invention intension, therefore the present invention is not limited by following public specific implementation.
The tobacco juice for electronic smoke with milk odor type of one implementation method, including basal liquid, essence and cream enzymolysis and extraction Thing.Wherein the quality parts ratio of basal liquid, essence and cream enzymatic hydrolyzed extract is 90 parts~99 parts:1 part~10 parts:1 part~ 10 parts.Essence be selected from vanillic aldehyde, Ethyl vanillin, capric acid, lauric acid/dodecanoic acid, tetradecylic acid, hexadecylic acid, ethyl caprate, ethyl laurate, Ethyl myristate, ethyl palmitate, gamma decalactone, milk lactone, third dodecalactone, delta-decalactone and fourth position 12 At least one in lactone.
Basal liquid can improve amount of smoke, and larynx sense is hit in generation, while also functioning to the dissolved dilution effect to essence.Wherein In one embodiment, basal liquid is selected from least one in propane diols, glycerine and ethanol, and the atomized liquid can produce smog Larynx sense is hit in generation.It should be noted that the composition of basal liquid is not limited to above-mentioned several compositions, the solvent of cognate interaction can be reached Can.
Wherein in one embodiment, basal liquid includes that quality parts ratio is 10 parts~80 parts:The third the two of 10 parts~80 parts Alcohol and glycerine.
Wherein in one embodiment, essence includes 5 parts~30 parts of vanillic aldehyde, 5 parts of Ethyl vanillin according to the mass fraction ~30 parts, 0.1 part~10 parts of capric acid, 0.1 part~20 parts of lauric acid/dodecanoic acid, 0.1 part~20 parts of tetradecylic acid, 0.1 part~10 parts of hexadecylic acid, 0.1 part~5 parts of ethyl caprate, 0.1 part~10 parts of ethyl laurate, 0.5 part~20 parts of ethyl myristate, ethyl palmitate 0.5 Part~30 parts, 0.5 part~10 parts of gamma decalactone, milk lactone 1 part~20 parts, third 0.1 part~10 parts of dodecalactone, Ding Wei 1 part~20 parts of decalactone and 1 part~20 parts of the dodecalactone in fourth position.
The essence that the spices of each component is deployed into has abundant milk fragrance, and its component is the spices of food grade, By synthesis or commercially available purchase.
Wherein, chinese cymbidium have strong milk, the effect with flavouring.
Ethyl vanillin is in sweet chocolate and the aroma of vanillic aldehyde.
Capric acid has oranges and tangerines, rose, fatty breath, can be used to modify milk taste.
Lauric acid/dodecanoic acid has the adipocere fragrance of rose, in fatty fragrant.
Tetradecylic acid is a kind of saturated higher fatty acid, with Typical fatty fragrance, for milk taste and mixture.
Hexadecylic acid is a kind of saturated higher fatty acid, with faint fatty fragrance.
Ethyl caprate has coconut aroma, for milk taste blending.
Ethyl laurate has the fatty taste of peanut fragrance.
Ethyl myristate smell is faint, can increase fragrance remaining time as fixastive.
Ethyl palmitate has faint wax fragrant, milk, and can make fixastive increases fragrance remaining time.
Gamma decalactone has strong coconut fragrant, peach fragrance.
Milk lactone has strong milk characteristic perfume.
Third dodecalactone has fine and smooth milk and peach fragrance.
Delta-decalactone has creamy, and coconut is fragrant.
Fourth position dodecalactone has cream fragrance and fruity fragrance.
Wherein in one embodiment, capric acid, lauric acid/dodecanoic acid in essence, tetradecylic acid, hexadecylic acid, ethyl caprate, lauric acid/dodecanoic acid It it is 0 part when at least two is different in ethyl ester, ethyl myristate, ethyl palmitate, gamma decalactone and third dodecalactone.
Wherein in one embodiment, essence includes that 10 parts~15 parts of vanillic aldehyde vanillic aldehyde, ethyl are fragrant according to the mass fraction Blue 15 parts~20 parts of element, 0.1 part~1 part of capric acid, 0.1 part~0.2 part of lauric acid/dodecanoic acid, 0.4 part~0.5 part of tetradecylic acid, hexadecylic acid 0.4 Part~0.5 part, 0.1 part~0.2 part of ethyl caprate, 0.2 part~0.5 part of ethyl laurate, 1 part~6 parts of ethyl myristate, 16 3 parts~8 parts of acetoacetic ester, 1 part~2 parts of gamma decalactone, milk lactone 5 parts~6 parts, third 2 parts~4 parts of dodecalactone, Ding Wei 8 parts~10 parts of decalactone and 1 part~20 parts of the dodecalactone in fourth position.
Wherein in one embodiment, essence includes 5 parts~30 parts of vanillic aldehyde, 5 parts of Ethyl vanillin according to the mass fraction ~30 parts, 1 part~20 parts of milk lactone, 1 part~20 parts of delta-decalactone and 1 part~20 parts of the dodecalactone in fourth position.Only contain The essence and basal liquid and cream enzyme of vanillic aldehyde, Ethyl vanillin, milk lactone, delta-decalactone and fourth position dodecalactone The tobacco juice for electronic smoke formed after solution extract mixing also still has plain chocolate note, but fragrance is slightly worse with satisfaction.
The innovation of above-mentioned tobacco juice for electronic smoke is not use pure natural milk, but will be eaten by blending mode With level spices by rational allocation, the essence with abundant milk fragrance is made, and will allocate using milk enzymatic hydrolyzed extract Milk flavour be provided commonly for the tobacco juice of electronic cigarette, close to crude milk local flavor and reduce its cost to greatest extent, prepare one Brand-new tobacco juice for electronic smoke is planted, the tobacco juice for electronic smoke has the note of plain chocolate.
It should be noted that, although having used the original with dense milk characteristic perfume in the formula of above-mentioned tobacco juice for electronic smoke Material milk lactone, but how to select the type and quantity of remaining each spices and match precisely to mix plain chocolate with milk lactone Odor type, it is by no means easy.In fact, this is spices allocates industrial hard nut to crack, because only edible essence and flavoring agent Just there are as many as thousands of kinds, therefrom select all uncertain several combination of species and number and determine their own appropriate amount Precisely to mix the note of plain chocolate, its limited trials absolutely not can just be completed, because only between thousands of kinds of spices The uncertain number of combinations of number be exactly astronomical figure, still more it is also contemplated that the influence factor of the content of each component, then treat Bigger surprising of the assembled scheme number of screening, it is impossible to completed by limited trials.The electronic cigarette of above example Tobacco juice creatively proposes such formula combination, the note of accurate reproducing plain chocolate, and because without using pure natural Milk, therefore also in the absence of the problem that apt to deteriorate and fragrance is unstable.
Certainly, essence auxiliary element can also be included in tobacco juice for electronic smoke, wherein, essence auxiliary element is selected from butyric acid second In ester, ethyl lactate, ethyl 2-methylbutyrate, raspberry ketone, isobutyric acid chinese cymbidium ester, anisic aldehyde, lactic acid and benzyl carbinol It is at least one.
Ethyl butyrate has agile hesperidium fragrant, with sweetened promoting or transferring effect.
Ethyl lactate has fermentation aroma, and acid is fragrant.
Ethyl 2-methylbutyrate has apple fruity, fragrant and sweet.
Raspberry ketone has sweet raspberry fragrance, and fruit is sweet, and fragrance remaining time is long.
Isobutyric acid chinese cymbidium ester has graceful vanilla butter aroma.
Anisic aldehyde delicate fragrance, fennel green grass or young crops fragrance, like hawthorn.
Lactic acid has fermentation acid fragrant.
Benzyl carbinol has rose sweetness fragrance.
Wherein in one embodiment, essence auxiliary element is 1 part~3 parts with the quality parts ratio of essence:4 parts~9 parts. For example, essence auxiliary element can be 2.26 parts with the quality parts ratio of essence:5.87 parts, 2.22 parts:6.15 parts, 2.21 parts: 6.4 parts 7 or 2.4 parts:7.23 parts.
Wherein in one embodiment, essence auxiliary element includes 1 part~10 parts of ethyl butyrate, lactic acid according to the mass fraction 1 part~20 parts of ethyl ester, 0.5 part~10 parts of ethyl 2-methylbutyrate, 0.1 part~10 parts of raspberry ketone, 0.5 part of isobutyric acid chinese cymbidium ester 0.1 part~10 parts of~10 parts, 0.1 part~5 parts of anisic aldehyde, 0.1 part~20 parts of lactic acid and benzyl carbinol.
Wherein in one embodiment, ethyl 2-methylbutyrate, raspberry ketone, isobutyric acid chinese cymbidium in essence auxiliary element It it is 0 part when at least two is different in ester, anisic aldehyde, lactic acid and benzyl carbinol.
Wherein in one embodiment, essence auxiliary element includes 3 parts~5 parts of ethyl butyrate, lactic acid according to the mass fraction It is 4 parts~6 parts of ethyl ester, 2 parts~3 parts of ethyl 2-methylbutyrate, 2 parts~6 parts of raspberry ketone, 5 parts~6 parts of isobutyric acid chinese cymbidium ester, big 0.1 part~2 parts of 0.1 part~0.2 part of anisaldehyde, 0.5 part~2 parts of lactic acid and benzyl carbinol.Above-mentioned essence auxiliary element and essence Auxiliary element is used with essence compatibility, each raw material synergy, plays maximum effect so that the plain chocolate of tobacco juice for electronic smoke is fragrant Gas is denseer.
In the present invention, the effect of ethyl butyrate and ethyl lactate both ester perfumes is very crucial, has added both groups After point, tobacco juice for electronic smoke plain chocolate fragrance on the whole is especially prominent, and fragrance is denseer, and the residence time is longer, more surely It is fixed.But in fact, both components are in itself and without milk fragrance, there is ethyl butyrate agile hesperidium fragrance to cease, and lactic acid Ethyl ester has fermentation aroma, is ceased in sour fragrance.After this explanation adds both perfume compositions, may be deposited between various perfume compositions In some still not well known synergies, after causing these spices to be blended, strong plain chocolate note is generated.
Cream enzymatic hydrolyzed extract has dense fragrance, by the mass parts of basal liquid, essence and cream enzymatic hydrolyzed extract Number is than being 90 parts~99 parts:1 part~10 parts:After 1 part~10 parts of proportioning mixing, cream enzymatic hydrolyzed extract can cover basal liquid And the taste of the chemical stimulation in essence, flavouring is modified, so as to prepare, fragrance is abundant, comfortable taste, satisfaction are good The tobacco juice for electronic smoke of plain chocolate odor type.
Wherein in one embodiment, cream enzymatic hydrolyzed extract is with cream as raw material, by the decomposition of lipase The extract for obtaining.
Wherein in one embodiment, the quality parts ratio of basal liquid, essence and cream enzymatic hydrolyzed extract is 94 parts:5 Part:1 part.Basal liquid, essence and each raw material of cream enzymatic hydrolyzed extract are uniformly mixed system at normal temperatures by a certain percentage It is standby to obtain the tobacco juice for electronic smoke with milk odor type.
Wherein in one embodiment, nicotine is not contained in the tobacco juice for electronic smoke of the milk odor type, therefore will not during atomization The hazardous substances such as nicotine are produced, the harm without second-hand-cigarette can also be used completely in public, smoker's suction can not only be met Cigarette demand, and smell mouthfeel is true to nature comfortable, does not interfere with other people health.
The tobacco juice for electronic smoke of above-mentioned milk odor type by the blending means of science by spices by rational allocation, preparation is provided There is the essence of abundant milk fragrance, and the essence of allotment is provided commonly in tobacco juice for electronic smoke using cream enzymatic hydrolyzed extract, most Limits are close to crude milk local flavor and reduce its cost, are successfully prepared out a kind of electronic cigarette with stabilised milk odor type Liquid.
Additionally, the present invention also provides the electronic cigarette of an implementation method, it is mounted with the electronic cigarette above-mentioned with milk odor type Tobacco juice for electronic smoke.For example, the electronic cigarette includes body and tobacco juice for electronic smoke.It is mounted with body above-mentioned with milk odor type Tobacco juice for electronic smoke.When user is when above-mentioned electronic cigarette is aspirated, tobacco juice for electronic smoke atomization produces the smell of plain chocolate, excites people's Appetite, does not interfere with other people health during smoking.
It is below specific embodiment part.
Following examples unless otherwise instructed, the experimental technique of unreceipted actual conditions, generally according to normal condition.Implement Number in example is mass fraction.The cream enzymatic hydrolyzed extract for being used is Qingdao Hua Di food ingredients Co., Ltd, model It is the acid of B7018 butters.
Embodiment 1
The preparation of milk flavour:Weigh 10 parts of vanillic aldehyde (1g), 20 parts of Ethyl vanillin (2g), 0.1 part of capric acid 0.2 part of (0.01g), lauric acid/dodecanoic acid (0.02g), 0.4 part of tetradecylic acid (0.04g), hexadecylic acid 0.4 part of (0.04g), ethyl caprate 0.2 Part (0.02g), 0.4 part of ethyl laurate (0.04g), 1 part of ethyl myristate (0.1g), 3 parts of ethyl palmitate (0.3g), third 2 parts of decalactone (0.2g), 5 parts of milk lactone (0.5g), third 4 parts of dodecalactone (0.4g), 4 parts of delta-decalactone (0.4g), Fourth 8 parts of the dodecalactone in position (0.8g), 3 parts of ethyl butyrate (0.3g), 4 parts of ethyl lactate (0.4g), 2 parts of ethyl 2-methylbutyrate 6 parts of (0.2g), raspberry ketone (0.6g), 5 parts of isobutyric acid chinese cymbidium ester (0.5g), 0.1 part of anisic aldehyde (0.01g), 0.5 part of lactic acid 2 parts of (0.05g), benzyl carbinol (0.2g), it is 10g standby that total amount is dissolved and added to propylene glycol solvent.
The preparation of tobacco juice:In clean reactor, propane diols (24g) and glycerine (70g) are separately added into, added above-mentioned The well mixed electronic cigarette for obtaining final product plain chocolate taste type of milk flavour (5g) and cream enzymatic hydrolyzed extract (1g) obtained by allotment Tobacco juice.
Embodiment 2
The preparation of milk flavour:Weigh 12 parts of vanillic aldehyde (1.2g), 20 parts of Ethyl vanillin (2g), 0.1 part of capric acid 0.1 part of (0.01g), lauric acid/dodecanoic acid (0.01g), 0.3 part of tetradecylic acid (0.03g), hexadecylic acid 0.4 part of (0.04g), ethyl caprate 0.1 Part (0.01g), 0.5 part of ethyl laurate (0.05g), 2 parts of ethyl myristate (0.2g), 4 parts of ethyl palmitate (0.4g), third 1 part of decalactone (0.1g), 6 parts of milk lactone (0.6g), third 5 parts of dodecalactone (0.5g), 2 parts of delta-decalactone (0.2g), Fourth 8 parts of the dodecalactone in position (0.8g), 4 parts of ethyl butyrate (0.4g), 5 parts of ethyl lactate (0.5g), 3 parts of ethyl 2-methylbutyrate 4 parts of (0.3g), raspberry ketone (0.4g), 5 parts of isobutyric acid chinese cymbidium ester (0.5g), 0.2 part of anisic aldehyde (0.02g), 1 part of lactic acid 0.1 part of (0.1g), benzyl carbinol (0.01g), are dissolved with propylene glycol solvent and to add to 10g standby.
The preparation of tobacco juice:In clean reactor, propane diols (24g) and glycerine (70g) are separately added into, added above-mentioned Milk flavour (5g) and cream enzymatic hydrolyzed extract (1g) obtained by allotment are well mixed and obtain final product plain chocolate taste type electronic cigarette Liquid.
Embodiment 3
The preparation of milk flavour:Weigh 12 parts of vanillic aldehyde (1.2g), 16 parts of Ethyl vanillin (1.6g), 0.1 part of capric acid 0.2 part of (0.01g), lauric acid/dodecanoic acid (0.02g), 0.5 part of tetradecylic acid (0.05g), hexadecylic acid 0.5 part of (0.05g), ethyl caprate 0.1 Part (0.01g), 0.4 part of ethyl laurate (0.04g), 4 parts of ethyl myristate (0.4g), 6 parts of ethyl palmitate (0.6g), third 1 part of decalactone (0.1g), 6 parts of milk lactone (0.6g), third 5 parts of dodecalactone (0.5g), 3 parts of delta-decalactone (0.3g), Fourth 10 parts of the dodecalactone in position (1g), 4 parts of ethyl butyrate (0.4g), 5 parts of ethyl lactate (0.5g), 2 parts of ethyl 2-methylbutyrate 3 parts of (0.2g), raspberry ketone (0.3g), 6 parts of isobutyric acid chinese cymbidium ester (0.6g), 0.1 part of anisic aldehyde (0.01g), 1 part of lactic acid 1 part of (0.1g), benzyl carbinol (0.1g), are dissolved with propylene glycol solvent and to add to 10g standby.
The preparation of tobacco juice:In clean reactor, propane diols (24g) and glycerine (70g) are separately added into, added above-mentioned Milk flavour (5g) and cream enzymatic hydrolyzed extract (1g) obtained by allotment are well mixed and obtain final product plain chocolate taste type electronic cigarette Liquid.
Embodiment 4
The preparation of milk flavour:Weigh 15 parts of vanillic aldehyde (1.5g), 15 parts of Ethyl vanillin (1.5g), 1 part of capric acid 0.1 part of (0.1g), lauric acid/dodecanoic acid (0.01g), 0.5 part of tetradecylic acid (0.05g), 0.5 part of hexadecylic acid (0.05g), 0.1 part of ethyl caprate 0.2 part of (0.01g), ethyl laurate (0.02g), 6 parts of ethyl myristate (0.6g), 8 parts of ethyl palmitate (0.8g), third last of the ten Heavenly stems 2 parts of lactone (0.2g), 6 parts of milk lactone (0.6g), third 4 parts of dodecalactone (0.4g), delta-decalactone 4 parts of (0.4g), fourths 10 parts of the dodecalactone in position (1g), 5 parts of ethyl butyrate (0.5g), 5 parts of ethyl lactate (0.6g), 2 parts of ethyl 2-methylbutyrate 2 parts of (0.2g), raspberry ketone (0.2g), 6 parts of isobutyric acid chinese cymbidium ester (0.6g), 0.1 part of anisic aldehyde (0.01g), 2 parts of lactic acid 1 part of (0.2g), benzyl carbinol (0.1g), are dissolved with propylene glycol solvent and to add to 10g standby.
The preparation of tobacco juice:In clean reactor, propane diols (24g) and glycerine (70g) are separately added into, added above-mentioned Milk flavour (5g) and cream enzymatic hydrolyzed extract (1g) obtained by allotment are well mixed and obtain final product plain chocolate taste type electronic cigarette Liquid.
Evaluation test
Tobacco juice for electronic smoke in above-described embodiment 1~4 is added in electronic cigarette carries out sensory effects evaluation respectively.
Sensory effects evaluation method is comprised the following steps:
There is provided 6 evaluation indexes, including excitant, satisfaction, feature style, milk, fragrance and smoke amount, and according to Every evaluation index assigns different score values to the Different Effects degree of tobacco juice for electronic smoke aesthetic quality.
Excitant refers to:Suction tobacco juice for electronic smoke includes oral cavity, throat and nose through the flue gas that atomization is produced to sense organ The discomfort that chamber produces is received;
Satisfaction refers to:Flue gas strength, concentration and the note that tobacco juice for electronic smoke is produced through atomization on sense organ to producing Comprehensive impression;
Feature style refers to:A kind of tobacco juice for electronic smoke is different from the sense organ master of other homogeneous e cigarette tobacco juices in pleasant feeling Difference is wanted to show;
Milk refers to:Breath of the sensory feel to milk perfume during smokeing panel test;
Fragrance refers to:The good and bad degree of pleasant breath is felt during smokeing panel test by smell and the sense of taste;
Smoke amount refers to:Tobacco juice for electronic smoke through atomization produce exhaust gas volumn number.
The member of smoking of 9 people is set, everyone a tobacco juice for electronic smoke sensory quality assessment table, using the marking mode secretly commented, Smoked panel test method using overall circulation, tobacco juice for electronic smoke is aspirated, according to 6 sensory quality assessment index score values in table 1 Implication, comprehensive grading is carried out to the aesthetic quality of tobacco juice for electronic smoke using hundred-mark system point system, and every evaluation index presses 15 points System and twenty point system scoring.
Table 1:Tobacco juice for electronic smoke quality evaluation index and score value implication table
Evaluation method:Evaluation index and score value in table 1, member of smoking should carry out aesthetic quality to each evaluation index Evaluate, and record its evaluation result, the minimum score unit of score value is 0.5.
Result is counted:Remove one minimum point and a best result in the sensory quality assessment result of all members of smoking, count The arithmetic mean of instantaneous value of remaining effective single item evaluation index scoring is calculated, as a result retains two-decimal, the sense of last tobacco juice for electronic smoke Official's quality evaluation comprehensive grading is the arithmetic mean of instantaneous value sum for calculating each single index scoring, obtains total score, as a result retains one Decimal.Total score score value is higher, then it represents that the sensory evaluation effect of this tobacco juice for electronic smoke is better, and above-described embodiment 1~4 evaluates knot Fruit is shown in Table 2.
Table 2:The evaluation result of the comparative example of embodiment 1~4
Evaluation index Excitant Satisfaction Feature style Milk Fragrance Smoke amount Total score
Embodiment 1 12.00 16.50 12.00 12.20 11.40 15.60 79.7
Embodiment 2 11.00 16.40 12.10 12.00 11.40 15.50 78.4
Embodiment 3 12.00 16.40 12.00 11.90 11.30 15.60 79.2
Embodiment 4 12.00 16.60 12.10 12.40 11.60 15.50 80.2
Integrated comparative, has denseer plain chocolate odor type after the tobacco juice for electronic smoke atomization of embodiment 1~4.4 Ns of embodiment Milk aroma effect is optimal.The food flavor species and ratio for being used produce Different Effects to 6 indexs.The milk foot of embodiment 1, Slightly head is fragrant lays particular stress on, and stimulates, and slightly lacks the mellow sense of milk.The pungent perfume of embodiment 2 is on the high side, and whole style is varied from, with embodiment 4 It is more unstable compared to smell.The fat perfume of embodiment 3 is somewhat highlighted.The whole structure of embodiment 4 compares most satisfactory, ox Milk local flavor enriches true to nature.Comfortable taste.
Embodiment described above only expresses several embodiments of the invention, and its description is more specific and detailed, but simultaneously Therefore the limitation to the scope of the claims of the present invention can not be interpreted as.It should be pointed out that for one of ordinary skill in the art For, without departing from the inventive concept of the premise, various modifications and improvements can be made, these belong to guarantor of the invention Shield scope.Therefore, the protection domain of patent of the present invention should be determined by the appended claims.

Claims (10)

1. a kind of tobacco juice for electronic smoke with milk odor type, it is characterised in that including basal liquid, essence and cream enzymolysis and extraction Thing, the quality parts ratio of the basal liquid, the essence and the cream enzymatic hydrolyzed extract is 90 parts~99 parts:1 part~10 Part:1 part~10 parts, the essence is selected from vanillic aldehyde, Ethyl vanillin, capric acid, lauric acid/dodecanoic acid, tetradecylic acid, hexadecylic acid, capric acid second Ester, ethyl laurate, ethyl myristate, ethyl palmitate, gamma decalactone, milk lactone, third dodecalactone, in the fourth position last of the ten Heavenly stems At least one in ester and fourth position dodecalactone.
2. the tobacco juice for electronic smoke with milk odor type according to claim 1, it is characterised in that the essence presses mass parts Number meter includes 5 parts~30 parts of vanillic aldehyde, 5 parts~30 parts of Ethyl vanillin, 0.1 part~10 parts of capric acid, lauric acid/dodecanoic acid 0.1 part~20 Part, 0.1 part~20 parts of tetradecylic acid, 0.1 part~10 parts of hexadecylic acid, 0.1 part~5 parts of ethyl caprate, ethyl laurate 0.1 part~10 Part, 0.5 part~20 parts of ethyl myristate, 0.5 part~30 parts of ethyl palmitate, 0.5 part~10 parts of gamma decalactone, milk lactone 1 part~20 parts, third 0.1 part~10 parts of dodecalactone, 1 part~20 parts of delta-decalactone and fourth position dodecalactone 1 part~20 Part.
3. the tobacco juice for electronic smoke with milk odor type according to claim 1 and 2, it is characterised in that the essence presses matter Amount number meter includes 10 parts~15 parts of vanillic aldehyde, 15 parts~20 parts of Ethyl vanillin, 0.1 part~1 part of capric acid, 0.1 part of lauric acid/dodecanoic acid ~0.2 part, 0.4 part~0.5 part of tetradecylic acid, 0.4 part~0.5 part of hexadecylic acid, 0.1 part~0.2 part of ethyl caprate, ethyl laurate 0.2 part~0.5 part, 1 part~6 parts of ethyl myristate, 3 parts~8 parts of ethyl palmitate, 1 part~2 parts of gamma decalactone, in milk 1 part~20 parts of the dodecalactone in 5 parts~6 parts, third 2 parts~4 parts of dodecalactone of ester, 8 parts~10 parts of delta-decalactone and fourth position.
4. the tobacco juice for electronic smoke with milk odor type according to claim 1, it is characterised in that also aided in into including essence Point, the essence auxiliary element is selected from ethyl butyrate, ethyl lactate, ethyl 2-methylbutyrate, raspberry ketone, isobutyric acid chinese cymbidium At least one in ester, anisic aldehyde, lactic acid and benzyl carbinol.
5. the tobacco juice for electronic smoke with milk odor type according to claim 4, it is characterised in that the essence auxiliary element It it is 1 part~3 parts with the quality parts ratio of the essence:4 parts~9 parts.
6. the tobacco juice for electronic smoke with milk odor type according to claim 4, it is characterised in that the essence auxiliary element Include 1 part~10 parts of ethyl butyrate, 1 part~20 parts of ethyl lactate, ethyl 2-methylbutyrate 0.5 part~10 according to the mass fraction Part, 0.1 part~10 parts of raspberry ketone, 0.5 part~10 parts of isobutyric acid chinese cymbidium ester, 0.1 part~5 parts of anisic aldehyde, 0.1 part of lactic acid~ 20 parts and 0.1 part~10 parts of benzyl carbinol.
7. the tobacco juice for electronic smoke with milk odor type according to claim 4, it is characterised in that the essence auxiliary element Include 3 parts~5 parts of ethyl butyrate, 4 parts~6 parts of ethyl lactate according to the mass fraction, 2 parts~3 parts of ethyl 2-methylbutyrate, cover basin 2 parts~6 parts of sub- ketone, 5 parts~6 parts of isobutyric acid chinese cymbidium ester, 0.1 part~0.2 part of anisic aldehyde, 0.5 part~2 parts of lactic acid and benzene second 0.1 part~2 parts of alcohol.
8. the tobacco juice for electronic smoke with milk odor type according to claim 1, it is characterised in that the basal liquid is selected from third At least one in glycol, glycerine and ethanol.
9. the tobacco juice for electronic smoke with milk odor type according to claim 1, it is characterised in that the basal liquid includes matter Amount portion rate is 10 parts~80 parts:10 parts~80 parts of propane diols and glycerine.
10. a kind of electronic cigarette, it is characterised in that loaded in the electronic cigarette just like having described in any one of claim 1~9 The tobacco juice for electronic smoke of milk odor type.
CN201710082028.8A 2017-02-15 2017-02-15 Tobacco juice for electronic smoke and electronic cigarette with milk odor type Pending CN106858703A (en)

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Application publication date: 20170620