CN115948200B - Tobacco material with spicy flavor, preparation method and application thereof - Google Patents
Tobacco material with spicy flavor, preparation method and application thereof Download PDFInfo
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- CN115948200B CN115948200B CN202310061081.5A CN202310061081A CN115948200B CN 115948200 B CN115948200 B CN 115948200B CN 202310061081 A CN202310061081 A CN 202310061081A CN 115948200 B CN115948200 B CN 115948200B
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- spicy
- cigarettes
- tobacco material
- cigarette
- isopropenyl
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- 239000000463 material Substances 0.000 title claims abstract description 39
- 235000002637 Nicotiana tabacum Nutrition 0.000 title claims abstract description 35
- 239000000796 flavoring agent Substances 0.000 title claims abstract description 21
- 235000019634 flavors Nutrition 0.000 title claims abstract description 21
- 238000002360 preparation method Methods 0.000 title description 3
- 244000061176 Nicotiana tabacum Species 0.000 title 1
- 235000019504 cigarettes Nutrition 0.000 claims abstract description 45
- 241000208125 Nicotiana Species 0.000 claims abstract description 34
- DNIAPMSPPWPWGF-UHFFFAOYSA-N Propylene glycol Chemical compound CC(O)CO DNIAPMSPPWPWGF-UHFFFAOYSA-N 0.000 claims abstract description 18
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 16
- LLCOQBODWBFTDD-UHFFFAOYSA-N 1h-triazol-1-ium-4-thiolate Chemical compound SC1=CNN=N1 LLCOQBODWBFTDD-UHFFFAOYSA-N 0.000 claims abstract description 7
- MIZDPYBNDZVDLH-UHFFFAOYSA-N 2,5-dimethyl-2-prop-1-en-2-ylcyclohexan-1-one Chemical compound CC1CCC(C)(C(C)=C)C(=O)C1 MIZDPYBNDZVDLH-UHFFFAOYSA-N 0.000 claims abstract description 7
- YQMUZRNPCVSBEH-UHFFFAOYSA-N 4-prop-1-en-2-ylcyclohexan-1-one Chemical compound CC(=C)C1CCC(=O)CC1 YQMUZRNPCVSBEH-UHFFFAOYSA-N 0.000 claims abstract description 7
- 238000000034 method Methods 0.000 claims abstract description 7
- 239000000126 substance Substances 0.000 claims abstract description 7
- YSTPAHQEHQSRJD-UHFFFAOYSA-N 3-Carvomenthenone Chemical compound CC(C)C1CCC(C)=CC1=O YSTPAHQEHQSRJD-UHFFFAOYSA-N 0.000 claims abstract description 6
- 125000003469 3-methylhexyl group Chemical group [H]C([H])([H])C([H])([H])C([H])([H])C([H])(C([H])([H])[H])C([H])([H])C([H])([H])* 0.000 claims abstract description 6
- XAPCMTMQBXLDBB-UHFFFAOYSA-N butanoic acid hexyl ester Natural products CCCCCCOC(=O)CCC XAPCMTMQBXLDBB-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000002156 mixing Methods 0.000 claims description 5
- 239000000203 mixture Substances 0.000 claims description 4
- 239000003205 fragrance Substances 0.000 abstract description 3
- 239000002304 perfume Substances 0.000 abstract 1
- 235000013599 spices Nutrition 0.000 description 11
- 239000000523 sample Substances 0.000 description 8
- 238000011156 evaluation Methods 0.000 description 5
- 230000001953 sensory effect Effects 0.000 description 4
- 238000001035 drying Methods 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- 238000007789 sealing Methods 0.000 description 3
- 239000013068 control sample Substances 0.000 description 2
- RRAFCDWBNXTKKO-UHFFFAOYSA-N eugenol Chemical compound COC1=CC(CC=C)=CC=C1O RRAFCDWBNXTKKO-UHFFFAOYSA-N 0.000 description 2
- 239000012535 impurity Substances 0.000 description 2
- 239000002994 raw material Substances 0.000 description 2
- RUVINXPYWBROJD-ONEGZZNKSA-N trans-anethole Chemical compound COC1=CC=C(\C=C\C)C=C1 RUVINXPYWBROJD-ONEGZZNKSA-N 0.000 description 2
- KJPRLNWUNMBNBZ-QPJJXVBHSA-N (E)-cinnamaldehyde Chemical compound O=C\C=C\C1=CC=CC=C1 KJPRLNWUNMBNBZ-QPJJXVBHSA-N 0.000 description 1
- NPBVQXIMTZKSBA-UHFFFAOYSA-N Chavibetol Natural products COC1=CC=C(CC=C)C=C1O NPBVQXIMTZKSBA-UHFFFAOYSA-N 0.000 description 1
- 241000196324 Embryophyta Species 0.000 description 1
- 239000005770 Eugenol Substances 0.000 description 1
- 241000628997 Flos Species 0.000 description 1
- YUECNVSODFDKOQ-JTQLQIEISA-N Hexyl 3-methyl butyrate Natural products CCCCCCOC(=O)[C@@H](C)CC YUECNVSODFDKOQ-JTQLQIEISA-N 0.000 description 1
- RSDDTPVXLMVLQE-UHFFFAOYSA-N Hexyl 3-methylbutanoate Chemical compound CCCCCCOC(=O)CC(C)C RSDDTPVXLMVLQE-UHFFFAOYSA-N 0.000 description 1
- UVMRYBDEERADNV-UHFFFAOYSA-N Pseudoeugenol Natural products COC1=CC(C(C)=C)=CC=C1O UVMRYBDEERADNV-UHFFFAOYSA-N 0.000 description 1
- 235000008089 Syzygium polyanthum Nutrition 0.000 description 1
- 240000000278 Syzygium polyanthum Species 0.000 description 1
- 229940011037 anethole Drugs 0.000 description 1
- 230000036528 appetite Effects 0.000 description 1
- 235000019789 appetite Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 229940117916 cinnamic aldehyde Drugs 0.000 description 1
- KJPRLNWUNMBNBZ-UHFFFAOYSA-N cinnamic aldehyde Natural products O=CC=CC1=CC=CC=C1 KJPRLNWUNMBNBZ-UHFFFAOYSA-N 0.000 description 1
- 235000013399 edible fruits Nutrition 0.000 description 1
- 229960002217 eugenol Drugs 0.000 description 1
- 239000000284 extract Substances 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 238000004519 manufacturing process Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- RUVINXPYWBROJD-UHFFFAOYSA-N para-methoxyphenyl Natural products COC1=CC=C(C=CC)C=C1 RUVINXPYWBROJD-UHFFFAOYSA-N 0.000 description 1
- 210000000582 semen Anatomy 0.000 description 1
- 230000000391 smoking effect Effects 0.000 description 1
- 238000010561 standard procedure Methods 0.000 description 1
- 239000002023 wood Substances 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02A—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE
- Y02A50/00—TECHNOLOGIES FOR ADAPTATION TO CLIMATE CHANGE in human health protection, e.g. against extreme weather
- Y02A50/30—Against vector-borne diseases, e.g. mosquito-borne, fly-borne, tick-borne or waterborne diseases whose impact is exacerbated by climate change
Landscapes
- Manufacture Of Tobacco Products (AREA)
Abstract
The invention belongs to the field of application in tobacco industry, and particularly relates to a material for cigarettes with spicy flavor and cigarettes containing the material. Based on the weight percent of the perfume, it comprises: (1) 1% -3% of 2, 5-dimethyl-2-isopropenyl-1-cyclohexanone; (2) 2% -6% of 4-isopropenyl cyclohexanone; (3) 3% -7% of 4-isopropyl-l-methyl-1-cyclohexene-3-one; (4) 4% -8% of 3-ethyl-4-phenyl-2 (3H) -triazolethione; (5) 2% -6% of 3-methyl hexyl butyrate; (6) 10-15% of propylene glycol and 60-75% of ethanol. The tobacco material with obvious spicy flavor is obtained by combining the substances according to a certain proportion. And the fragrance is fine and soft, and has no rough feeling and other bad smell. The cigarette material prepared by the method is used for cigarettes, and the product has obvious spicy flavor, and has better performance in improving the taste of cigarettes, improving the quality of the aroma and enriching the aroma.
Description
Technical Field
The invention belongs to the field of tobacco industry application, and particularly relates to a tobacco material with spicy flavor, a preparation method and application thereof.
Background
The spice is generally derived from spice, which has a pungent odor, and natural spice can be extracted from leaves, branches, stems, flowers, fruits, seeds, bark, wood, roots, etc. of spice plants. Common natural spicy fragrance comprises fructus Anisi Stellati, fructus Foeniculi, fructus Zanthoxyli, flos Caryophylli, cortex Cinnamomi Japonici, cortex Cinnamomi, laurel leaf, semen Myristicae, etc. The synthetic natural spice comprises anethole, eugenol, cinnamaldehyde, etc. The spicy flavor has more application in the aspect of edible flavoring, and can remove fishy smell and promote appetite. In the essence for cigarettes, if the essence is added properly, the product types can be enriched, and the style characteristics of the cigarette products can be highlighted.
At present, some natural spices are influenced by the production place and the quality of raw materials, the quality fluctuation of the spice substances in the extracts is large, the quality is unstable, and in addition, impurities are difficult to remove in the extraction process, so that the smell of the spice is difficult to reach an ideal state. Some synthetic spices have poor flavor and are difficult to achieve a coordinated feel, so that the application of the spices in tobacco is hindered.
The present invention has been made to solve the above problems.
Disclosure of Invention
The invention discloses a tobacco material with spicy flavor, which comprises the following components in percentage by mass:
(1) 1% -3% of 2, 5-dimethyl-2-isopropenyl-1-cyclohexanone;
(2) 2% -6% of 4-isopropenyl cyclohexanone;
(3) 3% -7% of 4-isopropyl-l-methyl-1-cyclohexene-3-one;
(4) 4% -8% of 3-ethyl-4-phenyl-2 (3H) -triazolethione;
(5) 2% -6% of 3-methyl hexyl butyrate;
(6) 10-15% of propylene glycol and 60-75% of ethanol.
Preferably, the mass concentration of the ethanol is 65-70%.
Preferably, the sum of the mass percentages of the components (1) - (6) is 100%.
According to a second aspect of the present invention, there is provided a method for preparing a tobacco material having a spicy note according to the first aspect, the method comprising the steps of:
and (3) sequentially taking the substances (1) - (6) according to the mass percentage of the spice, oscillating at room temperature, and mixing the obtained solutions to obtain the tobacco material with the spicy flavor.
The third aspect of the invention discloses the application of the spicy flavor tobacco material in cigarettes.
Preferably, the material for cigarettes with the spicy note is added to cut tobacco, cigarette bobbin paper or cigarette filter.
Preferably, the cigarette material is added into the cut tobacco of the cigarette according to the dosage of 3-5wt%, and the rest formula is unchanged, so that the cigarette sample is prepared.
Preferably, the cigarette material is sprayed on cigarette bobbin paper according to the dosage of 1-3wt%, and the rest formula is unchanged, so that the cigarette sample is prepared.
Preferably, the cigarette material is added into a cigarette filter according to the dosage of 0.5-1wt%, and the rest formula is unchanged, so that the cigarette sample is prepared.
The cigarette comprises conventional cigarette or heating non-combustible cigarette.
Compared with the prior art, the invention has the following beneficial effects:
1. according to the invention, 2, 5-dimethyl-2-isopropenyl-1-cyclohexanone, 4-isopropenyl cyclohexanone, 4-isopropyl-l-methyl-1-cyclohexene-3-ketone, 3-ethyl-4-phenyl-2 (3H) -triazolethione and 3-methyl hexyl butyrate are combined according to a certain proportion, so that a tobacco material with obvious spicy flavor is obtained. And the fragrance is fine and soft, and has no rough feeling and other bad smell.
2. The spicy and fragrant tobacco material prepared by the invention does not contain impurities, has simple formula and is simple and efficient.
3. The cigarette material prepared by the method is used for cigarettes, and the product has obvious spicy flavor, and has better performance in improving the taste of cigarettes, improving the quality of the aroma and enriching the aroma.
Detailed Description
The present invention will be described in further detail with reference to the following examples, but is not limited thereto, and any changes or modifications made based on the teachings of the present invention will fall within the scope of the present invention. The specific techniques or conditions are not identified in the examples and are performed according to techniques or conditions described in the literature in this field or according to the product specifications. The reagents or apparatus used were conventional products available commercially without the manufacturer's attention.
Example 1
A tobacco material with a spicy note, comprising, based on mass percent:
1. 1% of 2, 5-dimethyl-2-isopropenyl-1-cyclohexanone;
2. 2% of 4-isopropenyl cyclohexanone;
3. 3% of 4-isopropyl-l-methyl-1-cyclohexen-3-one;
4. 4% of 3-ethyl-4-phenyl-2 (3H) -triazolethione;
5. 2% of hexyl 3-methylbutyrate;
6. propylene glycol 15%, ethanol 73%.
And (3) sequentially taking the substances 1-6 according to the mass percentage of the tobacco material, slowly oscillating for 15min at room temperature, uniformly mixing, sealing, drying in shade and keeping away from light, and obtaining the solution which is the tobacco material with the spicy flavor.
Example 2
A tobacco material with a spicy note comprising, in weight percent:
1. 2, 5-dimethyl-2-isopropenyl-1-cyclohexanone;
2. 4-isopropenyl cyclohexanone 4%;
3. 4-isopropyl-l-methyl-1-cyclohexen-3-one 5%;
4. 6% of 3-ethyl-4-phenyl-2 (3H) -triazolethione;
5. 5% of 3-methyl hexyl butyrate;
6. propylene glycol 8%, ethanol 70%.
And (3) sequentially taking the substances 1-6 according to the weight percentage of the tobacco material, slowly oscillating for 15min at room temperature, uniformly mixing, sealing, drying in shade and keeping away from light, and obtaining the solution which is the tobacco material with the spicy flavor.
Example 3
A tobacco material with a spicy note comprising, in weight percent:
1. 3% of 2, 5-dimethyl-2-isopropenyl-1-cyclohexanone;
2. 6% of 4-isopropenyl cyclohexanone;
3. 7% of 4-isopropyl-l-methyl-1-cyclohexen-3-one;
4. 8% of 3-ethyl-4-phenyl-2 (3H) -triazolethione;
5. 6% of 3-methyl hexyl butyrate;
6. propylene glycol 10%, ethanol 60%.
And sequentially taking 1-6 substances according to the weight percentage of the tobacco material, slowly oscillating for 15min at room temperature, uniformly mixing, sealing, drying in shade and keeping away from light, and obtaining the solution which is the tobacco material with spicy flavor.
Application example 1
The tobacco material of example 1 was added to cut tobacco of cigarettes in an amount of 5wt%, and the remaining formulation was unchanged, to prepare a cigarette sample a.
The tobacco material of example 2 was added to cigarette paper in an amount of 2wt%, and the remaining formulation was unchanged, to prepare a cigarette sample B.
The tobacco material of example 3 was added to a cigarette filter in an amount of 1wt%, and the remaining formulation was unchanged, to prepare a cigarette sample C.
The sample of cigarettes without any tobacco material added was used as a control.
The samples were evaluated for sensory comfort according to the tobacco industry standard method for evaluation of sensory comfort of cigarettes (YC/T496-2014). Sensory evaluation is carried out on the cigarette sample by a plurality of sensory evaluation staff, and three aspects of aroma characteristics, taste characteristics and aroma styles are mainly inspected. The smell and style of the cigarettes are both positive values compared with those of a reference cigarette control sample, and the positive score is higher as the improvement is larger; negative effects compared with the reference cigarette control sample adopt negative values, and the larger the negative effects are, the higher the negative score is. The results are shown in Table 1.
Table 1 flavoring effect and style evaluation of raw materials cigarette
Through smoking evaluation, the cigarette product has obvious spicy flavor, obvious improvement of flavor characteristics and taste characteristics, and is particularly embodied in improvement of flavor quality, increase of flavor quantity and fine and soft taste.
Claims (5)
1. A spicy tobacco material, characterized in that it comprises the following components, based on the mass percentage of the material:
(1) 1% -3% of 2, 5-dimethyl-2-isopropenyl-1-cyclohexanone;
(2) 2% -6% of 4-isopropenyl cyclohexanone;
(3) 3% -7% of 4-isopropyl-l-methyl-1-cyclohexene-3-one;
(4) 4% -8% of 3-ethyl-4-phenyl-2 (3H) -triazolethione;
(5) 2% -6% of 3-methyl hexyl butyrate;
(6) 10-15% of propylene glycol and 60-75% of ethanol;
the sum of the mass percentages of the components (1) to (6) is 100 percent.
2. The spicy flavor cigarette material according to claim 1, wherein the mass concentration of ethanol is 65-70%.
3. The method for preparing the spicy tobacco material according to claim 1, comprising the following steps:
according to the mass percentage composition of the material, sequentially taking the substances (1) to (6) in claim 1, oscillating at room temperature, and mixing the obtained solutions to obtain the spicy fragrant tobacco material.
4. Use of a material for cigarettes comprising the spicy note of claim 1 in cigarettes.
5. The use according to claim 4, characterized in that the spicy tobacco material is added to cut tobacco, cigarette tipping paper or cigarette filters.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310061081.5A CN115948200B (en) | 2023-01-19 | 2023-01-19 | Tobacco material with spicy flavor, preparation method and application thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN202310061081.5A CN115948200B (en) | 2023-01-19 | 2023-01-19 | Tobacco material with spicy flavor, preparation method and application thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN115948200A CN115948200A (en) | 2023-04-11 |
| CN115948200B true CN115948200B (en) | 2024-01-19 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN202310061081.5A Active CN115948200B (en) | 2023-01-19 | 2023-01-19 | Tobacco material with spicy flavor, preparation method and application thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN115948200B (en) |
Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102204717A (en) * | 2011-01-29 | 2011-10-05 | 广州市澳键丰泽生物科技有限公司 | Formula of mint fragrant tobacco additive essence |
| CN106858703A (en) * | 2017-02-15 | 2017-06-20 | 深圳瀚星翔科技有限公司 | Tobacco juice for electronic smoke and electronic cigarette with milk odor type |
| CN110584214A (en) * | 2019-09-25 | 2019-12-20 | 湖北中烟工业有限责任公司 | Composite fragrant essence for low-temperature cigarettes and application thereof |
| CN110699183A (en) * | 2019-11-04 | 2020-01-17 | 四川中烟工业有限责任公司 | Tobacco essence with spicy fragrance |
-
2023
- 2023-01-19 CN CN202310061081.5A patent/CN115948200B/en active Active
Patent Citations (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102204717A (en) * | 2011-01-29 | 2011-10-05 | 广州市澳键丰泽生物科技有限公司 | Formula of mint fragrant tobacco additive essence |
| CN106858703A (en) * | 2017-02-15 | 2017-06-20 | 深圳瀚星翔科技有限公司 | Tobacco juice for electronic smoke and electronic cigarette with milk odor type |
| CN110584214A (en) * | 2019-09-25 | 2019-12-20 | 湖北中烟工业有限责任公司 | Composite fragrant essence for low-temperature cigarettes and application thereof |
| CN110699183A (en) * | 2019-11-04 | 2020-01-17 | 四川中烟工业有限责任公司 | Tobacco essence with spicy fragrance |
Non-Patent Citations (4)
| Title |
|---|
| 款冬花挥发油的提取及其在卷烟中的应用;闫克玉;贾玉红;李卫;闫洪洋;闫洪喜;高远翔;冯喜生;;烟草科技(05);第27-33页 * |
| 番木瓜叶挥发油化学成分分析及其在卷烟中的应用;林凯;;江西农业学报(02);第104-106页、第109页 * |
| 辛夷净油中致香组分的制备、成分分析及其在卷烟中的应用;孙胜南;卢真保;黄艳;周仲良;;香料香精化妆品(05);第19-23页 * |
| 香兰素-α-D-葡糖苷的热裂解分析及在卷烟中的应用;岳海波;陈义坤;王娟;刘华臣;;湖北农业科学(24);第6156-6158页 * |
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| Publication number | Publication date |
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| CN115948200A (en) | 2023-04-11 |
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