CN105105315A - Throat-clearing type tobacco powder spray and preparation method thereof - Google Patents
Throat-clearing type tobacco powder spray and preparation method thereof Download PDFInfo
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Abstract
The invention discloses a throat-clearing type tobacco powder spray which consists of main materials and auxiliary materials, wherein the main materials comprise any one kind of tobacco raw material powder or tobacco extract powder, lactose, olive extract, loquat extract, licorice powder, water-soluble starch, water chestnut extract and lemon extract; the auxiliary materials comprise a sweetening agent, edible salt, edible flavor and fragrance and citric acid. The invention also provides a preparation method of the throat-clearing type tobacco powder spray. The throat-clearing type tobacco powder spray disclosed by the invention is sprayed into an oral cavity in a powdery type during use, is refreshing and delicate in mouth feel and has the actions of keeping breath fresh, and refreshing and promoting salivation; by using the throat-clearing type tobacco powder spray, a user gets the satisfaction similar to that brought by smoking traditional cigarettes; meanwhile, the throat-clearing type tobacco powder spray also has the effects of clearing the heat of throat and promoting the production of body fluid to relieve thirst.
Description
Technical field
The invention belongs to novel tobacco technical field, be specifically related to a kind of clear throat type tobacco powder spray and preparation method thereof.
Background technology
Along with the continuous propelling of international Tobacco Control campaign, the restriction of national governments to public place smoking is more and more stricter.Countries in the world tobacco business is using the research and development of tobacco product of new generation and the important means of introducing to the market as solving tobacco business future development, smoke-free tobacco product is developing in the mode of sucking of its uniqueness always, and having caused the extensive concern of transnational tobacco company, smoke-free tobacco product becomes the important supplement of traditional cigarette.Relative to the harmfulness of traditional cigarette and cigar, smoke-free tobacco product is considered to the lower [BatesC of the harmfulness of human body, FagerstromK, JarvisMJ, etal.EuropeanUnionpolicyonsmokelesstobacco:astatementinf avorofevidencebasedregulationforpublichealth.TobaccoCont rol, 2003,12:360].The research display of Critchley group, compared with cigarette, smoke-free tobacco product will low at least two orders of magnitude [15-20 day the 4th in November, 2010 session report file FCTC/COP/4/12 " Control and prevention smokeless tobacco articles and electronic cigarette "] to the harmfulness of human body.On the other hand, smoke-free tobacco product is sucked by oral cavity or nasal cavity, does not need burning, can not produce flue gas, stop the harm of " second-hand-cigarette ", decreased the harm of smoking to public health.
The main traditional smoke-free tobacco product sold has two kinds of snuff and snus in the market, these products are after oral cavity has been sucked, consumer also will spue the residue of residue or Soft Roll, can to environment, and its taste and consumption habit are not suitable for domestic consumer.Therefore, research and develop Novel smokeless gas tobacco product and seem particularly necessary.Some patent reports tobacco oral spray agent and preparation method thereof, by tobacco extract, Chinese herbal medicine extract, flavouring essence for tobacco, auxiliary material, stir, adjust ph, then filling in spraying bottle, make finished product, and give second different effect of product, as fresh breath, inrigorating qi and promoting blood circulation, antiphlogistic antibacterial, preventing decayed tooth are good for tooth, anti-blooming antiemetic etc.As a kind of fresh breath type tobacco oral spray agent and preparation method thereof, number of patent application: 201410027098.X; A kind of inrigorating qi and promoting blood circulation type tobacco oral spray agent and preparation method thereof 201410027484.9; A kind of antiphlogistic antibacterial type tobacco oral spray agent and preparation method thereof 201410027414.3; A kind of preventing decayed tooth is good for flute profile tobacco oral spray agent and preparation method thereof, number of patent application: 201410027070.6; A kind of anti-blooming antiemetic type tobacco oral spray agent and preparation method thereof, number of patent application: 201410026870.6; A kind of expelling phlegm and arresting coughing type tobacco oral spray agent and preparation method thereof, number of patent application: 201410028227.7, a kind of throat-clearing throat-moistening type tobacco oral spray agent and preparation method thereof, number of patent application: 201410026989.3, a kind of nourishing Yin and falling fire type tobacco oral spray agent and preparation method thereof, number of patent application: 201410026952.0.These sprays are all liquid sprays, need use special push-type vacuum spray bottle.
Those are in for a long time in the air-polluting environment such as thickness dirt, chemically gas, talk more, or throat by the people of the stimulation of tobacco and wine, maror, all can damage its mucous epithelium of pharynx and body of gland for a long time, easily suffer from acute and chronic pharyngitis and there is the common symptons such as throat discomfort.If take certain prevention and hygienic measures at ordinary times, can play an important role for pharyngitis prevention and control and supplemental treatment.So the present invention increases the component of clear throat in tobacco powder spray, allow consumer not only can experience the satisfaction of the similar smoking that tobacco powder spray brings, simultaneously this tobacco powder spray effect of also having throat clearly, promoting the production of body fluid to quench thirst.About clear throat type tobacco powder spray, there is not been reported both at home and abroad at present.
Summary of the invention
The object of the invention is to be to provide a kind of clear throat type tobacco powder spray, enrich the kind of novel tobacco goods.These goods spray into oral cavity with Powdered when using, and clean taste is fine and smooth, can be supplied to the satisfaction of the similar smoking of consumer, comfort, effectively can alleviate again and eliminate the common symptons such as pharyngeal dryness, cough, throat discomfort.
Object of the present invention can be achieved through the following technical solutions:
First aspect present invention relates to a kind of clear throat type tobacco powder spray, it is made up of major ingredient and auxiliary material, wherein said major ingredient comprise in tobacco material powder or tobacco extract powder any one, lactose, Fructus Canrii Albi extract, loquat extract, licorice powder, water soluble starch, water chestnut extract and lemon extract; Described auxiliary material comprises sweetener, salt, flavoring essence spices and citric acid.
In a preferred embodiment of the present invention, described tobacco material powder is prepared by following steps: be soaked in water by raw tobacco material, rinsing post-drying to moisture well is 6 ~ 8wt%, again low-temperature submicron powder carried out to the tobacco leaf after drying broken or be ground to particle diameter and be less than or equal to 400 object ultra-micro powders, obtain described tobacco material powder; Wherein said low temperature refers to room temperature under normal pressure.
In a preferred embodiment of the present invention, described tobacco extract powder is prepared by following steps: will clean the ethanol water heating and refluxing extraction of the raw tobacco material 50-95wt% of its 5-10 times of weight of drying 2-3 time, each extraction 2-4 hour; Merge extract and filter, filtrate reduced in volume is become medicinal extract, then by spray-dried for described medicinal extract, pulverizing, making particle diameter and be less than or equal to 200 object ultra-micro powders, obtain described tobacco extract powder.
Described tobacco material is a kind of in flue-cured tobacco, airing cigarette, Turkish tobaccos or the mixture between them.The tobacco leaf of the kinds such as the large gold dollar of the preferred safflower of Domestic Flue-cured Tobacco, K326, Yun yan85, cloud and mist 97, external flue-cured tobacco preferred Zimbabwe flue-cured tobacco and Brazilian flue-cured tobacco; Turkish tobaccos preferred Baoshan Turkish tobaccos, Turkey's Turkish tobaccos; Airing cigarette preferred Sichuan Dazhou City burley tobaccos, Red River Sun cured tobacco.Do not add external burley tobaccos, airing cigarette in goods, reduce the pungent and excitant that burley tobaccos bring, make products taste gentle, stimulus to the sense organ is moderate, is more applicable to domestic consumer groups.Tobacco material is broken or be ground to particle diameter and be less than or equal to 400 object micropowders through low-temperature submicron powder.After tobacco micronizing, if improve the dissolution rate of active ingredient, improve bioavilability; Be easy to form dust cloud, when use procedure directly by buccal absorption, human absorptivity improves several times, cost-saving.
In a preferred embodiment of the present invention, any one in described Fructus Canrii Albi extract, water chestnut extract, lemon extract, loquat extract is prepared by following steps: dry cleaning and be ground into the block plant material ethanol water of the 50-95wt% of its 5-10 times of weight ultrasonic extraction 2-4 hour, repeats to extract 2-3 time; Merge extract and filter, filtrate reduced in volume is become medicinal extract, then by spray-dried for described medicinal extract, pulverizing, making particle diameter and be less than or equal to 200 object ultra-micro powders, obtain plant extracts.
The plant extracts that the present invention relates to is edible plants extract.They have throat clearly, the effect promoted the production of body fluid to quench thirst.
Olive: the fruit of Burseraceae magaphanerophytes olive.Also known as olive, Chinese olive, blue or green olive, Gan Lan.All there is distribution on the ground such as China Guangdong, Guangxi, Fujian, Sichuan, Yunnan, Taiwan, mostly are cultivation.Olive performance: taste is sweet, sour, property is put down; Effect: removing heat from the lung and relieving sorethroat, promotes the production of body fluid to quench thirst, removing toxic substances; Cure mainly: cough phlegm blood, abscess of throat, hot summer weather polydipsia, drunk, fish crab is poisoning.Olive complex chemical composition, mainly containing flavone compound, coumarin and phenolic compound, volatile materials, triterpene compound, also containing mineral matter and the trace element such as amino acid, aliphatic acid and calcium, phosphorus, iron.Clinical research observation, containing the Chinese patent drug Chinese white olive pieces of olive medicinal material, Chinese olive ball and Chinese olive mouth-keeping tablet for reliving sore-throat, good curative effect is all had to diseases such as acute and chronic pharyngitis, chronic bronchitis, bronchiectasis. illustrate that Chinese white olive pieces has good anti-inflammatory, analgesia and bacteriostasis [Chang Qiang, Su Minghua, Chen Qing. olive chemical composition and pharmacology activity research are in progress. tropical crops journal, 2013 (8): 75-76].King is identical thinks that clearing heat, relieving sore-throat effect of olive may form [Wang Heng by the synergy of gallic acid, scopolactone, escoparone, Song Liangke, Tang Wu, Deng. the research of matter Chinese olive clearing heat, relieving sore-throat chemical constituent not of the same race. CHINA JOURNAL OF CHINESE MATERIA MEDICA, 2010 (6): 669-672].
Water chestnut: have another name called water chestnut, Shui Li, Chinese herbaceous peony, an ancient name for water chestnut, black taro, Bodhisattva's shepherd's purse, a kind of wild plant, the subteranean stem of which is like water chestnut, monocot genus Cyperaceae, for perennial root herbaceous plant, oblateness, above point, smooth surface is glossy, aubergine or pitchy, growth is in pond, and bottle green stem is on the ground grown thickly, and the bulb of underground can be edible.Water chestnut is cold in nature, have that clearing heat and detoxicating, cool blood promotes the production of body fluid, diuresis defaecation, Cleering damp and dissolving phlegm, the de-swelling that helps digestion effect, can be used for treating jaundice, dysentery, polio, constipation and other diseases; Water chestnut contains a kind of antimicrobial component, and to the certain effect that reduced blood pressure, this material also has preventive and therapeutic effect to cancer.Compendium of Material Medica is thought, water chestnut " taste is sweet, be slightly cold, sliding, nontoxic "." lower borax, disappear its function wind poison, except stagnancy of pathogens in chest hot gas, can make powder food for numbness of quenching one's thirst heat, Wen Zhongyi gas.Improve visual and auditory acuity, disappear jaundice, whetting the appetite.Make powder food, thick people's stomach, not flesh; Can detoxify, take metal and stone people and should it.Treat five kinds of diaphragm gas, disappear place food, should eat it after meal.Control and gulp down copper thing by mistake, blood under main bloody flux, metrorrhagia, keeps away disease due to noxious agents produced by various parasites ".Water chestnut is sweet, cold; Can clearing lung-heat heat, be rich in lymphatic temperament again, have promoting production of body fluid and nourishing the lung, the removing toxic substances of the sharp intestines that reduce phlegm, diuresis promoting, the carbuncle that disappears, cool blood dampness elimination, help digestion the effects such as de-swelling.
Lemon: the evergreen dungarunga being Rutaceae both citrus, mainly containing compositions such as volatile oil, limonin, alkaloid, Coumarins, flavonoids.Lemon is most one of fruit having medical value in the world, and taste acid is sweet, property is put down, and enters liver, stomach warp; There is preventing phlegm from forming and stopping coughing, promote the production of body fluid, effect of invigorating the spleen; Mainly treating bronchitis, pertussis, vitamin C deficiency, heatstroke polydipsia, poor appetite, pregnant woman's disorder of stomach-energy, receive subtract, gas etc.Lemon is rich in vitamin C, carbohydrate, calcium, phosphorus, iron, vitamin B1, vitamin B2, very useful to human body.It is called as " anti-inflammatory fruit ", and the effect played human body, just as natural antibiotics, has anti-inflammation, strengthens the multiple efficacies such as body immunity.
Loquat: be rosaceous plant, Loquat-Shaped Cake is rich in the various nutrients of needed by human body, soft and succulency, local flavor sour-sweet, is nutritious health fruit.Really: the sweet acid of taste, property are put down; Core: bitter, property are flat, enter lung, stomach warp.Really: there is clearing lung-heat, promote the production of body fluid to quench thirst; Core: expelling phlegm and arresting coughing, harmonizing stomach and lowering adverse Qi; The illness such as be used for the treatment of lung heat and cough, chronic cough are not healed, dry throat and mouth and stomach Qi are not enough.
Described plant extracts extracts according to following steps:
Select non-rot, free from extraneous odour, the plant material of free from insect pests cleans and dry, be ground into fritter, add the ethanol water ultrasonic extraction 2-4 hour of the 50-95wt% of its 5-10 times of weight, repeat to extract 2-3 time, merge extract, filter, decompression filtrate recycling ethanol is condensed into medicinal extract, again by spray-dried for described medicinal extract, pulverize, make particle diameter and be less than or equal to 200 object ultra-micro powders, for subsequent use.
Lactose: lactose exists only in mammiferous milk at occurring in nature, its molecular structure is formed by a part glucose and the condensation of a part galactolipin.A part lactose digestion can be got a point sub-glucose and a part galactolipin.Galactolipin can promote the generation of cerebroside and glutinous polysaccharide, thus grows extremely important to infant intelligence.Lactose is crystallinity particle or the powder of white, and odorless, taste is micro-sweet.Sugariness is 15% of sucrose.Be mainly used in: as the absorption dispersant of powdered food pigment, reduce pigment concentration, easy to use and reduce the variable color of duration of storage.Utilize the easy compression molding of lactose and the low feature of water imbibition, made the excipient such as compressing tablet.
In a preferred embodiment of the present invention, described clear throat type tobacco powder spray is made up of following component by weight percentage: tobacco material powder 75-90%, lactose 2-5%, water soluble starch 0.5-5%, Fructus Canrii Albi extract 1-5%, water chestnut extract 0.5-2%, lemon extract 0.5-2%, loquat extract 1-3%, licorice powder 1-5%, salt 0.5-2%, citric acid 1-3%, sweetener 0.1-2%, flavoring essence spices 0.3-2%.
In a preferred embodiment of the present invention, described clear throat type tobacco powder spray is made up of following component by weight percentage: tobacco extract powder 10-25%, lactose 40-60%, water soluble starch 5-15%, Fructus Canrii Albi extract 1-5%, water chestnut extract 0.5-2%, lemon extract 0.5-2%, loquat extract 1-3%, licorice powder 1-5%, salt 0.4-2%, citric acid 1-3%, sweetener 0.01-2%, flavoring essence spices 0.3-2%.
In a preferred embodiment of the present invention, the powder diameter scope in described clear throat type tobacco powder spray is 200 order-800 orders.Such as 200 orders, 250 orders, 300 orders, 400 orders, 500 orders, 600 orders or 800 orders, preferably, described powder diameter is preferably less than or equal to 400 orders.
In a preferred embodiment of the present invention, described sweetener comprise that Sucralose, maltitol, isomaltoketose, sorbierite, antierythrite, lactitol, honey element, acesulfame potassium, stevioside, Aspartame, knob are sweet, a kind of in xylitol or any combination between them; Described flavoring essence spices comprises any one in lemon extract, Mint Essence, tamarind essence, red bayberry essence, Green tea essence, jasmine tea essence.
Flavoring essence spices can give goods different flavor characteristics.The existing perfume monomer of flavouring agent used in the present invention, also has essence and various natural extract.Comprise vanilla, coffee, chocolate/cocoa, cream, tamarind, red bayberry, peppermint, Pu'er tea, green tea, jasmine tea, spearmint, menthol, American mint, Chinese ilex, lavender, cardamom, nutmeg, Chinese cassia tree, honey, ginger, fennel, Salvia japonica, lemon, apple, peach, sour lime, cherry, strawberry, oranges and tangerines, Radix Glycyrrhizae, spearmint, peppermint, lavender, Amomum cardamomum, cloves, sandalwood, hawthorn, fish pelargonium, vanillon, orange-seed oil, cornmint, caraway, camomile etc.Preferred essence and flavoring agent is: any one in lemon, peppermint, tamarind, red bayberry, green tea, jasmine tea essence.
Second aspect present invention relates to the preparation method of clear throat type tobacco powder spray described according to a first aspect of the present invention, comprises the following steps:
1) raw tobacco material is soaked in water, rinsing post-drying to moisture well is 6 ~ 8wt%, again low-temperature submicron powder carried out to the tobacco leaf after drying broken or be ground to particle diameter and be less than or equal to 400 object ultra-micro powders, wherein said low temperature refers to room temperature under normal pressure, obtain described tobacco material powder, for subsequent use; Or, will the ethanol water heating and refluxing extraction of the raw tobacco material 50-95wt% of its 5-10 times of weight of drying be cleaned 2-3 time, each extraction 2-4 hour; Merge extract and filter, filtrate reduced in volume is become medicinal extract, then by spray-dried for described medicinal extract, pulverizing, making particle diameter and be less than or equal to 200 object ultra-micro powders, obtain described tobacco extract powder, for subsequent use; Preferably, the described tobacco material powder obtained or described tobacco extract powder are inserted in sealed dry container for subsequent use.
2) need to prepare Fructus Canrii Albi extract, water chestnut extract, lemon extract or loquat extract as follows according to formula: dry cleaning and be ground into the block plant material ethanol water of the 50-95wt% of its 5-10 times of weight ultrasonic extraction 2-4 hour, repeat to extract 2-3 time; Merge extract and filter, filtrate reduced in volume is become medicinal extract, then by spray-dried for described medicinal extract, pulverizing, making particle diameter and be less than or equal to 200 object ultra-micro powders, obtain plant extracts;
3) all the other component raw material described being crushed to respectively particle diameter is 200 order-800 orders (75-18 μm), takes all the other component raw material and mix by formula;
4) by formula rate by step 1)-3) each raw material of preparing mixes, and loads bottle mouth position with in the plastics spray bottle of pipe, sterilizing, packs and obtain described clear throat type tobacco powder spray.
The using method of this clear throat type tobacco powder spray is as follows: the bottle cap opening described plastics spray bottle, the tubule of bottle mouth position is stretched into oral cavity, the body of finger extruding plastic spray bottle, the clear throat type tobacco powder in plastics spray bottle directly sprays into oral cavity and eats for consumer.
The present invention has the following advantages:
(1) clear throat type tobacco powder spray of the present invention can be supplied to the satisfaction of the similar smoking cigarette of consumer, joyful sense and comfort, and clean taste is fine and smooth, breath freshening, refrigerantly promotes the production of body fluid.
(2) clear throat type tobacco powder spray of the present invention has throat clearly, the effect of quenching one's thirst of promoting the production of body fluid, and effectively can alleviate and eliminate the common symptons such as pharyngeal dryness, cough, throat discomfort.
(3) compared with traditional buccal cigarette, clear throat type tobacco powder spray of the present invention is by the body of extruding plastic spray bottle, material is wherein with dust cloud state entrance chamber, directly contact with mucous membrane of mouth, human absorptivity improves several times, and bioavilability is high, can reduce dosage, cost-saving, to have efficiently, advantage fast, easily.Compared with liquid sprays, product of the present invention is without the need to using special hard push-type vacuum spray bottle, and only need the flexible plastic spray bottle using preparation simple and with low cost, make this product preparation process relatively simple, be easy to produce, cost is low.
(4) product of the present invention is Powdered, for liquid sprays, carries, stores, edible more simple and convenient.Product of the present invention uses and does not limit by place simultaneously, does not produce residue.
(5) without burning tobacco when using product of the present invention, can not flue gas be produced, second-hand-cigarette can be avoided the harm of non-smokers and environment.
Detailed description of the invention
Detailed description below by specific embodiment illustrates the present invention further, but is not limitation of the present invention.
Embodiment 1
Formula (by weight percentage): tobacco material powder 85%, lactose 3%, water soluble starch 0.5%, Fructus Canrii Albi extract 3%, water chestnut extract 1%, lemon extract 0.5%, loquat extract 0.5%, licorice powder 1.5%, salt 0.5%, citric acid 2%, xylitol 2%, Mint Essence 0.5%.
Preparation method is as follows:
1) be soaked in water by raw tobacco material, after rinsing well, drying to moisture is 6 ~ 8wt%, and low-temperature submicron powder is broken or be ground to particle diameter and be less than or equal to 400 object micropowders, puts micropowder into sealed dry container for subsequent use;
2) olive, water chestnut, lemon, loquat are cleaned and dry, be ground into fritter, the EtOH Sonicate adding the 50-95wt% of its 5-10 times of weight extracts 3 hours, repeat extraction 3 times, merge extract, filter, decompression filtrate recycling ethanol, be condensed into medicinal extract, spray-dried, pulverize, make particle diameter and be less than or equal to 200 object ultra-micro powders, for subsequent use;
3) all the other component raw material are crushed to particle diameter 200 order-800 order (18-75 μm), take each raw material by formula, mix;
4) mixing of materials above steps prepared well loads in plastics spray bottle afterwards, and namely sterilizing, packaging obtain throat type tobacco powder spray clearly.
Product effect assessment: this clear throat type tobacco powder spray has the distinctive breath of tobacco and peppermint cooling fragrance, stimulates moderate, satisfaction is comparatively strong, has the satisfaction similar with suction traditional cigarette after using; And there is throat clearly, the effect of quenching one's thirst of promoting the production of body fluid, can effectively alleviate the symptoms such as pharyngeal dryness, cough, throat discomfort.
Embodiment 2
Formula (by weight percentage): tobacco material powder 75%, lactose 5%, water soluble starch 2%, Fructus Canrii Albi extract 5%, water chestnut extract 0.5%, lemon extract 0.5%, loquat extract 4%, licorice powder 3%, salt 0.5%, citric acid 1.2%, xylitol 3%, lemon extract 0.3%.
Preparation method is as follows:
1) be soaked in water by raw tobacco material, after rinsing well, drying to moisture is 6 ~ 8wt%, and low-temperature submicron powder is broken or be ground to particle diameter and be less than or equal to 400 object micropowders, puts micropowder into sealed dry container for subsequent use;
2) olive, water chestnut, lemon, loquat are cleaned and dry, be ground into fritter, the EtOH Sonicate adding the 50-95wt% of its 5-10 times of weight extracts 2 hours, repeat extraction 3 times, merge extract, filter, decompression filtrate recycling ethanol, be condensed into medicinal extract, spray-dried, pulverize, make particle diameter and be less than or equal to 200 object ultra-micro powders, for subsequent use;
3) all the other component raw material are crushed to particle diameter 200 order-800 order (18-75 μm), take each raw material by formula, mix;
4) mixing of materials above steps prepared well loads in plastics spray bottle afterwards, and namely sterilizing, packaging obtain throat type tobacco powder spray clearly.
This clear throat type tobacco powder spray has the distinctive breath of tobacco and lemon cooling taste, stimulates moderate, and satisfaction is comparatively strong, has the satisfaction similar with suction traditional cigarette after using; And there is throat clearly, the effect of quenching one's thirst of promoting the production of body fluid, can effectively alleviate the symptoms such as pharyngeal dryness, cough, throat discomfort.
Embodiment 3
Formula (by weight percentage): tobacco material powder 90%, lactose 2%, water soluble starch 0.5%, Fructus Canrii Albi extract 2.5%, water chestnut extract 1%, lemon extract 0.5%, loquat extract 0.5%, licorice powder 1%, salt 0.5%, citric acid 1%, Sucralose 0.05%, Aspartame 0.05%, Mint Essence 0.4%.
Preparation method is identical with embodiment 2.
Product effect assessment: this clear throat type tobacco powder spray has the distinctive breath of tobacco and peppermint cooling fragrance, stimulates moderate, satisfaction is comparatively strong, has the satisfaction similar with suction traditional cigarette after using; And there is throat clearly, the effect of quenching one's thirst of promoting the production of body fluid.
Embodiment 4
Formula (by weight percentage): tobacco extract powder 25%, lactose 55%, water soluble starch 10%, Fructus Canrii Albi extract 3%, water chestnut extract 0.5%, lemon extract 0.5%, loquat extract 1%, Radix Glycyrrhizae powder 2%, salt 0.45%, citric acid 2%, knob are sweet 0.05%, tamarind extract 0.5%.
Preparation method is as follows:
1) will the ethanol water heating and refluxing extraction of the raw tobacco material 50-95wt% of its 5-10 times of weight of drying be cleaned 3 times, to extract 2 hours at every turn; Merge extract and filter, filtrate reduced in volume is become medicinal extract, then by spray-dried for described medicinal extract, pulverizing, making particle diameter and be less than or equal to 200 object ultra-micro powders, obtain described tobacco extract powder, for subsequent use;
2) olive, water chestnut, lemon, loquat are cleaned and dry, be ground into fritter, the EtOH Sonicate adding the 50-95wt% of its 5-10 times of weight extracts 2 hours, repeat extraction 3 times, merge extract, filter, decompression filtrate recycling ethanol, be condensed into medicinal extract, spray-dried, pulverize, make particle diameter and be less than or equal to 200 object ultra-micro powders, for subsequent use;
3) all the other component raw material are crushed to particle diameter 200 order-800 order (18-75 μm), take each raw material by formula, mix;
4) mixing of materials above steps prepared well loads in plastics spray bottle afterwards, and namely sterilizing, packaging obtain throat type tobacco powder spray clearly.
Product effect assessment: this clear throat type tobacco powder spray has the distinctive breath of tobacco and sour-sweet fragrance, stimulates moderate, satisfaction is comparatively strong, has the satisfaction similar with suction traditional cigarette after using; And there is throat clearly, the effect of quenching one's thirst of promoting the production of body fluid.
Embodiment 5
Formula (by weight percentage): tobacco extract powder 15%, lactose 60%, water soluble starch 10%, Fructus Canrii Albi extract 5%, water chestnut extract 1.5%, lemon extract 0.5%, loquat extract 3%, Radix Glycyrrhizae powder 3%, salt 0.45%, citric acid 1%, Aspartame 0.05%, Green tea essence 0.5%.
Preparation method is identical with embodiment 4.
This clear throat type tobacco powder spray has the distinctive breath of tobacco and green tea fragrance, and delicate mouthfeel is pure and fresh, stimulate and satisfaction moderate, have after using and the similar satisfaction of suction traditional cigarette; And there is throat clearly, the effect of quenching one's thirst of promoting the production of body fluid.
Embodiment 6
Formula (by weight percentage): tobacco extract powder 10%, lactose 60%, water soluble starch 12.8%, Fructus Canrii Albi extract 5%, water chestnut extract 1.5%, lemon extract 1%, loquat extract 3%, Radix Glycyrrhizae powder 5%, salt 0.5%, citric acid 1%, Sucralose 0.05%, acesulfame potassium 0.05%, jasmine tea essence 0.1%.
Preparation method is identical with embodiment 4.
This clear throat type tobacco powder spray has the distinctive breath of tobacco and jasmine tea fragrance, and delicate mouthfeel is pure and fresh, stimulates moderate, and physiology satisfaction is moderate, has the satisfaction similar with suction traditional cigarette after using; And there is throat clearly, the effect of quenching one's thirst of promoting the production of body fluid.
Embodiment 7
Formula (by weight percentage): tobacco extract powder 12%, lactose 60%, water soluble starch 13.2%, Fructus Canrii Albi extract 5%, loquat extract 3%, lemon extract 0.5%, loquat extract 0.5%, Radix Glycyrrhizae powder 4%, salt 0.5%, citric acid 1%, knob are sweet 0.1%, Mint Essence 0.2%.
Preparation method is identical with embodiment 4.
Product effect assessment: this clear throat type tobacco powder spray has the distinctive breath of tobacco and peppermint cooling fragrance, stimulates moderate, satisfaction is comparatively strong, has the satisfaction similar with suction traditional cigarette after using; And there is throat clearly, the effect of quenching one's thirst of promoting the production of body fluid.
The experiment of smokeing panel test of clear throat type tobacco powder spray described in embodiment 8-
Organize the 5-7 name tobacco result of use of personnel to the arbitrary clear throat type tobacco powder spray goods prepared in embodiment 1-7 of smokeing panel test to evaluate, comprise the index such as impression, physiology satisfaction in the flavour of product, oral cavity.Evaluation time should be arranged in point-10 point in morning 9, afternoon 3 point-4 or carry out ante cibum or 1 hour after meal.Under spraying 3-4 during evaluation at every turn.Experimental result shows, this spray has sour-sweet fragrance, and delicate mouthfeel is salubrious, and sense of promoting the production of body fluid is strong, can effectively alleviate the symptoms such as pharyngeal dryness, cough, throat discomfort; And there is the satisfaction of suction traditional cigarette, after using this spray 5-10 second, want that the desire of aspirating traditional cigarette disappears, and without the desire of suction traditional cigarette in 30-60 minute.
Claims (9)
1. a clear throat type tobacco powder spray, it is characterized in that, it is made up of major ingredient and auxiliary material, wherein said major ingredient comprise in tobacco material powder or tobacco extract powder any one, lactose, Fructus Canrii Albi extract, loquat extract, licorice powder, water soluble starch, water chestnut extract and lemon extract; Described auxiliary material comprises sweetener, salt, flavoring essence spices and citric acid.
2. clear throat type tobacco powder spray according to claim 1, it is characterized in that, described tobacco material powder is prepared by following steps: be soaked in water by raw tobacco material, rinsing post-drying to moisture well is 6 ~ 8wt%, again low-temperature submicron powder carried out to the tobacco leaf after drying broken or be ground to particle diameter and be less than or equal to 400 object ultra-micro powders, obtain described tobacco material powder; Wherein said low temperature refers to room temperature under normal pressure.
3. clear throat type tobacco powder spray according to claim 1, it is characterized in that, described tobacco extract powder is prepared by following steps: will clean its 5-10 times of weight of raw tobacco material of drying
The ethanol water heating and refluxing extraction of 50-95wt% 2-3 time, each extraction 2-4 hour; Merge extract and filter, filtrate reduced in volume is become medicinal extract, then by spray-dried for described medicinal extract, pulverizing, making particle diameter and be less than or equal to 200 object ultra-micro powders, obtain described tobacco extract powder.
4. clear throat type tobacco powder spray according to claim 1, it is characterized in that, any one in described Fructus Canrii Albi extract, water chestnut extract, lemon extract, loquat extract is prepared by following steps: dry cleaning and be ground into the block plant material ethanol water of the 50-95wt% of its 5-10 times of weight ultrasonic extraction 2-4 hour, repeats to extract 2-3 time; Merge extract and filter, filtrate reduced in volume is become medicinal extract, then by spray-dried for described medicinal extract, pulverizing, making particle diameter and be less than or equal to 200 object ultra-micro powders, obtain plant extracts.
5. clear throat type tobacco powder spray according to claim 1, it is characterized in that, it is made up of following component by weight percentage: tobacco material powder 75-90%, lactose 2-5%, water soluble starch 0.5-5%, Fructus Canrii Albi extract 1-5%, water chestnut extract 0.5-2%, lemon extract 0.5-2%, loquat extract 1-3%, licorice powder 1-5%, salt 0.5-2%, citric acid 1-3%, sweetener 0.01-2%, flavoring essence spices 0.3-2%.
6. clear throat type tobacco powder spray according to claim 1, it is characterized in that, it is made up of following component by weight percentage: tobacco extract powder 10-25%, lactose 40-60%, water soluble starch 5-15%, Fructus Canrii Albi extract 1-5%, water chestnut extract 0.5-2%, lemon extract 0.5-2%, loquat extract 1-3%, licorice powder 1-5%, salt 0.4-2%, citric acid 1-3%, sweetener 0.01-2%, flavoring essence spices 0.3-2%.
7. clear throat type tobacco powder spray according to claim 1, is characterized in that, powder diameter scope is wherein 200 order-800 orders.
8. clear throat type tobacco powder spray according to claim 1, it is characterized in that, described sweetener comprises that Sucralose, maltitol, isomaltoketose, sorbierite, antierythrite, lactitol, honey element, acesulfame potassium, stevioside, Aspartame, knob are sweet, a kind of in xylitol or any combination between them; Described flavoring essence spices comprises any one in lemon extract, Mint Essence, tamarind essence, red bayberry essence, Green tea essence, jasmine tea essence.
9. the preparation method of clear throat type tobacco powder spray according to claim 1, is characterized in that, comprise the following steps:
1) raw tobacco material is soaked in water, rinsing post-drying to moisture well is 6 ~ 8wt%, again low-temperature submicron powder carried out to the tobacco leaf after drying broken or be ground to particle diameter and be less than or equal to 400 object ultra-micro powders, wherein said low temperature refers to room temperature under normal pressure, obtain described tobacco material powder, for subsequent use; Or, will the ethanol water heating and refluxing extraction of the raw tobacco material 50-95wt% of its 5-10 times of weight of drying be cleaned 2-3 time, each extraction 2-4 hour; Merge extract and filter, filtrate reduced in volume is become medicinal extract, then by spray-dried for described medicinal extract, pulverizing, making particle diameter and be less than or equal to 200 object ultra-micro powders, obtain described tobacco extract powder, for subsequent use;
2) need to prepare Fructus Canrii Albi extract, water chestnut extract, lemon extract or loquat extract as follows according to formula: dry cleaning and be ground into the block plant material ethanol water of the 50-95wt% of its 5-10 times of weight ultrasonic extraction 2-4 hour, repeat to extract 2-3 time; Merge extract and filter, filtrate reduced in volume is become medicinal extract, then by spray-dried for described medicinal extract, pulverizing, making particle diameter and be less than or equal to 200 object ultra-micro powders, obtain plant extracts;
3) all the other component raw material described being crushed to respectively particle diameter is 200 order-800 orders, takes all the other component raw material and mix by formula;
4) by formula rate by step 1)-3) each raw material of preparing mixes, and loads bottle mouth position with in the plastics spray bottle of pipe, sterilizing, packs and obtain described clear throat type tobacco powder spray.
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| CN109554225A (en) * | 2018-11-29 | 2019-04-02 | 四川中烟工业有限责任公司 | A kind of fragrance functional additive increasing cigarette " profit sweet tea sense " |
| CN109984374A (en) * | 2019-05-16 | 2019-07-09 | 铂德（深圳）科技有限公司 | Citrus extracts solution, citrus electronics tobacco tar and preparation method thereof |
| ES2895269A1 (en) * | 2020-08-18 | 2022-02-18 | Saiz Salvador Saiz | Medicinal composition with nispero extract for treatment of respiratory conditions (Machine-translation by Google Translate, not legally binding) |
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|---|---|
| CN105105315B (en) | 2017-07-28 |
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