CN111387541A - Watermelon extract solution, watermelon electronic cigarette oil and preparation method thereof - Google Patents
Watermelon extract solution, watermelon electronic cigarette oil and preparation method thereof Download PDFInfo
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- CN111387541A CN111387541A CN202010361797.3A CN202010361797A CN111387541A CN 111387541 A CN111387541 A CN 111387541A CN 202010361797 A CN202010361797 A CN 202010361797A CN 111387541 A CN111387541 A CN 111387541A
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- watermelon
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- extract solution
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
- A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
Abstract
The invention discloses a watermelon extract solution, watermelon electronic cigarette oil and a preparation method thereof, wherein the watermelon extract solution comprises the following components: the watermelon extract and the alcohol solvent are mixed according to the weight ratio of 1: 5-1: 10; the alcohol solvent is at least one of ethanol, propylene glycol and glycerol. The watermelon extract solution of the invention is rich in malic acid, proteinic amino acid, lycopene, vitamin C and various mineral substances, etc., namely, the watermelon extract solution has the health care efficacies of clearing away summer-heat, quenching thirst, moistening intestines, promoting urination, etc., and the watermelon electronic cigarette oil prepared by the watermelon extract solution also has the health care function, so that smokers can improve the body of the smokers while quitting smoking or using cigarette substitutes, and the watermelon extract also contains aromatic components, so the electronic cigarette oil prepared by the watermelon extract solution has watermelon aroma.
Description
Technical Field
The invention relates to a watermelon extract solution, watermelon electronic cigarette oil prepared from the watermelon extract solution and a preparation method thereof.
Background
Electronic cigarettes, as a novel tobacco system, present a huge market prospect, whose main reasons lie in: on the one hand, electronic cigarettes can provide similar consumption habits and satisfaction as traditional cigarettes, and on the other hand, the hazard index of electronic cigarettes is greatly reduced compared to traditional cigarettes. Compared with the traditional cigarette, the low harm of the electronic cigarette is that atomized liquid is inhaled into a human body instead of combustion cracking products in a non-combustion mode; the electronic cigarette does not burn, does not generate harmful substances such as tar, carbon monoxide, carbon dioxide, acrolein and the like, hardly generates second-hand smoke harm, is regarded as a nuisanceless smoking cessation product or a tobacco substitute, and is highly concerned and widely researched by various large tobacco enterprises at home and abroad.
In recent years, Chinese smoking control is continuously strengthened, not only is smoking prohibited in public places comprehensively, but also the supporting force for the development of smoking cessation and control products is increased, and the electronic cigarette serving as one important smoking cessation and control product is greatly supported and popularized by the government, so that the technical development is not blocked.
At present, the most common electronic cigarette tobacco tar is prepared by mixing propylene glycol, essence and the like according to a certain proportion, the flavor components of the tobacco tar are provided by the essence, the flavor is single, the tobacco tar only simulates the flavor of certain food and tobacco, and the tobacco tar does not have the health-care effect of some food.
Disclosure of Invention
Aiming at the defects of the prior art, the invention provides a watermelon extract solution, watermelon electronic cigarette oil and a preparation method thereof.
In order to solve the technical problems, the invention provides a watermelon extract solution, which comprises the following components: the watermelon extract and the alcohol solvent are mixed according to the weight ratio of 1: 5-1: 10; the alcohol solvent is at least one of ethanol, propylene glycol and glycerol.
The watermelon electronic cigarette oil prepared by adopting the watermelon extract solution comprises the following components in parts by weight: 0-5 parts of nicotine and 80-90 parts of the watermelon extract solution.
Further, the watermelon electronic cigarette oil also comprises the following components in parts by weight: 5-20 parts of essence and flavor.
Further, the essence and flavor comprises the following components in parts by weight: 1-5 parts of cucumber aldehyde, 1-10 parts of butyl acetate, 10-40 parts of isoamyl acetate, 20-40 parts of ethyl maltol, 10-20 parts of geranyl acetate, 1-5 parts of cis-6-nonenol and 1-5 parts of hexanal.
Also provides a preparation method of the watermelon electronic cigarette oil, which comprises the following steps:
s1, respectively weighing watermelon extract solution, essence and spice and nicotine according to the weight part ratio;
s2, adding essence, spice and nicotine into the watermelon extract solution, and then sealing and stirring to obtain the finished watermelon electronic cigarette oil.
Further, step S0 is included before step S1, to prepare a watermelon extract solution: weighing the watermelon extract and the alcohol solvent according to the weight part ratio, mixing, stirring at constant temperature, and finally filtering to remove filter residue to obtain the watermelon extract solution.
Further, in step S0, the temperature of constant temperature stirring is 40-50 ℃, and the time of constant temperature stirring is 40-60 min.
Further, in step S0, the uniformly stirred solution is allowed to stand and cooled to room temperature before being filtered.
Further, a step S01 is further included between the steps S0 and S1, wherein the step of preparing the essence and flavor comprises: weighing cucumber aldehyde, butyl acetate, isoamyl acetate, ethyl maltol, geranyl acetate, cis-6-nonenol and hexanal according to the weight part ratio, and mixing and stirring uniformly to obtain the essence and spice.
Further, in step S2, the time for sealing and stirring is 2-3 h.
Compared with the prior art, the watermelon extract solution has the beneficial effects that: the watermelon extract is rich in malic acid, proteinic amino acid, lycopene, vitamin C and various minerals, and has effects of clearing away summer-heat, quenching thirst, moisturizing intestine, and promoting urination, and the watermelon extract solution obtained by dissolving watermelon extract in alcohol solution has health promotion effect; the watermelon electronic cigarette oil prepared by the watermelon extract solution also has a health-care effect, so that a smoker can improve the body of the smoker while quitting smoking or using a cigarette substitute (namely an electronic cigarette), and the watermelon extract also contains aromatic components, so that the electronic cigarette oil prepared by the watermelon electronic cigarette oil has watermelon aroma.
Detailed Description
In order to more fully understand the technical contents of the present invention, the technical solutions of the present invention will be further described and illustrated with reference to specific embodiments.
The most key concept of the invention is as follows: malic acid, protein amino acid, lycopene, vitamin C and various mineral substances with health care effects are introduced into an electronic cigarette oil product used by an electronic cigarette.
In order to explain the feasibility of the inventive concept, the technical contents, the achieved objects and the effects of the present invention are described in detail.
The watermelon extract solution consists of watermelon extract and an alcohol solvent, wherein the weight ratio of the watermelon extract to the alcohol solvent is 1: 5-1: 10; the alcohol solvent is at least one of ethanol, propylene glycol and glycerol. The watermelon extract is rich in malic acid, proteinic amino acids, lycopene, vitamin C and various minerals, and has effects of clearing away summer-heat, quenching thirst, moisturizing intestine, and promoting urination. According to efficacy verification, the health-care components malic acid, proteinic amino acid, lycopene, vitamin C, various mineral substances and the like of the watermelon extract solution prepared according to the weight ratio (1: 5-1: 10 of the watermelon extract: the alcohol solvent) reach the effective amount. Watermelon extract is generally used in the form of powdered product due to its convenience in processing, transportation, and use. The watermelon extract used as the raw material in the invention is powdery, so the watermelon extract needs to be dissolved by using an alcohol solution, is convenient to use and is also convenient to remove impurities insoluble in the alcohol solution. Malic acid, proteinic amino acid, lycopene, vitamin C, various mineral substances and the like in the watermelon extract and aromatic odor components contained in the watermelon extract have good solubility in alcohol reagents such as ethanol, propylene glycol, glycerol and the like, the ethanol, the propylene glycol and the glycerol are used as common basic components of the electronic cigarette oil, the safety of the electronic cigarette oil is proved, one or more alcohol solutions can be selected according to requirements to dissolve the watermelon extract, and the watermelon extract solution prepared by using the alcohol reagents such as the ethanol, the propylene glycol and the glycerol is convenient to be directly used in the preparation of the electronic cigarette oil.
Specifically, the main components of the watermelon extract comprise protein, glucose, sucrose, fructose, malic acid, glutamic acid, citrulline, sucrase, calcium, iron, phosphorus, crude fiber, vitamin (A, B, C) and the like, and the nutritional components comprise glucose, malic acid, fructose, proteinogenic amino acid, lycopene, vitamin A, B1, B2, C and the like; the extraction method of the watermelon extract comprises the following steps: juicing watermelon, extracting at 80 deg.C for 45min, filtering, vacuum distilling at 35-45 deg.C to 1/10 volume, cooling to 8 deg.C, filtering, and drying to obtain dry powder.
The watermelon electronic tobacco tar comprises the following components in parts by weight: 0-5 parts of nicotine and 80-90 parts of the watermelon extract solution; because the watermelon extract solution has health care efficacy, the watermelon electronic cigarette oil prepared by the watermelon extract solution also has health care effect, a smoker can improve the body of the smoker while quitting smoking or using a cigarette substitute (namely an electronic cigarette), and because the watermelon extract also contains other aromatic components, the electronic cigarette oil prepared by the watermelon extract solution has watermelon aroma; the tobacco tar product containing nicotine with different components in the above proportion is produced according to smoking cessation requirements, so that a smoker can gradually stop smoking, and pain caused by smoking cessation is reduced.
Further, the watermelon electronic cigarette oil also comprises the following components in parts by weight: 5-20 parts of essence and spice; the watermelon extract solution contains less watermelon aromatic substances, and essence and spice are added for supplement, so that the overall smell of the product is stronger.
Further, the essence and flavor comprises the following components in parts by weight: 1-5 parts of cucumber aldehyde, 1-10 parts of butyl acetate, 10-40 parts of isoamyl acetate, 20-40 parts of ethyl maltol, 10-20 parts of geranyl acetate, 1-5 parts of cis-6-nonenol and 1-5 parts of hexanal. The essence and flavor are prepared by matching multiple components, the mixture ratio of the components is obtained by combining watermelon aromatic components contained in the watermelon extract solution through repeated experimental research, and after the essence and flavor prepared according to the mixture ratio is added into the watermelon extract solution, the obtained electronic cigarette oil is more mellow and full in flavor and is layered.
The preparation method of the watermelon electronic cigarette oil comprises the following steps:
s1, respectively weighing watermelon extract solution, essence and spice and nicotine according to the weight part ratio;
s2, adding essence, spice and nicotine into the watermelon extract solution, and then sealing and stirring to obtain a finished watermelon electronic cigarette oil product; through stirring, make each component misce bene, and stir under sealed, prevent the pollution.
Further, step S0 is included before step S1, to prepare a watermelon extract solution: weighing the watermelon extract and the alcohol solvent according to the weight part ratio, mixing, stirring at constant temperature, and finally filtering to remove filter residues to obtain a watermelon extract solution; stirring at constant temperature to dissolve the watermelon extract completely.
Further, in step S0, the temperature of constant temperature stirring is 40-50 ℃, and the time of constant temperature stirring is 40-60 min; by controlling the temperature and time during stirring, the volatilization loss of the alcohol solution caused by overhigh temperature is reduced while the solid (watermelon extract) is ensured to be dissolved quickly.
Further, in step S0, before filtering, the uniformly stirred solution is first allowed to stand and cooled to room temperature; the solution is kept stand before being filtered, so that solid matters are precipitated, undissolved filter residues can be sufficiently filtered, the filtering effect is better, the total liquid surface area is increased in the filtering process, and if the temperature is too high and the volatilization speed is too high, the production investment is increased, so the filtering is carried out after the solution temperature is cooled to room temperature.
Further, a step S01 is further included between the steps S0 and S1, wherein the step of preparing the essence and flavor comprises: weighing cucumber aldehyde, butyl acetate, isoamyl acetate, ethyl maltol, geranyl acetate, cis-6-nonenol and hexanal according to the weight part ratio, and mixing and stirring uniformly to obtain the essence and spice; the addition amount of each component in the essence and flavor is small, and if the components are directly and respectively weighed and added, the deviation is large, so that the components in the essence and flavor are firstly blended, and then the essence and flavor are blended into the watermelon extract solution according to the requirement, so that the actual content and the expected content of each component in the electronic cigarette oil product are not greatly different, and the large deviation among products produced in each batch is ensured.
Further, in step S2, the time for sealing and stirring is 2-3h, and the components are fully and uniformly mixed by fully stirring.
To illustrate the feasibility of the inventive concept, reference is made to the following specific examples:
example 1:
a preparation method of watermelon electronic cigarette oil comprises the following steps:
1) the preparation method of the watermelon extract solution comprises the following steps: according to the weight ratio: ethanol: propylene glycol: 1, glycerol: 1: 3: 5, weighing the watermelon extract, ethanol, propylene glycol and glycerol (namely the weight ratio of the watermelon extract to the alcohol solvent is 1: 9), mixing, stirring for 40min at 40 ℃, standing, cooling to room temperature, and finally filtering to remove filter residues to obtain the watermelon extract solution.
2) The preparation steps of the essence and the spice are as follows: 1 part by weight of cucumber aldehyde, 3 parts by weight of butyl acetate, 10 parts by weight of isoamyl acetate, 20 parts by weight of ethyl maltol, 10 parts by weight of geranyl acetate, 3 parts by weight of cis-6-nonenol and 5 parts by weight of hexanal are mixed and stirred uniformly to obtain the essence and flavor.
3) The manufacturing steps of the finished product are as follows: and (3) adding 10 parts by weight of essence and spice into 80 parts by weight of the watermelon extract solution, and then sealing and stirring for 2 hours to obtain the finished watermelon electronic cigarette oil.
Example 2:
a preparation method of watermelon electronic cigarette oil comprises the following steps:
1) the preparation method of the watermelon extract solution comprises the following steps: according to the weight ratio: propylene glycol: 1, glycerol: 4: 5, weighing the watermelon extract, propylene glycol and glycerol (namely the weight ratio of the watermelon extract to the alcohol solvent is 1: 9), mixing, stirring for 60min at 50 ℃, standing, cooling to room temperature, and finally filtering to remove filter residues to obtain the watermelon extract solution.
2) The preparation steps of the essence and the spice are as follows: mixing 5 parts by weight of cucumber aldehyde, 10 parts by weight of butyl acetate, 40 parts by weight of isoamyl acetate, 40 parts by weight of ethyl maltol, 20 parts by weight of geranyl acetate, 5 parts by weight of cis-6-nonenol and 1 part by weight of hexanal, and uniformly stirring to obtain the essence and flavor.
3) The manufacturing steps of the finished product are as follows: and adding 20 parts by weight of essence and spice and 5 parts by weight of nicotine into 90 parts by weight of the watermelon extract solution, and then sealing and stirring for 3 hours to obtain the finished watermelon electronic cigarette oil.
Example 3:
a preparation method of watermelon electronic cigarette oil comprises the following steps:
1) the preparation method of the watermelon extract solution comprises the following steps: according to the weight ratio: 1, propylene glycol: 8, mixing the watermelon extract and propylene glycol, stirring for 50min at 45 ℃, standing, cooling to room temperature, and finally filtering to remove filter residues to obtain the watermelon extract solution.
2) The preparation steps of the essence and the spice are as follows: mixing and stirring 2 parts by weight of cucumber aldehyde, 5 parts by weight of butyl acetate, 20 parts by weight of isoamyl acetate, 25 parts by weight of ethyl maltol, 15 parts by weight of geranyl acetate, 2 parts by weight of cis-6-nonenol and 4 parts by weight of hexanal uniformly to obtain the essence and spice.
3) The manufacturing steps of the finished product are as follows: and adding 10 parts by weight of essence and flavor and 3 parts by weight of nicotine into 85 parts by weight of the watermelon extract solution, and then sealing and stirring for 2.5 hours to obtain the finished watermelon electronic cigarette oil.
Example 4:
a preparation method of watermelon electronic cigarette oil comprises the following steps:
1) the preparation method of the watermelon extract solution comprises the following steps: according to the weight ratio: ethanol: 1, glycerol: 1: 7, weighing the watermelon extract, ethanol and glycerol (namely the weight ratio of the watermelon extract to the alcohol solvent is 1: 8), mixing, stirring for 45min at 42 ℃, standing, cooling to room temperature, and finally filtering to remove filter residues to obtain the watermelon extract solution.
2) The preparation steps of the essence and the spice are as follows: mixing and stirring 3 parts by weight of cucumber aldehyde, 8 parts by weight of butyl acetate, 30 parts by weight of isoamyl acetate, 35 parts by weight of ethyl maltol, 15 parts by weight of geranyl acetate, 1 part by weight of cis-6-nonenol and 3 parts by weight of hexanal uniformly to obtain the essence and flavor.
3) The manufacturing steps of the finished product are as follows: adding 15 parts by weight of essence and flavor and 2 parts by weight of nicotine into 88 parts by weight of the watermelon extract solution, and then sealing and stirring for 3 hours to obtain the finished watermelon electronic cigarette oil.
The products produced according to the above examples 1-4 were extracted for testing: it has a relative density (20/20 ℃) of 1.1098, a refractive index (20 ℃) of 1.4382, a boiling point (101.3kPa) of 194.5 ℃ and is in a nonvolatile state under conventional storage conditions; the color, aroma and fragrance are evaluated according to a quality guarantee period evaluation test, and the quality guarantee period of the product reaches more than three years; namely, the electronic cigarette oil produced according to the formula of the invention is easy to store under normal temperature and pressure conditions, has excellent stability and long shelf life, and is easy to atomize when in use.
In conclusion, the watermelon extract solution provided by the invention is rich in vitamin malic acid, proteinic amino acid, lycopene, vitamin C, various minerals and the like, namely, the watermelon extract solution has the health-care effects of clearing summer-heat, quenching thirst, moistening intestines, promoting urination and the like; the watermelon electronic cigarette oil prepared by the watermelon extract solution also has a health-care effect, so that smokers can quit smoking or use cigarette substitutes and improve their bodies; the watermelon extract also contains other aromatic components, so that the electronic cigarette oil prepared by using the watermelon extract solution has watermelon aroma, and the aromatic components contained in the watermelon extract are supplemented by adding essence and spices, so that the overall smell of the product is stronger, mellow and full; the production process is that the mixture is evenly mixed by stirring, the dissolving speed is increased by controlling the temperature during stirring, the volatilization speed of the alcohol solution is reduced, and impurities are removed by filtering.
The above description is only an embodiment of the present invention, and not intended to limit the scope of the present invention, and all equivalent flow transformations made by the present specification, or directly or indirectly applied to other related technical fields, are included in the scope of the present invention. Meanwhile, for a person skilled in the art, according to the embodiments of the present invention, there may be variations in the specific implementation manners and application ranges, and in summary, the content of the present description should not be construed as a limitation to the present invention.
Claims (10)
1. The watermelon extract solution is characterized by comprising the following components: the watermelon extract and the alcohol solvent are mixed according to the weight ratio of 1: 5-1: 10; the alcohol solvent is at least one of ethanol, propylene glycol and glycerol.
2. The watermelon electronic tobacco tar is characterized by comprising the following components in parts by weight: 0-5 parts nicotine and 80-90 parts of the watermelon extract solution of claim 1.
3. The watermelon electronic cigarette liquid of claim 2, further comprising the following components in parts by weight: 5-20 parts of essence and flavor.
4. The watermelon electronic cigarette oil of claim 3, wherein the essence and flavor comprise the following components in parts by weight: 1-5 parts of cucumber aldehyde, 1-10 parts of butyl acetate, 10-40 parts of isoamyl acetate, 20-40 parts of ethyl maltol, 10-20 parts of geranyl acetate, 1-5 parts of cis-6-nonenol and 1-5 parts of hexanal.
5. The preparation method of the watermelon electronic cigarette oil of claim 4, which comprises the following steps:
s1, respectively weighing watermelon extract solution, essence and spice and nicotine according to the weight part ratio;
s2, adding essence, spice and nicotine into the watermelon extract solution, and then sealing and stirring to obtain the finished watermelon electronic cigarette oil.
6. The method for preparing watermelon electronic cigarette liquid according to claim 5, further comprising step S0 before step S1, wherein the method comprises the following steps: weighing the watermelon extract and the alcohol solvent according to the weight part ratio, mixing, stirring at constant temperature, and finally filtering to remove filter residue to obtain the watermelon extract solution.
7. The method for preparing watermelon electronic cigarette oil according to claim 6, wherein in step S0, the stirring temperature is 40-50 ℃ and the stirring time is 40-60 min.
8. The method for preparing watermelon electronic cigarette oil according to claim 7, wherein in step S0, the uniformly stirred solution is left to stand and cooled to room temperature before being filtered.
9. The method for preparing watermelon electronic cigarette oil according to claim 6, wherein step S01 is further included between steps S0 and S1, wherein the method comprises the following steps: weighing cucumber aldehyde, butyl acetate, isoamyl acetate, ethyl maltol, geranyl acetate, cis-6-nonenol and hexanal according to the weight part ratio, and mixing and stirring uniformly to obtain the essence and spice.
10. The method for preparing watermelon electronic cigarette oil according to claim 5, wherein in step S2, the sealing and stirring time is 2-3 h.
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