CN104544552A - Electronic cigarette smoke solution prepared through oolong leaf extract - Google Patents
Electronic cigarette smoke solution prepared through oolong leaf extract Download PDFInfo
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- CN104544552A CN104544552A CN201410848686.XA CN201410848686A CN104544552A CN 104544552 A CN104544552 A CN 104544552A CN 201410848686 A CN201410848686 A CN 201410848686A CN 104544552 A CN104544552 A CN 104544552A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/241—Extraction of specific substances
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- A24F47/002—
Abstract
The invention relates to an electronic cigarette smoke solution. The electronic cigarette smoke solution is prepared from the following components in parts by mass: 1 to 30 parts of tobacco extract, 0.5 to 13 parts of tobacco flavor, 1 to 30 parts of oolong leaf extract, 2 to 5 parts of edible alcohol, 5 to 30 parts of edible glycerinum, and 50 to 80 parts of propylene glycol. According to the electronic cigarette smoke solution prepared through the oolong leaf extract, the oolong leaf extract is mixed with the tobacco extract, and the proper tobacco flavor is added, so that the electronic cigarette smoke solution is rich in fragrance, and is good in taste; the disadvantages of insufficient fragrance and taste of the electronic cigarette smoke solution can be improved to some extent; meanwhile, the oolong leaf extract contains a plurality of effective ingredients which bring a healthcare effect to some extent.
Description
Technical field
The present invention relates to electronic cigarette technical field, be specifically related to a kind of tobacco juice for electronic smoke prepared with oolong tea leaf extract.
Background technology
Along with the progressively enforcement of the international Framework Convention on Tobacco Control and the enhancing gradually of health of people consciousness, traditional cigarette selling market is subject to powerful impact.In order to tackle change and the consumer demand in market, the novel tobacco goods of a series of less harmful receive showing great attention to of domestic and international each large tobacco enterprise and extensively study.Wherein, electronic cigarette, as a class staple product in novel tobacco goods, is to contain or not to be atomized into particulate containing nicotine solution, directly to be sucked by consumer.Electronic cigarette generates smog sensation owing to taking atomizing type, does not produce tar and CO, produces second-hand-cigarette harm hardly simultaneously, be regarded as non-harmful smoking cessation product or substitute of tobacco.Particularly showed powerful development trend in European and American developed countries in the last few years, data show world's electronic cigarette gross sales amount over nearly 3 years average annual growth rate up to 40%.Wherein only at American market, within 2013, electronic cigarette gross sales amount is more than 1,000,000,000 dollars, increases nearly one times than 2012.
The market potential that electronic cigarette is huge excites broad interest and the further investigation of each large tobacco enterprises and individuals.Current existing atomization technique can produce good atomizing effect, to electronic cigarette smoker with the impression of swallowing clouds and blowing out fog, but is but barely satisfactory compared with traditional cigarette on mouthfeel, fragrance.Improving the most important thing that electronic cigarette formula of liquid is the research of current electronic cigarette, is the core technology that tobacco enterprise bases oneself upon in electronic cigarette industry and develops.
In order to simulate the fragrance of traditional cigarette, fragrance and mouthfeel to the full extent, solution the most general at present adds tobacco extract in tobacco juice.Tobacco extractive technique mainly comprises the means of different combinations such as steam distillation, solvent extraction, simultaneous distillation method, enzymolysis extraction, supercritical extraction, molecularly distilled and extracts aroma component in tobacco.Tobacco juice for electronic smoke is mixed to get according to a certain ratio by the essential oil of tobaccos and Alevaire, flavouring essence for tobacco that extract acquisition, although but smoking result shows that the tobacco juice obtained by this approach is containing certain this perfume of tobacco, mouthfeel and fragrance enrich degree and also have larger gap compared with traditional cigarette.Trace it to its cause and may be: on the one hand different extraction means extraction efficiency is different, Partial Tobacco aroma component cannot greater efficiency be transferred in extract; On the other hand, tobacco, without combustion process, lacks the fragrance component produced through cracking in extract.In order to make up the deficiency of tobacco extract further, finding a kind of plant with tobacco with similarity, improving through blending, formula, prepare the abundant and obvious tobacco juice for electronic smoke of feature of fragrance.
Tealeaves and tobacco are that present people live the two indispensable large class consumer goods.Both have numerous similarity, as the odor type of tealeaves and tobacco seemingly, the fragrance matter contained in tealeaves is similar to tobacco.Meanwhile, tealeaves special causes perfume (or spice) and health-care components, as catechin, caffeine, abundant mineral matter, vitamin and other active ingredient flavonols, saponin etc. containing self again.Tobacco extract is mixed with into electronic cigarette liquid by a certain percentage with tea extract, not only can supplements the shortcoming of tobacco aroma concentration deficiency, make fragrance component abundanter; The harm simultaneously can alleviating or suppress tobacco to bring containing much active ingredient in tea extraction liquid.It is reported that the application study of Tea Polyphenols in Tea has a lot of aspect, comprise anticancer, anti-oxidant and delay senility, antibacterial and antiviral, reducing blood lipid, lipid-antioxidant activity effect, pigment protective effect, deodorant, anticaries action, the several functions such as suppression atherosclerotic.Tea Polyphenols has become the focus of medicine, the exploitation of food circle.Cigarette is pungent and fragrant, the sweet and delicate fragrance in tea Tianjin, uses together and can bring out the best in each other.
Tea tree is because of differences such as hereditary capacity, growing environment, geographical situation and sweats, and all there is some difference to make chemical composition in tealeaves and content, tea leaf quality and odor type.Oolong Camellia semi-fermented tea, through the carving that completes, withers, shake green grass or young crops, partly ferment, the operation such as to cure after the teas of excellent quality made.Its existing green tea fresh dense, has again the sweet and pure of black tea.Because being green in the middle of its blade, leaf margin takes on a red color, therefore has the title of " greenery red margination ".Oolong tea principal item has the north of Fujian Province narcissus, clovershrub, Chinese cassia tree etc., the south of Fujian Province Iron Guanyin, strange orchid, narcissus, gold osmanthus etc., Guangdong phoenix single fir, phoenix narcissus, ridge head Dan Cong etc.Wherein, the north of Fujian Province oolong tea take Wuyi cliff tea as representative, and the sharp then dense Changqing of fragrance is then deep and remote far away; The south of Fujian Province oolong tea is representative with Iron Guanyin, gives off a strong fragrance lasting, band orchid perfume or fragrance of osmanthus.According to existing, the fragrance component of oolong tea is studied, think nerolidol, jasmine lactone, methyl jasmonate, indoles, 3,7-dimethyl-1,5,7-sarohornene-3-alcohol, linalool and oxide thereof, geraniol, phenmethylol, 2 phenylethyl alcohol, cis-jasmone, jasmone lactone, methyl jasmonate, salicylic acid-3-hexene ester etc. are oolong tea characteristic perfumes.
The present invention extracts the frozen fresh oolong tea of different cultivars by supercritical extract, it is mixed with tobacco extract afterwards, is aided with suitable essence spice for cigarette and Alevaire, can prepare that fragrance enriches, the tobacco juice for electronic smoke of comfortable taste.
Summary of the invention
The object of the present invention is to provide a kind of tobacco juice for electronic smoke, not good to improve existing tobacco juice for electronic smoke mouthfeel, the shortcomings such as fragrance is not enough.
For achieving the above object and other relevant objects, the present invention is by the following technical solutions:
A kind of tobacco juice for electronic smoke, its raw material according to the mass fraction, comprises following component:
Preferably, described a kind of tobacco juice for electronic smoke, its raw material according to the mass fraction, comprises following component:
Most preferred, described a kind of tobacco juice for electronic smoke, its raw material according to the mass fraction, comprises following component:
Preferably, described tobacco extract is that tobacco tobacco leaf is through extracting obtained concentrate.
Further, described tobacco leaf is selected from one or more the combination in Luzhou-flavor flue-cured tobacco, burley tobaccos or Sun cured tobacco.
Preferred, described tobacco leaf is the combination of Luzhou-flavor flue-cured tobacco and burley tobaccos, and the mass ratio of the two is 1:0.9 ~ 1.1.
Tobacco extract described in the present invention can adopt method conventional in prior art to obtain.
Preferably, the extracting method of described tobacco extract, specifically comprises the steps:
(1) get drying tobacco, be cooled to room temperature, pulverize, obtain offal;
(2) get gained offal, add Extraction solvent and soak, extract under uniform temperature, through sedimentation, filtration, concentrate, obtain tobacco extract.
Preferably, in step (1), the temperature of described drying is 30 ~ 80 DEG C, and the dry time is 1 ~ 9h.Preferred, described drying is specifically at 40 DEG C of dry 3h.
Preferably, in step (1), the Average Particle Diameters of described offal is 40 ~ 100 orders; Be more preferably 40 ~ 60 orders.
Preferably, in step (2), described Extraction solvent is deionized water or ethanol.
Preferably, in step (2), the feed liquid mass ratio of offal and Extraction solvent is 1:2 ~ 5; Be more preferably 1:2.5 ~ 3.5; Most preferably be 1:3.
Preferably, in step (2), described in be extracted as ultrasonic extraction; The temperature of described ultrasonic extraction is 30 ~ 60 DEG C; The time of ultrasonic extraction is 2 ~ 5h.Preferred, the temperature of described ultrasonic extraction is 45 ~ 55 DEG C; The time of ultrasonic extraction is 3.5 ~ 4.5h.
Preferably, in step (2), the time of described sedimentation is >=4h.
Preferably, in step (2), described simmer down to reduced pressure concentration.
Further, the temperature of described reduced pressure concentration is 50 ~ 90 DEG C; Be more preferably 60 ~ 80 DEG C.
Preferably; described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3; 5; 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine, 2; combination multiple arbitrarily in 3,5-trimethylpyrazine.
Further, the total content of described flavouring essence for tobacco with percentage by weight shared by flavouring essence for tobacco in described tobacco juice for electronic smoke for benchmark.
Further, described flavouring essence for tobacco is selected from 1-10% Ethyl vanillin, 1-10% benzyl acetate, 1-8% furfural, 4-20% dorinone, 2-15% β-damascone, 10-30% Megastigmatrienone, 2-15% dihydroactinidiolide, 1-8% dimethyl succinate, 1-5%2, 6, 6-trimethyl-2-cyclohexene-1, 4-diketone, 1-5%2-hydroxyl-3, 5, 5-trimethyl-2-cyclonene, 3-15% geranyl acetone, 5-30% alpha, beta-lonone, 3-15% phenmethylol, 2-7% palmitic acid, 1-4% isovaleric acid, 1-4%2-methylvaleric acid, 1-3% indoles, 1-3% pyridine, 1-3%3-acetylpyridine, 1-5%2, 3, any multiple combination in 5-trimethylpyrazine.Above-mentioned tobacco flavor components content with 100% weight percent meter.
Preferred, described flavouring essence for tobacco is following several formula (percentage by weight):
Formula one: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Said components is mixed in vortex oscillator.Above-mentioned tobacco flavor components content with 100% weight percent meter.
Formula two: 15% dorinones, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol.Said components is mixed in vortex oscillator.Above-mentioned tobacco flavor components content with 100% weight percent meter.
Preferably, described oolong tea leaf extract is that frozen fresh oolong tea is through extracting obtained concentrate.
Preferred, described frozen fresh oolong tea is selected from one or more combinations in clovershrub, narcissus, Chinese cassia tree, Iron Guanyin, strange orchid, phoenix narcissus, ridge head list fir, gold osmanthus, the single fir of phoenix.
Most preferred, any one or multiple combination in described frozen fresh oolong tea chosen from Fe kwan-yin, clovershrub, gold osmanthus.
The leaf extract of oolong tea described in the present invention can adopt method conventional in prior art to obtain.
Preferably, the extracting method of described oolong tea leaf extract is: get frozen fresh oolong tea crushed after being dried, then carries out supercritical extract and obtains oolong tea leaf extract.
Preferred, described supercritical extraction method is: get frozen fresh oolong tea crushed after being dried, load in extraction kettle, setting extraction temperature, supercritical solvent is forced into setting pressure by high-pressure plunger pump, controls flow and the extraction time of setting, the supercritical fluid being dissolved with extract after extraction is reduced pressure by choke valve, enter in separating still and become gas, extract is separated out in separating still, is collected in receiving bottle and namely obtains oolong tea leaf extract.
Further, in dry rear tealeaves, moisture weight percentage is less than 20%.Preferred, after dry, in tealeaves, moisture weight percentage is less than 10%;
Further, described oolong tea powder size is 10 ~ 70 orders; Be more preferably 20-30 order; Most preferably be 25 orders.
Further, described supercritical solvent is supercritical CO
2.
Further, described supercritical carbon dioxide extracting pressure is 10 ~ 50MPa; Be more preferably 25MPa.
Preferably, the flow of described supercritical carbon dioxide is 1 ~ 40L/h; Preferred extraction flow is 25L/h.
Preferably, the extraction temperature of described supercritical carbon dioxide is 10 ~ 60 DEG C; Preferred extraction temperature is 45 DEG C.
Preferably, the extraction time of described supercritical carbon dioxide is 1 ~ 10h; Preferred extraction time is 3h.
Preferably, described edible ethanol, edible glycerol, propane diols are market and buy.
Second aspect present invention discloses the preparation method of above-mentioned tobacco juice for electronic smoke, for described each component is mixed by setting number mix and blend and be get final product.
The invention also discloses aforementioned electronic cigarette tobacco juice and prepare the application in electronic cigarette.
Compared with prior art, the present invention has following beneficial effect:
(1) the present invention utilizes supercritical carbon dioxide to extract means and obtains the frozen fresh oolong tea derived essential oil relevant with tobacco leaf, farthest maintains this perfume of oolong tea.
(2) the present invention is by mixing oolong tea extract with tobacco extract, and make tobacco juice for electronic smoke fragrance abundanter, fragrance is coordinated more, to some extent solves the shortcoming of tobacco juice for electronic smoke fragrance and taste deficiency.
(3) tobacco juice for electronic smoke of the present invention generates smog sensation owing to taking atomizing type, does not produce tar and CO, does not produce second-hand-cigarette harm simultaneously.
(4) the present invention is by adding the oolong tea leaf essential oil containing the active ingredient such as Tea Polyphenols, have anticancer, anti-oxidant and delay senility, antibacterial and antiviral, reducing blood lipid, the effect such as lipid-antioxidant activity.
(5) solvent in electronic cigarette liquid provided by the invention and flavouring essence for tobacco are food-grade, harmless to smoker.
Detailed description of the invention
Below by way of specific instantiation, embodiments of the present invention are described, those skilled in the art the content disclosed by this description can understand other advantages of the present invention and effect easily.The present invention can also be implemented or be applied by detailed description of the invention different in addition, and the every details in this description also can based on different viewpoints and application, carries out various modification or change not deviating under spirit of the present invention.
The leaf tobacco extract used in the present invention, if Luzhou-flavor flue-cured tobacco, burley tobaccos, Sun cured tobacco are manufacturer's self-control; Tobacco flavor components also can adopt commercial goods; Frozen fresh oolong tea, edible ethanol, edible glycerol, propane diols also can be commercially.Deionized water is that manufacturer adopts water purification machine self-control.The equipment used in the present invention and reagent needed for other are all commercially available.
In addition should be understood that the one or more method steps mentioned in the present invention do not repel and can also to there is additive method step or can also insert additive method step before and after described combination step between these steps clearly mentioned, except as otherwise noted.
Embodiment 1
The preparation of tobacco extract in the present embodiment: get Luzhou-flavor cured tobacco leaf sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, be crushed to 40 ~ 60 orders.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, afterwards standing sedimentation 4h, sand core funnel filters to get filtrate, and 70 ± 10 DEG C of vacuum rotary steams are concentrated into 3mL, obtain tobacco extract.
In the present embodiment, frozen fresh oolong tea is Tie Guanyin tea, and the extracting method of extra-strong tea leaf extract is: take Iron Guanyin 100g, grinds as 20-30 order powder through pulverizer, load in the extraction kettle of 1L, control extracting pressure is 25MPa, and extraction temperature is 45 DEG C, regulates supercritical CO
2flow be 25L/h, extraction time is 3h.The supercritical fluid being dissolved with extract after extraction is reduced pressure by choke valve, and enter in separating still and become gas, extract is separated out in separating still, is collected in receiving bottle and namely obtains extra-strong tea leaf extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
The composition of the tobacco juice for electronic smoke in the present embodiment and the mass fraction of each component are: tobacco extract 20 parts, flavouring essence for tobacco 9 parts, extra-strong tea leaf extract 18 parts, glycerine 20 parts, edible ethanol 3 parts, propane diols 70 parts.Mix and obtain tobacco juice for electronic smoke 1# by each component vortex oscillator.
The tobacco juice for electronic smoke 1# obtained smokes panel test by the present invention, and result is as shown in table 2.
Embodiment 2
The preparation of tobacco extract in the present embodiment: get burley tobaccos tobacco sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, be crushed to 40 ~ 100 orders.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h, standing sedimentation 4h afterwards under 50 ± 5 DEG C of conditions, sand core funnel filters to get filtrate, and 70 ± 10 DEG C of vacuum rotary steams are concentrated into 3mL, obtain tobacco extract.
In the present embodiment, frozen fresh oolong tea is clovershrub tealeaves, and the extracting method of clovershrub tea extract is: take clovershrub 100g, grinds as 20-30 order powder through pulverizer, load in the extraction kettle of 1L, control extracting pressure is 25MPa, and extraction temperature is 45 DEG C, regulates supercritical CO
2flow be 25L/h, extraction time is 3h.The supercritical fluid being dissolved with extract after extraction is reduced pressure by choke valve, and enter in separating still and become gas, extract is separated out in separating still, is collected in receiving bottle and namely obtains clovershrub tea extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 15% dorinone, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
Composition and each weight percentages of components of the tobacco juice for electronic smoke in the present embodiment are: tobacco extract 15 parts, flavouring essence for tobacco 5 parts, clovershrub tea extract 15 parts, glycerine 25 parts, edible ethanol 4 parts, propane diols 75 parts.Mix and obtain tobacco juice for electronic smoke 2# by each component vortex oscillator.
The tobacco juice for electronic smoke 2# obtained smokes panel test by the present invention, and result is as shown in table 2.
Embodiment 3
Tobacco extract preparation in the present embodiment: get Sun cured tobacco tobacco sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, be crushed to 40 ~ 100 object offals.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, standing sedimentation 4h afterwards, sand core funnel filters to get filtrate, and vacuum rotary steam is concentrated into 3mL, obtains tobacco extract.
In the present embodiment, frozen fresh oolong tea is gold osmanthus, and the extracting method of gold osmanthus tea extract is: take gold osmanthus 100g, grinds as 20-30 order powder through pulverizer, load in the extraction kettle of 1L, control extracting pressure is 25MPa, and extraction temperature is 45 DEG C, regulates supercritical CO
2flow be 25L/h, extraction time is 3h.The supercritical fluid being dissolved with extract after extraction is reduced pressure by choke valve, and enter in separating still and become gas, extract is separated out in separating still, is collected in receiving bottle and namely obtains gold osmanthus tea extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
Composition and each weight percentages of components of the tobacco juice for electronic smoke in the present embodiment are: tobacco extract 10 parts, flavouring essence for tobacco 3 parts, gold osmanthus tea extract 7 parts, glycerine 20 parts, edible ethanol 3 parts, propane diols 65 parts.Mix and obtain tobacco juice for electronic smoke 3# by each component vortex oscillator.
The tobacco juice for electronic smoke 3# obtained smokes panel test by the present invention, and result is as shown in table 2.
Embodiment 4
Tobacco extract preparation in the present embodiment: the Luzhou-flavor flue-cured tobacco and the burley tobaccos tobacco sample dry 3h in 40 DEG C of baking ovens that get 1:1, after being cooled to room temperature, be crushed to 40 ~ 100 object offals.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, standing sedimentation 4h afterwards, sand core funnel filters to get filtrate, and vacuum rotary steam is concentrated into 3mL, obtains tobacco extract.
In the present embodiment, frozen fresh oolong tea is the extracting method of Iron Guanyin, extra-strong tea leaf extract: take Iron Guanyin 100g, grinds as 20-30 order powder through pulverizer, load in the extraction kettle of 1L, control extracting pressure is 25MPa, and extraction temperature is 45 DEG C, regulates supercritical CO
2flow be 25L/h, extraction time is 3h.The supercritical fluid being dissolved with extract after extraction is reduced pressure by choke valve, and enter in separating still and become gas, extract is separated out in separating still, is collected in receiving bottle and namely obtains extra-strong tea leaf extract.
Suitable component is selected to be made into flavouring essence for tobacco again.Described flavouring essence for tobacco mainly comprises: 15% dorinone, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol.Above-mentioned tobacco flavor components content with 100% weight percent meter.Said components is mixed in vortex oscillator.
Composition and each weight percentages of components of the tobacco juice for electronic smoke in the present embodiment are: tobacco extract 10 parts, flavouring essence for tobacco 3 parts, extra-strong tea leaf extract 20 parts, glycerine 10 parts, edible ethanol 2 parts, propane diols 60 parts.Mix and obtain tobacco juice for electronic smoke 4# by each component vortex oscillator.
The tobacco juice for electronic smoke 4# obtained smokes panel test by the present invention, and result is as shown in table 2.
Embodiment 5
Frozen fresh oolong tea in the present embodiment is Iron Guanyin, and composition and each weight percentages of components of tobacco juice for electronic smoke are: tobacco extract 5 parts, flavouring essence for tobacco 3 parts, extra-strong tea leaf extract 10 parts, glycerine 25 parts, edible ethanol 3 parts, propane diols 70 parts.
Wherein tobacco extract and extracting method, tea extract and extracting method, flavouring essence for tobacco are with embodiment 4.
Mix and obtain tobacco juice for electronic smoke 5# by each component vortex oscillator.
The tobacco juice for electronic smoke 5# obtained smokes panel test by the present invention, and result is as shown in table 2.
Comparative example 1
Select the component of the tobacco juice for electronic smoke in embodiment 1 except tea extract in this comparative example, each weight percentages of components is: tobacco extract 20 parts, flavouring essence for tobacco 9 parts, glycerine 20 parts, edible ethanol 3 parts, propane diols 70 parts.
Wherein tobacco extract composition and extracting method, flavouring essence for tobacco formula are with embodiment 1.
Mix and obtain tobacco juice for electronic smoke 1* by each component vortex oscillator.
The tobacco juice for electronic smoke 1* obtained smokes panel test by the present invention, and result is as shown in table 2.
Comparative example 2
Select the component of the tobacco juice for electronic smoke in embodiment 2 except tea extract in this comparative example, each weight percentages of components is: tobacco extract 15 parts, flavouring essence for tobacco 5 parts, glycerine 25 parts, edible ethanol 4 parts, propane diols 75 parts.
Wherein tobacco extract composition and extracting mode, flavouring essence for tobacco formula are with embodiment 2.
Mix and obtain tobacco juice for electronic smoke 2* by each component vortex oscillator.
The tobacco juice for electronic smoke 2* obtained smokes panel test by the present invention, and result is as shown in table 2.
Comparative example 3
Select the component of the tobacco juice for electronic smoke in embodiment 3 except tea extract in this comparative example, each weight percentages of components is: tobacco extract 10 parts, flavouring essence for tobacco 3 parts, glycerine 20 parts, edible ethanol 3 parts, propane diols 65 parts.
Wherein tobacco extract composition and extracting mode, tea extract composition and extracting mode are with embodiment 3.
Mix and obtain tobacco juice for electronic smoke 3* by each component vortex oscillator.
The tobacco juice for electronic smoke 3* obtained smokes panel test by the present invention, and result is as shown in table 2.
Tobacco juice for electronic smoke in above-described embodiment 1-5 and comparative example 1-3 is added in electronic cigarette device and carries out sensory effects evaluation respectively.
Sensory effects evaluation method comprises the following steps:
(1) 9 evaluation indexes are provided with, comprise excitant, satisfaction, concentration, comfort level, feature style, tobacco perfume, aroma quality, perfume quantity and the amount of being fuming, and give different score value according to the Different Effects degree of every evaluation index to tobacco juice for electronic smoke aesthetic quality.
Wherein, described excitant refers to: suck the discomfort that flue gas comprises oral cavity to sense organ, throat and nasal cavity produce that tobacco juice for electronic smoke produces through atomization and be subject to.Described satisfaction refers to: the flue gas strength that tobacco juice for electronic smoke produces through atomization, concentration and note are to the comprehensive impression that sense organ produces.Described concentration refers to: the impression of tobacco juice for electronic smoke oral cavity filling degree when the flue gas firm suction inlet that atomization produces.Described comfort level refers to: the impact of flue gas on oral cavity level of comfort after sucking oral cavity and exhalation that tobacco juice for electronic smoke produces through atomization.Described feature style refers to: a kind of tobacco juice for electronic smoke is different from the sense organ Main Differences performance of other homogeneous e cigarette tobacco juices in joyful sense.Described tobacco perfume (or spice) refers to: in process of smokeing panel test, sensory feel is to the breath of this perfume (or spice) of tobacco.Described aroma quality refers to: felt the good and bad degree of pleasant breath in process of smokeing panel test by sense of smell and the sense of taste.Described perfume quantity refers to: in process of smokeing panel test by oral cavity and nasal cavity weigh pleasant breath amount number.The described amount of being fuming refers to: tobacco juice for electronic smoke through atomization produce exhaust gas volumn number.
(2) member of smoking of 9 people is set, everyone a tobacco juice for electronic smoke sensory quality assessment table, adopt the marking mode secretly commented, adopt the overall method of smokeing panel test that circulates, tobacco juice for electronic smoke is aspirated, according to the implication of 9 sensory quality assessment index score values in table 1, adopt hundred-mark system point system to carry out comprehensive grading to the aesthetic quality of tobacco juice for electronic smoke, every evaluation index is by five points, ten point system or the scoring of ten the five-grade marking systems.
Described hundred-mark system point system refers to: 9 sensory quality assessment indexs respectively by five points, very or ten the five-grade marking systems mark, and the score value summation of 9 sensory quality assessment indexs is a percentage.The concrete meaning of the score value of tobacco juice for electronic smoke evaluation index sees the following form 1.The minimum score unit of score value is 0.5.
The score value implication table of table 1 tobacco juice for electronic smoke sensory quality assessment index
(3) the sensory quality assessment result of member of smoking is added up.By the score value of every sensory quality assessment index of all members of smoking, remove one minimum point and a best result respectively, calculate the mean value of effective score value of every sensory quality assessment index by formula I.The mean value sum of the score value of every sensory quality assessment index is calculated by formula II.
Described formula I is:
In formula:
---the average score value of the effective sense organ quality evaluation index of certain individual event, result retains two-decimal;
---the summation of the score value of the effective sense organ quality evaluation index of certain individual event;
N---total number of persons of effectively smokeing panel test.
Described formula II is:
In formula: S---general comment score value, result retains a decimal;
---the average score value sum of every effective sense organ quality evaluation index.
The tobacco juice for electronic smoke 1*-3* prepared in the tobacco juice for electronic smoke 1#-5# of the tea extract prepared in embodiment 1-5 and comparative example 1-3 is added in electronic cigarette and carries out sensory quality assessment.Concrete evaluation result is in table 2, and in table 2, the scoring of every evaluation index is that the arithmetic average that 9 members of smoking effectively mark is divided.
Table 2 tobacco juice for electronic smoke sensory effects evaluation result
Table 2 result shows, in above-described embodiment, when tobacco juice for electronic smoke is embodied in suction, fog is dense, fragrance abundant, flue gas delicate fragrance, mouthfeel alcohol and, cigarette tea perfume is coordinated, strength is moderate, without obvious irritation.The tea type used, Tobacco Types, extract adding proportion, essence spice for cigarette adding proportion produce Different Effects to adopted 9 indexs; Tea extract used also has effect of health care.
The above; be only preferred embodiment of the present invention; above-described embodiment is illustrative principle of the present invention and effect thereof only; and not to any formal and substantial restriction of the present invention; it should be pointed out that for those skilled in the art, under the prerequisite not departing from the inventive method; also can make some improvement and supplement, these improve and supplement and also should be considered as protection scope of the present invention.All those skilled in the art, without departing from the spirit and scope of the present invention, a little change made when utilizing disclosed above technology contents, the equivalent variations of modifying and developing, be Equivalent embodiments of the present invention; Meanwhile, all according to substantial technological of the present invention to the change of any equivalent variations that above-described embodiment is done, modify and differentiation, all still belong in the scope of technical scheme of the present invention.
Claims (10)
1. a tobacco juice for electronic smoke, its raw material according to the mass fraction, comprises following component:
2. a kind of tobacco juice for electronic smoke according to claim 1, is characterized in that, described tobacco extract is that tobacco tobacco leaf is through extracting obtained concentrate; Described tobacco leaf is selected from one or more the combination in Luzhou-flavor flue-cured tobacco, burley tobaccos or Sun cured tobacco.
3. a kind of tobacco juice for electronic smoke according to claim 2, is characterized in that, the extracting method of described tobacco extract, specifically comprises the steps:
1) get drying tobacco, be cooled to room temperature, pulverize, obtain offal;
2) get gained offal, add Extraction solvent and soak, extract under uniform temperature, through sedimentation, filtration, concentrate, obtain tobacco extract.
4. a kind of tobacco juice for electronic smoke according to claim 3, is characterized in that, described extracting method also to comprise any one of following condition or multinomial:
I) temperature of described drying is 30 ~ 80 DEG C, and the dry time is 1 ~ 9h;
II) Average Particle Diameters of described offal is 40 ~ 100 orders;
III) described Extraction solvent is deionized water or ethanol;
IV) the feed liquid mass ratio of offal and Extraction solvent is 1:2 ~ 5;
V) be extracted as ultrasonic extraction described in, the temperature of described ultrasonic extraction is 30 ~ 60 DEG C, and the time of ultrasonic extraction is 2 ~ 5h;
VI) time of described sedimentation is >=4h;
VII) described simmer down to reduced pressure concentration, the temperature of described reduced pressure concentration is 50 ~ 90 DEG C.
5. a kind of tobacco juice for electronic smoke according to claim 1; it is characterized in that; described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3; 5; 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine, 2; combination multiple arbitrarily in 3,5-trimethylpyrazine.
6. a kind of tobacco juice for electronic smoke according to claim 1, is characterized in that, described oolong tea leaf extract is that frozen fresh oolong tea is through extracting obtained concentrate; Described frozen fresh oolong tea is selected from one or more combinations in clovershrub, narcissus, Chinese cassia tree, Iron Guanyin, strange orchid, phoenix narcissus, ridge head list fir, gold osmanthus, the single fir of phoenix.
7. a kind of tobacco juice for electronic smoke according to claim 6, is characterized in that, the extracting method of described oolong tea leaf extract is: get frozen fresh oolong tea crushed after being dried, then carries out supercritical extract and obtains oolong tea leaf extract.
8. a kind of tobacco juice for electronic smoke according to claim 7, is characterized in that, described extracting method also to comprise any one of following condition or multinomial:
A) dry rear Measuring Moisture Content of Tea percentage by weight is less than 20%;
B) described oolong tea powder size is 10 ~ 70 orders;
C) described Extraction solvent is supercritical CO
2;
D) described supercritical carbon dioxide extracting pressure is 10 ~ 50MPa;
E) flow of described supercritical carbon dioxide is 1 ~ 40L/h;
F) described supercritical carbon dioxide temperature is 10 ~ 60 DEG C;
G) extraction time of described supercritical carbon dioxide is 1 ~ 10h.
9. according to the preparation method of the arbitrary described a kind of tobacco juice for electronic smoke of claim 1 ~ 8, for described each component is mixed by setting number mix and blend and get final product.
10. according to the arbitrary described application of a kind of tobacco juice for electronic smoke in electronic cigarette of claim 1 ~ 8.
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| CN106174683A (en) * | 2016-07-29 | 2016-12-07 | 福建中烟工业有限责任公司 | A kind of compositions and the tobacco juice for electronic smoke containing said composition |
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| CN106037012B (en) * | 2016-07-18 | 2019-03-15 | 福建中烟工业有限责任公司 | A kind of tobacco juice for electronic smoke |
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| CN106174683B (en) * | 2016-07-29 | 2018-05-15 | 福建中烟工业有限责任公司 | A kind of composition and the tobacco juice for electronic smoke containing said composition |
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| CN111205922A (en) * | 2018-11-21 | 2020-05-29 | 广州华芳烟用香精有限公司 | Supercritical extraction process of phoenix Dancong absolute oil |
| CN110200310A (en) * | 2019-03-20 | 2019-09-06 | 福建绿色黄金生物科技有限公司 | It is a kind of for the oolong tea of electronic cigarette and the composition of lemon and its application |
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| CN111671133A (en) * | 2020-06-22 | 2020-09-18 | 福建中烟工业有限责任公司 | Tea-flavored flue-cured tobacco type tobacco flavor electronic cigarette atomized liquid |
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