CN109744584A - Blueberry extract solution, blueberry electronics tobacco tar and preparation method thereof - Google Patents

Blueberry extract solution, blueberry electronics tobacco tar and preparation method thereof Download PDF

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Publication number
CN109744584A
CN109744584A CN201910165342.1A CN201910165342A CN109744584A CN 109744584 A CN109744584 A CN 109744584A CN 201910165342 A CN201910165342 A CN 201910165342A CN 109744584 A CN109744584 A CN 109744584A
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China
Prior art keywords
blueberry
weight
tobacco tar
parts
blueberry extract
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CN201910165342.1A
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Inventor
汪泽其
王强彬
易忠斌
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Pt De (shenzhen) Technology Co Ltd
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Pt De (shenzhen) Technology Co Ltd
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Priority to CN201910165342.1A priority Critical patent/CN109744584A/en
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  • Medicines Containing Plant Substances (AREA)

Abstract

The present invention provides a kind of blueberry extract solution, are made of blueberry extract and alcohols solvent, and the weight ratio of the blueberry extract and the alcohols solvent is 1:5~1:10;The alcohols solvent is at least one of ethyl alcohol, propylene glycol, glycerine.A kind of blueberry electronics tobacco tar, component include the nicotine of 0-5 parts by weight and the blueberry extract solution of 80-90 parts by weight.Blueberry extract solution, containing blueberry anthocyanin, i.e., it is with anti-radiation, protection eyesight, the permeability for adjusting capillary, anti-oxidant, the internal inflammation of removing, anticancer, strengthen immunity and anti-aging etc. health-care efficacy.It is also with health role using blueberry electronics tobacco tar made from blueberry extract solution, so that smoker is improved own bodies while giving up smoking or using cigarette substitute.Again since there is blueberry fragrance using electronics tobacco tar obtained by blueberry extract solution containing other fragrance ingredients are also contained in blueberry extract.

Description

Blueberry extract solution, blueberry electronics tobacco tar and preparation method thereof
Technical field
The present invention relates to a kind of blueberry extract solution, a kind of blueberry electronics tobacco tar produced using blueberry extract solution And preparation method thereof.
Background technique
Huge market prospects, main cause is presented as one of new tobacco products form in electronic cigarette Be: on the one hand, electronic cigarette is capable of providing the consumption habit and satisfaction similar with conventional cigarette, on the other hand, electronic cigarette Hazard index is substantially reduced than conventional cigarette.Relative to conventional cigarette, the less harmful of electronic cigarette is made by incombustible mode Human body must be sucked is atomized liquid and non-burning pyrolysis product.Electronic cigarette, which neither burns, will not generate tar, carbon monoxide, two The harmful substances such as carbonoxide methacrylaldehyde are nearly free from secondhand smoke harm, are considered as non-harmful smoking cessation product or tobacco substitute Product receive the highest attention and research extensively of domestic and international major tobacco enterprise.
In recent years, Chinese tobacco control dynamics is also constantly being reinforced, and not only comprehensive smoking ban in public places, also increases to smoking cessation The supporting dynamics of tobacco control product development.
Currently, the most common electronic cigarette tobacco tar is mixed according to a certain ratio by propylene glycol, glycerine and essence etc. , this tobacco tar flavor component is only provided by essence, and fragrance is relatively simple, and is only the fragrance for imitating certain food, tobacco, Do not have the health-care effect of some foods.
Summary of the invention
The technical problems to be solved by the present invention are: providing the product with health-care efficacy.
In order to solve the above-mentioned technical problem, the technical solution adopted by the present invention are as follows:
A kind of blueberry extract solution, is made of blueberry extract and alcohols solvent, the blueberry extract and the alcohol The weight ratio of class solvent is 1:5~1:10;The alcohols solvent is at least one of ethyl alcohol, propylene glycol, glycerine.
A kind of blueberry electronics tobacco tar, component include that the nicotine of 0-5 parts by weight and the blueberry of 80-90 parts by weight mention Take object solution.
Further, component further includes the flavors and fragrances of 5-20 parts by weight.
Further, the flavors and fragrances is by 1-5 parts by weight methyl anthranilate, 1-5 parts by weight irisone, 10-40 Weight parts Benzyl Acetate, 20-40 parts by weight maltol, 10-30 parts by weight vanillic aldehyde are constituted.
A kind of preparation method of blueberry electronics tobacco tar, including finished product making step: by weighing blueberry extract needed for technique Solution, flavors and fragrances and nicotine call in flavors and fragrances and nicotine into blueberry extract solution, are then sealed and stir It mixes, obtains blueberry electronics tobacco tar finished product.
Further, before finished product making step, including blueberry extract solution making step: by weighing indigo plant needed for technique Certain kind of berries extract and alcohols solvent carry out constant temperature stirring, obtain blueberry extract solution finally by filter residue is filtered to remove after mixing.
Further, before finished product making step, including flavors and fragrances making step: by weighing adjacent aminobenzene needed for technique Methyl formate, irisone, benzyl acetate, maltol, vanillic aldehyde etc. are mixed evenly to obtain the flavors and fragrances.
Further, the sealing mixing time is 2-3 hours.
Further, before the filtering, the solution stirred evenly should be stood, and be cooled to room temperature;It is described Constant temperature whipping temp is 40-50 DEG C, and the constant temperature mixing time is 40-60min.
The beneficial effects of the present invention are: contain blueberry anthocyanin in blueberry extract, blueberry anthocyanin can be dissolved in alcohol, and It is with anti-radiation, protection eyesight, the permeability for adjusting capillary, anti-oxidant, the internal inflammation of removing, anticancer, strengthen immunity With the effect of anti-aging etc., blueberry extract is dissolved in blueberry extract solution obtained in alcoholic solution with health-care efficacy. It is also with health role using blueberry electronics tobacco tar made from blueberry extract solution, so that smoker is being given up smoking or use cigarette Improve own bodies while substitute.Due to containing, there are also other fragrance ingredients in blueberry extract again, obtained by it Electronics tobacco tar have blueberry fragrance.
Specific embodiment
The most critical design of the present invention is: importing the blueberry anthocyanin with health-care efficacy into product.
In order to illustrate the feasibility of design, it is explained in detail in conjunction with technology contents of the invention, the objects and the effects.
A kind of blueberry extract solution, is made of blueberry extract and alcohols solvent, the blueberry extract and the alcohol The weight ratio of class solvent is 1:5~1:10;The alcohols solvent is at least one of ethyl alcohol, propylene glycol, glycerine.Blueberry mentions Take and contain blueberry anthocyanin in object, blueberry anthocyanin can be dissolved in alcohol, and its with it is anti-radiation, protection eyesight, adjust capillary The effect of permeability, anti-oxidant, the internal inflammation of removing, anticancer, strengthen immunity and anti-aging etc., blueberry extract is dissolved in Blueberry extract solution obtained in alcoholic solution has health-care efficacy.By efficacy validation, extracted using according to weight ratio blueberry Object: the prepared blueberry extract solution of alcohols solvent=1:5~1:10 ratio, health-care components blueberry anthocyanin reach The amount played effectiveness.Blueberry extract is usually sharp with the product form of powdery due to the factors such as processing, transport, easy-to-use With.Raw material blueberry extract used in the present invention is powdery, so needing to dissolve it using alcoholic solution, convenient for utilizing, together When be also convenient for removing impurity insoluble in alcoholic solution.Blueberry anthocyanin in blueberry extract and the aroma contained by itself Taste ingredient has good solubility in the alcohol reagents such as ethyl alcohol, propylene glycol, glycerine, and ethyl alcohol, propylene glycol, glycerine are made For the common basis of electronics tobacco tar, safety has been proved.It can select according to demand one such or a variety of Alcoholic solution dissolves blueberry extract.It is molten using the made blueberry extract of the alcohol reagents such as ethyl alcohol, propylene glycol, glycerine Liquid is convenient in the middle of the preparation for directly using electronics tobacco tar.
A kind of blueberry electronics tobacco tar, component include that the nicotine of 0-5 parts by weight and the blueberry of 80-90 parts by weight mention Take object solution.Since blueberry extract solution has health-care efficacy, blueberry electronics tobacco tar made from blueberry extract solution is utilized Also with health role, so that smoker is improved own bodies while giving up smoking or using cigarette substitute.Again due to containing Also contain other fragrance ingredients in blueberry extract, there is blueberry virtue using electronics tobacco tar obtained by blueberry extract solution It is fragrant.The tobacco tar product that different component nicotines are produced according to smoking cessation demand selection, enables smokers gradually to give up smoking, reduces smoking cessation Process bring pain.
Further, component further includes the flavors and fragrances of 5-20 parts by weight.The blueberry carried in blueberry extract solution Aromatic substance is less, needs to add flavors and fragrances and is supplemented, and keeps the smell of product entirety more strong.
Further, the flavors and fragrances is by 1-5 parts by weight methyl anthranilate, 1-5 parts by weight irisone, 10-40 Weight parts Benzyl Acetate, 20-40 parts by weight maltol, 10-30 parts by weight vanillic aldehyde are constituted.Flavors and fragrances passes through multiple groups Distribution is closed, and the proportion of each component is that blueberry fragrance ingredient contained in blueberry extract solution is combined to grind by countless experiments Study carefully to obtain.According to the flavors and fragrances of this proportion allotment, after calling in blueberry extract solution, resulting electronic cigarette incense oil taste is more It is mellow and full full, rich in level.
A kind of preparation method of blueberry electronics tobacco tar, including finished product making step: by weighing blueberry extract needed for technique Solution, flavors and fragrances and nicotine call in flavors and fragrances and nicotine into blueberry extract solution, are then sealed and stir It mixes, obtains blueberry electronics tobacco tar finished product.By stirring, so that each ingredient is uniformly mixed.It should be sealed in whipping process, prevent dirt Dye.
Further, before finished product making step, including blueberry extract solution making step: by weighing indigo plant needed for technique Certain kind of berries extract and alcohols solvent carry out constant temperature stirring, obtain blueberry extract solution finally by filter residue is filtered to remove after mixing. Constant temperature stirring, dissolves blueberry extract sufficiently.By temperature control, while guaranteeing that solids accelerates dissolution, reduce because of temperature It is excessively high to cause alcoholic solution volatilization loss.
Further, before finished product making step, including flavors and fragrances making step: by weighing adjacent aminobenzene needed for technique Methyl formate, irisone, benzyl acetate, maltol, vanillic aldehyde etc. are mixed evenly to obtain the flavors and fragrances.Essence The additive amount of each component in fragrance is less, is added if directly weighed respectively, and deviation is larger.First each component is adjusted Match, then according to demand again call in flavors and fragrances in blueberry extract solution, so that each component actual content and pre- in product Phase content is not much different, and guarantees that between the product of each batch production be not in relatively large deviation.
Further, the sealing mixing time is 2-3 hours.Being sufficiently stirred is sufficiently mixed each ingredient uniformly.
Further, before the filtering, the solution stirred evenly should be stood, and be cooled to room temperature;It is described Constant temperature whipping temp is 40-50 DEG C, and the constant temperature mixing time is 40-60min.It is stood before solution filtering, solids is heavy It forms sediment, makes filter effect more preferably.Since filter process increases overall liquid surface area, if temperature is excessively high, evaporation rate is too fast, It then will increase the investment of production, so filtering should carry out after temperature is cooled to room temperature.
In order to illustrate the feasibility of design, it is explained in conjunction with following specific embodiments:
Embodiment one:
A kind of preparation method of blueberry electronics tobacco tar, comprising steps of
One, blueberry extract solution making step: according to weight ratio blueberry extract: ethyl alcohol: propylene glycol: glycerine=1: The ratio of 1:3:5 weighs blueberry extract, ethyl alcohol, propylene glycol and glycerine, stirs 40min under the conditions of 40 DEG C after mixing, so After stood and be cooled to room temperature, obtain blueberry extract solution finally by filter residue is filtered to remove.
Two, flavors and fragrances making step: by 1 parts by weight methyl anthranilate, 1 parts by weight irisone, 10 weight Part benzyl acetate, 20 parts by weight maltols, 10 parts by weight vanillic aldehydes etc. are mixed evenly to obtain the flavors and fragrances.
Three, finished product making step: the flavors and fragrances of 5 parts by weight is called in into the blueberry extract solution of 80 parts by weight, so After be sealed stirring 2 hours, obtain blueberry electronics tobacco tar finished product.
Embodiment two:
A kind of preparation method of blueberry electronics tobacco tar, comprising steps of
One, blueberry extract solution making step: according to weight ratio blueberry extract: propylene glycol: glycerine=1:4:5 Ratio weighs blueberry extract, propylene glycol and glycerine, stirs 60min under the conditions of 50 DEG C after mixing, is then stood simultaneously It is cooled to room temperature, obtains blueberry extract solution finally by filter residue is filtered to remove.
Two, flavors and fragrances making step: by 5 parts by weight methyl anthranilates, 5 parts by weight irisones, 40 weight Part benzyl acetate, 40 parts by weight maltols, 30 parts by weight vanillic aldehydes etc. are mixed evenly to obtain the flavors and fragrances.
Three, the flavors and fragrances and 5 of 20 parts by weight finished product making step: is called in into the blueberry extract solution of 90 parts by weight Then the nicotine of parts by weight is sealed stirring 3 hours, obtains blueberry electronics tobacco tar finished product.
Embodiment three:
A kind of preparation method of blueberry electronics tobacco tar, comprising steps of
One, blueberry extract solution making step: according to weight ratio blueberry extract: propylene glycol=1:8 ratio weighs Blueberry extract and propylene glycol stir 50min under the conditions of 45 DEG C after mixing, are then stood and be cooled to room temperature, finally Filter residue is removed by filtration and obtains blueberry extract solution.
Two, flavors and fragrances making step: by 2 parts by weight methyl anthranilates, 2 parts by weight irisones, 20 weight Part benzyl acetate, 25 parts by weight maltols, 15 parts by weight vanillic aldehydes etc. are mixed evenly to obtain the flavors and fragrances.
Three, the flavors and fragrances and 3 of 10 parts by weight finished product making step: is called in into the blueberry extract solution of 85 parts by weight Then the nicotine of parts by weight is sealed stirring 2.5 hours, obtains blueberry electronics tobacco tar finished product.
Example IV:
A kind of preparation method of blueberry electronics tobacco tar, comprising steps of
One, blueberry extract solution making step: according to weight ratio blueberry extract: ethyl alcohol: glycerine=1:1:7 Ratio weighs blueberry extract, ethyl alcohol and glycerine, stirs 45min under the conditions of 42 DEG C after mixing, then carry out stand and it is cold But to room temperature, blueberry extract solution is obtained finally by filter residue is filtered to remove.
Two, flavors and fragrances making step: by 3 parts by weight methyl anthranilates, 3 parts by weight irisones, 30 weight Part benzyl acetate, 35 parts by weight maltols, 25 parts by weight vanillic aldehydes etc. are mixed evenly to obtain the flavors and fragrances.
Three, the flavors and fragrances and 2 of 15 parts by weight finished product making step: is called in into the blueberry extract solution of 88 parts by weight Then the nicotine of parts by weight is sealed stirring 3 hours, obtains blueberry electronics tobacco tar finished product.
Extraction is tested according to above-described embodiment product produced: (20/20 DEG C) of its relative density is 1.1149, (20 DEG C) of refraction index are 1.4457, and it is non-volatile state under normal storage conditions that boiling point (101.3kPa), which is 197.3 DEG C,. The evaluation of color shape, fragrance, fragrance is carried out according to shelf-life qualification test, the shelf-life of product was up to 3 years or more.I.e. according to this hair It is easy to save under the electronics tobacco tar normal temperature and pressure conditions of bright formula production, stability is splendid, long shelf-life, and when use is easy to mist Change.
In conclusion a kind of blueberry extract solution provided by the invention, containing blueberry anthocyanin, i.e., it is with anti-spoke Permeability, anti-oxidant, the internal inflammation of removing, anticancer, strengthen immunity and the anti-aging penetrating, protect eyesight, adjusting capillary Etc. health-care efficacy.It is also with health role using blueberry electronics tobacco tar made from blueberry extract solution, guarding against smoker Cigarette or using cigarette substitute while, improve own bodies.Again due to containing in blueberry extract also containing other fragrance at Point, there is blueberry fragrance using electronics tobacco tar obtained by blueberry extract solution.It needs to add flavors and fragrances to extract blueberry Fragrance ingredient contained in object is supplemented, and keeps the smell of product entirety more strong, mellow and full, full.Production process is by stirring Mixing makes to be uniformly mixed, and impurity is removed by filtration.Increase solution rate by temperature control, reduces alcohol solution evaporation rate.
The above description is only an embodiment of the present invention, is not intended to limit the scope of the invention, all to utilize this hair Equivalent process transformation made by bright description is applied directly or indirectly in other relevant technical fields, and similarly wraps It includes in scope of patent protection of the invention.

Claims (9)

1. a kind of blueberry extract solution, which is characterized in that be made of blueberry extract and alcohols solvent, the blueberry extract Weight ratio with the alcohols solvent is 1:5~1:10;The alcohols solvent is ethyl alcohol, propylene glycol, at least one in glycerine Kind.
2. a kind of blueberry electronics tobacco tar, which is characterized in that its component includes the nicotine and 80-90 parts by weight of 0-5 parts by weight Blueberry extract solution as described in claim 1.
3. blueberry electronics tobacco tar as claimed in claim 2, which is characterized in that its component further includes that the essence of 5-20 parts by weight is fragrant Material.
4. blueberry electronics tobacco tar as claimed in claim 3, which is characterized in that the flavors and fragrances is by 1-5 parts by weight neighbour's aminobenzene Methyl formate, 1-5 parts by weight irisone, 10-40 Weight parts Benzyl Acetate, 20-40 parts by weight maltol, 10-30 parts by weight Vanillic aldehyde is constituted.
5. a kind of preparation method of blueberry electronics tobacco tar, which is characterized in that including finished product making step: by weighing indigo plant needed for technique Certain kind of berries extract solution, flavors and fragrances and nicotine call in flavors and fragrances and nicotine into blueberry extract solution, then carry out Sealing stirring, obtains blueberry electronics tobacco tar finished product.
6. the preparation method of blueberry electronics tobacco tar as claimed in claim 5, which is characterized in that before finished product making step, including Blueberry extract solution making step: by blueberry extract and alcohols solvent is weighed needed for technique, carrying out constant temperature stirring after mixing, Blueberry extract solution is obtained finally by filter residue is filtered to remove.
7. the preparation method of blueberry electronics tobacco tar as claimed in claim 6, which is characterized in that before finished product making step, including Flavors and fragrances making step: by weighing methyl anthranilate, irisone, benzyl acetate, maltol, chinese cymbidium needed for technique Element etc. is mixed evenly to obtain the flavors and fragrances.
8. the preparation method of blueberry electronics tobacco tar as claimed in claim 7, which is characterized in that the sealing mixing time is 2-3 Hour.
9. the preparation method of blueberry electronics tobacco tar as claimed in claim 8, which is characterized in that before the filtering, should will stir It mixes uniform solution to be stood, and is cooled to room temperature;The constant temperature whipping temp is 40-50 DEG C, the constant temperature mixing time For 40-60min.
CN201910165342.1A 2019-03-05 2019-03-05 Blueberry extract solution, blueberry electronics tobacco tar and preparation method thereof Pending CN109744584A (en)

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Cited By (5)

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CN109984374A (en) * 2019-05-16 2019-07-09 铂德(深圳)科技有限公司 Citrus extracts solution, citrus electronics tobacco tar and preparation method thereof
CN109984372A (en) * 2019-05-16 2019-07-09 铂德(深圳)科技有限公司 Mango extract solution, mango electronics tobacco tar and preparation method thereof
CN109984373A (en) * 2019-05-16 2019-07-09 铂德(深圳)科技有限公司 Pear extract solution, pear electronics tobacco tar and preparation method thereof
CN110959903A (en) * 2019-09-12 2020-04-07 深圳雾芯科技有限公司 Flavor composition and electronic cigarette liquid containing same
CN113974205A (en) * 2021-10-26 2022-01-28 河南中烟工业有限责任公司 Blueberry essence, blueberry extract, and preparation methods and applications thereof

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN109984374A (en) * 2019-05-16 2019-07-09 铂德(深圳)科技有限公司 Citrus extracts solution, citrus electronics tobacco tar and preparation method thereof
CN109984372A (en) * 2019-05-16 2019-07-09 铂德(深圳)科技有限公司 Mango extract solution, mango electronics tobacco tar and preparation method thereof
CN109984373A (en) * 2019-05-16 2019-07-09 铂德(深圳)科技有限公司 Pear extract solution, pear electronics tobacco tar and preparation method thereof
CN110959903A (en) * 2019-09-12 2020-04-07 深圳雾芯科技有限公司 Flavor composition and electronic cigarette liquid containing same
CN113974205A (en) * 2021-10-26 2022-01-28 河南中烟工业有限责任公司 Blueberry essence, blueberry extract, and preparation methods and applications thereof

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Application publication date: 20190514