CN104489912A - Strong-flavor electronic cigarette liquid - Google Patents
Strong-flavor electronic cigarette liquid Download PDFInfo
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- CN104489912A CN104489912A CN201410788600.9A CN201410788600A CN104489912A CN 104489912 A CN104489912 A CN 104489912A CN 201410788600 A CN201410788600 A CN 201410788600A CN 104489912 A CN104489912 A CN 104489912A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/26—Use of organic solvents for extraction
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Abstract
The invention provides a strong-flavor electronic cigarette liquid. The raw materials include, by weight proportion: 1 to 30% of tobacco extracts, 0.5 to 10% of tobacco flavor, 0.5 to 15% of strong-flavor liquor, 0.5 to 10% of taste and flavor regulator, 1 to 15% of deionized water, 1 to 25% of edible glycerol, and the balance of propylene glycol. The cigarette liquid is manufactured by the extracts of strong-flavor liquor cellar tobaccos, the strong-flavor liquor is adopted, the electronic cigarette liquid is provided with unique tobacco flavor and strong cellar liquor flavor. The strong-flavor electronic cigarette liquid with unique tobacco flavor and strong cellar flavor has the advantages that the requirements on taste and flavor by customers can be met better.
Description
Technical field
The present invention relates to electronic cigarette technical field, be specifically related to a kind of Luzhou-flavor tobacco juice for electronic smoke.
Background technology
In recent years, along with promulgation and the enforcement of " Framework Convention on Tobacco Control ", carrying out of global Tobacco Control anti-smoking campaign, the raising of common people's health perception, forms larger impact to the production and selling of traditional cigarette.In order to the demand of the person that meets market and consumption, various dissimilar novel tobacco goods arise at the historic moment, wherein popular with electronic cigarette.
Electronic cigarette is the electronic atomized utensil copying traditional cigarette to be convenient for carrying, and by atomization utensil, the solution mist containing nicotine is changed into particulate, directly sucks human body.Its basic structure is generally made up of battery rod, atomizer and cigarette bullet three part.Electronic cigarette does not in use participate in burning, does not produce tar, carbon monoxide and other harmful substances, does not produce " second-hand-cigarette " yet, do not pollute public's environment, do not have disaster hidden-trouble, have profound significance to public health and environmental protection.
Usual commercially available electronic cigarette smoke agent majority is the dilute solution containing nicotine.Therefore its taste, fragrance can not meet the demand that consumer sucks completely, especially fragrance problem.These problems directly have influence on the quality of electronic cigarette, also govern the development of electronic cigarette simultaneously.Luzhou-flavor tobacco juice for electronic smoke of the present invention is the extract adopting aromatic Chinese spirit wine cellar to store sth. in a cellar tobacco leaf is raw material, and the interpolation of aromatic Chinese spirit makes tobacco juice for electronic smoke not only have this perfume of unique tobacco, has again the aromatic strongly fragrant aroma in cellar for storing things simultaneously.Mouthfeel fragrance conditioning agent compensate for the deficiency of tobacco juice for electronic smoke at mouthfeel and fragrance, effectively improve mouthfeel and the fragrance of existing tobacco juice for electronic smoke, shorten the gap of tobacco juice for electronic smoke in mouthfeel and fragrance and traditional cigarette, meet consumer further to the demand of sucking electronic cigarette.
Summary of the invention
The deficiency of existing tobacco juice for electronic smoke in mouthfeel and fragrance in view of the above, the object of the present invention is to provide a kind of Luzhou-flavor tobacco juice for electronic smoke, the extract that this tobacco juice adopts aromatic Chinese spirit wine cellar to store sth. in a cellar tobacco leaf is raw material, the interpolation of aromatic Chinese spirit makes tobacco juice for electronic smoke not only have this perfume of unique tobacco, has again the aromatic strongly fragrant aroma in cellar for storing things simultaneously.This cigarette perfume (or spice) is given prominence to, store aromatic strongly fragrant Luzhou-flavor tobacco juice for electronic smoke more can satisfy the demands of consumers in mouthfeel and fragrance.
For achieving the above object and other relevant objects, the present invention is by the following technical solutions:
A kind of Luzhou-flavor tobacco juice for electronic smoke, its raw material by mass percentage, comprises following component:
Preferably, described Luzhou-flavor tobacco juice for electronic smoke, its raw material by mass percentage, comprises following component:
Leaf tobacco extract described in the present invention can adopt method conventional in prior art to obtain.
Preferably, described leaf tobacco extract to be selected from cured tobacco leaf extract, burley tobaccos leaf tobacco extract, Oriental Tobacco leaf extract or Sun cured tobacco leaf tobacco extract any one or a few combination.The raw tobacco material preparing described leaf tobacco extract stores sth. in a cellar alcoholization in aromatic Chinese spirit wine cellar.
Preferably, described in store sth. in a cellar alcoholization process and store sth. in a cellar for tobacco leaf is placed in aromatic Chinese spirit wine cellar, the flavor matter of aroma is infiltrated in tobacco leaf equably, the quality making its tobacco leaf more alcohol and.
Preferably, the extracting method of described leaf tobacco extract is: get tobacco leaf, crushed after being dried powdered, is placed in solvent and carries out ultrasonic extraction, through sedimentation, filtration and reduced pressure concentration, i.e. and obtained described leaf tobacco extract.
Preferably, the grinding particle size of described tobacco leaf is 40 ~ 100 orders, is more preferably 40 ~ 60 orders.
Preferably, described ultrasonic extraction process, the mass ratio of tobacco leaf or pipe tobacco powder and solvent is 1:(2 ~ 5); Be more preferably 1:(2.5 ~ 3.5).
Preferably, described solvent is deionized water or ethanol.
Preferably, the temperature of described ultrasonic extraction is 30 ~ 60 DEG C, is more preferably 40 ~ 60 DEG C.
Preferably, the time of described ultrasonic extraction is 2 ~ 5 hours, is more preferably 3.5 ~ 4.5 hours.
Preferably, under 60 ~ 80 DEG C of conditions, described extract reduced pressure concentration is obtained leaf tobacco extract.
The present invention does not have special restriction to the kind of described flavouring essence for tobacco and source, adopts flavouring essence for tobacco well known to those skilled in the art.
Preferably; described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3; 5; 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine, 2; one or more combination in 3,5-trimethylpyrazine.
In an embodiment, those skilled in the art can according to personal like and/or the market demand, and select to add suitable flavouring essence for tobacco, the present invention does not have special restriction to this.
In embodiment in the present invention, preferably, described flavouring essence for tobacco is following several formula (percentage by weight):
Formula one: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Said components is mixed in vortex oscillator.
Formula two: 15% dorinones, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol; Said components is mixed in vortex oscillator.
The present invention does not have special restriction to the kind of described aromatic Chinese spirit and source, adopts brand common on market.Preferably, described aromatic Chinese spirit is selected from any one or the multiple combination in five-Grain Liquor, Luzhou Old Cellar, Jian Nan Chun, Jin Liufu, the indigo plant in sky, Yang He Da Qu, Xiaohutuxian and a small bay in a river board Daqu.
Preferably, described mouthfeel fragrance conditioning agent is selected from: ethyl acetate, 2-methyl isophthalic acid-propyl alcohol, 3-methyl-butanal, 2-methyl-1-butene aldehyde, ethyl propionate, acetal, 2-methvl-propionic acid ethvl ester, ethyl butyrate, ethyl lactate, ethyl 2-methylbutyrate, 3 Methylbutanoic acid ethyl ester, furfuryl alcohol, ethyl valerate, benzaldehyde, ethyl hexanoate, phenmethylol, cognac oil, any one or multiple combination in ethyl caprilate.
Preferably, the formula (percentage by weight) of described mouthfeel fragrance conditioning agent is normal propyl alcohol 1.5 ~ 3.0%, ethyl acetate 5.5 ~ 7.0%, 2-methyl isophthalic acid-propyl alcohol 1.0 ~ 2.0%, 3-methyl-butanal 1.0 ~ 2.0%, 2-methyl-1-butene aldehyde 1.5 ~ 2.5%, ethyl propionate 1.0 ~ 2.5%, acetal 9.0 ~ 14.0%, 2-methvl-propionic acid ethvl ester 0.1 ~ 1.0%, ethyl butyrate 4.0 ~ 5.5%, ethyl lactate 1.0 ~ 2.5%, ethyl 2-methylbutyrate 0.3 ~ 1.5%, 3 Methylbutanoic acid ethyl ester 1.0 ~ 2.0%, furfuryl alcohol 3.5 ~ 5.0%, ethyl valerate 2.0 ~ 3.0%, benzaldehyde 2.0 ~ 3.0%, ethyl hexanoate 15 ~ 20%, phenmethylol 25 ~ 35%, cognac oil 2.0 ~ 3.0%, ethyl caprilate 3.5 ~ 5.0%.
More preferably, described mouthfeel fragrance conditioning agent can be the following stated formula (percentage by weight):
Formula one: normal propyl alcohol 2.0%, ethyl acetate 6.0%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 2.0%, acetal 10.0%, 2-methvl-propionic acid ethvl ester 0.5%, ethyl butyrate 4.5%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.7%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.2%, ethyl valerate 2.5%, benzaldehyde 2.5%, ethyl hexanoate 18.0%, phenmethylol 32.7%, cognac oil 2.5%, ethyl caprilate 4.5%.
Formula two: normal propyl alcohol 2.4%, ethyl acetate 6.5%, 2-methyl isophthalic acid-propyl alcohol 1.4%, 3-methyl-butanal 1.3%, 2-methyl-1-butene aldehyde 2.1%, ethyl propionate 1.9%, acetal 12.0%, 2-methvl-propionic acid ethvl ester 0.6%, ethyl butyrate 4.9%, ethyl lactate 1.3%, ethyl 2-methylbutyrate 0.8%, 3 Methylbutanoic acid ethyl ester 1.6%, furfuryl alcohol 4.3%, ethyl valerate 2.4%, benzaldehyde 2.6%, ethyl hexanoate 17.5%, phenmethylol 29.2%, cognac oil 2.6%, ethyl caprilate 4.6%.
Formula three: normal propyl alcohol 2.2%, ethyl acetate 6.4%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 1.8%, acetal 11.5%, 2-methvl-propionic acid ethvl ester 0.6%, ethyl butyrate 4.7%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.6%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.0%, ethyl valerate 2.2%, benzaldehyde 2.7%, ethyl hexanoate 17.8%, phenmethylol 31.8%, cognac oil 2.3%, ethyl caprilate 4.0%.
Preferably, described propane diols is food grade propane diols.Described food grade propane diols is that market is bought.
The invention also discloses the preparation method of aforementioned Luzhou-flavor tobacco juice for electronic smoke, fully stir and evenly mix and get final product after only each raw material need being mixed in proportion.
The invention also discloses described Luzhou-flavor tobacco juice for electronic smoke and prepare the purposes in electronic cigarette.
As mentioned above, a kind of Luzhou-flavor tobacco juice for electronic smoke provided by the invention, the extract adopting aromatic Chinese spirit wine cellar to store sth. in a cellar tobacco leaf is raw material, the deficiency of tobacco juice for electronic smoke at mouthfeel and fragrance is compensate for by mouthfeel fragrance conditioning agent, and add aromatic Chinese spirit, thus make tobacco juice not only have this perfume of unique tobacco, there is again the aromatic strongly fragrant aroma in cellar for storing things simultaneously.The white wine giving off a strong fragrance of its uniqueness and this fragrant ingenious combination of pure and sweet natural tobacco, make flue gas exquisiteness mellow and full, aftertaste Tianjin is sweet long, can satisfy the demands of consumers on taste and fragrance, improve mouthfeel and the fragrance of existing tobacco juice for electronic smoke, shorten the gap of tobacco juice for electronic smoke in mouthfeel and fragrance and traditional cigarette, meet consumer further to the demand of sucking electronic cigarette.
Detailed description of the invention
The invention provides a kind of Luzhou-flavor tobacco juice for electronic smoke, its raw material by mass percentage, comprises following component: leaf tobacco extract: 1 ~ 30%; Flavouring essence for tobacco: 0.5 ~ 10%; Aromatic Chinese spirit: 0.5 ~ 15%; Mouthfeel fragrance conditioning agent: 0.5 ~ 10%; Deionized water: 1 ~ 15%; Edible glycerol: 1 ~ 25%; Propane diols: surplus.Concrete constituent content is: leaf tobacco extract: 1 ~ 30%; Flavouring essence for tobacco: 0.5 ~ 10%; Aromatic Chinese spirit: 0.5 ~ 15%; Mouthfeel fragrance conditioning agent: 0.5 ~ 10%; Deionized water: 1 ~ 15%; Edible glycerol: 1 ~ 25%; Propane diols: 30 ~ 70%.Preferred scope is: leaf tobacco extract: 8 ~ 20%; Flavouring essence for tobacco: 1.5 ~ 6%; Aromatic Chinese spirit: 5 ~ 10%; Mouthfeel fragrance conditioning agent: 1.5 ~ 6%; Deionized water: 1 ~ 5%; Edible glycerol: 10 ~ 20%; Propane diols: 40 ~ 60%.In an embodiment of the present invention, the mass concentration of described raw material components can be specially certain the concrete numerical value in above-mentioned scope.
The leaf tobacco extract used in the present invention, if flue-cured tobacco, burley tobaccos, Turkish tobaccos or Sun cured tobacco extract are manufacturer's self-control.
Tobacco flavor components is as Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3; 5; 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine, 2,3,5-trimethylpyrazines etc. adopt commercial goods.
Aromatic Chinese spirit such as five-Grain Liquor, Luzhou Old Cellar, Jian Nan Chun, Jin Liufu, the indigo plant in sky, Yang He Da Qu, Xiaohutuxian, a small bay in a river board Daqu etc. all can be commercially.
Various mouthfeel fragrance conditioning agent as normal propyl alcohol, ethyl acetate, 2-methyl isophthalic acid-propyl alcohol, 3-methyl-butanal, 2-methyl-1-butene aldehyde, ethyl propionate, acetal, 2-methvl-propionic acid ethvl ester, ethyl butyrate, ethyl lactate, ethyl 2-methylbutyrate, 3 Methylbutanoic acid ethyl ester, furfuryl alcohol, ethyl valerate, benzaldehyde, ethyl hexanoate, phenmethylol, cognac oil, ethyl caprilate etc. can be commercially.Edible glycerol, propane diols also can be commercially.Deionized water adopts water purification machine self-control.The equipment used in the present invention and reagent needed for other are all commercially available.
Present invention also offers a kind of preparation method of Luzhou-flavor tobacco juice for electronic smoke, first, tobacco leaf is got at the oven drying 3 ± 0.1h of 40 ± 2 DEG C in aromatic Chinese spirit wine cellar, after being cooled to room temperature, grind, after offal screening is 40 ~ 100 orders (preferably 40 ~ 60 orders) with pulverizer, with solvent deionized water or alcohol steep, wherein the mass ratio of tobacco leaf and solvent is 1:2 ~ 1:5 (preferred 1:2.5 ~ 1:3.5).Carry out ultrasonic extraction again, ultrasonic extraction temperature is 30 ~ 60 DEG C (preferably 40 ~ 60 DEG C), and the ultrasonic extraction time is 2 ~ 5h (preferably 3.5 ~ 4.5h).Then, through sedimentation, filtration and reduced pressure concentration, leaf tobacco extract is obtained.
Suitable component is selected to be made into flavouring essence for tobacco.Described flavouring essence for tobacco is selected from: Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3; 5; 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine, 2; any one or two or more mixing in 3,5-trimethylpyrazine etc.
Suitable component is selected to be made into aromatic Chinese spirit.Described aromatic Chinese spirit is selected from any one or multiple combination in five-Grain Liquor, Luzhou Old Cellar, Jian Nan Chun, Jin Liufu, the indigo plant in sky, Yang He Da Qu, Xiaohutuxian, a small bay in a river board Daqu and other aromatic Chinese spirits.
Suitable component is selected to be made into mouthfeel fragrance conditioning agent.Described mouthfeel fragrance conditioning agent is selected from normal propyl alcohol, ethyl acetate, 2-methyl isophthalic acid-propyl alcohol, 3-methyl-butanal, 2-methyl-1-butene aldehyde, ethyl propionate, acetal, 2-methvl-propionic acid ethvl ester, ethyl butyrate, ethyl lactate, ethyl 2-methylbutyrate, 3 Methylbutanoic acid ethyl ester, furfuryl alcohol, ethyl valerate, benzaldehyde, ethyl hexanoate, phenmethylol, cognac oil, in the mouthfeel fragrance conditioning agents such as ethyl caprilate any one or multiplely to mix mutually.
Finally, leaf tobacco extract, flavouring essence for tobacco, mouthfeel fragrance conditioning agent are mixed by above-mentioned mass percent with other component, fully stirs 30 ± 5min, obtain Luzhou-flavor tobacco juice for electronic smoke.
In an embodiment of the present invention, the related data of described preparation method's conditional can specific to the concrete numerical value of certain in the condition and range of said method.
Set forth the present invention further below in conjunction with specific embodiment, should be understood that these embodiments are only not used in for illustration of the present invention and limit the scope of the invention.
Below by way of specific instantiation, embodiments of the present invention are described, those skilled in the art the content disclosed by this description can understand other advantages of the present invention and effect easily.The present invention can also be implemented or be applied by detailed description of the invention different in addition, and the every details in this description also can based on different viewpoints and application, carries out various modification or change not deviating under spirit of the present invention.
In addition should be understood that the one or more method steps mentioned in the present invention do not repel and can also to there is additive method step or can also insert additive method step before and after described combination step between these steps clearly mentioned, except as otherwise noted.
Glycerine described in the embodiment of the present invention, propane diols and flavouring essence for tobacco are commercially available existing food grade product.
Embodiment 1
In the present embodiment, mouthfeel adjustment agent comprises the following composition of percentage by weight: normal propyl alcohol 2.0%, ethyl acetate 6.0%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 2.0%, acetal 10.0%, 2-methvl-propionic acid ethvl ester 0.5%, ethyl butyrate 4.5%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.7%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.2%, ethyl valerate 2.5%, benzaldehyde 2.5%, ethyl hexanoate 18.0%, phenmethylol 32.7%, cognac oil 2.5%, ethyl caprilate 4.5%.
In the present embodiment, the composition of Luzhou-flavor tobacco juice for electronic smoke and each weight percentages of components are: cured tobacco leaf extract 15%, flavouring essence for tobacco 3%, Luzhou Old Cellar 6%, mouthfeel fragrance conditioning agent 3%, deionized water 4%, edible glycerol 10%, surplus is propane diols.Each raw material is mixed according to the above ratio, and in stirred at ambient temperature 30min, each component is fully mixed.
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Embodiment 2
In the present embodiment, mouthfeel fragrance conditioning agent mainly comprises the following composition of percentage by weight: normal propyl alcohol 2.4%, ethyl acetate 6.5%, 2-methyl isophthalic acid-propyl alcohol 1.4%, 3-methyl-butanal 1.3%, 2-methyl-1-butene aldehyde 2.1%, ethyl propionate 1.9%, acetal 12.0%, 2-methvl-propionic acid ethvl ester 0.6%, ethyl butyrate 4.9%, ethyl lactate 1.3%, ethyl 2-methylbutyrate 0.8%, 3 Methylbutanoic acid ethyl ester 1.6%, furfuryl alcohol 4.3%, ethyl valerate 2.4%, benzaldehyde 2.6%, ethyl hexanoate 17.5%, phenmethylol 29.2%, cognac oil 2.6%, ethyl caprilate 4.6%.
In the present embodiment, the composition of Luzhou-flavor tobacco juice for electronic smoke and each weight percentages of components are: Sun cured tobacco leaf tobacco extract 18%, flavouring essence for tobacco 3.5%, golden six good fortune 6.5%, mouthfeel fragrance conditioning agent 3.5%, deionized water 4.5%, edible glycerol 11%, surplus is propane diols.Each raw material is mixed according to the above ratio, and in stirred at ambient temperature 30min, each component is fully mixed.
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Embodiment 3
In the present embodiment, mouthfeel fragrance conditioning agent mainly comprises the following composition of percentage by weight: normal propyl alcohol 2.2%, ethyl acetate 6.4%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 1.8%, acetal 11.5%, 2-methvl-propionic acid ethvl ester 0.6%, ethyl butyrate 4.7%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.6%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.0%, ethyl valerate 2.2%, benzaldehyde 2.7%, ethyl hexanoate 17.8%, phenmethylol 31.8%, cognac oil 2.3%, ethyl caprilate 4.0%.
In the present embodiment, the composition of Luzhou-flavor tobacco juice for electronic smoke and each weight percentages of components are: cured tobacco leaf extract 20%, flavouring essence for tobacco 4%, Jian Nan Chun 7%, mouthfeel fragrance conditioning agent 4.5%, deionized water 5%, edible glycerol 10%, surplus is propane diols.Each raw material is mixed according to the above ratio, and in stirred at ambient temperature 30min, each component is fully mixed.
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Embodiment 4
In the present embodiment, mouthfeel fragrance conditioning agent will comprise the following composition of percentage by weight: normal propyl alcohol 2.0%, ethyl acetate 6.0%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 2.0%, acetal 10.0%, 2-methvl-propionic acid ethvl ester 0.5%, ethyl butyrate 4.5%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.7%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.2%, ethyl valerate 2.5%, benzaldehyde 2.5%, ethyl hexanoate 18.0%, phenmethylol 32.7%, cognac oil 2.5%, ethyl caprilate 4.5%.
In the present embodiment, the composition of Luzhou-flavor tobacco juice for electronic smoke and each weight percentages of components are: cured tobacco leaf extract 1%, flavouring essence for tobacco 10%, a small bay in a river board Daqu 15%, mouthfeel fragrance conditioning agent 0.5%, deionized water 5%, edible glycerol 20%, surplus is propane diols.Each raw material is mixed according to the above ratio, and in stirred at ambient temperature 30min, each component is fully mixed.
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Embodiment 5
In the present embodiment, mouthfeel fragrance conditioning agent mainly comprises the following composition of percentage by weight: normal propyl alcohol 2.4%, ethyl acetate 6.5%, 2-methyl isophthalic acid-propyl alcohol 1.4%, 3-methyl-butanal 1.3%, 2-methyl-1-butene aldehyde 2.1%, ethyl propionate 1.9%, acetal 12.0%, 2-methvl-propionic acid ethvl ester 0.6%, ethyl butyrate 4.9%, ethyl lactate 1.3%, ethyl 2-methylbutyrate 0.8%, 3 Methylbutanoic acid ethyl ester 1.6%, furfuryl alcohol 4.3%, ethyl valerate 2.4%, benzaldehyde 2.6%, ethyl hexanoate 17.5%, phenmethylol 29.2%, cognac oil 2.6%, ethyl caprilate 4.6%.
In the present embodiment, the composition of Luzhou-flavor tobacco juice for electronic smoke and each weight percentages of components are: cured tobacco leaf extract 30%, flavouring essence for tobacco 0.5%, Xiaohutuxian 1%, mouthfeel fragrance conditioning agent 10%, deionized water 1%, edible glycerol 1%, surplus is propane diols.Each raw material is mixed according to the above ratio, and in stirred at ambient temperature 30min, each component is fully mixed.
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Comparative example 1
In the present embodiment, mouthfeel fragrance conditioning agent will comprise the following composition of percentage by weight: normal propyl alcohol 2.0%, ethyl acetate 6.0%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 2.0%, acetal 10.0%, 2-methvl-propionic acid ethvl ester 0.5%, ethyl butyrate 4.5%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.7%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.2%, ethyl valerate 2.5%, benzaldehyde 2.5%, ethyl hexanoate 18.0%, phenmethylol 32.7%, cognac oil 2.5%, ethyl caprilate 4.5%.
In the present embodiment, the composition of Luzhou-flavor tobacco juice for electronic smoke and each weight percentages of components are: cured tobacco leaf extract 15%, flavouring essence for tobacco 3%, mouthfeel fragrance conditioning agent 3%, deionized water 4%, edible glycerol 10%, surplus is propane diols.Each raw material is mixed according to the above ratio, and in stirred at ambient temperature 30min, each component is fully mixed.
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Comparative example 2
In the present embodiment, mouthfeel fragrance conditioning agent will comprise the following composition of percentage by weight: normal propyl alcohol 2.0%, ethyl acetate 6.0%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 2.0%, acetal 10.0%, 2-methvl-propionic acid ethvl ester 0.5%, ethyl butyrate 4.5%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.7%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.2%, ethyl valerate 2.5%, benzaldehyde 2.5%, ethyl hexanoate 18.0%, phenmethylol 32.7%, cognac oil 2.5%, ethyl caprilate 4.5%.
In the present embodiment, the composition of Luzhou-flavor tobacco juice for electronic smoke and each weight percentages of components are: cured tobacco leaf extract 15%, Luzhou Old Cellar 6%, mouthfeel fragrance conditioning agent 3%, deionized water 4%, edible glycerol 10%, surplus is propane diols.Each raw material is mixed according to the above ratio, and in stirred at ambient temperature 30min, each component is fully mixed.
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Comparative example 3
In the present embodiment, mouthfeel fragrance conditioning agent will comprise the following composition of percentage by weight: normal propyl alcohol 2.0%, ethyl acetate 6.0%, 2-methyl isophthalic acid-propyl alcohol 1.5%, 3-methyl-butanal 1.2%, 2-methyl-1-butene aldehyde 2.0%, ethyl propionate 2.0%, acetal 10.0%, 2-methvl-propionic acid ethvl ester 0.5%, ethyl butyrate 4.5%, ethyl lactate 1.2%, ethyl 2-methylbutyrate 0.7%, 3 Methylbutanoic acid ethyl ester 1.5%, furfuryl alcohol 4.2%, ethyl valerate 2.5%, benzaldehyde 2.5%, ethyl hexanoate 18.0%, phenmethylol 32.7%, cognac oil 2.5%, ethyl caprilate 4.5%.
In the present embodiment, the composition of Luzhou-flavor tobacco juice for electronic smoke and each weight percentages of components are: cured tobacco leaf extract 15%, flavouring essence for tobacco 3%, Luzhou Old Cellar 6%, deionized water 4%, edible glycerol 10%, surplus is propane diols.Each raw material is mixed according to the above ratio, and in stirred at ambient temperature 30min, each component is fully mixed.
The tobacco juice for electronic smoke obtained is smoked panel test by the present invention, and result is as shown in table 2, and table 2 is the smoking result of the tobacco juice for electronic smoke that the embodiment of the present invention and comparative example obtain.
Electronic cigarette sensory quality assessment method is adopted to evaluate the sample obtained in embodiment and comparative example.Sensory quality assessment method comprises the following steps:
(1) 9 sensory quality assessment indexs are provided with, comprise excitant, satisfaction, concentration, comfort level, feature style, tobacco perfume, aroma quality, perfume quantity and the amount of being fuming, and give different score value according to the Different Effects degree of every evaluation index to tobacco juice for electronic smoke aesthetic quality.
Described excitant refers to: suck the discomfort that flue gas comprises oral cavity to sense organ, throat and nasal cavity produce that tobacco juice for electronic smoke produces through atomization and be subject to.
Described satisfaction refers to: the flue gas strength that tobacco juice for electronic smoke produces through atomization, concentration and note are to the comprehensive impression that sense organ produces.
Described concentration refers to: the impression of tobacco juice for electronic smoke oral cavity filling degree when the flue gas firm suction inlet that atomization produces.
Described comfort level refers to: the impact of flue gas on oral cavity level of comfort after sucking oral cavity and exhalation that tobacco juice for electronic smoke produces through atomization.
Described feature style refers to: a kind of tobacco juice for electronic smoke is different from the sense organ Main Differences performance of other homogeneous e cigarette tobacco juices in joyful sense.
Described tobacco perfume (or spice) refers to: in process of smokeing panel test, sensory feel is to the breath of this perfume (or spice) of tobacco.
Described aroma quality refers to: felt the good and bad degree of pleasant breath in process of smokeing panel test by sense of smell and the sense of taste.
Described perfume quantity refers to: in process of smokeing panel test by oral cavity and nasal cavity weigh pleasant breath amount number.
The described amount of being fuming refers to: tobacco juice for electronic smoke through atomization produce exhaust gas volumn number.
(2) member of smoking of 9 people is set, everyone a tobacco juice for electronic smoke sensory quality assessment table, adopt the marking mode secretly commented, adopt the overall method of smokeing panel test that circulates, tobacco juice for electronic smoke is aspirated, according to the implication of 9 sensory quality assessment index score values in table 1, adopt hundred-mark system point system to carry out comprehensive grading to the aesthetic quality of tobacco juice for electronic smoke, every evaluation index is by five points, ten point system or the scoring of ten the five-grade marking systems.The concrete meaning of the score value of tobacco juice for electronic smoke evaluation index sees the following form 1.The minimum score unit of score value is 0.5.
Described hundred-mark system point system refers to: 9 sensory quality assessment indexs respectively by five points, very or ten the five-grade marking systems mark, and the score value summation of 9 sensory quality assessment indexs is a percentage.The concrete meaning of the score value of described 9 sensory quality assessment indexs sees the following form 1.
(4) the sensory quality assessment result of member of smoking is added up.By the score value of every sensory quality assessment index of all members of smoking, remove one minimum point and a best result respectively, calculate the mean value of effective score value of every sensory quality assessment index by formula I.The mean value sum of the score value of every sensory quality assessment index is calculated by formula II.
Described formula I is:
In formula:
---the average score value of the effective sense organ quality evaluation index of certain individual event, result retains two-decimal;
---the summation of the score value of the effective sense organ quality evaluation index of certain individual event;
N---total number of persons of effectively smokeing panel test.
Described formula II is:
In formula: S---general comment score value, result retains a decimal;
---the average score value sum of every effective sense organ quality evaluation index.
The score value implication table of table 1 sensory quality assessment index
The tobacco juice for electronic smoke prepared in the tobacco juice for electronic smoke prepared in embodiment 1-5 and comparative example 1-3 is added in electronic cigarette and carries out sensory quality assessment.Concrete evaluation result is in table 2, and in table 2, the scoring of every evaluation index is that the arithmetic average that 9 members of smoking effectively mark is divided.
Table 2 Luzhou-flavor tobacco juice for electronic smoke sensory effects evaluation result
Note: in table, the scoring of every evaluation index is that the arithmetic average that 9 members of smoking effectively mark is divided
Show from the sensory effects evaluation result of table 2, Luzhou-flavor tobacco juice for electronic smoke provided by the invention, cigarette perfume is outstanding, store aromatic strongly fragrant, less to throat irritation, fragrance fragrance, make tobacco juice for electronic smoke not only have this perfume of unique tobacco, there is again the aromatic strongly fragrant aroma in cellar for storing things simultaneously.Luzhou-flavor tobacco juice for electronic smoke provided by the invention, delicate mouthfeel is soft, and wine rhythm cigarette perfume (or spice) makes us enjoying endless aftertastes, and sensory evaluation is effective, is better than the tobacco juice for electronic smoke in comparative example, and mouthfeel and fragrance more can satisfy the demands of consumers.
The above; be only preferred embodiment of the present invention; above-described embodiment is illustrative principle of the present invention and effect thereof only; and not to any formal and substantial restriction of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the inventive method; also can make some improvement and supplement, these improve and supplement and also should be considered as protection scope of the present invention.All those skilled in the art, without departing from the spirit and scope of the present invention, a little change made when utilizing disclosed above technology contents, the equivalent variations of modifying and developing, be Equivalent embodiments of the present invention; Meanwhile, all according to substantial technological of the present invention to the change of any equivalent variations that above-described embodiment is done, modify and differentiation, all still belong in the scope of technical scheme of the present invention.
Claims (10)
1. a Luzhou-flavor tobacco juice for electronic smoke, its raw material by mass percentage, comprises following component:
2. Luzhou-flavor tobacco juice for electronic smoke according to claim 1, is characterized in that, described leaf tobacco extract to be selected from cured tobacco leaf extract, burley tobaccos leaf tobacco extract, Oriental Tobacco leaf extract or Sun cured tobacco leaf tobacco extract any one or a few combination.
3. Luzhou-flavor tobacco juice for electronic smoke according to claim 1, it is characterized in that, the raw tobacco material preparing described leaf tobacco extract stores sth. in a cellar alcoholization in aromatic Chinese spirit wine cellar, and the flavor matter of aroma is infiltrated in tobacco leaf equably, the quality making its tobacco leaf more alcohol and.
4. Luzhou-flavor tobacco juice for electronic smoke according to claim 1, it is characterized in that, the extracting method of described leaf tobacco extract is: get tobacco leaf, crushed after being dried powdered, be placed in solvent and carry out ultrasonic extraction, through sedimentation, filtration and reduced pressure concentration i.e. obtained described leaf tobacco extract.
5. Luzhou-flavor tobacco juice for electronic smoke according to claim 4, is characterized in that, described solvent is deionized water or ethanol.
6. Luzhou-flavor tobacco juice for electronic smoke according to claim 1, it is characterized in that, described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2, 6, 6-trimethyl-2-cyclohexene-1, 4-diketone, 2-hydroxyl-3, 5, 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine, 2, 3, one or more combination in 5-trimethylpyrazine.
7. Luzhou-flavor tobacco juice for electronic smoke according to claim 1, it is characterized in that, described aromatic Chinese spirit is selected from any one or multiple combination in five-Grain Liquor, Luzhou Old Cellar, Jian Nan Chun, Jin Liufu, the indigo plant in sky, Yang He Da Qu, Xiaohutuxian, a small bay in a river board Daqu and other aromatic Chinese spirits.
8. Luzhou-flavor tobacco juice for electronic smoke according to claim 1, is characterized in that, described mouthfeel fragrance conditioning agent is selected from, ethyl acetate, 2-methyl isophthalic acid-propyl alcohol, 3-methyl-butanal, 2-methyl-1-butene aldehyde, ethyl propionate, acetal, 2-methvl-propionic acid ethvl ester, ethyl butyrate, ethyl lactate, ethyl 2-methylbutyrate, 3 Methylbutanoic acid ethyl ester, furfuryl alcohol, ethyl valerate, benzaldehyde, ethyl hexanoate, phenmethylol, cognac oil, any one or multiple combination in ethyl caprilate.
9. the preparation method of Luzhou-flavor tobacco juice for electronic smoke according to the arbitrary claim of claim 1 ~ 8, is characterized in that, after being mixed in proportion by each raw material, fully stir and evenly mix and get final product.
10. according to the arbitrary claim of claim 1 ~ 8, Luzhou-flavor tobacco juice for electronic smoke is preparing the purposes in electronic cigarette.
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Application publication date: 20150408 |