CN114343231A - Electronic cigarette liquid with citrus-flavor aroma and preparation method thereof - Google Patents
Electronic cigarette liquid with citrus-flavor aroma and preparation method thereof Download PDFInfo
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- CN114343231A CN114343231A CN202111480929.5A CN202111480929A CN114343231A CN 114343231 A CN114343231 A CN 114343231A CN 202111480929 A CN202111480929 A CN 202111480929A CN 114343231 A CN114343231 A CN 114343231A
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Abstract
The invention discloses an electronic cigarette liquid with citrus-flavor aroma and a preparation method thereof, wherein the electronic cigarette liquid is prepared from the following raw materials in parts by weight: 0.1-10 parts of sweet orange oil, 0.01-1 part of tangerine oil, 0.01-1 part of orange oil, 0.005-0.25 part of grapefruit oil, 0.005-0.25 part of ethyl acetoacetate, 0.001-0.1 part of raspberry ketone, 0.001-0.1 part of nonadienal, 1-5 parts of ethanol, 10-20 parts of water, 10-80 parts of propylene glycol and 20-80 parts of glycerol. The electronic cigarette liquid can enrich the smoking flavor of the electronic cigarette, meet the requirements of different consumer groups, and simultaneously effectively reduce the potential harm to the health of consumers.
Description
Technical Field
The invention relates to the technical field of electronic cigarette liquid, in particular to electronic cigarette liquid with citrus-flavor aroma and a preparation method thereof.
Background
The direct harm of smoking to smokers and the influence of second-hand smoke on the surrounding environment are increasingly receiving attention from society. The electronic cigarette is a novel tobacco product, and compared with the traditional cigarette, the electronic cigarette does not contain harmful substances such as tar, carbon monoxide and the like, and has less harm to the body of a smoker; in addition, the aerosol formed by atomizing nicotine of the electronic cigarette is quickly diluted in the air, so that the risk of harm to surrounding people is reduced. Electronic cigarettes as a substitute for cigarettes have gained market acceptance worldwide, and sales are on the rising trend year by year.
The electronic cigarette liquid is an important factor influencing the smoking quality. Through the development of several generations, although the electronic cigarettes have the shape, hand feeling, smoke and the like cigarettes, the cigarette liquid used for the electronic cigarettes has some defects. In order to simulate the taste of cigarettes, mainstream electronic cigarettes sold in the market generally adopt tobacco raw material extracts, and then are mixed with tobacco flavors, deionized water and the like to prepare electronic cigarette liquid. The smoke generated by the electronic cigarette liquid can imitate cigarettes to a certain extent, but the released smoke also contains a small amount of harmful substances, smokers generally feel that the fragrance and the taste of the electronic cigarettes do not meet the physiological requirements, the smoking flavor is monotonous, and the health and sustainable development of the electronic cigarettes are greatly influenced by the problems.
Disclosure of Invention
In order to overcome the technical defects, the invention provides the electronic cigarette liquid with the citrus-flavor aroma and the preparation method thereof.
In order to achieve the technical effect, the invention provides electronic cigarette liquid with citrus-flavor aroma, which is prepared from the following raw materials in parts by weight: 0.1-10 parts of sweet orange oil, 0.01-1 part of tangerine oil, 0.01-1 part of orange oil, 0.005-0.25 part of grapefruit oil, 0.005-0.25 part of ethyl acetoacetate, 0.001-0.1 part of raspberry ketone, 0.001-0.1 part of nonadienal, 1-5 parts of ethanol, 10-20 parts of water, 10-80 parts of propylene glycol and 20-80 parts of glycerol.
The electronic cigarette liquid is prepared from the following raw materials in parts by weight: 0.5-8 parts of sweet orange oil, 0.05-1 part of tangerine oil, 0.05-1 part of orange oil, 0.01-0.25 part of grapefruit oil, 0.01-0.25 part of ethyl acetoacetate, 0.001-0.01 part of raspberry ketone, 0.001-0.01 part of nonadienal, 1-5 parts of ethanol, 10-20 parts of water, 10-80 parts of propylene glycol and 40-80 parts of glycerol.
The electronic cigarette liquid is prepared from the following raw materials in parts by weight: 1-8 parts of sweet orange oil, 0.1-1 part of tangerine oil, 0.1-1 part of orange oil, 0.1-0.25 part of grapefruit oil, 0.01-0.2 part of ethyl acetoacetate, 0.001-0.01 part of raspberry ketone, 0.001-0.01 part of nonadienal, 1-5 parts of ethanol, 10-20 parts of water, 10-80 parts of propylene glycol and 40-80 parts of glycerol.
The invention also provides a preparation method of the electronic cigarette liquid with citrus flavor, which is characterized in that the electronic cigarette liquid with lemon flavor can be obtained by fully mixing the following raw materials in parts by weight: 0.1-10 parts of sweet orange oil, 0.01-1 part of tangerine oil, 0.01-1 part of orange oil, 0.005-0.25 part of grapefruit oil, 0.005-0.25 part of ethyl acetoacetate, 0.001-0.1 part of raspberry ketone, 0.001-0.1 part of nonadienal, 1-5 parts of ethanol, 10-20 parts of water, 10-80 parts of propylene glycol and 20-80 parts of glycerol.
In the invention, the raw materials for providing citrus fragrance mainly comprise sweet orange oil, tangerine oil, orange oil and grapefruit oil, wherein the sweet orange oil has the characteristic fragrance of fresh sweet oranges, and the main components comprise decanal, hexanal, octanol, d-linalool, citral, undecanal, sinenseal and the like.
Red tangerine oil has the special fragrance of fresh oranges, and the main components of the red tangerine oil comprise limonene, nerol, geraniol, terpineol, decanal, octanal and the like.
Orange oil has a fragrance peculiar to fresh oranges and contains D-limonene as a main component.
The grapefruit oil has fresh, sweet and soft citrus fragrance, and contains main components of limonene, citral, linalool, geraniol, octanal, decanal, etc.
The four raw materials show a certain fruity flavor more or less according to the respective material composition basis, and have a certain citrus flavor when being used alone, but the aroma fullness is not enough, and the fidelity is not good enough. Sweet orange oil mainly provides basic fragrant substances, red orange oil mainly improves quality and fidelity, orange oil mainly serves as coordination aid, and grapefruit oil mainly improves freshness. In order to make the fragrance of the electronic cigarette liquid plump, harmonious and vivid, the four raw materials and various monomer raw materials are blended to obtain the electronic cigarette liquid with plump, harmonious and vivid fragrance and lasting effect.
The invention also adds ethyl acetoacetate, raspberry ketone and nonadienal. The ethyl acetoacetate mainly shows green fruit fragrance and enriches fragrance; the raspberry ketone mainly shows compound fruit fragrance and improves the thick feeling; the nonadienal mainly shows faint scent and improves the freshness of the nonadienal.
Compared with the prior art, the invention has the following beneficial effects: the electronic cigarette liquid prepared by the invention has strong citrus fragrance, enriches the smoking flavor of the electronic cigarette, and can meet the requirements of different consumer groups. Compared with the prior product, the product has the advantages of greatly improving the aspects of aroma, taste and the like, and obviously increasing the satisfaction of smokers.
Detailed Description
Example 1
Sweet orange oil 2.5 parts, tangerine oil 0.6 part, orange oil 0.5 part, grapefruit oil 0.1 part, ethyl acetoacetate 0.02 part, raspberry ketone 0.002 part, nonadienal 0.001 part, ethanol 5 parts, water 15 parts, propylene glycol 15 parts, and glycerol 61.276 parts.
1mL of electronic cigarette liquid is added into an atomizer, and the electronic cigarette liquid has an obvious citrus fruity flavor after being evaluated by professional evaluation personnel.
Comparative example 1
The raw materials and the preparation method are the same as example 1 except that the raw materials do not contain sweet orange oil.
Example 2
Sweet orange oil 2.5 parts, tangerine oil 0.6 part, orange oil 0.5 part, grapefruit oil 0.1 part, ethyl acetoacetate 0.01 part, raspberry ketone 0.002 part, nonadienal 0.002 part, ethanol 5 parts, water 15 parts, propylene glycol 15 parts, and glycerol 61.285 parts.
1mL of electronic cigarette liquid is added into an atomizer, and the electronic cigarette liquid has an obvious citrus fruity flavor after being evaluated by professional evaluation personnel.
Comparative example 2
The raw materials and the preparation method are the same as example 2 except that the raw materials do not contain tangerine oil.
Example 3
Sweet orange oil 2.5 parts, tangerine oil 1 part, orange oil 0.5 part, grapefruit oil 0.2 part, ethyl acetoacetate 0.01 part, raspberry ketone 0.002 part, nonadienal 0.002 part, ethanol 5 parts, water 15 parts, propylene glycol 15 parts, and glycerol 60.785 parts.
1mL of electronic cigarette liquid is added into an atomizer, and the electronic cigarette liquid has an obvious citrus fruity flavor after being evaluated by professional evaluation personnel.
Comparative example 3
The raw materials and the preparation method are the same as example 3 except that the raw materials do not contain orange oil.
Example 4
Sweet orange oil 2.5 parts, tangerine oil 1 part, orange oil 0.5 part, grapefruit oil 0.2 part, ethyl acetoacetate 0.02 part, raspberry ketone 0.001 part, nonadienal 0.001 part, ethanol 5 parts, water 15 parts, propylene glycol 15 parts, and glycerol 60.777 parts.
1mL of electronic cigarette liquid is added into an atomizer, and the electronic cigarette liquid has an obvious citrus fruity flavor after being evaluated by professional evaluation personnel.
Comparative example 4
The preparation method of the raw materials is the same as that of example 4 except that the raw materials do not contain grapefruit oil.
Comparative example 5
The procedure of example 4 was repeated except that the starting materials contained no ethyl acetoacetate.
Comparative example 6
The preparation method of the raw materials is the same as that of example 4 except that raspberry ketone is not contained in the raw materials.
Comparative example 7
The raw materials and the preparation method are the same as example 4 except that the raw materials do not contain nonadienal.
According to the cigarette sensory quality evaluation standard GB5606.4-2005, in combination with the sensory characteristics of electronic cigarettes, 6 evaluation indexes and scores are set according to different weights, see Table 1
TABLE 1
Sensory evaluation is carried out on the electronic cigarette liquid of the embodiment and the comparison example, an arithmetic mean value is obtained according to evaluation results of each expert, a valid number is reserved in the results, and statistical results are shown in table 2.
TABLE 2
Although the present invention has been described herein with reference to the illustrated embodiments thereof, which are intended to be preferred embodiments of the present invention, it is to be understood that the invention is not limited thereto, and that numerous other modifications and embodiments can be devised by those skilled in the art that will fall within the spirit and scope of the principles of this disclosure.
Claims (4)
1. The electronic cigarette liquid with the citrus-flavor aroma is characterized by being prepared from the following raw materials in parts by weight: 0.1-10 parts of sweet orange oil, 0.01-1 part of tangerine oil, 0.01-1 part of orange oil, 0.005-0.25 part of grapefruit oil, 0.005-0.25 part of ethyl acetoacetate, 0.001-0.1 part of raspberry ketone, 0.001-0.1 part of nonadienal, 1-5 parts of ethanol, 10-20 parts of water, 10-80 parts of propylene glycol and 20-80 parts of glycerol.
2. The electronic cigarette liquid with citrus-flavor aroma according to claim 1, wherein the electronic cigarette liquid is prepared from the following raw materials in parts by weight: 0.5-8 parts of sweet orange oil, 0.05-1 part of tangerine oil, 0.05-1 part of orange oil, 0.01-0.25 part of grapefruit oil, 0.01-0.25 part of ethyl acetoacetate, 0.001-0.01 part of raspberry ketone, 0.001-0.01 part of nonadienal, 1-5 parts of ethanol, 10-20 parts of water, 10-80 parts of propylene glycol and 40-80 parts of glycerol.
3. The electronic cigarette liquid with citrus-flavor aroma according to claim 1, wherein the electronic cigarette liquid is prepared from the following raw materials in parts by weight: 1-8 parts of sweet orange oil, 0.1-1 part of tangerine oil, 0.1-1 part of orange oil, 0.1-0.25 part of grapefruit oil, 0.01-0.2 part of ethyl acetoacetate, 0.001-0.01 part of raspberry ketone, 0.001-0.01 part of nonadienal, 1-5 parts of ethanol, 10-20 parts of water, 10-80 parts of propylene glycol and 40-80 parts of glycerol.
4. The preparation method of the electronic cigarette liquid with citrus flavor is characterized in that the electronic cigarette liquid with lemon flavor is obtained by fully mixing the following raw materials in parts by weight: 0.1-10 parts of sweet orange oil, 0.01-1 part of tangerine oil, 0.01-1 part of orange oil, 0.005-0.25 part of grapefruit oil, 0.005-0.25 part of ethyl acetoacetate, 0.001-0.1 part of raspberry ketone, 0.001-0.1 part of nonadienal, 1-5 parts of ethanol, 10-20 parts of water, 10-80 parts of propylene glycol and 20-80 parts of glycerol.
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| Application Number | Priority Date | Filing Date | Title |
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| CN202111480929.5A CN114343231A (en) | 2021-12-06 | 2021-12-06 | Electronic cigarette liquid with citrus-flavor aroma and preparation method thereof |
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| CN202111480929.5A CN114343231A (en) | 2021-12-06 | 2021-12-06 | Electronic cigarette liquid with citrus-flavor aroma and preparation method thereof |
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Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102551023A (en) * | 2011-12-27 | 2012-07-11 | 上海百润香精香料股份有限公司 | Kumquat essence |
| CN104382223A (en) * | 2014-10-22 | 2015-03-04 | 浙江中烟工业有限责任公司 | Solvent suitable for preparation of fruity nicotine liquid, and nicotine liquid and electronic cigarette prepared by solvent |
| CN105077162A (en) * | 2015-08-11 | 2015-11-25 | 广州市名花香料有限公司 | Citrus flavoring combination and preparation method thereof |
| CN105124750A (en) * | 2015-07-27 | 2015-12-09 | 浙江中烟工业有限责任公司 | Sweet and fragrant electronic cigarette liquid and preparation method thereof |
| CN105167169A (en) * | 2015-08-06 | 2015-12-23 | 云南中烟工业有限责任公司 | Fruit-flavored composite E-cigarette tobacco tar |
| US20170087199A1 (en) * | 2016-02-10 | 2017-03-30 | Senomyx, Inc. | Compositions for delivering a cooling sensation |
| CN106723301A (en) * | 2016-12-19 | 2017-05-31 | 深圳瀚星翔科技有限公司 | Tobacco juice for electronic smoke |
| CN107125803A (en) * | 2017-05-10 | 2017-09-05 | 深圳瀚星翔科技有限公司 | A kind of electronic cigarette tobacco tar and preparation method thereof |
| CN109984374A (en) * | 2019-05-16 | 2019-07-09 | 铂德（深圳）科技有限公司 | Citrus extracts solution, citrus electronics tobacco tar and preparation method thereof |
| CN110295088A (en) * | 2019-07-30 | 2019-10-01 | 福建中烟工业有限责任公司 | A kind of gold Orange-flavored essence and application thereof |
| CN110771946A (en) * | 2018-07-11 | 2020-02-11 | 普瑞斯生物科技（湖南）有限公司 | Electronic cigarette atomized liquid |
-
2021
- 2021-12-06 CN CN202111480929.5A patent/CN114343231A/en active Pending
Patent Citations (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102551023A (en) * | 2011-12-27 | 2012-07-11 | 上海百润香精香料股份有限公司 | Kumquat essence |
| CN104382223A (en) * | 2014-10-22 | 2015-03-04 | 浙江中烟工业有限责任公司 | Solvent suitable for preparation of fruity nicotine liquid, and nicotine liquid and electronic cigarette prepared by solvent |
| CN105124750A (en) * | 2015-07-27 | 2015-12-09 | 浙江中烟工业有限责任公司 | Sweet and fragrant electronic cigarette liquid and preparation method thereof |
| CN105167169A (en) * | 2015-08-06 | 2015-12-23 | 云南中烟工业有限责任公司 | Fruit-flavored composite E-cigarette tobacco tar |
| CN105077162A (en) * | 2015-08-11 | 2015-11-25 | 广州市名花香料有限公司 | Citrus flavoring combination and preparation method thereof |
| US20170087199A1 (en) * | 2016-02-10 | 2017-03-30 | Senomyx, Inc. | Compositions for delivering a cooling sensation |
| CN106723301A (en) * | 2016-12-19 | 2017-05-31 | 深圳瀚星翔科技有限公司 | Tobacco juice for electronic smoke |
| CN107125803A (en) * | 2017-05-10 | 2017-09-05 | 深圳瀚星翔科技有限公司 | A kind of electronic cigarette tobacco tar and preparation method thereof |
| CN110771946A (en) * | 2018-07-11 | 2020-02-11 | 普瑞斯生物科技（湖南）有限公司 | Electronic cigarette atomized liquid |
| CN109984374A (en) * | 2019-05-16 | 2019-07-09 | 铂德（深圳）科技有限公司 | Citrus extracts solution, citrus electronics tobacco tar and preparation method thereof |
| CN110295088A (en) * | 2019-07-30 | 2019-10-01 | 福建中烟工业有限责任公司 | A kind of gold Orange-flavored essence and application thereof |
Non-Patent Citations (1)
| Title |
|---|
| 艾萍等: "西瓜香精的调配技术", 《上海应用技术学院学报》 * |
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Application publication date: 20220415 |