CN111269752A - Essence, cigarette leaf group formula and application thereof - Google Patents
Essence, cigarette leaf group formula and application thereof Download PDFInfo
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- CN111269752A CN111269752A CN202010191747.5A CN202010191747A CN111269752A CN 111269752 A CN111269752 A CN 111269752A CN 202010191747 A CN202010191747 A CN 202010191747A CN 111269752 A CN111269752 A CN 111269752A
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/301—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by aromatic compounds
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/28—Treatment of tobacco products or tobacco substitutes by chemical substances
- A24B15/30—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances
- A24B15/32—Treatment of tobacco products or tobacco substitutes by chemical substances by organic substances by acyclic compounds
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- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0003—Compounds of unspecified constitution defined by the chemical reaction for their preparation
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
- C11B9/0007—Aliphatic compounds
- C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
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- General Chemical & Material Sciences (AREA)
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- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Manufacture Of Tobacco Products (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention belongs to the technical field of essence and spice, and particularly relates to essence which comprises phenethyl alcohol, phenethyl acetate, nerol, geraniol, indole, jasmone, nerolidol, methyl jasmonate, tea ketone, pyran type linalool oxide, furan type linalool oxide, linalool, jasmine extract, rose extract, sweet osmanthus extract and other components, a fragrance fixative and a solvent. The invention also relates to a cigarette leaf group formula, and application of the essence and the cigarette leaf group formula. The essence can endow the fragrance characteristics of composite Tie Guanyin tea fragrance with the fragrance of cigarette fragrance (orchid fragrance, osmanthus fragrance or jasmine fragrance), and can improve the fragrance style of cigarettes.
Description
Technical Field
The invention belongs to the technical field of flavors and fragrances, and particularly relates to a flavor, a cigarette leaf formula containing the flavor, and application of the cigarette leaf formula and the cigarette leaf formula in tobacco products.
Background
The essence and the spice are widely applied to the fields of tobacco, food, daily chemicals and the like. The tobacco essence not only endows the cigarette products with unique style characteristics, but also improves the taste of the cigarettes, and is one of important connotations for building Chinese style cigarette core competitiveness. At present, domestic cigarette products still have defects in the aspect of quality of fragrance evaluation, and a new essence for cigarettes needs to be developed urgently.
Tieguanyin belongs to oolong tea, is native to Anxi, and is called tea king. The Tieguanyin with excellent quality has unique taste, sweet and rich flavor and special 'guanyin rhyme', has aftertaste after being brewed for seven times, and has the saying that 'Guanyin is heavier than iron'. Researches find that the finished Tie Guanyin tea mainly comprises fragrance, fruit fragrance, faint scent, sweet scent, milk scent and other scents, the scent is rich, elegant and attractive, and the unique scent characteristic is mainly derived from substance conversion in the processing process.
The fragrance of the flower is an important fragrance in the fragrance style of the flue-cured tobacco type cigarette, and the fragrance of the flower can be endowed to the cigarette, and the smoking quality of the cigarette can be obviously improved.
The essence obtained by compounding the flower fragrance and the Tieguanyin tea fragrance is always a fragrance blending target which is desired but can not be achieved by a fragrance blender. Therefore, the tobacco essence with the composite flower fragrance and Tie Guanyin tea fragrance is needed urgently.
Disclosure of Invention
The essence disclosed by the invention has the fragrance of a flower fragrance (orchid fragrance, osmanthus fragrance or jasmine fragrance) compounded with the Tieguanyin tea fragrance, and can endow the fragrance characteristic of the cigarette flower fragrance compounded with the Tieguanyin tea fragrance and improve the fragrance style of cigarettes by adding the essence into cigarette tobacco shreds. On the basis, the invention provides a cigarette leaf group formula and application of essence and the cigarette leaf group formula in tobacco products.
The invention relates to a perfume in a first aspect, comprising:
1 to 15 parts by weight (for example, 2 parts by weight, 3.5 parts by weight, 4 parts by weight, 5 parts by weight, 5.5 parts by weight, 6 parts by weight, 10 parts by weight, 12 parts by weight, 15 parts by weight)
0.001 to 0.9 part by weight of phenethylacetate (e.g., 0.002 part by weight, 0.003 part by weight, 0.005 part by weight, 0.007 part by weight, 0.008 part by weight, 0.01 part by weight, 0.02 part by weight, 0.03 part by weight, 0.05 part by weight, 0.07 part by weight, 0.09 part by weight, 0.1 part by weight, 0.2 part by weight, 0.3 part by weight, 0.4 part by weight, 0.5 part by weight, 0.6 part by weight, 0.7 part by weight, 0.8 part by weight)
0.1 to 4 parts by weight of nerol (e.g., 0.15 part by weight, 0.2 part by weight, 0.25 part by weight, 0.3 part by weight, 0.35 part by weight, 0.4 part by weight, 0.5 part by weight, 0.6 part by weight, 0.8 part by weight, 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight)
Geraniol 0.08 to 3 parts by weight (e.g., 0.1 part by weight, 0.15 part by weight, 0.2 part by weight, 0.25 part by weight, 0.3 part by weight, 0.4 part by weight, 0.5 part by weight, 0.7 part by weight, 0.9 part by weight, 1 part by weight, 2 parts by weight, 3 parts by weight)
Indole 0.008 to 0.1 part by weight (e.g., 0.01 part by weight, 0.015 part by weight, 0.018 part by weight, 0.02 part by weight, 0.022 part by weight, 0.025 part by weight, 0.03 part by weight, 0.05 part by weight, 0.07 part by weight, 0.1 part by weight)
0.01 to 0.3 part by weight (e.g., 0.02 part by weight, 0.03 part by weight, 0.04 part by weight, 0.05 part by weight, 0.06 part by weight, 0.07 part by weight, 0.08 part by weight, 0.1 part by weight, 0.2 part by weight, 0.3 part by weight) of jasmone
1 to 16 parts by weight of nerolidol (e.g., 2 parts by weight, 2.8 parts by weight, 3 parts by weight, 3.5 parts by weight, 4.5 parts by weight, 5 parts by weight, 7 parts by weight, 9 parts by weight, 10 parts by weight, 11 parts by weight, 13 parts by weight, 14 parts by weight, 15 parts by weight)
0.1 to 10 parts by weight (e.g., 0.2 part by weight, 0.3 part by weight, 0.4 part by weight, 0.5 part by weight, 0.6 part by weight, 0.7 part by weight, 1 part by weight, 1.2 parts by weight, 2 parts by weight, 3 parts by weight, 5 parts by weight, 7 parts by weight, 9 parts by weight)
0.0001 to 0.01 part by weight (for example, 0.0003 part by weight, 0.0005 part by weight, 0.0006 part by weight, 0.0007 part by weight, 0.00075 part by weight, 0.0009 part by weight, 0.001 part by weight, 0.0012 part by weight, 0.0015 part by weight, 0.002 part by weight, 0.005 part by weight, 0.007 part by weight, 0.008 part by weight, 0.009 part by weight)
0.05 to 6 parts by weight (e.g., 0.1 part by weight, 0.3 part by weight, 0.5 part by weight, 0.7 part by weight, 0.9 part by weight, 1 part by weight, 1.2 parts by weight, 1.5 parts by weight, 2 parts by weight, 2.2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight, 6 parts by weight) of linalool oxide of pyran type
0.01 to 3 parts by weight (e.g., 0.02 part by weight, 0.03 part by weight, 0.05 part by weight, 0.07 part by weight, 0.09 part by weight, 0.1 part by weight, 0.15 part by weight, 0.2 part by weight, 0.28 part by weight, 0.3 part by weight, 0.5 part by weight, 0.7 part by weight, 1 part by weight, 2 parts by weight, 3 parts by weight) of furan-type linalool oxide
Linalool 0.02 to 3 parts by weight (e.g., 0.05 parts by weight, 0.07 parts by weight, 0.08 parts by weight, 0.09 parts by weight, 0.1 parts by weight, 0.12 parts by weight, 0.15 parts by weight, 0.2 parts by weight, 0.3 parts by weight, 0.5 parts by weight, 0.7 parts by weight, 1 part by weight, 2 parts by weight, 3 parts by weight)
0.001 to 0.1 part by weight (e.g., 0.003 part by weight, 0.005 part by weight, 0.007 part by weight, 0.0075 part by weight, 0.009 part by weight, 0.01 part by weight, 0.015 part by weight, 0.02 part by weight, 0.03 part by weight, 0.04 part by weight, 0.05 part by weight, 0.06 part by weight, 0.07 part by weight, 0.08 part by weight) of the jasmine flower extract
0.01 to 0.6 part by weight (e.g., 0.02 part by weight, 0.03 part by weight, 0.04 part by weight, 0.05 part by weight, 0.07 part by weight, 0.08 part by weight, 0.09 part by weight, 0.1 part by weight, 0.12 part by weight, 0.15 part by weight, 0.2 part by weight, 0.3 part by weight, 0.4 part by weight, 0.5 part by weight, 0.6 part by weight)
0.006 to 0.5 parts by weight (e.g., 0.01 part by weight, 0.03 part by weight, 0.04 part by weight, 0.05 part by weight, 0.06 part by weight, 0.07 part by weight, 0.09 part by weight, 0.1 part by weight, 0.12 part by weight, 0.14 part by weight, 0.2 part by weight, 0.3 part by weight, 0.4 part by weight, 0.5 part by weight)
16 to 47 parts by weight of a fragrance-fixing agent (for example, 17 parts by weight, 18 parts by weight, 20 parts by weight, 21 parts by weight, 22 parts by weight, 22.47 parts by weight, 23 parts by weight, 25 parts by weight, 26 parts by weight, 28 parts by weight, 30 parts by weight, 32 parts by weight, 33 parts by weight, 34 parts by weight, 34.73 parts by weight, 35 parts by weight, 36 parts by weight, 37 parts by weight, 38 parts by weight, 39 parts by weight, 39.95 parts by weight, 40 parts by weight, 41 parts by weight, 43 parts by weight, 45 parts by weight, 46 parts by weight)
35 to 81 parts by weight of a solvent (e.g., 37 parts by weight, 40 parts by weight, 42 parts by weight, 44 parts by weight, 46 parts by weight, 47 parts by weight, 48 parts by weight, 48.52 parts by weight, 49 parts by weight, 49.16 parts by weight, 50 parts by weight, 51 parts by weight, 53 parts by weight, 55 parts by weight, 57 parts by weight, 58 parts by weight, 60 parts by weight, 62 parts by weight, 64 parts by weight, 65 parts by weight, 65.93 parts by weight, 66 parts by weight, 67 parts by weight, 68 parts by weight, 70 parts by weight, 72 parts by weight, 74 parts by weight, 75 parts by weight, 80 parts by weight);
and the essence also comprises the following components in any one of (1) to (3):
(1)
β -0.0007 to 0.007 wt% ionone (for example, 0.001 wt%, 0.002 wt%, 0.004 wt%, 0.005 wt%)
1 to 10 parts by weight (for example, 2 parts by weight, 3 parts by weight, 5 parts by weight, 6 parts by weight, 7 parts by weight, 9 parts by weight)
0.5 to 8 parts by weight (e.g., 1 part by weight, 2 parts by weight, 3 parts by weight, 4 parts by weight, 5 parts by weight, 6 parts by weight, 7 parts by weight) of amyl salicylate;
(2)
β -ionone 0.005-0.05 part by weight (e.g., 0.008 part by weight, 0.01 part by weight, 0.02 part by weight, 0.03 part by weight, 0.04 part by weight)
0.005 to 0.05 part by weight (e.g., 0.008 part by weight, 0.01 part by weight, 0.02 part by weight, 0.03 part by weight, 0.04 part by weight)
Peach aldehyde 0.001 to 0.01 parts by weight (e.g., 0.003 parts by weight, 0.005 parts by weight, 0.007 parts by weight, 0.008 parts by weight);
(3)
0.01 to 0.1 part by weight (for example, 0.02 part by weight, 0.03 part by weight, 0.04 part by weight, 0.05 part by weight, 0.06 part by weight, 0.07 part by weight, 0.08 part by weight) of a magnolia extract.
In some embodiments of the first aspect of the present invention, the perfume comprises:
in some embodiments of the first aspect of the present invention, the perfume comprises:
in some embodiments of the first aspect of the present invention, the perfume comprises:
in some embodiments of the first aspect of the present invention, the perfume has one or more of the following characteristics (1) to (7):
(1) the jasmine flower extract is selected from jasmine flower essential oil, jasmine flower absolute oil and jasmine flower tincture, and is preferably jasmine flower absolute oil;
(2) the rose extract is selected from rose essential oil, rose absolute oil and rose tincture, and is preferably rose essential oil;
(3) the osmanthus fragrans extract is selected from osmanthus fragrans essential oil, osmanthus fragrans absolute oil and osmanthus fragrans tincture, and preferably is osmanthus fragrans absolute oil;
(4) the magnolia extract is selected from magnolia essential oil, magnolia absolute oil and magnolia tincture, and is preferably magnolia absolute oil;
(5) the perfume fixative is selected from propylene glycol, glycerol and sorbitol, preferably propylene glycol;
(6) the solvent is selected from water, ethanol, propylene glycol, glycerol and a mixture of a plurality of the solvents, preferably ethanol water solution, more preferably the concentration of the ethanol water solution is 65% (W/W) to 99% (W/W), for example, 70% (W/W), 72% (W/W), 74% (W/W), 74.1% (W/W), 75% (W/W), 75.1% (W/W), 78% (W/W), 80% (W/W), 82% (W/W), 85% (W/W), 87% (W/W), 90% (W/W), 92% (W/W), 95% (W/W), 95.4% (W/W), 95.5% (W/W), 96% (W/W), 97% (W/W), 98% (W/W);
(7) the essence is tobacco essence.
In the invention, jasmine essential oil, jasmine absolute oil, jasmine tincture, rose essential oil, rose absolute oil, rose tincture, sweet osmanthus essential oil, sweet osmanthus absolute oil, sweet osmanthus tincture, tree orchid essential oil, tree orchid absolute oil and tree orchid tincture are conventional commodities in the field and can be directly purchased from the market.
In some embodiments of the first aspect of the present invention, the absolute oil of jasmine, the essential oil of rose, the absolute oil of osmanthus fragrans and the absolute oil of tree orchid are purchased from huabao essences and fragrances (shanghai) limited.
The second aspect of the invention relates to a cigarette tobacco leaf composition formula which comprises the essence of the first aspect of the invention.
In a third aspect, the present invention relates to a smoking article comprising a flavour according to the first aspect of the present invention or a tobacco leaf blend according to the second aspect of the present invention.
In some embodiments of the third aspect of the present invention, the smoking article is a cigarette.
In some embodiments of the third aspect of the present invention, the content of the essence in each cigarette is 1-100 μ L, such as 5 μ L, 10 μ L, 15 μ L, 20 μ L, 25 μ L, 30 μ L, 40 μ L, 50 μ L, 60 μ L, 70 μ L, 80 μ L, 90 μ L.
In a fourth aspect, the present invention relates to the use of a flavour according to the first aspect of the invention or a tobacco leaf composition according to the second aspect of the invention in a smoking article.
In some embodiments of the fourth aspect of the present invention, the smoking article is a cigarette.
A fifth aspect of the invention relates to the use of the flavour of the first aspect of the invention or the cigarette leaf formulation of the second aspect of the invention to impart the aroma characteristics of a compound Tieguanyin tea aroma to a floral cigarette or to improve the aroma style of a cigarette.
In some embodiments of the fifth aspect of the present invention, the floral fragrance is selected from the group consisting of orchid fragrance, osmanthus fragrance and jasmine fragrance.
In some embodiments of the fifth aspect of the present invention, the floral fragrance is an orchid, osmanthus or jasmine fragrance.
In the present invention, the term "essential oil" is used in a broad sense to refer to a general term for volatile aromatic-containing products obtained by processing and extracting the organs of aromatic plants and animals, and in a narrow sense, to refer to aromatic-containing products obtained by steam distillation, squeezing, cold milling or dry distillation from the organs (such as flowers, leaves, branches, skins, stems, roots, fruits, seeds, etc.) of aromatic plants. In practical applications, the narrow definition is often adopted.
In the present invention, the term "absolute" is a generic term for a flavor product obtained by extracting a solution of a flavor-imparting component in an extract, a gum, a balm or a balsam with high-concentration ethanol, freezing the solution (for example, at-10 ℃ to-20 ℃), filtering off insoluble matter, and then evaporating the ethanol under reduced pressure.
In the present invention, the term "tincture" or "tincture" refers to a perfume preparation containing a certain amount of ethanol obtained by extracting perfume plant organs or exudates and perfume-containing organs of odoriferous animals or perfume-containing secretions thereof with a certain concentration of ethanol. The tincture prepared at normal temperature is called as "cold tincture"; the tincture prepared under the condition of heating reflux is called as 'hot tincture'.
In the present invention, the term "tobacco product" is a favorite product produced from tobacco leaves. According to the characteristics of different types of tobacco leaves, a variety of tobacco products are produced by different processing and manufacturing methods so as to meet the hobby requirements of different consumers. Most of them are cigarettes.
The invention obtains at least one of the following beneficial effects:
1. the essence disclosed by the invention has the fragrance of a flower fragrance (orchid fragrance, osmanthus fragrance or jasmine fragrance) compounded with the Tieguanyin tea fragrance, and can endow the fragrance characteristic of the cigarette flower fragrance compounded with the Tieguanyin tea fragrance.
2. The essence provided by the invention can improve the aroma style of cigarettes when added into the cigarettes.
Detailed Description
Embodiments of the present invention will now be described more fully hereinafter with reference to the accompanying examples, in which some, but not all embodiments of the invention are shown. The following description of at least one exemplary embodiment is merely illustrative in nature and is in no way intended to limit the invention, its application, or uses. All other embodiments, which can be derived by a person skilled in the art from the embodiments given herein without making any creative effort, shall fall within the protection scope of the present invention.
The jasmine absolute oil, rose essential oil, osmanthus absolute oil and tree orchid absolute oil in the following examples were purchased from huabao essence and fragrance (shanghai) limited.
The preparation methods of the comparative samples related to examples 1 to 3 were as follows:
weighing 15Kg of finished Tieguanyin tea leaves, placing the finished Tieguanyin tea leaves on a sieve plate of a steam distillation kettle, introducing steam into the distillation kettle from the lower part, fully contacting with a tea material layer, dispersing and gasifying, leading out formed mixed steam of water and volatile essential oil from a steam outlet at the upper part of a distillation tank, controlling the steaming flow to be 25Kg/h, controlling the distillation time to be 2.5h, condensing the mixed steam by a condenser, and then separating the condensed steam by an oil-water separator to obtain 62.5Kg of finished Tieguanyin tea leaf hydrolat serving as a comparison sample.
EXAMPLE 1 blueFlower fragrance composite Tieguanyin tea fragrance characteristic essence
The raw materials are uniformly mixed according to the formula in the table 1-1 to obtain the essence 1, wherein the solvents used for preparing 10% (W/W) phenethylacetate, 10% (W/W) nerol, 1% (W/W) indole, 10% (W/W) jasmone, 0.1% (W/W) theanone, 1% (W/W) β -ionone, 5% (W/W) jasmine absolute oil, 10% (W/W) rose essential oil and 10% (W/W) osmanthus flower absolute oil are obtained by mixing anhydrous ethanol and propylene glycol in a weight ratio of 7: 3.
TABLE 1-1 essence 1 formulation
| Raw materials | Parts by weight |
| Phenylethanolic acid | 4.00 |
| 10% (W/W) phenethylacetate | 0.10 |
| 10% (W/W) nerol | 2.50 |
| Geraniol | 0.15 |
| 1% (W/W) indole | 1.50 |
| 10% (W/W) jasmone | 0.50 |
| Nerolidol | 3.00 |
| Jasmonic acid methyl ester | 0.40 |
| 0.1% (W/W) theascented Ketone | 0.75 |
| Linalool oxide (pyran type) | 1.00 |
| Linalool oxide (furan type) | 0.05 |
| Linalool | 0.10 |
| 1% (W/W) β -ionone | 0.10 |
| Salicylic acid isobutyl ester | 5.00 |
| Salicylic acid amyl ester | 2.00 |
| 5% (W/W) jasmine flower absolute oil | 0.10 |
| 10% (W/W) rose essential oil | 0.40 |
| 10% (W/W) osmanthus flower absolute oil | 0.40 |
| Propylene glycol | 32.95 |
| 95% (W/W) ethanol aqueous solution | 45.00 |
According to the judgment of the smell index in YC/T497-2014, namely, the Chinese style cigarette style sensory evaluation method, 12 professional evaluators evaluate the smell of the fragrance characteristics of the essence 1 and the reference sample, the full score is 3, and the average result is shown in tables 1-2.
TABLE 1-2 evaluation results of the odor of essence 1, comparative sample
| Sample (I) | Fragrance | Fruit incense | Radix aucklandiae | Qingzi incense | Flower fragrance | Milk fragrance | Sweet incense |
| Control sample | 1.5 | 1.0 | 0.5 | 0.6 | 1.0 | 0.5 | 1.0 |
| Essence 1 | 1.5 | 0.8 | 0.5 | 0.8 | 2.0 | 0.5 | 1.5 |
Note: the odor scores of the essence 1 and the comparative sample are 0 respectively for the spicy flavor, the herb flavor, the bean flavor, the cocoa flavor, the paste flavor and the baking flavor.
The odor evaluation results show that: compared with a comparison sample, the fragrance and sweet note of the essence 1 are obviously stronger; the orchid fragrance of the essence 1 is prominent and has the characteristic of Tie Guanyin tea fragrance.
Taking an unflavored conventional blank cigarette, injecting the essence 1 and a comparison sample into tobacco shreds according to the dosage of 10 mu L per cigarette, and after injection, balancing the cigarette for 48 hours in an environment with the temperature of 22 +/-1 ℃ and the relative humidity (60 +/-2)% to respectively obtain the cigarette 1 and the comparison cigarette. The sensory evaluation committee consisted of 12 professional evaluation personnel, and evaluation was performed on the aroma characteristics of the blank sample (conventional blank cigarette), the cigarette 1 and the comparative cigarette according to the evaluation index evaluation in YC/T497 + 2014 "sensory evaluation method for Chinese style cigarette style in cigarette", with a full score of 10, and the results are shown in tables 1-3.
TABLE 1-3 test results for blank samples, cigarette 1 and control cigarettes
Note: the smoking scores of the banksia rose, herb, bean, cocoa and cream of the blank sample, cigarette 1 and the comparative cigarette were all 0.
The results of the smoke panel test show that: compared with a blank sample, the cigarette added with the essence 1 has more obvious faint scent, fruit scent, flower scent, milk scent and sweet scent when being smoked; the fragrance and the flower fragrance note of the cigarette added with the essence 1 are more obvious than those of the comparative cigarettes during smoking evaluation. The cigarette added with the essence 1 has obvious orchid fragrance and Tie Guanyin tea fragrance.
Example 2 essence with composite Tieguanyin tea aroma characteristics and osmanthus fragrans fragrance
Mixing the raw materials uniformly according to the formula in Table 2-1 to obtain essence 2, wherein 10% (W/W) phenethylacetate, 10% (W/W) nerol, 1% (W/W) indole, 10% (W/W) jasmone, 0.1% (W/W) theanone, 1% (W/W) β -ionone, 1% (W/W) methylionone, 1% (W/W) peach aldehyde and 5%
The (W/W) jasmine flower absolute oil, 10% (W/W) rose essential oil and 10% (W/W) sweet osmanthus flower absolute oil are prepared by mixing anhydrous ethanol and propylene glycol in a weight ratio of 7: 3.
TABLE 2-1 essence 2 formulation
According to the evaluation of the smell indexes in YC/T497-.
TABLE 2-2 evaluation results of the odor of essence 2, comparative sample
| Sample (I) | Fragrance | Fruit incense | Radix aucklandiae | Qingzi incense | Flower fragrance | Milk fragrance | Sweet incense |
| Control sample | 1.5 | 1.0 | 0.5 | 0.6 | 1.0 | 0.5 | 1.0 |
| Essence 2 | 1.5 | 0.8 | 0.5 | 0.6 | 2.0 | 0.8 | 1.5 |
Note: the odor scores of the essence 2 and the comparative sample are 0 respectively.
The odor evaluation results show that: compared with a comparison sample, the fragrance, milk fragrance and sweet fragrance of the essence 2 are obviously stronger; the osmanthus fragrance of the essence 2 is prominent and has the characteristic of Tie Guanyin tea fragrance.
Injecting essence 2 and a reference sample into tobacco shreds according to the dosage of 10 mu L per cigarette, and after injection, balancing the cigarettes for 48 hours in an environment with the temperature of 22 +/-1 ℃ and the relative humidity (60 +/-2)% to respectively obtain cigarette 2 and a reference cigarette. The sensory evaluation committee consisted of 12 professional evaluation personnel, and evaluation was performed on the aroma characteristics of the blank sample (conventional blank cigarette), the cigarette 2 and the comparative cigarette according to the evaluation index evaluation in YC/T497 + 2014 "sensory evaluation method for Chinese style cigarette style in cigarette", with a full score of 10, and the results are shown in tables 2-3.
TABLE 2-3 smoking evaluation results for blank, cigarette 2 and control cigarette
Note: the smoking scores of the banksia rose, herb, bean, cocoa and cream of the blank sample, cigarette 2 and the comparative cigarette were all 0.
The results of the smoke panel test show that: compared with a blank sample, the cigarette added with the essence 2 has more obvious faint scent, fruit scent, flower scent, milk scent and sweet scent when being smoked; the cigarette added with the essence 2 has more obvious faint scent and flowery scent when being compared with the control cigarette. The cigarette added with the essence 2 has obvious characteristics of sweet osmanthus fragrance and Tie Guanyin tea fragrance.
Example 3 essence with jasmine fragrance combined with Tieguanyin tea aroma characteristics
The raw materials were mixed uniformly according to the formulation in table 3-1 to obtain essence 3. Wherein, the solvents adopted by 10 percent (W/W) nerol, 1 percent (W/W) indole, 10 percent (W/W) jasmone, 0.1 percent (W/W) theanone, 5 percent (W/W) tree orchid absolute oil, 5 percent (W/W) jasmine absolute oil, 10 percent (W/W) rose essential oil and 10 percent (W/W) sweet osmanthus absolute oil are obtained by mixing anhydrous ethanol and propylene glycol according to the weight ratio of 7: 3.
TABLE 3-1 essence 3 formulation
| Raw materials | Parts by weight |
| Phenylethanolic acid | 5.50 |
| Phenylethyl acetate | 0.20 |
| 10% (W/W) nerol | 3.00 |
| Geraniol | 0.25 |
| 1% (W/W) indole | 1.00 |
| 10% (W/W) jasmone | 0.40 |
| Nerolidol | 3.00 |
| Jasmonic acid methyl ester | 0.60 |
| 0.1% (W/W) theascented Ketone | 1.00 |
| Linalool oxide (pyran type) | 1.20 |
| Linalool oxide (furan type) | 0.15 |
| Linalool | 0.12 |
| 5% (W/W) tree orchid absolute oil | 1.00 |
| 5% (W/W) jasmine flower absolute oil | 1.20 |
| 10% (W/W) rose essential oil | 0.80 |
| 10% (W/W) osmanthus flower absolute oil | 0.40 |
| Propylene glycol | 20.00 |
| 95% ethanol aqueous solution | 60.18 |
According to the evaluation of the smell indexes in YC/T497-.
TABLE 3-2 essence 3, reference sample odor evaluation results
Note: the odor scores of the essence 3 and the comparative sample are 0 respectively.
The odor evaluation results show that: compared with a comparison sample, the fragrance, milk fragrance and sweet fragrance of the essence 3 are obviously stronger; the jasmine flower fragrance of the essence 2 is prominent and has the aroma characteristic of Tie Guanyin tea fragrance.
Taking an unflavored conventional blank cigarette, injecting the essence 3 and a comparison sample into tobacco shreds according to the dosage of 10 mu L per cigarette, and after injection, balancing the cigarette for 48 hours in an environment with the temperature of 22 +/-1 ℃ and the relative humidity (60 +/-2)% to respectively obtain the cigarette 3 and the comparison cigarette. The sensory evaluation committee consisted of 12 professional evaluation personnel, and evaluation was performed on the aroma characteristics of the blank sample (conventional blank cigarette), the cigarette 3 and the comparative cigarette according to the evaluation index evaluation in YC/T497 + 2014 "sensory evaluation method for Chinese style cigarette style in cigarette", with a full score of 10, and the results are shown in tables 3-3.
TABLE 3-3 smoking evaluation results for blank, cigarette 3 and control cigarette
Note: the smoking scores of the banksia rose, herb, bean, cocoa and cream of the blank sample, cigarette 3 and the comparative cigarette were all 0.
The results of the smoke panel test show that: compared with a blank sample, the cigarette added with the essence 3 has more obvious faint scent, fruit scent, flower scent, milk scent and sweet scent when being smoked; the cigarette added with the essence 3 has more obvious faint scent and flowery scent when being compared with the cigarette for evaluation. The cigarette added with the essence 3 has obvious jasmine flower fragrance and Tie Guanyin tea fragrance.
It should be understood that the above examples are only for clarity of illustration and are not intended to limit the embodiments. Other variations and modifications will be apparent to persons skilled in the art in light of the above description. And are neither required nor exhaustive of all embodiments. And obvious variations or modifications therefrom are within the scope of the invention.
Claims (10)
1. A fragrance, comprising:
and the essence also comprises the following components in any one of (1) to (3):
(1)
β -ionone 0.0007-0.007 weight portion
1-10 parts by weight of isobutyl salicylate
0.5-8 parts by weight of amyl salicylate;
(2)
β -ionone 0.005-0.05 weight part
0.005-0.05 part by weight of methylionone
0.001-0.01 parts by weight of peach aldehyde;
(3)
0.01-0.1 part by weight of a tree orchid extract.
2. A perfume according to claim 1 comprising:
3. a perfume according to claim 1 comprising:
4. a perfume according to claim 1 comprising:
5. essence according to any of claims 1 to 4, characterized by one or more of the following (1) to (7):
(1) the jasmine flower extract is selected from jasmine flower essential oil, jasmine flower absolute oil and jasmine flower tincture;
(2) the rose extract is selected from rose essential oil, rose absolute oil and rose tincture;
(3) the sweet osmanthus extract is selected from sweet osmanthus essential oil, sweet osmanthus absolute oil and sweet osmanthus tincture;
(4) the magnolia extract is selected from magnolia essential oil, magnolia absolute oil and magnolia tincture;
(5) the perfume fixative is selected from propylene glycol, glycerol and sorbitol;
(6) the solvent is selected from water, ethanol, propylene glycol, glycerol and a mixture of a plurality of the solvents;
(7) the essence is tobacco essence.
6. A tobacco leaf formulation comprising the flavour of any one of claims 1 to 5.
7. A smoking article comprising the flavour of any one of claims 1 to 5 or the tobacco leaf blend formulation of claim 6;
preferably, the tobacco product is a cigarette;
more preferably, the content of the essence in each cigarette is 1-100 mu L.
8. Use of the flavour of any one of claims 1 to 5 or the tobacco leaf blend formulation of claim 6 in a tobacco product;
preferably, the tobacco product is a cigarette.
9. Use of the flavour of any one of claims 1 to 5 or the cigarette leaf formulation of claim 6 for imparting aroma characteristics of the composite Tieguanyin tea aroma of a cigarette floral aroma or for improving the aroma style of a cigarette.
10. Use according to claim 9, wherein the floral fragrance is selected from the group consisting of orchid fragrance, osmanthus fragrance and jasmine fragrance.
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| CN115725366A (en) * | 2022-11-09 | 2023-03-03 | 河北中烟工业有限责任公司 | Lotus-flavored essence for cigarettes and cigarettes |
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| CN106854494A (en) * | 2017-03-15 | 2017-06-16 | 湖南嘉利香料有限公司 | A kind of compound fragrance of a flower odor type flavouring essence for tobacco and preparation method and application |
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| CN106854494A (en) * | 2017-03-15 | 2017-06-16 | 湖南嘉利香料有限公司 | A kind of compound fragrance of a flower odor type flavouring essence for tobacco and preparation method and application |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN115725366A (en) * | 2022-11-09 | 2023-03-03 | 河北中烟工业有限责任公司 | Lotus-flavored essence for cigarettes and cigarettes |
| CN115725366B (en) * | 2022-11-09 | 2024-05-10 | 河北中烟工业有限责任公司 | Lotus-flavored essence for cigarettes and cigarettes |
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