CN109984374A - Citrus extracts solution, citrus electronics tobacco tar and preparation method thereof - Google Patents
Citrus extracts solution, citrus electronics tobacco tar and preparation method thereof Download PDFInfo
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- CN109984374A CN109984374A CN201910410537.8A CN201910410537A CN109984374A CN 109984374 A CN109984374 A CN 109984374A CN 201910410537 A CN201910410537 A CN 201910410537A CN 109984374 A CN109984374 A CN 109984374A
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- citrus
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- tobacco tar
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/241—Extraction of specific substances
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
-
- A24F47/002—
-
- C—CHEMISTRY; METALLURGY
- C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
- C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
- C11B9/00—Essential oils; Perfumes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Wood Science & Technology (AREA)
- Organic Chemistry (AREA)
- Fats And Perfumes (AREA)
Abstract
The invention discloses a kind of citrus extracts solution, citrus electronics tobacco tar and preparation method thereof, the citrus extracts solution includes following components: citrus extracts and alcohols solvent, and the weight ratio of the citrus extracts and the alcohols solvent is 1:5~1:10；The alcohols solvent is at least one of ethyl alcohol, propylene glycol, glycerine.Citrus extracts solution in the present invention is rich in vitamin A, vitamin C, flavonoids, carotenoid, cumarin etc., i.e. its with it is anti-oxidant, consolidate connective tissue, promote collagen synthesis, participate in cholesterol metabolic, promote the health-care efficacies such as irony and calcareous absorption, and utilize citrus electronics tobacco tar made from citrus extracts solution also with health role, smoker is set to improve own bodies while giving up smoking or using cigarette substitute, and due to also containing fragrance ingredient in citrus extracts, there is citrus aroma using the electronics tobacco tar obtained by it.
Description
Technical field
A kind of produced the present invention relates to citrus extracts solution, using citrus extracts solution citrus electronics tobacco tar and its
Preparation method.
Background technique
Huge market prospects are presented as novel tobacco standard in electronic cigarette, main reason is that: on the one hand, electronics
Cigarette is capable of providing the consumption habit and satisfaction similar with conventional cigarette, and on the other hand, the hazard index of electronic cigarette is more fragrant than tradition
Cigarette substantially reduces.Relative to conventional cigarette, the less harmful of electronic cigarette is by incombustible mode to suck human body to be mist
Change liquid and non-burning pyrolysis product；Electronic cigarette, which neither burns, will not generate tar, carbon monoxide, carbon dioxide, methacrylaldehyde etc.
Harmful substance is nearly free from secondhand smoke harm, is considered as non-harmful smoking cessation product or substitute of tobacco, receives both at home and abroad
The highest attention of major tobacco enterprise and extensively research.
In recent years, Chinese tobacco control dynamics is constantly being reinforced, not only comprehensive smoking ban in public places, also increases and controls to smoking cessation
The supporting dynamics of smoke product exploitation, electronic cigarette as one of important smoking cessation tobacco control product obtain the active support of the government with
It promotes, technology development is irresistible.
Currently, the most common electronic cigarette tobacco tar is mixed according to a certain ratio by propylene glycol, glycerine and essence etc.
, this tobacco tar flavor component is only provided by essence, and fragrance is relatively simple, and is only the fragrance for imitating certain food, tobacco, no
The health-care effect for having some foods.
Summary of the invention
The present invention is directed to above-mentioned existing technological deficiency, provide a kind of citrus extracts solution, citrus electronics tobacco tar and its
Preparation method.
In order to solve the above-mentioned technical problems, the present invention provides a kind of citrus extracts solution, including following components: citrus
Extract and alcohols solvent, and the weight ratio of the citrus extracts and the alcohols solvent is 1:5~1:10；The alcohols is molten
Agent is at least one of ethyl alcohol, propylene glycol, glycerine.
Additionally provide a kind of citrus electronics tobacco tar produced using citrus extracts solution, including following parts by weight of component:
0-5 parts of nicotines and 80-90 parts of citrus extracts solution as described above.
Further, the citrus electronics tobacco tar further includes following parts by weight of component: 5-20 parts of flavors and fragrancess.
Further, the flavors and fragrances is grouped as by the group of following parts by weight: 1-10 parts of citrals, 1-10 parts of formic acid second
Ester, 10-20 parts of ethyl valerates, 20-40 parts of ethyl acetate, 20-40 parts of orange oils, 1-5 portions of wintergreens, 1-5 parts of tartaric acid.
Additionally provide a kind of preparation method of citrus electronics tobacco tar as described above, comprising the following steps:
S1, by weight ratio weigh citrus extracts solution, flavors and fragrances and nicotine respectively；
S2, flavors and fragrances and nicotine are called in into citrus extracts solution, be then sealed stirring, obtain citrus electricity
Sub- tobacco tar finished product.
It further, further include step S0 before step S1, make citrus extracts solution: ratio weighs by weight
Citrus extracts and alcohols solvent carry out constant temperature stirring after mixing, finally by filter residue is filtered to remove, to obtain citrus extracts molten
Liquid.
Further, in step S0, the temperature of constant temperature stirring is 40-50 DEG C, and the time of constant temperature stirring is 40-60min.
Further, in step S0, before filtration, first the solution stirred evenly is stood, and is cooled to room temperature.
It further, further include step S01 between step S0 and S1, make flavors and fragrances: ratio weighs by weight
Citral, Ethyl formate, ethyl valerate, ethyl acetate, orange oil, wintergreen, tartaric acid are mixed evenly to obtain the perfume (or spice)
Smart fragrance.
Further, in step S2, the time for sealing stirring is 2-3h.
Compared with prior art, the beneficial effects of the present invention are the vitamin A, the vitamins that are rich in citrus extracts
C, flavonoids, carotenoid, cumarin etc. can be dissolved in alcohol, and its with it is anti-oxidant, consolidate connective tissue, promote collagen
The effect of synthesis, participation cholesterol metabolic, promotion irony and calcareous absorption etc., citrus extracts are dissolved in alcoholic solution and are obtained
Citrus extracts solution have health-care efficacy；And also there is health care using citrus electronics tobacco tar made from citrus extracts solution
Effect makes smoker improve own bodies while giving up smoking or using cigarette substitute (i.e. electronic cigarette), and due to citrus
Also contain fragrance ingredient in extract, there is citrus aroma using the electronics tobacco tar obtained by it.
Specific embodiment
In order to more fully understand technology contents of the invention, below in conjunction with specific embodiment to technical side of the invention
Case is described further and illustrates.
The most critical design of the present invention is: importing into the electronic cigarette oil products that electronic cigarette uses has health-care efficacy
Vitamin A, vitamin C, flavonoids, carotenoid, cumarin etc..
In order to illustrate the feasibility of inventive concept, given in detail in conjunction with technology contents of the invention, the objects and the effects
It is bright.
A kind of citrus extracts solution, is made of citrus extracts and alcohols solvent, the citrus extracts and the alcohol
The weight ratio of class solvent is 1:5~1:10；The alcohols solvent is at least one of ethyl alcohol, propylene glycol, glycerine.In citrus
Vitamin A, vitamin C, flavonoids, carotenoid, cumarin for being rich in extract etc. can be dissolved in alcohol, and it is with antioxygen
The effect for changing, consolidating connective tissue, promoting collagen synthesis, participate in cholesterol metabolic, promote irony and calcareous absorption etc.,
Citrus extracts are dissolved in citrus extracts solution obtained in alcoholic solution with health-care efficacy.By efficacy validation, using pressing
According to the prepared citrus extracts solution of ratio of above-mentioned weight ratio (citrus extracts: alcohols solvent=1:5~1:10),
Health-care components vitamin A, vitamin C, flavonoids, carotenoid, cumarin etc. reach the amount played effectiveness.Citrus extracts
Object is usually utilized due to the factors such as processing, transport, easy-to-use with the product form of powdery.Raw material used in the present invention
Citrus extracts are powdery, so needing to dissolve it using alcoholic solution, convenient for utilizing, while being also convenient for removing molten insoluble in alcohol
The impurity of liquid.Vitamin A, vitamin C, flavonoids, carotenoid, cumarin in citrus extracts etc. and itself contained by
Some aromatic odor ingredients have good solubility, and ethyl alcohol, the third two in the alcohol reagents such as ethyl alcohol, propylene glycol, glycerine
The common basis of alcohol, glycerine as electronics tobacco tar, safety have been proved, and can be selected according to demand therein
One or more alcoholic solutions dissolve citrus extracts, utilize the mandarin orange that the alcohol reagents such as ethyl alcohol, propylene glycol, glycerine are made
Tangerine extract solution is convenient in the middle of the preparation for directly using electronics tobacco tar.
Specifically, the extracting method of citrus extracts: full fruit juicing after citrus is cleaned up；The fruit juice squeezed is filtered
It is concentrated later, it is 20%~50% by the concentration of juices to solid content that thickening temperature, which is controlled at 40~60 DEG C,
Afterwards, it is spray-dried, obtains the citrus extracts of dry powder-shaped.
A kind of citrus electronics tobacco tar, including following parts by weight of component: 0-5 parts of nicotine and 80-90 are part as described above
Citrus extracts solution；Since citrus extracts solution has health-care efficacy, the electricity of citrus made from citrus extracts solution is utilized
Sub- tobacco tar is also with health role, and smoker is made to improve itself while giving up smoking or using cigarette substitute (i.e. electronic cigarette)
Body, and due to also containing other fragrance ingredients in citrus extracts, utilize electronics tobacco tar obtained by citrus extracts solution
With citrus aroma；According to the tobacco tar product of different component nicotines of the smoking cessation demand selection production comprising aforementioned proportion, make to guard against
Cigarette person can gradually give up smoking, and reduce smoking cessation process bring pain.
Further, which further includes following parts by weight of component: 5-20 parts of flavors and fragrances；Citrus extracts
The citrus aroma substance carried in object solution is less, needs to add flavors and fragrances and is supplemented, makes the smell of product entirety more
It is strong.
Further, the flavors and fragrances is grouped as by the group of following parts by weight: 1-10 parts of citrals, 1-10 parts of formic acid second
Ester, 10-20 parts of ethyl valerates, 20-40 parts of ethyl acetate, 20-40 parts of orange oils, 1-5 portions of wintergreens, 1-5 parts of tartaric acid.Essence
Fragrance is cooperated by multicomponent, and the proportion of each component is to combine the warp of citrus aroma ingredient contained in citrus extracts solution
Repeated multiple times experimental study is crossed to obtain, it is resulting after calling in citrus extracts solution according to the flavors and fragrances of this proportion allotment
Electronic cigarette incense oil taste is more mellow and full full, rich in level.
A kind of preparation method of citrus electronics tobacco tar as described above, comprising the following steps:
S1, by weight ratio weigh citrus extracts solution, flavors and fragrances and nicotine respectively；
S2, flavors and fragrances and nicotine are called in into citrus extracts solution, be then sealed stirring, obtain citrus electricity
Sub- tobacco tar finished product；By stirring, so that each ingredient is uniformly mixed, and it is stirred under sealing, prevents from polluting.
It further, further include step S0 before step S1, make citrus extracts solution: ratio weighs by weight
Citrus extracts and alcohols solvent carry out constant temperature stirring after mixing, finally by filter residue is filtered to remove, to obtain citrus extracts molten
Liquid；Citrus extracts are dissolved sufficiently by constant temperature stirring.
Further, in step S0, the temperature of constant temperature stirring is 40-50 DEG C, and the time of constant temperature stirring is 40-60min；It is logical
Temperature and time when control stirring is crossed, while guaranteeing that solids (citrus extracts) accelerate dissolution, is reduced because of temperature mistake
Height causes alcoholic solution volatilization loss.
Further, in step S0, before filtration, first the solution stirred evenly is stood, and is cooled to room temperature；It is molten
It is stood before liquid filtering, makes precipitation of solid material, sufficiently undissolved filter residue can be filtered out, make filter effect more preferably, and by
Overall liquid surface area is increased in filter process, if temperature is excessively high, evaporation rate is too fast, then it will increase the investment of production,
So filtering should carry out after solution temperature is cooled to room temperature.
It further, further include step S01 between step S0 and S1, make flavors and fragrances: ratio weighs by weight
Citral, Ethyl formate, ethyl valerate, ethyl acetate, orange oil, wintergreen, tartaric acid are mixed evenly to obtain the perfume (or spice)
Smart fragrance；The additive amount of each component in flavors and fragrances is less, is added if directly weighed respectively, and deviation is larger, thus first
Each component in flavors and fragrances is deployed, then flavors and fragrances is called in citrus extracts solution again according to demand, is made
It obtains each component actual content in electronic cigarette oil products to be not much different with expected content, guarantee between the product of each batch production not
It will appear relatively large deviation.
Further, in step S2, the time for sealing stirring is 2-3h, and being sufficiently stirred is sufficiently mixed each ingredient uniformly.
In order to illustrate the feasibility of present inventive concept, it is explained in conjunction with following specific embodiments:
Embodiment 1:
A kind of preparation method of citrus electronics tobacco tar, comprising the following steps:
1) making step of citrus extracts solution: according to weight ratio citrus extracts: ethyl alcohol: propylene glycol: glycerine=
The ratio of 1:1:3:5 weighs citrus extracts, ethyl alcohol, propylene glycol and glycerine (the i.e. weight of citrus extracts and alcohols solvent
Than stirring 40min under the conditions of 40 DEG C after mixing, then being stood and be cooled to room temperature for 1:9), filtered out finally by crossing
Filter residue is gone to obtain citrus extracts solution.
2) making step of flavors and fragrances: by 5 parts by weight of lemon aldehyde, 1 parts by weight Ethyl formate, 10 parts by weight valeric acid second
Ester, 40 weight part of ethylacetate, 20 parts by weight orange oils, 1 parts by weight wintergreen, 1 parts by weight tartaric acid etc. are mixed evenly
Obtain flavors and fragrances.
3) making step of finished product: calling in the flavors and fragrances of 10 parts by weight into the citrus extracts solution of 80 parts by weight,
Then it is sealed stirring 2 hours, obtains citrus electronics tobacco tar finished product.
Embodiment 2:
A kind of preparation method of citrus electronics tobacco tar, comprising the following steps:
1) making step of citrus extracts solution: according to weight ratio citrus extracts: propylene glycol: glycerine=1:4:5
Ratio weigh citrus extracts, propylene glycol and glycerine (i.e. the weight ratio of citrus extracts and alcohols solvent is 1:9), mixing
60min is stirred under the conditions of 50 DEG C afterwards, is then stood and is cooled to room temperature, obtains citrus finally by filter residue is filtered to remove
Extract solution.
2) making step of flavors and fragrances: by 5 parts by weight of lemon aldehyde, 10 parts by weight Ethyl formates, 20 parts by weight valeric acid second
Ester, 40 weight part of ethylacetate, 20 parts by weight orange oils, 5 parts by weight wintergreens, 5 parts by weight tartaric acid etc. are mixed evenly
Obtain flavors and fragrances.
3) making step of finished product: called in into the citrus extracts solution of 90 parts by weight 20 parts by weight flavors and fragrances and
Then the nicotine of 5 parts by weight is sealed stirring 3 hours, obtains citrus electronics tobacco tar finished product.
Embodiment 3:
A kind of preparation method of citrus electronics tobacco tar, comprising the following steps:
1) making step of citrus extracts solution: according to weight ratio citrus extracts: propylene glycol=1:8 ratio weighs
Citrus extracts and propylene glycol stir 50min under the conditions of 45 DEG C after mixing, are then stood and be cooled to room temperature, finally
Filter residue is removed by filtration and obtains citrus extracts solution.
2) making step of flavors and fragrances: by 2 parts by weight of lemon aldehyde, 5 parts by weight Ethyl formates, 20 parts by weight valeric acid second
Ester, 30 weight part of ethylacetate, 25 parts by weight orange oils, 2 parts by weight wintergreens, 2 parts by weight tartaric acid etc. are mixed evenly
Obtain the flavors and fragrances.
3) making step of finished product: called in into the citrus extracts solution of 85 parts by weight 10 parts by weight flavors and fragrances and
Then the nicotine of 3 parts by weight is sealed stirring 2.5 hours, obtains citrus electronics tobacco tar finished product.
Embodiment 4:
A kind of preparation method of citrus electronics tobacco tar, comprising the following steps:
1) making step of citrus extracts solution: according to weight ratio citrus extracts: ethyl alcohol: glycerine=1:1:7
Ratio weighs citrus extracts, ethyl alcohol and glycerine (i.e. the weight ratio of citrus extracts and alcohols solvent is 1:8), after mixing
45min is stirred under the conditions of 42 DEG C, is then stood and is cooled to room temperature, and obtains citrus extraction finally by filter residue is filtered to remove
Object solution.
2) making step of flavors and fragrances: by 10 parts by weight of lemon aldehyde, 8 parts by weight Ethyl formates, 15 parts by weight valeric acid second
Ester, 35 weight part of ethylacetate, 15 parts by weight orange oils, 3 parts by weight wintergreens, 1 parts by weight tartaric acid etc. are mixed evenly
Obtain flavors and fragrances.
3) making step of finished product: called in into the citrus extracts solution of 88 parts by weight 15 parts by weight flavors and fragrances and
Then the nicotine of 2 parts by weight is sealed stirring 3 hours, obtains citrus electronics tobacco tar finished product.
Extraction is tested according to above-described embodiment product produced: (20/20 DEG C) of its relative density is 1.1127, folding
(20 DEG C) of optical index are 1.4409, and it is non-volatile state under normal storage conditions that boiling point (101.3kPa), which is 197.5 DEG C,；Root
The evaluation of color shape, fragrance, fragrance is carried out according to shelf-life qualification test, the shelf-life of product was up to 3 years or more；I.e. according to the present invention
It is formulated under the electronics tobacco tar normal temperature and pressure conditions of production and is easy to save, stability is splendid, long shelf-life, and when use is easy to be atomized.
In conclusion a kind of citrus extracts solution provided by the invention, is rich in vitamin A, vitamin C, flavonoids, class
Carrotene, cumarin etc., i.e., its with it is anti-oxidant, consolidate connective tissue, promote collagen synthesis, participate in cholesterol generation
It thanks, promote the health-care efficacies such as irony and calcareous absorption；Also have using citrus electronics tobacco tar made from citrus extracts solution
Health-care effect makes smoker improve own bodies while giving up smoking or using cigarette substitute；And due to citrus extracts
In also contain other fragrance ingredients, there is citrus aroma using electronics tobacco tar obtained by citrus extracts solution, and by adding
Add flavors and fragrances to supplement fragrance ingredient contained in citrus extracts, make the smell of product entirety it is more strong, it is mellow and full,
It is full；Production process makes to be uniformly mixed by stirring, and increases solution rate by temperature control in stirring, and reduce alcohol solution
Impurity is also removed by filtration in evaporation rate.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair
Equivalent process transformation made by bright description is applied directly or indirectly in other relevant technical fields, and similarly wraps
It includes in scope of patent protection of the invention.At the same time, for those skilled in the art, according to an embodiment of the present invention,
There will be changes in specific embodiment and application range, in conclusion the content of the present specification should not be construed as to this
The limitation of invention.
Claims (10)
1. a kind of citrus extracts solution, which is characterized in that including following components: citrus extracts and alcohols solvent, and it is described
The weight ratio of citrus extracts and the alcohols solvent is 1:5~1:10；The alcohols solvent is ethyl alcohol, propylene glycol, glycerine
At least one of.
2. a kind of citrus electronics tobacco tar, which is characterized in that including following parts by weight of component: 0-5 parts of nicotines and 80-90 parts such as power
Benefit require 1 described in citrus extracts solution.
3. citrus electronics tobacco tar as claimed in claim 2, which is characterized in that further include following parts by weight of component: 5-20 parts of essence
Fragrance.
4. citrus electronics tobacco tar as claimed in claim 3, which is characterized in that the flavors and fragrances is grouped by the group of following parts by weight
At: 1-10 parts of citrals, 1-10 parts of Ethyl formates, 10-20 parts of ethyl valerates, 20-40 parts of ethyl acetate, 20-40 parts of orange oils,
1-5 portions of wintergreens, 1-5 parts of tartaric acid.
5. a kind of preparation method of pineapple electronics tobacco tar as claimed in claim 4, which comprises the following steps:
S1, by weight ratio weigh pineapple extract solution, flavors and fragrances and nicotine respectively；
S2, flavors and fragrances and nicotine are called in into citrus extracts solution, be then sealed stirring, obtain citrus electronic cigarette
Oily finished product.
6. the preparation method of citrus electronics tobacco tar as claimed in claim 5, which is characterized in that before step S1 further include step
S0, make citrus extracts solution: ratio weighs citrus extracts and alcohols solvent by weight, and constant temperature is carried out after mixing and is stirred
It mixes, obtains citrus extracts solution finally by filter residue is filtered to remove.
7. the preparation method of citrus electronics tobacco tar as claimed in claim 6, which is characterized in that in step S0, the temperature of constant temperature stirring
Degree is 40-50 DEG C, and the time of constant temperature stirring is 40-60min.
8. the preparation method of citrus electronics tobacco tar as claimed in claim 7, which is characterized in that in step S0, before filtration, first will
The solution stirred evenly is stood, and is cooled to room temperature.
9. the preparation method of citrus electronics tobacco tar as claimed in claim 6, which is characterized in that further include between step S0 and S1
Step S01, make flavors and fragrances: ratio weighs citral, Ethyl formate, ethyl valerate, ethyl acetate, orange peel by weight
Oil, wintergreen, tartaric acid are mixed evenly to obtain the flavors and fragrances.
10. the preparation method of citrus electronics tobacco tar as claimed in claim 5, which is characterized in that in step S2, seal stirring when
Between be 2-3h.
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Application publication date: 20190709 |