CN111329103B - Electronic cigarette spice composition with Tie Guanyin tea aroma characteristics, electronic cigarette liquid and application of electronic cigarette spice composition and electronic cigarette liquid - Google Patents
Electronic cigarette spice composition with Tie Guanyin tea aroma characteristics, electronic cigarette liquid and application of electronic cigarette spice composition and electronic cigarette liquid Download PDFInfo
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
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- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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Abstract
The invention belongs to the technical field of tobacco product flavor blending, and particularly relates to an electronic cigarette spice composition with Tie Guanyin tea flavor characteristics, electronic cigarette liquid and application of the electronic cigarette spice composition and the electronic cigarette liquid. Wherein the electronic cigarette flavor composition with Tieguanyin tea aroma characteristics comprises: ethanol; leaf alcohol; benzaldehyde; ethyl caproate; benzyl alcohol; phenylacetaldehyde; linalool oxide (furan type); linalool; phenyl ethyl alcohol; tea scented ketone; linalool oxide (pyran type); alpha-terpineol; nerol; geraniol; citral; indole; gamma-nonalactone; jasmone; nerolidol; methyl jasmonate. The electronic cigarette spice composition disclosed by the invention is used for improving the overall quality of an electronic cigarette in the electronic cigarette, endows the electronic cigarette with the flavor characteristics of Tieguanyin tea fragrance, and meanwhile enriches the cigarette flavor, softens the smoke, coordinates the cigarette flavor and reduces the stimulation.
Description
Technical Field
The invention belongs to the technical field of tobacco product flavor blending, and particularly relates to an electronic cigarette spice composition with Tie Guanyin tea flavor characteristics, electronic cigarette liquid and application of the electronic cigarette spice composition and the electronic cigarette liquid.
Background
The Tieguanyin is originally produced in Anxi county in Fujian Quanzhou city, belongs to one of the representatives of the green tea in the traditional famous tea in China, and is highly popular with consumers because of unique fragrant elegant and elegant fragrance, and fragrant flower fragrance and fruit fragrance. The processing technology of the Tieguanyin tea comprises the procedures of picking green, drying green, performing green-making, deactivating the green, wrapping and kneading, drying and the like, and each process endows the Tieguanyin tea with special aroma characteristics. Compared with Tieguanyin tea leaves, the Tieguanyin tea leaves water-removing substance has more flower fragrance and fragrant substances, and the style of the Tieguanyin tea leaves is more prominent in tea fragrance, flower fragrance and sweet fragrance. The natural spice substance developed by tea and tea products is applied to the fields of food, daily chemicals, tobacco essence development and the like, and has very wide application prospect (Zhang Feng, Chen Xiao Ming, Van Qiang, and the like. the development of Tie Guanyin green-removing spice and the application thereof in cigarettes [ J ]. essence spice cosmetics, 2016,12(6):16-20 ].
On the other hand, in the large background of global smoking control and tobacco harm reduction, electronic cigarettes have been rapidly developed in recent years as a product that can simulate cigarette smoking and provide a sense of physiological satisfaction with nicotine. Because the background of tobacco is not available, the style of the electronic cigarette is more modeled by essence. However, the flavor style of the electronic cigarettes on the market is monotonous, and the electronic cigarettes mainly have mint, cocoa, fruit and other flavors. Therefore, in order to improve the smoking quality of the electronic cigarette and enrich the style characteristics of the electronic cigarette product, it is necessary to design an electronic cigarette perfume composition having the tea aroma characteristic of Tieguanyin for the electronic cigarette.
Disclosure of Invention
The inventor finds that the Tieguanyin tea de-enzyming substance has unique Tieguanyin tea fragrance, and the electronic cigarette spice composition with Tieguanyin tea fragrance characteristics can be obtained by formula modulation.
One object of the invention is to provide an electronic cigarette spice composition with Tieguanyin tea aroma characteristics, and another object of the invention is to provide an electronic cigarette liquid with Tieguanyin tea aroma characteristics. It is yet another object of the present invention to provide an electronic cigarette or electronic cigarette cartridge with Tieguanyin tea aroma characteristics. It is a further object of the present invention to provide the use of an electronic cigarette flavor composition or an electronic cigarette liquid having an Tieguanyin tea aroma characteristic in an electronic cigarette.
In a first aspect of the invention, there is provided an e-cigarette flavour composition having an Tieguanyin tea flavour profile, said composition consisting of:
0.02-0.15 parts of leaf alcohol;
0.02-0.1 part by weight of benzaldehyde;
0.002-0.05 weight part of ethyl caproate;
0.03-0.15 parts by weight of benzyl alcohol;
phenylacetaldehyde 0.0004-0.0015 weight portions;
0.3-1.5 parts by weight of linalool oxide (furan type);
0.04-0.15 part by weight of linalool;
5-10 parts of phenethyl alcohol;
0-0.015 parts of tea scented ketone;
2-8 parts of linalool oxide (pyran type);
0.02-0.15 part by weight of alpha-terpineol;
0.005-0.015 parts by weight of nerol;
0.03-0.15 part by weight of geraniol;
0.02-0.15 part by weight of citral;
1-5 parts of indole;
0-0.0015 parts of gamma-nonalactone;
0.02-0.15 parts of jasmone;
0.5-2 parts of nerolidol;
0.05-0.15 part by weight of methyl jasmonate.
In some embodiments of the invention, the e-cigarette flavour composition of the invention consists of:
0.02-0.1 part by weight of leaf alcohol;
0.02-0.1 part by weight of benzaldehyde;
0.002-0.01 weight part of ethyl caproate;
0.03-0.1 part by weight of benzyl alcohol;
phenylacetaldehyde 0.0004-0.001 weight portion;
0.3-1 part by weight of linalool oxide (furan type);
0.04-0.1 part by weight of linalool;
5-8 parts of phenethyl alcohol;
0-0.01 part by weight of tea scented ketone;
2-5 parts of linalool oxide (pyran type);
0.02-0.1 part by weight of alpha-terpineol;
0.005-0.01 weight part of nerol;
0.03-0.1 part by weight of geraniol;
0.02-0.1 part by weight of citral;
1-4 parts of indole;
0-0.001 weight part of gamma-nonalactone;
0.02-0.1 part by weight of jasmone;
0.5-2 parts of nerolidol;
0.05-0.1 part by weight of methyl jasmonate.
In some embodiments of the invention, the e-cigarette flavor composition of the invention is comprised of:
0.02-0.1 part by weight of leaf alcohol;
0.02-0.07 part by weight of benzaldehyde;
0.002-0.01 weight part of ethyl caproate;
0.03-0.1 part by weight of benzyl alcohol;
phenylacetaldehyde 0.0004-0.001 weight portion;
0.3-1 part by weight of linalool oxide (furan type);
0.04-0.1 part by weight of linalool;
5-8 parts of phenethyl alcohol;
0.004-0.01 weight portion of tea scented ketone;
2-5 parts of linalool oxide (pyran type);
0.02-0.1 part by weight of alpha-terpineol;
0.005-0.01 weight part of nerol;
0.03-0.1 part by weight of geraniol;
0.02-0.1 part by weight of citral;
1-4 parts of indole;
0.0002 to 0.001 weight part of gamma-nonalactone;
0.02-0.1 part by weight of jasmone;
0.5-2 parts of nerolidol;
0.05-0.1 part by weight of methyl jasmonate.
In some embodiments of the present invention, there is provided an e-cigarette flavour composition having an Tieguanyin tea flavour profile, the composition comprising:
0.02-0.15 parts of leaf alcohol;
0.02-0.1 part by weight of benzaldehyde;
0.002-0.05 weight part of ethyl caproate;
0.03-0.15 parts by weight of benzyl alcohol;
phenylacetaldehyde 0.0004-0.0015 weight portions;
0.3-1.5 parts by weight of linalool oxide (furan type);
0.04-0.15 part by weight of linalool;
5-10 parts of phenethyl alcohol;
0-0.015 parts of tea scented ketone;
2-8 parts of linalool oxide (pyran type);
0.02-0.15 part by weight of alpha-terpineol;
0.005-0.015 parts by weight of nerol;
0.03-0.15 parts by weight of geraniol;
0.02-0.15 part by weight of citral;
1-5 parts of indole;
0-0.0015 weight parts of gamma-nonalactone;
0.02-0.15 parts of jasmone;
0.5-2 parts of nerolidol;
0.05-0.15 part of methyl jasmonate.
In some embodiments of the invention, the e-cigarette flavor composition of the invention comprises:
0.02-0.1 part by weight of leaf alcohol;
0.02-0.1 part by weight of benzaldehyde;
0.002-0.01 weight part of ethyl caproate;
0.03-0.1 part by weight of benzyl alcohol;
phenylacetaldehyde 0.0004-0.001 weight portion;
0.3-1 part by weight of linalool oxide (furan type);
0.04-0.1 part by weight of linalool;
5-8 parts of phenethyl alcohol;
0-0.01 part by weight of tea scented ketone;
2-5 parts of linalool oxide (pyran type);
0.02-0.1 part by weight of alpha-terpineol;
0.005-0.01 part by weight of nerol;
0.03-0.1 part by weight of geraniol;
0.02-0.1 part by weight of citral;
1-4 parts of indole;
0-0.001 weight part of gamma-nonalactone;
0.02-0.1 part by weight of jasmone;
0.5-2 parts of nerolidol;
0.05-0.1 part of methyl jasmonate.
In some embodiments of the invention, the e-cigarette flavor composition of the invention comprises:
0.02-0.1 part by weight of leaf alcohol;
0.02-0.07 part by weight of benzaldehyde;
0.002-0.01 weight portion of ethyl caproate;
0.03-0.1 part by weight of benzyl alcohol;
phenylacetaldehyde 0.0004-0.001 weight portion;
0.3-1 part by weight of linalool oxide (furan type);
0.04-0.1 part by weight of linalool;
5-8 parts of phenethyl alcohol;
0.004-0.01 weight portion of tea scented ketone;
2-5 parts of linalool oxide (pyran type);
0.02-0.1 part by weight of alpha-terpineol;
0.005-0.01 weight part of nerol;
0.03-0.1 part by weight of geraniol;
0.02-0.1 part by weight of citral;
1-4 parts of indole;
0.0002 to 0.001 weight part of gamma-nonalactone;
0.02-0.1 part by weight of jasmone;
0.5-2 parts of nerolidol;
0.05-0.1 part by weight of methyl jasmonate.
In some embodiments of the invention, the amount of leaf alcohol in the electronic cigarette flavour composition of the invention is from 0.02 to 0.15 parts by weight, such as from 0.02 to 0.1 parts by weight, for example including any one of 0.02, 0.03, 0.04, 0.05, 0.06, 0.07, 0.08, 0.09, 0.1, 0.15 parts by weight and all values within any combination thereof.
In some embodiments of the invention, the amount of benzaldehyde in the electronic cigarette flavor composition of the invention is 0.02 to 0.1 parts by weight, such as 0.02 to 0.07 parts by weight, for example including any one of 0.02, 0.03, 0.04, 0.05, 0.06, 0.07, 0.08, 0.09, or 0.1 parts by weight and all values within any combination thereof.
In some embodiments of the invention, the amount of ethyl hexanoate in the electronic cigarette flavor composition of the invention is 0.002 to 0.05 parts by weight, such as 0.002 to 0.01 parts by weight, including for example any one of 0.002, 0.003, 0.004, 0.005, 0.006, 0.007, 0.008, 0.009, 0.01, 0.05 parts by weight, and all values within any combination thereof.
In some embodiments of the invention, the amount of benzyl alcohol in the electronic cigarette flavor composition of the invention is 0.03 to 0.15 parts by weight, such as 0.03 to 0.1 parts by weight, including for example any of 0.03, 0.04, 0.05, 0.06, 0.07, 0.08, 0.09, or 0.1 parts by weight and all values within any combination thereof.
In some embodiments of the invention, the amount of phenylacetaldehyde in the electronic cigarette perfume composition of the present invention is 0.0004 to 0.0015 parts by weight, such as 0.0004 to 0.001 parts by weight, for example including any one of 0.0004, 0.0005, 0.0006, 0.0007, 0.0008, 0.0009, 0.001 parts by weight, 0.0015 parts by weight and all values within any combination thereof.
In some embodiments of the invention, the amount of linalool oxide (furan type) in the electronic cigarette flavor composition of the invention is 0.3 to 1.5 parts by weight, such as 0.3 to 1 part by weight, such as 0.35 to 0.8 part by weight, including for example, any of 0.3, 0.4, 0.5, 0.6, 0.7, 0.8, 0.9, 1, 1.5 parts by weight and all values within any combination thereof.
In some embodiments of the invention, the amount of linalool in the electronic cigarette flavorant composition of the invention is 0.04 to 0.15 parts by weight, such as 0.04 to 0.1 parts by weight, such as 0.04 to 0.095 parts by weight, such as 0.04 to 0.085 parts by weight, including for example any of 0.04, 0.05, 0.06, 0.07, 0.08, 0.09, 0.1, 0.15 parts by weight and all values within any combination thereof.
In some embodiments of the invention, the amount of phenylethyl alcohol in the e-cigarette flavor composition of the invention is 5-10 parts by weight, such as 5-8 parts by weight, such as 5.3-8 parts by weight, such as 5.5-8 parts by weight, including for example any one of 5, 6, 7, 8, 9, 10 parts by weight and all values within any combination thereof.
In some embodiments of the invention, the amount of theascented ketone in the electronic cigarette fragrance composition of the invention is 0 to 0.015 parts by weight, such as 0 to 0.01 parts by weight, such as 0.004 to 0.01 parts by weight, such as 0.005 to 0.008 parts by weight, including for example any of 0.001, 0.002, 0.003, 0.004, 0.005, 0.006, 0.007, 0.008, 0.009, 0.01, 0.015 parts by weight, and all values within any combination thereof.
In some embodiments of the invention, the amount of linalool oxide (pyran-type) in the electronic cigarette flavor composition of the present invention is from 2 to 8 parts by weight, such as from 2 to 5 parts by weight, such as from 2.3 to 5 parts by weight, such as from 2.5 to 5 parts by weight, from 2.8 to 4.5 parts by weight, from 3.3 to 4.5 parts by weight, including for example, all values within any one of 2, 3, 4, 5, 6, 7, 8 parts by weight and any combination thereof.
In some embodiments of the invention, the amount of alpha-terpineol in the e-cigarette fragrance composition of the invention is 0.02 to 0.15 parts by weight, such as 0.02 to 0.1 parts by weight, for example including any one of 0.02, 0.03, 0.04, 0.05, 0.06, 0.07, 0.08, 0.09, 0.1, 0.15 parts by weight and all values within any combination thereof.
In some embodiments of the invention, the amount of nerol in the e-cigarette perfume composition of the invention is from 0.005 to 0.015 parts by weight, such as from 0.005 to 0.01 parts by weight, including for example any one of 0.005, 0.006, 0.007, 0.008, 0.009, 0.01, 0.015 parts by weight and all values in any combination thereof.
In some embodiments of the invention, the amount of geraniol in the electronic cigarette flavor composition of the invention is 0.03-0.15 parts by weight, such as 0.03-0.1 parts by weight, including for example any of 0.03, 0.04, 0.05, 0.06, 0.07, 0.08, 0.09, 0.1, 0.15 parts by weight, and all values within any combination thereof.
In some embodiments of the invention, the amount of citral in the electronic cigarette flavor composition of the invention is 0.02 to 0.15 parts by weight, such as 0.02 to 0.1 parts by weight, including for example any one of 0.02, 0.03, 0.04, 0.05, 0.06, 0.07, 0.08, 0.09, 0.1, 0.15 parts by weight and all values within any combination thereof.
In some embodiments of the invention, the amount of indole in the e-cigarette flavor composition of the invention is 1 to 5 parts by weight, such as 1 to 4 parts by weight, such as 1.2 to 4 parts by weight, such as 2 to 3.7 parts by weight, such as 2.5 to 3.6 parts by weight, including for example, all values within the range of any one of 1, 2, 3, 4, 5 and any combination thereof.
In some embodiments of the invention, the amount of γ -nonalactone in the e-cigarette perfume composition of the invention is 0 to 0.0015 parts by weight, such as 0 to 0.001 parts by weight, for example 0.0002 to 0.001 parts by weight, including for example any and all values within the range of 0.0001, 0.0002, 0.0003, 0.0004, 0.0005, 0.0006, 0.0007, 0.0008, 0.0009 or 0.001 parts by weight.
In some embodiments of the invention, the amount of jasmone in the e-cigarette flavor composition of the invention is 0.02 to 0.15 parts by weight, such as 0.02 to 0.1 parts by weight, for example including any one of 0.02, 0.03, 0.04, 0.05, 0.06, 0.07, 0.08, 0.09, 0.1, 0.15 parts by weight and all values within any combination thereof.
In some embodiments of the invention, the amount of nerolidol in the e-cigarette flavor composition of the invention is 0.5 to 2 parts by weight, for example including any of 0.5, 0.6, 0.7, 0.8, 0.9, 1, 1.1, 1.2, 1.3, 1.4, 1.5, 1.6, 1.7, 1.8, 1.9, 2, 2.5 parts by weight and all values within any combination thereof.
In some embodiments of the invention, the amount of methyl jasmonate in the e-cigarette flavor composition of the invention is 0.05 to 0.15 parts by weight, such as 0.05 to 0.1 parts by weight, for example including any of 0.05, 0.06, 0.07, 0.08, 0.09, 0.1, 0.15 parts by weight and all values within any combination thereof.
In some embodiments of the invention, the e-cigarette flavor composition of the invention further comprises 80 to 95 parts by weight of a flavorant auxiliary, such as 80 to 90 parts by weight, such as 85 to 90 parts by weight, such as 83.12 to 88.26 parts by weight, for example including any one of 80, 81, 82, 83, 84, 85, 86, 87, 88, 89, 90, 91, 92, 93, 94, or 95 (e.g., 88.26, 86.45, 87.89, 83.12, 84.04, 84.27, 85.12, 86.39, 86.55) parts by weight and all values within any combination thereof.
In some embodiments of the invention, the flavor adjuvant is selected from water, ethanol (e.g., 60-80 wt% ethanol), propylene glycol, and glycerin, or combinations thereof; preferably, the flavor adjuvant is selected from propylene glycol, ethanol (e.g., 70 wt% ethanol), or a combination thereof; more preferably, the flavor adjuvant is ethanol (e.g., 70 wt% ethanol), or a combination of propylene glycol and ethanol (e.g., 70 wt% ethanol).
In some embodiments of the invention, the e-cigarette flavor composition of the invention further comprises 80 to 95 parts by weight, such as 80 to 90 parts by weight, such as 85 to 90 parts by weight, such as 83.12 to 88.26 parts by weight of a flavor adjuvant, wherein the flavor adjuvant is ethanol (e.g., 70% by weight ethanol), or a combination of propylene glycol and ethanol (e.g., 70% by weight ethanol), wherein preferably the weight ratio of propylene glycol to ethanol (e.g., 70% by weight ethanol) is 1:4 to 1:1, such as 1:3.9 to 1:1.1, such as 1:3.8 to 1:1.2, such as 1:3.7 to 1:1.3, such as 1:3.6 to 1:1.4, such as 1:3.5 to 1: 1.4.
In a second aspect of the invention, there is provided an electronic cigarette liquid comprising the electronic cigarette flavor composition of the invention.
In some embodiments of the invention, the e-cigarette liquid further comprises an e-cigarette liquid adjunct (also referred to as a smoke agent).
In some embodiments of the present invention, the e-cigarette liquid additive comprises 50-95%, such as 60-95%, such as 70-95%, such as 80-92%, for example including any one of 50%, 60%, 70%, 80%, 90%, 91%, 92%, 93%, 94%, 95% and all values within any combination thereof, by volume of the e-cigarette liquid.
In some embodiments of the invention, the volume ratio of the e-cigarette flavor composition of the invention to the e-cigarette liquid adjuvant is 1:1 to 1:20, such as 1:5 to 1:10, including, for example, any one of 1:1, 1:2, 1:3, 1:4, 1:5, 1:6, 1:7, 1:7.5, 1:8, 1:9, 1:10, 1:11, 1:12, 1:13, 1:14, 1:15, 1:16, 1:17, 1:18, 1:19, 1:20, and all values within any combination thereof.
In some embodiments of the invention, the e-cigarette liquid adjunct is selected from the group consisting of propylene glycol, glycerin, and combinations thereof. Preferably, the electronic cigarette liquid auxiliary material is a combination of propylene glycol and glycerol. The propylene glycol has large using amount and good fluidity, but the smoke amount is small, the glycerol has large using amount and poor fluidity, but the smoke amount is large, so the propylene glycol and the glycerol have a certain proportion. Preferably, the volume ratio of the propylene glycol to the glycerol in the electronic cigarette liquid accessory is 7:3-7:3, such as 6:4-4:6, such as 6:4, 5:5, 4: 6.
In a third aspect of the invention, there is provided an electronic cigarette or an electronic cigarette cartridge comprising the electronic cigarette flavour composition of the invention or the electronic cigarette liquid of the invention.
In a fourth aspect of the invention, there is provided a use of the e-cigarette flavour composition or e-cigarette liquid of the invention in an e-cigarette.
Preferably, the electronic cigarette spice composition or the electronic cigarette liquid is used in an electronic cigarette for endowing the electronic cigarette with Tie Guanyin tea fragrance characteristics or enriching the cigarette fragrance, softening the smoke, coordinating the smoke flavor and reducing the stimulation.
Interpretation of terms
In the present invention, unless otherwise specified, "enzyme deactivation" refers to a process of deactivating or inactivating enzymes in fresh leaves at a certain temperature. The water-removing method comprises the following steps: roller fixation, pan frying fixation, hot air fixation, steam fixation, microwave fixation or steam-hot air mixed fixation, etc. "enzyme-deactivating substance" refers to a substance which has been subjected to enzyme deactivation.
The e-cigarette flavor composition having an Tieguanyin tea aroma characteristic of the present invention has one or more of the following benefits, including but not limited to:
(1) the components of the electronic cigarette spice composition with the Tie Guanyin tea aroma characteristic can endow the electronic cigarette with the Tie Guanyin tea de-enzyming object aroma characteristic, improve the smoke softness, reduce the irritation and obviously improve the smoking quality.
(2) The electronic cigarette spice composition with the Tieguanyin tea aroma characteristics is strong in pertinence, clear in purpose in use and convenient in aroma blending process.
(3) The electronic cigarette spice composition with the Tie Guanyin tea aroma characteristic is easy to obtain raw materials and simple in production process.
Detailed Description
The technical solution of the present invention is further described in detail by the following examples. The exemplary embodiments of the present invention and their description are intended to illustrate the present invention and should not be construed as limiting the present invention in any way. The raw materials used in the preparation of the electronic cigarette spice composition are all common raw materials which can be purchased; the preparation process is a conventional stirring, mixing and standing process in the field of flavoring, and special equipment is not required.
Example 1
The ingredients were mixed uniformly according to the formulation in table 1-1 to prepare a perfume composition having a prominent tea aroma of the Tieguanyin enzyme-deactivated substance.
TABLE 1-1 fragrance compositions
The tea aroma note and aroma-holding capacity of the prepared 1# to 3# spice composition are subjected to aroma smelling judgment, the aroma smelling judgment adopts an olfactory discrimination mode, the number of the evaluated persons is 12, and the specific judgment result is shown in a table 1-2:
TABLE 1-2 evaluation results of flavor-smelling of Tie Guanyin tea flavor composition
As can be seen from tables 1-2, the tea notes of the # 1 and # 3 fragrance compositions are better than the tea notes of the # 2 fragrance, with the tea note and the aroma-holding capacity of the # 1 composition performing best.
The fragrance smelling judgment result shows that: the 1#, 2#, 3# spice compositions have outstanding tea aroma of Tieguanyin water-removing substances, and the aroma is relatively durable and stable.
2mL of the prepared 1# to 3# spice composition is added into 20mL of electronic cigarette liquid auxiliary materials (propylene glycol: glycerol (6:4)) and evenly mixed to obtain the electronic cigarette liquid.
And adding 4mL of the electronic cigarette liquid into an electronic cigarette cartridge, standing for 2 hours, and then smoking the electronic cigarette by a sensory evaluation staff. The aroma characteristics of the electronic cigarette liquid and the sensory quality evaluation result show that the electronic cigarette added with the 1#, 2#, 3# spice compositions has obvious tea aroma, wherein the 1#, 3# tea aroma concentration is larger than that of the 2# tea aroma, and the perception degree is stronger.
Example 2
The components were mixed uniformly according to the formulation in table 2-1 to prepare a tea aroma perfume composition having a complex floral aroma.
TABLE 2-1 fragrance compositions
The tea aroma and aroma maintaining capability of the composite floral aroma of the 4# -6 # spice composition prepared above are subjected to aroma smelling judgment, the aroma smelling judgment adopts an olfactory discrimination mode, the number of the evaluated persons is 12, and the specific judgment result is shown in table 2-2:
TABLE 2-2 evaluation of the flavor of Tie Guanyin tea flavor composition by smelling
As can be seen from tables 2-2, the complex floral notes of the 4# and 5# fragrance compositions were better than the 6# fragrance, with the complex floral tea note and the holding capacity of the 4# composition performing best.
The fragrance smelling judgment result shows that: the Tie Guanyin green-removing compound floral aroma of the 4#, 5#, 6# spice compositions has outstanding tea aroma characteristics and relatively lasting and stable aroma.
Adding 2mL of the prepared 4# to 6# spice composition into 15mL of electronic cigarette liquid auxiliary material (propylene glycol: glycerol (5:5)) and uniformly mixing to obtain the electronic cigarette liquid
4mL of the electronic cigarette liquid is added into an electronic cigarette cartridge, after standing for 2 hours, a sensory evaluator sucks the electronic cigarette, and the aroma characteristics and sensory quality evaluation results of the electronic cigarette liquid show that the electronic cigarette added with the 4#, 5# and 6# spice compositions has outstanding compound flower-fragrance tea aroma and elegant aroma, wherein the 4# spice composition has the most outstanding flower-fragrance aroma.
Example 3
The components are uniformly mixed according to the formula in the table 3-1 to prepare the tea aroma perfume composition with composite faint scent.
TABLE 3-1 fragrance composition
The tea aroma and aroma retention capacity of the composite faint scent of the 7# to 9# spice composition are subjected to aroma smelling judgment, the aroma smelling judgment adopts an aroma distinguishing mode, the number of evaluated persons is 12, and the specific judgment result is shown in a table 3-2:
TABLE 3-2 evaluation results of flavor-smelling of Tie Guanyin tea flavor composition
As can be seen from tables 3-2, the complex scent notes of the 7# and 9# perfume compositions are better than the 8# perfume, with the complex scent note and fragrance-holding capacity of the 7# composition performing best.
The fragrance smelling judgment result shows that: the Tie Guanyin water-removing compound faint scent of the 7#, 8#, 9# spice compositions has outstanding tea scent characteristics and relatively lasting and stable scent.
And adding 2mL of the 7# to 9# spice composition prepared in the above step into 10mL of electronic cigarette liquid auxiliary materials (propylene glycol: glycerol (4:6)) and uniformly mixing to obtain the electronic cigarette liquid.
And adding 4mL of the electronic cigarette liquid into an electronic cigarette cartridge, standing for 2 hours, and then smoking the electronic cigarette by an electronic cigarette sensory evaluation personnel. The aroma characteristics of the cigarette liquid of the electronic cigarette and sensory quality evaluation results show that the electronic cigarette added with the 7#, 8#, and 9# spice compositions can obviously sense the aroma of the composite fragrant tea, the aroma is attractive, and the 7# sample fragrance is more prominent.
Finally, it should be noted that: the above examples are only intended to illustrate the technical solution of the present invention and not to limit it; although the present invention has been described in detail with reference to preferred embodiments, those skilled in the art will understand that: modifications to the specific embodiments of the invention or equivalent substitutions for parts of the technical features may be made; without departing from the spirit of the invention, it is intended to cover all modifications within the scope of the invention as claimed.
Claims (21)
1. An electronic cigarette flavor composition having an Tieguanyin tea aroma characteristic, the composition consisting of:
0.02-0.15 weight part of leaf alcohol;
0.02-0.1 part by weight of benzaldehyde;
0.002-0.05 weight part of ethyl caproate;
0.03-0.15 parts by weight of benzyl alcohol;
phenylacetaldehyde 0.0004-0.0015 weight portions;
0.3-1.5 parts by weight of furan linalool oxide;
0.04-0.15 part by weight of linalool;
5-10 parts of phenethyl alcohol;
0-0.015 parts of tea scented ketone;
2-8 parts of pyran linalool oxide;
0.02-0.15 part by weight of alpha-terpineol;
0.005-0.015 parts by weight of nerol;
0.03-0.15 part by weight of geraniol;
0.02-0.15 part by weight of citral;
1-5 parts of indole;
0-0.0015 weight parts of gamma-nonalactone;
0.02-0.15 parts of jasmone;
0.5-2 parts of nerolidol;
0.05-0.15 part by weight of methyl jasmonate;
80-95 parts of perfume auxiliary materials.
2. The e-cigarette flavorant composition of claim 1, consisting of:
0.02-0.1 weight part of leaf alcohol;
0.02-0.1 part by weight of benzaldehyde;
0.002-0.01 weight part of ethyl caproate;
0.03-0.1 part by weight of benzyl alcohol;
phenylacetaldehyde 0.0004-0.001 weight portion;
0.3-1 part by weight of furan linalool oxide;
0.04-0.1 part by weight of linalool;
5-8 parts of phenethyl alcohol;
0-0.01 part by weight of tea scented ketone;
2-5 parts of pyran linalool oxide;
0.02-0.1 part by weight of alpha-terpineol;
0.005-0.01 part by weight of nerol;
0.03-0.1 part by weight of geraniol;
0.02-0.1 part by weight of citral;
1-4 parts of indole;
0-0.001 weight part of gamma-nonalactone;
0.02-0.1 part by weight of jasmone;
0.5-2 parts of nerolidol;
0.05-0.1 part by weight of methyl jasmonate;
80-95 parts of perfume auxiliary materials.
3. The e-cigarette flavorant composition of claim 1, said composition consisting of:
0.02-0.1 part by weight of leaf alcohol;
0.02-0.07 part by weight of benzaldehyde;
0.002-0.01 weight part of ethyl caproate;
0.03-0.1 part by weight of benzyl alcohol;
phenylacetaldehyde 0.0004-0.001 weight portion;
0.3-1 part by weight of furan linalool oxide;
0.04-0.1 part by weight of linalool;
5-8 parts of phenethyl alcohol;
0.004-0.01 part by weight of tea scented ketone;
2-5 parts of pyran linalool oxide;
0.02-0.1 part by weight of alpha-terpineol;
0.005-0.01 weight part of nerol;
0.03-0.1 part by weight of geraniol;
0.02-0.1 part by weight of citral;
1-4 parts of indole;
0.0002 to 0.001 weight part of gamma-nonalactone;
0.02-0.1 part by weight of jasmone;
0.5-2 parts of nerolidol;
0.05-0.1 part by weight of methyl jasmonate;
80-95 parts of perfume auxiliary materials.
4. The e-cigarette flavor composition of any one of claims 1-3, comprising 85-90 parts by weight of a flavor adjuvant selected from water, ethanol, propylene glycol, glycerol, or a combination thereof.
5. The e-cigarette flavor composition of any one of claims 1-3, wherein the composition comprises 83.12-88.26 parts by weight of a flavor adjuvant selected from water, ethanol, propylene glycol, glycerol, or a combination thereof.
6. The e-cigarette flavor composition of claim 4, wherein ethanol is 60-80% ethanol by weight.
7. The e-cigarette flavor composition of claim 4, wherein the flavor adjuvant is selected from propylene glycol, ethanol, or a combination thereof.
8. The e-cigarette flavor composition of claim 4, wherein the flavor adjunct is ethanol, or a combination of propylene glycol and ethanol.
9. The e-cigarette flavor composition of claim 8, wherein the weight ratio of propylene glycol to ethanol is 1:4 to 1:1.
10. The e-cigarette flavor composition of claim 9, wherein the weight ratio of propylene glycol to ethanol is 1:3.5-1: 1.4.
11. The electronic cigarette flavor composition of any one of claims 7-10, wherein ethanol is 70 wt% ethanol.
12. An e-cigarette liquid comprising the e-cigarette flavor composition of any one of claims 1-11.
13. The e-cigarette liquid of claim 12, further comprising an e-cigarette liquid adjunct; the electronic cigarette liquid auxiliary material is selected from propylene glycol, glycerol or a combination of the propylene glycol and the glycerol.
14. The e-cigarette liquid of claim 13, wherein the e-cigarette liquid accessory comprises 50-95% by volume of the e-cigarette liquid.
15. The e-cigarette liquid of claim 14, wherein the e-cigarette liquid accessory comprises 80-92% by volume of the e-cigarette liquid.
16. The e-vaping liquid of claim 13, wherein the e-vaping liquid adjuvant is a combination of propylene glycol and glycerol.
17. The e-cigarette liquid of claim 16, wherein the volume ratio of propylene glycol to glycerin is 7: 3.
18. The e-cigarette liquid of claim 16, wherein the volume ratio of propylene glycol to glycerin is 6:4-4: 6.
19. An electronic cigarette or an electronic cigarette cartridge containing the electronic cigarette flavor composition of any one of claims 1-11 or the electronic cigarette liquid of any one of claims 12-18.
20. Use of the e-cigarette flavor composition of any one of claims 1-11 or the e-cigarette liquid of any one of claims 12-18 in an e-cigarette.
21. Use according to claim 20 for imparting a tieguanyin tea aroma characteristic or enriching the aroma of a cigarette, softening the smoke, harmonizing the smoke taste, reducing irritation to an electronic cigarette.
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| CN202010191282.3A CN111329103B (en) | 2020-03-18 | 2020-03-18 | Electronic cigarette spice composition with Tie Guanyin tea aroma characteristics, electronic cigarette liquid and application of electronic cigarette spice composition and electronic cigarette liquid |
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| CN202010191282.3A CN111329103B (en) | 2020-03-18 | 2020-03-18 | Electronic cigarette spice composition with Tie Guanyin tea aroma characteristics, electronic cigarette liquid and application of electronic cigarette spice composition and electronic cigarette liquid |
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| CN112126520B (en) * | 2020-09-21 | 2023-10-27 | 江西中烟工业有限责任公司 | Preparation method of incense base for cigarettes |
| EP4245155A1 (en) * | 2020-11-13 | 2023-09-20 | Japan Tobacco Inc. | Tobacco extract containing tobacco terpenes, and method for manufacturing said tobacco extract |
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| KR20090097069A (en) * | 2008-03-10 | 2009-09-15 | 김희빈 | Composition of Volatile Liquid Tobacco Nicotine |
| CN105996115B (en) * | 2016-07-18 | 2018-08-17 | 福建中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke with extra-strong tea just object extract preparation processed |
| CN106037012B (en) * | 2016-07-18 | 2019-03-15 | 福建中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke |
| CN105962426B (en) * | 2016-07-29 | 2019-07-16 | 福建中烟工业有限责任公司 | Composition and tobacco juice for electronic smoke containing extra-strong tea extract |
| CN105969524A (en) * | 2016-07-29 | 2016-09-28 | 福建中烟工业有限责任公司 | Composition and application of composition in cigarettes |
| CN110506980A (en) * | 2019-09-12 | 2019-11-29 | 深圳雾芯科技有限公司 | Flavour compositions and electronic cigarette liquid comprising the flavour compositions |
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