CN104489908A - Tobacco juice of electronic cigarette - Google Patents
Tobacco juice of electronic cigarette Download PDFInfo
- Publication number
- CN104489908A CN104489908A CN201410789177.4A CN201410789177A CN104489908A CN 104489908 A CN104489908 A CN 104489908A CN 201410789177 A CN201410789177 A CN 201410789177A CN 104489908 A CN104489908 A CN 104489908A
- Authority
- CN
- China
- Prior art keywords
- tobacco
- electronic smoke
- parts
- extract
- tobacco juice
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Classifications
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
-
- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
Abstract
The invention relates to a tobacco juice of an electronic cigarette. The tobacco juice comprises, by weight, 50-80 parts of propylene glycol, 5-30 parts of glycerinum, 2-5 parts of edible alcohol, 1-30 parts of tobacco extracts, 0.5-15 parts of tobacco flavor and 0.5-10 parts of Chinese herb extracts having a liver clearing and vision improving function. The Chinese herb extracts having the liver clearing and vision improving function are mixed with the tobacco extracts, so that the tobacco juice of the electronic cigarette is richer and more harmonious in fragrance and good in satisfaction feeling, the shortcoming of lacking fragrance and taste of the tobacco juice of the electronic cigarette is improved to some extent, and the tobacco juice has the effects of tonifying liver, improving vision and clearing away heat and toxic materials.
Description
Technical field
The present invention relates to a kind of tobacco juice for electronic smoke, belong to electronic cigarette technical field.
Background technology
Traditional cigarette is generally provide nicotine and relevant aroma components by the mode of cigarette of burning to consumer.Because the reasons such as Pintsch process and flue gas migration cause containing a large amount of harmful components in main flume in sucking process, fraction is wherein had to have carcinogenic danger as condensed-nuclei aromatics is proved.Also produce a large amount of flue gas smog in the process of smoking property of cigarette, not only cause environmental pollution, also bring the harm of second-hand-cigarette simultaneously to non-smoker.Along with the progressively enforcement of the international Framework Convention on Tobacco Control and the enhancing gradually of health of people consciousness, traditional cigarette selling market is subject to powerful impact.Electronic cigarette takes atomizing type to generate smog sensation, does not produce tar and CO, produces second-hand-cigarette harm hardly simultaneously, is regarded as non-harmful smoking cessation product or substitute of tobacco, receives showing great attention to and extensively studying of domestic and international each large tobacco enterprise.The selling market of current electronic cigarette is mainly in the U.S., and Europe, Asia then possess good growth trends, and particularly the market of China Electronics's cigarette is also in the cultivation and exploitation stage.The electronic cigarette product taste developed at present is partial to blended type cigarette, compares the taste custom meeting foreign consumers, and Chinese Consumer's preference flue-cured tobacco, taste is comparatively strong, and the mouthfeel of electronic cigarette is difficult to reach requirement.It is the key opening Chinese market that improvement electronic cigarette formula of liquid makes it to meet Chinese Consumer's custom.
Electronic cigarette, as a kind of form in novel tobacco goods, presents great market prospect, and reason is mainly to provide the consumption habit similar with traditional cigarette and satisfaction on the one hand, and the hazard index of electronic cigarette reduces greatly than traditional cigarette on the other hand.Electronic cigarette formula of liquid is the key highlighting electronic cigarette advantage.In order to simulate the fragrance of traditional cigarette, fragrance and mouthfeel to the full extent, solution the most general at present adds tobacco extract in tobacco juice.Tobacco juice for electronic smoke is mixed to get according to a certain ratio by the essential oil of tobaccos and Alevaire, flavouring essence for tobacco that extract acquisition.The less harmful of electronic cigarette is that what to make to suck human body by incombustible mode is atomized liquid and non-burning pyrolysis product.Many Chinese herbal medicine compositions not only have certain characteristic flavor compounds, also have certain health-care effect simultaneously, have even and alleviate some disease effect.Tobacco extract is combined with Chinese herbal medicine extract, not only compensate for the shortcoming of tobacco juice for electronic smoke flavor component deficiency to a certain extent, be different from external tobacco juice for electronic smoke simultaneously, the tobacco juice for electronic smoke of Chinese style characteristic can be built, meet consumer's custom, certain health-care effect is provided simultaneously.
The present invention has the Chinese herbal medicine extract of function of clearing liver and improving vision by preparation, afterwards it is mixed with tobacco extract, be aided with and use suitable essence spice for cigarette to modify, can prepare that fragrance enriches, comfortable taste, satisfaction are got well and there is the tobacco juice for electronic smoke of the health care that necessarily clears liver and improve vision.
Summary of the invention
The object of the present invention is to provide a kind of tobacco juice for electronic smoke, improve existing tobacco juice for electronic smoke mouthfeel not good, the shortcomings such as fragrance is not enough, give the health care that electronic cigarette necessarily clears liver and improve vision simultaneously.
The present invention is achieved by the following technical solutions:
A kind of tobacco juice for electronic smoke, comprises the component of following weight portion: propane diols 50 ~ 80 parts, glycerine 5 ~ 30 parts, edible alcohol 2 ~ 5 parts, tobacco extract 1 ~ 30 part, flavouring essence for tobacco 0.5 ~ 15 part, has the Chinese herbal medicine extract 0.5 ~ 10 part of effect of clearing liver and improving vision.
Preferably, described a kind of tobacco juice for electronic smoke, comprises the component of following weight portion: propane diols 65 ~ 80 parts, glycerine 10 ~ 25 parts, edible alcohol 2 ~ 4 parts, tobacco extract 10 ~ 20 parts, flavouring essence for tobacco 1 ~ 5 part, has the Chinese herbal medicine extract 1 ~ 5 part of effect of clearing liver and improving vision.
Optimum, described a kind of tobacco juice for electronic smoke, comprises the component of following weight portion: propane diols 70 parts, glycerine 20 parts, edible alcohol 3 parts, tobacco extract 15 parts, flavouring essence for tobacco 3 parts, has the Chinese herbal medicine extract 3 parts of effect of clearing liver and improving vision.
Described Chinese herbal medicine extract is chrysanthemum, the root of herbaceous peony, keel, rhizoma Gastrodiae, the shell of seaear, mother-of-pearl, concha mauritiae, tribulus terrestris, bluish dogbane, peppermint, cicada slough, fructus viticis, mulberry leaf, the bark of ash, selfheal, dandelion, seed of feather cockscomb, butterflybush flower, scouring rush, cassia seed, the bark of ash, the seed of Chinese dodder, semen astragali complanati, the fruit of glossy privet, radix bupleuri, the dried rhizome of rehmannia, cultivated land, Radix Angelicae Sinensis, the root of large-flowered skullcap, the Radix Astragali, ginseng, the bighead atractylodes rhizome, the capsule of weeping forsythia, indigo naturalis, umbellate pore furgus, pseudo-ginseng, the red sage root, root tuber of aromatic turmeric, semen astragali complanati, the fruit of Chinese magnoliavine, coix seed, the fruit of Chinese wolfberry, Semen Lablab Album, felwort, stringy stonecrop, oldenlandia diffusa or other there is the one or more combination of clearing liver and improving vision in the Chinese herbal medicine of effect through extracting obtained concentrate.
Preferably, the extracting method of described Chinese herbal medicine extract, for: get Chinese herbal medicine raw material, crushed after being dried powdered, add hot reflux after solvent soaking, be then separated and remove filter residue, and the liquid of acquisition is carried out centrifugal treating, afterwards by the supernatant membrane filtration of centrifugal acquisition, finally by the filtrate reduced in volume of membrane filtration and get final product.
Preferably, the powder size after described pulverizing is 40 ~ 100 orders, is more preferably 40 ~ 60 orders.
Preferably, described solvent is the aqueous solution of ethanol, and volumetric concentration is 40% ~ 80%.
Preferably, during immersion, the mass ratio of described Chinese herbal medicine powder and described solvent is 1:2 ~ 5, shakes up, and sealing, soaks 8 ~ 12 hours; Preferred, the mass ratio of described Chinese herbal medicine powder and described solvent is 1:2.5 ~ 3.5.
Preferably, the time adding hot reflux described in is 1 ~ 5 hour; Be more preferably 2.5 ~ 3.5 hours.
Preferably, described centrifugal rotating speed is 2500 ~ 4000r/min, centrifugal 10 ~ 30min; More preferably at 4000r/min, centrifugal 20min.
Preferably, the specification of the filter sizes of described membrane filtration is 0.45 μm.
Preferably, described simmer down to is under 50 ~ 90 DEG C of conditions, and decompression is revolved and desolventized to obtain Chinese herbal medicine extract; More preferably concentrated at 60 ~ 80 DEG C.
Described tobacco extract is selected from the tobacco leaf of flue-cured tobacco, air-curing of tobacco leaves and suncured tabacco or pipe tobacco through extracting obtained extract; Described air-curing of tobacco leaves comprises burley tobaccos, Maryland; Described suncured tabacco comprises Turkish tobaccos, Dark sun-cured, Sun cured tobacco and Nicotiniana rustica.
Preferably, described tobacco extract to be mass ratio the be flue-cured tobacco of 1:0.9-1.1 and the tobacco leaf of burley tobaccos or pipe tobacco are through extracting obtained concentrate.
The extracting method of described tobacco extract, for: get tobacco leaf or pipe tobacco, crushed after being dried powdered, be placed in solvent and carry out ultrasonic extraction, through sedimentation, filtration and reduced pressure concentration i.e. obtained described tobacco extract.
Preferably, the grinding particle size of described tobacco leaf or pipe tobacco is 40 ~ 100 orders, is more preferably 40 ~ 60 orders.
Preferably, described ultrasonic extraction process, the mass ratio of tobacco leaf or pipe tobacco powder and solvent is 1:2 ~ 5; Be more preferably 1:2.5 ~ 3.5.
Preferably, described solvent is deionized water or ethanol.
Preferably, the temperature of described ultrasonic extraction is 30 ~ 60 DEG C, is more preferably 40 ~ 60 DEG C.
Preferably, the time of described ultrasonic extraction is 2 ~ 5 hours, is more preferably 3.5 ~ 4.5 hours.
Preferably, under 50 ~ 90 DEG C of conditions, decompression is revolved and is desolventized to obtain tobacco extract, and more excellent is 60 ~ 80 DEG C.
Preferably; described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3,5,5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine and 2; 3,5-trimethylpyrazine.
Preferably, with the total weight of flavouring essence for tobacco, described flavouring essence for tobacco is selected from the component of following weight percent: 1 ~ 10% Ethyl vanillin, 1 ~ 10% benzyl acetate, 1 ~ 8% furfural, 4 ~ 20% dorinones, 2 ~ 15% β-damascone, 10 ~ 30% Megastigmatrienones, 2 ~ 15% dihydroactinidiolides, 1 ~ 8% dimethyl succinate, 1 ~ 5%2, 6, 6-trimethyl-2-cyclohexene-1, 4-diketone, 1 ~ 5%2-hydroxyl-3, 5, 5-trimethyl-2-cyclonene, 3 ~ 15% geranyl acetones, 5 ~ 30% alpha, beta-lonones, 3 ~ 15% phenmethylols, 2 ~ 7% palmitic acids, 1 ~ 4% isovaleric acid, 1 ~ 4%2-methylvaleric acid, 1 ~ 3% indoles, 1 ~ 3% pyridine, 1 ~ 5%3-acetylpyridine and 1 ~ 5%2, 3, combination multiple arbitrarily in 5-trimethylpyrazine, and to meet summation be 100wt%.
Preferably, described flavouring essence for tobacco is following several formula (percentage by weight):
Formula one: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Said components is mixed in vortex oscillator.
Formula two: 15% dorinones, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol; Said components is mixed in vortex oscillator.
Formula three: 15% dorinones, 30% Megastigmatrienone, 5%2,3,5-trimethylpyrazines, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 12% phenmethylol.
Formula four: 30% Megastigmatrienones, 5% benzyl acetate, 6% furfural, 8% Ethyl vanillin, 7% palmitic acid, 3%2,3,5-trimethylpyrazines, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 15% phenmethylol.
Formula five: 15% dorinones, 30% Megastigmatrienone, 5%2,3,5-trimethylpyrazines, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% alpha, beta-lonone, 12% phenmethylol.
Preferably, described glycerine and propane diols are food grade product.
The preparation of electronic cigarette liquid of the present invention, for both obtaining described each component mix and blend mixing.
The Chinese herbal medicine extract with function of clearing liver and improving vision provided by the present invention, is mixed to get tobacco juice for electronic smoke with tobacco extract, flavouring essence for tobacco, propane diols, glycerine etc.Compared with prior art, the present invention has following beneficial effect:
(1) the present invention is by mixing the Chinese herbal medicine extract with function of clearing liver and improving vision with tobacco extract, make tobacco juice for electronic smoke fragrance abundanter, fragrance is coordinated more, and satisfaction is good, improves the shortcoming of tobacco juice for electronic smoke fragrance and taste deficiency to a certain extent.
(2) tobacco juice for electronic smoke of the present invention generates smog sensation owing to taking atomizing type, does not produce tar and CO, does not produce second-hand-cigarette harm simultaneously.
(3) action and efficacy such as the present invention is by adding containing the Chinese herbal medicine extract with effect of clearing liver and improving vision, and has the clear order of tonifying liver, clearing heat and detoxicating.
Detailed description of the invention
Below by way of specific instantiation, technical scheme of the present invention is described.Should be understood that one or more method steps that the present invention mentions do not repel and before and after described combination step, also to there is additive method step or can also insert additive method step between these steps clearly mentioned; Should also be understood that these embodiments are only not used in for illustration of the present invention to limit the scope of the invention.And, except as otherwise noted, the numbering of various method steps is only the convenient tool differentiating various method steps, but not be ordering or the enforceable scope of restriction the present invention of restriction various method steps, the change of its relativeness or adjustment, when changing technology contents without essence, when being also considered as the enforceable category of the present invention.
Embodiment 1: prepare a kind of tobacco juice for electronic smoke
The preparation of tobacco extract: get cured tobacco leaf sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, be crushed to 40 ~ 100 orders.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, afterwards standing sedimentation 4h, sand core funnel filters to get filtrate, and 70 ± 10 DEG C of vacuum rotary steams are concentrated into 3mL, obtain tobacco extract.
The preparation of Chinese herbal medicine extract: take chrysanthemum 100g, root of large-flowered skullcap 50g, mulberry leaf 50g, cassia seed 75g, selfheal 50g, tribulus terrestris 50g and felwort 100g, grind as mixing after 40-100 order powder through pulverizer, add 80% ethanol/water mixed solvent, controlling feed liquid weight ratio is 1:3, shake up, sealing, soaks 12 hours.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract is in the centrifugal 20min of 4000r/min, and supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 14mL, obtains Chinese herbal medicine extract.
With flavouring essence for tobacco total weight, the present embodiment flavouring essence for tobacco formula is: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
Prepared by tobacco juice for electronic smoke, get the component of following weight portion: tobacco extract 5 parts, flavouring essence for tobacco 10 parts, there is the Chinese herbal medicine extract 5 parts of effect of clearing liver and improving vision, glycerine 30 parts, edible alcohol 2 parts, propane diols 60 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Embodiment 2: prepare a kind of tobacco juice for electronic smoke
The preparation of tobacco extract: get burley tobaccos tobacco sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, be crushed to 40 ~ 100 orders.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h, standing sedimentation 4h afterwards under 50 ± 5 DEG C of conditions, sand core funnel filters to get filtrate, and 70 ± 10 DEG C of vacuum rotary steams are concentrated into 3mL, obtain tobacco extract.
Prepared by Chinese herbal medicine extract: take chrysanthemum 100g, root of large-flowered skullcap 50g, mulberry leaf 50g, cassia seed 75g, selfheal 50g, fruit of Chinese wolfberry 50g, felwort 100g and dried rhizome of rehmannia 50g, grind as mixing after 40-100 order powder through pulverizer, add 80% ethanol/water mixed solvent, controlling feed liquid weight ratio is 1:3, shake up, sealing, soaks 12h.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract is in the centrifugal 20min of 4000r/min, and supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 16mL, obtains Chinese herbal medicine extract.
With flavouring essence for tobacco total weight, the present embodiment flavouring essence for tobacco formula is: 15% dorinone, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
Prepare tobacco juice for electronic smoke, get the component of following weight portion: tobacco extract 20 parts, flavouring essence for tobacco 5 parts, there is the Chinese herbal medicine extract 10 parts of effect of clearing liver and improving vision, glycerine 10 parts, edible alcohol 5 parts, propane diols 80 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Embodiment 3: prepare a kind of tobacco juice for electronic smoke
Prepared by tobacco extract: get Sun cured tobacco tobacco sample, extract, extracting method is with embodiment 1.
Prepared by Chinese herbal medicine extract: take chrysanthemum 100g, root of large-flowered skullcap 50g, mulberry leaf 50g, cassia seed 75g, selfheal 50g, tribulus terrestris 50g, felwort 100g and fruit of glossy privet 50g, through pulverizer grind be 40 ~ 100 order powder after mix, add 80% ethanol/water mixed solvent, controlling feed liquid weight ratio is 1:3, shake up, sealing, soaks 10h.By soaked vlil 3h, be separated liquid and the dregs of a decoction after extraction, extract is in the centrifugal 20min of 4000r/min, and supernatant 0.45 μm of membrane filtration, control temperature is 70 ± 10 DEG C, and vacuum rotary steam is concentrated into 16mL, obtains Chinese herbal medicine extract.
With flavouring essence for tobacco total weight, the present embodiment flavouring essence for tobacco formula is: 15% dorinone, 30% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 12% phenmethylol.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
Prepare tobacco juice for electronic smoke, following components in mass portion number meter batching: tobacco extract 1 part, flavouring essence for tobacco 3 parts, there is the Chinese herbal medicine extract 1 part of effect of clearing liver and improving vision, glycerine 5 parts, edible alcohol 2 parts, propane diols 50 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Embodiment 4: prepare a kind of tobacco juice for electronic smoke
Prepared by tobacco extract: get flue-cured tobacco and the mixing of burley tobaccos tobacco leaf that mass ratio is 1:1, then extract obtained tobacco extract according to the mode of embodiment 1.
Prepared by Chinese herbal medicine extract: claim chrysanthemum 100g, fruit of Chinese wolfberry 200g, mulberry leaf 50g, dandelion 100g, by the extracting method of embodiment 1, obtains Chinese herbal medicine extract.
With flavouring essence for tobacco total weight, the present embodiment flavouring essence for tobacco formula is: 30% Megastigmatrienone, 5% benzyl acetate, 6% furfural, 8% Ethyl vanillin, 7% palmitic acid, 3%2,3,5-trimethylpyrazine, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 15% phenmethylol.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
Prepare tobacco juice for electronic smoke, following components in mass portion number meter batching: tobacco extract 15 parts, flavouring essence for tobacco 3 parts, there is the Chinese herbal medicine extract 3 parts of effect of clearing liver and improving vision, glycerine 20 parts, edible alcohol 3 parts, propane diols 70 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Embodiment 5: prepare a kind of tobacco juice for electronic smoke
Prepared by tobacco extract: the pipe tobacco mixing of getting flue-cured tobacco that mass ratio is 1:1 and burley tobaccos, then extracts obtained tobacco extract according to the mode of embodiment 1.
Prepared by Chinese herbal medicine extract: get chrysanthemum 100g, root of large-flowered skullcap 50g, mulberry leaf 50g, cassia seed 75g, selfheal 50g, tribulus terrestris 50g and felwort 100g, by the extracting method of embodiment 1, obtains Chinese herbal medicine extract.
With flavouring essence for tobacco total weight, the present embodiment flavouring essence for tobacco formula is: 15% dorinone, 30% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% alpha, beta-lonone, 12% phenmethylol.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
Prepare tobacco juice for electronic smoke, get the component of following weight portion: tobacco extract 10 parts, flavouring essence for tobacco 3 parts, there is effect Chinese herbal medicine extract 1 part that clears liver and improve vision, glycerine 20 parts, edible alcohol 3 parts, propane diols 70 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Comparative example 1 (not containing Chinese herbal medicine extract)
Prepared by tobacco juice for electronic smoke, get following parts by weight of component: tobacco extract 15 parts, flavouring essence for tobacco 3 parts, glycerine 20 parts, edible alcohol 3 parts, propane diols 70 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke;
Wherein tobacco extract composition and extracting mode, flavouring essence for tobacco formula are with embodiment 1;
Comparative example 2 (not containing Chinese herbal medicine extract)
Prepared by tobacco juice for electronic smoke, get following parts by weight of component: tobacco extract 15 parts, flavouring essence for tobacco 3 parts, glycerine 20 parts, edible alcohol 3 parts, propane diols 70 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke;
Wherein tobacco extract composition and extracting mode, flavouring essence for tobacco formula are with embodiment 4;
Comparative example 3 (not containing flavouring essence for tobacco)
Prepared by tobacco juice for electronic smoke, get following parts by weight of component: tobacco extract 15 parts, have the Chinese herbal medicine extract 3 parts of effect of clearing liver and improving vision, glycerine 20 parts, edible alcohol 3 parts, propane diols 70 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke;
Tobacco extract composition and extracting method, Chinese herbal medicine extract composition and extracting method thereof are with embodiment 4.
Tobacco juice for electronic smoke liquid in above-described embodiment and comparative example is added in electronic cigarette device and carries out sensory effects evaluation respectively.
Sensory effects evaluation method comprises the following steps:
(1) 9 indexs are provided with, comprise excitant, satisfaction, concentration, comfort level, feature style, tobacco perfume, aroma quality, perfume quantity and the amount of being fuming, and give different score value according to the Different Effects degree of indices to tobacco juice for electronic smoke aesthetic quality.
Excitant: suck the discomfort that flue gas comprises oral cavity to sense organ, throat and nasal cavity produce that tobacco juice for electronic smoke produces through atomization and be subject to.
Satisfaction: the flue gas strength that tobacco juice for electronic smoke produces through atomization, concentration and note are to the comprehensive impression that sense organ produces.
Concentration: the impression of tobacco juice for electronic smoke oral cavity filling degree when the flue gas firm suction inlet that atomization produces.
Comfort level: the impact of flue gas on oral cavity level of comfort after sucking oral cavity and exhalation that tobacco juice for electronic smoke produces through atomization.
Feature style: a kind of tobacco juice for electronic smoke is different from the sense organ Main Differences performance of other homogeneous e cigarette tobacco juices in joyful sense.
Tobacco is fragrant: in process of smokeing panel test, sensory feel is to the breath of this perfume (or spice) of tobacco.
Aroma quality: felt the good and bad degree of pleasant breath in process of smokeing panel test by sense of smell and the sense of taste.
Perfume quantity: in process of smokeing panel test by oral cavity and nasal cavity weigh pleasant breath amount number.
The amount of being fuming: tobacco juice for electronic smoke through atomization produce exhaust gas volumn number.
(2) member of smoking of 9 people is set, everyone a tobacco juice for electronic smoke sensory quality assessment table, adopt the marking mode secretly commented, adopt the overall method of smokeing panel test that circulates, tobacco juice for electronic smoke is aspirated, according to the implication of 9 sensory quality assessment index score values in table 1, adopt hundred-mark system point system to carry out comprehensive grading to the aesthetic quality of tobacco juice for electronic smoke, every evaluation index is by five points, ten point system or the scoring of ten the five-grade marking systems.The concrete meaning of the score value of tobacco juice for electronic smoke evaluation index sees the following form 1:
The score value implication table of table 1 tobacco juice for electronic smoke sensory quality assessment index
(3) evaluation method: according to the evaluation index in table 1 and score value, member of smoking tackles each evaluation index and carries out sensory quality assessment, and records its evaluation result, and the minimum score unit of score value is 0.5.
(4) result statistics: remove minimum point and a best result in the sensory quality assessment result of all members of smoking, calculate the arithmetic mean of instantaneous value of remaining effective single item evaluation index scoring, result retains two-decimal, the sensory quality assessment comprehensive grading of last tobacco juice for electronic smoke is the arithmetic mean of instantaneous value sum calculating the scoring of each single index, obtain total score, result retains a decimal.
The tobacco juice for electronic smoke prepared in the tobacco juice for electronic smoke with function of clearing liver and improving vision prepared in embodiment 1-5 and comparative example 1-3 is added in electronic cigarette and carries out sensory quality assessment.Concrete evaluation result is in table 2, and in table 2, the scoring of every evaluation index is that the arithmetic average that 9 members of smoking effectively mark is divided.
Table 2 tobacco juice for electronic smoke sensory effects evaluation result
Table 2 result shows, the amount of being fuming abundance when tobacco juice for electronic smoke is embodied in suction in above-described embodiment, and fragrance enriches strong, tobacco and faint medicine perfume are coordinated, and strength is moderate, comfortable taste, without obvious irritation and dry sensation, shorten the aesthetic quality's difference with traditional cigarette.But the difference of the Chinese herbal medicine kind used, Tobacco Types, extract adding proportion, essence spice for cigarette adding proportion, can produce Different Effects to investigated 9 indexs; The action and efficacy such as Chinese herbal medicine extract used can provide tonifying liver clear order simultaneously, clearing heat and detoxicating.
Claims (10)
1. a tobacco juice for electronic smoke, comprises the component of following weight portion: propane diols 50 ~ 80 parts, glycerine 5 ~ 30 parts, edible alcohol 2 ~ 5 parts, tobacco extract 1 ~ 30 part, flavouring essence for tobacco 0.5 ~ 15 part, has the Chinese herbal medicine extract 0.5 ~ 10 part of effect of clearing liver and improving vision.
2. a kind of tobacco juice for electronic smoke as claimed in claim 1, is characterized in that, described tobacco extract is selected from the tobacco leaf of flue-cured tobacco, air-curing of tobacco leaves and suncured tabacco or pipe tobacco through extracting obtained concentrate.
3. a kind of tobacco juice for electronic smoke as claimed in claim 2, is characterized in that, described air-curing of tobacco leaves comprises burley tobaccos, Maryland; Described suncured tabacco comprises Turkish tobaccos, Dark sun-cured, Sun cured tobacco and Nicotiniana rustica.
4. a kind of tobacco juice for electronic smoke as claimed in claim 2, is characterized in that, the extracting method of described tobacco extract is: get tobacco leaf or pipe tobacco, crushed after being dried powdered, be placed in solvent and carry out ultrasonic extraction, through sedimentation, filtration, reduced pressure concentration i.e. obtained described tobacco extract.
5. a kind of tobacco juice for electronic smoke as claimed in claim 4, is characterized in that, described extracting method also to comprise any one of following characteristics or multinomial:
(1) grinding particle size of described tobacco leaf or pipe tobacco is 40 ~ 100 orders;
(2) described ultrasonic extraction process, the mass ratio of tobacco leaf or pipe tobacco powder and solvent is 1:2 ~ 5;
(3) described solvent is deionized water or ethanol;
(4) temperature of described ultrasonic extraction is 30 ~ 60 DEG C;
(5) time of described ultrasonic extraction is 2 ~ 5 hours;
(6) under 50-90 DEG C of condition, described filtrate decompression is revolved and desolventizes to obtain tobacco extract.
6. a kind of tobacco juice for electronic smoke as claimed in claim 1, it is characterized in that, described Chinese herbal medicine extract is chrysanthemum, the root of herbaceous peony, keel, rhizoma Gastrodiae, the shell of seaear, mother-of-pearl, concha mauritiae, tribulus terrestris, bluish dogbane, peppermint, cicada slough, fructus viticis, mulberry leaf, the bark of ash, selfheal, dandelion, seed of feather cockscomb, butterflybush flower, scouring rush, cassia seed, the bark of ash, the seed of Chinese dodder, semen astragali complanati, the fruit of glossy privet, radix bupleuri, the dried rhizome of rehmannia, cultivated land, Radix Angelicae Sinensis, the root of large-flowered skullcap, the Radix Astragali, ginseng, the bighead atractylodes rhizome, the capsule of weeping forsythia, indigo naturalis, umbellate pore furgus, pseudo-ginseng, the red sage root, root tuber of aromatic turmeric, semen astragali complanati, the fruit of Chinese magnoliavine, coix seed, the fruit of Chinese wolfberry, Semen Lablab Album, felwort, one or more in stringy stonecrop or oldenlandia diffusa are through extracting obtained concentrate.
7. a kind of tobacco juice for electronic smoke as claimed in claim 6, it is characterized in that, the extracting method of described Chinese herbal medicine extract is: get Chinese herbal medicine raw material, crushed after being dried powdered, add hot reflux after solvent soaking, be then separated and remove filter residue, and the liquid of acquisition is carried out centrifugal treating, afterwards the supernatant of centrifugal acquisition is carried out membrane filtration, the filtrate of last membrane filtration concentrates and get final product.
8. a kind of tobacco juice for electronic smoke as claimed in claim 7, is characterized in that, described extracting method also comprises any one or multinomial in following characteristics:
(1) powder size after described pulverizing is 40 ~ 100 orders;
(2) described solvent is the aqueous solution of ethanol, and volumetric concentration is 40% ~ 80%;
(3) when soaking, the mass ratio of described Chinese herbal medicine powder and described solvent is 1:2 ~ 5, shakes up, and sealing, soaks 8 ~ 12 hours;
(4) time adding hot reflux described in is 1 ~ 5 hour;
(5) described centrifugal rotating speed is 2500 ~ 4000r/min, centrifugal 10 ~ 30min;
(6) specification of the filter sizes of described membrane filtration is 0.45 μm;
(7) described simmer down to is under 50 ~ 90 DEG C of conditions, and decompression is revolved and desolventized to obtain Chinese herbal medicine extract.
9. a kind of tobacco juice for electronic smoke as claimed in claim 1; it is characterized in that; described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3; 5; 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine and 2; 3,5-trimethylpyrazine.
10. according to the preparation method of the arbitrary described tobacco juice for electronic smoke of claim 1 ~ 9, for described each component mix and blend mixing was both obtained.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410789177.4A CN104489908A (en) | 2014-12-17 | 2014-12-17 | Tobacco juice of electronic cigarette |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201410789177.4A CN104489908A (en) | 2014-12-17 | 2014-12-17 | Tobacco juice of electronic cigarette |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN104489908A true CN104489908A (en) | 2015-04-08 |
Family
ID=52931441
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201410789177.4A Pending CN104489908A (en) | 2014-12-17 | 2014-12-17 | Tobacco juice of electronic cigarette |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN104489908A (en) |
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105029700A (en) * | 2015-06-17 | 2015-11-11 | 云南中烟工业有限责任公司 | Plant composite glycerol triacetate extract and application thereof in cigarettes |
| CN105029679A (en) * | 2015-06-09 | 2015-11-11 | 柳州市智融科技有限公司 | Filler for electronic cigarettes |
| CN105167168A (en) * | 2015-06-09 | 2015-12-23 | 柳州市智融科技有限公司 | Formula of filler for electronic cigarette |
| CN105410987A (en) * | 2015-12-17 | 2016-03-23 | 立场电子科技发展（上海）有限公司 | Nicotine liquid containing salvia miltiorrhiza extracts and preparing method of nicotine liquid |
| CN105520189A (en) * | 2015-12-30 | 2016-04-27 | 立场电子科技发展（上海）有限公司 | Method for preparing tobacco juice of electronic cigarettes by adopting Zimbabwean tobacco extract |
| CN106723300A (en) * | 2016-12-08 | 2017-05-31 | 深圳市华加生物科技有限公司 | Electronics tobacco tar perfume base and electronics tobacco tar |
| CN107090356A (en) * | 2017-04-27 | 2017-08-25 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl American Ginseng essence and its application in cigarette |
| CN107692318A (en) * | 2017-10-13 | 2018-02-16 | 上海烟草集团有限责任公司 | A kind of tobacco juice for electronic smoke and preparation method |
| CN108720130A (en) * | 2018-06-08 | 2018-11-02 | 邓超权 | A kind of production method for the mask for helping to give up smoking |
| CN110432536A (en) * | 2019-06-25 | 2019-11-12 | 内蒙古昆明卷烟有限责任公司 | A kind of fragrant and sweet type heating of sauce is not burnt tobacco product and preparation method thereof |
| CN110558601A (en) * | 2019-09-03 | 2019-12-13 | 深圳雾芯科技有限公司 | Electronic cigarette liquid |
| WO2021042269A1 (en) * | 2019-09-03 | 2021-03-11 | 深圳雾芯科技有限公司 | E-cigarette liquid |
| CN112956728A (en) * | 2021-03-10 | 2021-06-15 | 深圳市真味生物科技有限公司 | Electronic atomized liquid based on female warmth and preparation method thereof |
| CN113662235A (en) * | 2021-08-23 | 2021-11-19 | 深圳市真味生物科技有限公司 | Spine-reducing smooth electronic atomized liquid and preparation method thereof |
Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1994159A (en) * | 2006-12-15 | 2007-07-11 | 姜志荣 | Kidney-strengthening mind-refreshing tobacco liquid for electronic atomized cigarette |
| WO2008130813A1 (en) * | 2007-04-23 | 2008-10-30 | Sottera, Inc. | Improved electronic evaporable substance delivery device and method |
| KR20100028182A (en) * | 2008-09-04 | 2010-03-12 | 고정현 | Nicotine composition |
| EP2422633A1 (en) * | 2010-08-20 | 2012-02-29 | Magic Herbal S.A.R.L. | An electronic atomization hookah |
| CN102960852A (en) * | 2012-11-14 | 2013-03-13 | 湖北中烟工业有限责任公司 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
| WO2014089283A2 (en) * | 2012-12-05 | 2014-06-12 | Vire, L.L.C. | Electronic cigarette or inhaler |
| CN103989244A (en) * | 2014-06-06 | 2014-08-20 | 山东中烟工业有限责任公司 | Chinese style flue-cured tobacco odor type electronic cigarette tobacco juice capable of improving smoking satisfaction sense |
| CN104026731A (en) * | 2014-07-01 | 2014-09-10 | 安徽中烟工业有限责任公司 | Heart nourishing and nerve soothing functional electronic cigarette juice |
| CN104068467A (en) * | 2014-07-01 | 2014-10-01 | 安徽中烟工业有限责任公司 | Electronic cigarette liquid rich in plant flavone |
-
2014
- 2014-12-17 CN CN201410789177.4A patent/CN104489908A/en active Pending
Patent Citations (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1994159A (en) * | 2006-12-15 | 2007-07-11 | 姜志荣 | Kidney-strengthening mind-refreshing tobacco liquid for electronic atomized cigarette |
| WO2008130813A1 (en) * | 2007-04-23 | 2008-10-30 | Sottera, Inc. | Improved electronic evaporable substance delivery device and method |
| KR20100028182A (en) * | 2008-09-04 | 2010-03-12 | 고정현 | Nicotine composition |
| EP2422633A1 (en) * | 2010-08-20 | 2012-02-29 | Magic Herbal S.A.R.L. | An electronic atomization hookah |
| CN102960852A (en) * | 2012-11-14 | 2013-03-13 | 湖北中烟工业有限责任公司 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
| WO2014089283A2 (en) * | 2012-12-05 | 2014-06-12 | Vire, L.L.C. | Electronic cigarette or inhaler |
| CN103989244A (en) * | 2014-06-06 | 2014-08-20 | 山东中烟工业有限责任公司 | Chinese style flue-cured tobacco odor type electronic cigarette tobacco juice capable of improving smoking satisfaction sense |
| CN104026731A (en) * | 2014-07-01 | 2014-09-10 | 安徽中烟工业有限责任公司 | Heart nourishing and nerve soothing functional electronic cigarette juice |
| CN104068467A (en) * | 2014-07-01 | 2014-10-01 | 安徽中烟工业有限责任公司 | Electronic cigarette liquid rich in plant flavone |
Cited By (16)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105029679A (en) * | 2015-06-09 | 2015-11-11 | 柳州市智融科技有限公司 | Filler for electronic cigarettes |
| CN105167168A (en) * | 2015-06-09 | 2015-12-23 | 柳州市智融科技有限公司 | Formula of filler for electronic cigarette |
| CN105029700A (en) * | 2015-06-17 | 2015-11-11 | 云南中烟工业有限责任公司 | Plant composite glycerol triacetate extract and application thereof in cigarettes |
| CN105410987A (en) * | 2015-12-17 | 2016-03-23 | 立场电子科技发展（上海）有限公司 | Nicotine liquid containing salvia miltiorrhiza extracts and preparing method of nicotine liquid |
| CN105520189A (en) * | 2015-12-30 | 2016-04-27 | 立场电子科技发展（上海）有限公司 | Method for preparing tobacco juice of electronic cigarettes by adopting Zimbabwean tobacco extract |
| CN106723300A (en) * | 2016-12-08 | 2017-05-31 | 深圳市华加生物科技有限公司 | Electronics tobacco tar perfume base and electronics tobacco tar |
| CN107090356A (en) * | 2017-04-27 | 2017-08-25 | 河南中烟工业有限责任公司 | A kind of cigarette quick-fried pearl American Ginseng essence and its application in cigarette |
| CN107692318A (en) * | 2017-10-13 | 2018-02-16 | 上海烟草集团有限责任公司 | A kind of tobacco juice for electronic smoke and preparation method |
| CN108720130A (en) * | 2018-06-08 | 2018-11-02 | 邓超权 | A kind of production method for the mask for helping to give up smoking |
| CN108720130B (en) * | 2018-06-08 | 2021-04-16 | 邓超权 | Method for manufacturing mask beneficial to smoking cessation |
| CN110432536A (en) * | 2019-06-25 | 2019-11-12 | 内蒙古昆明卷烟有限责任公司 | A kind of fragrant and sweet type heating of sauce is not burnt tobacco product and preparation method thereof |
| CN110432536B (en) * | 2019-06-25 | 2021-10-29 | 内蒙古昆明卷烟有限责任公司 | Sweet and fragrant sauce type heating non-combustion tobacco product and preparation method thereof |
| CN110558601A (en) * | 2019-09-03 | 2019-12-13 | 深圳雾芯科技有限公司 | Electronic cigarette liquid |
| WO2021042269A1 (en) * | 2019-09-03 | 2021-03-11 | 深圳雾芯科技有限公司 | E-cigarette liquid |
| CN112956728A (en) * | 2021-03-10 | 2021-06-15 | 深圳市真味生物科技有限公司 | Electronic atomized liquid based on female warmth and preparation method thereof |
| CN113662235A (en) * | 2021-08-23 | 2021-11-19 | 深圳市真味生物科技有限公司 | Spine-reducing smooth electronic atomized liquid and preparation method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN104489908A (en) | Tobacco juice of electronic cigarette | |
| CN104489911A (en) | Tobacco juice of electronic cigarette | |
| CN104489904A (en) | E-cigarette nicotine liquid with functions of relieving cough and reducing sputum | |
| CN104544545A (en) | Electronic cigarette smoke solution with blood pressure decreasing function | |
| CN104544555A (en) | Electronic cigarette smoke solution with blood sugar decreasing function | |
| CN104489902A (en) | E-cigarette nicotine liquid with function of immunity improving | |
| CN104770863B (en) | Electronic cigarette liquid with herbal tea flavor and application thereof | |
| CN104585863B (en) | A kind of tobacco juice for electronic smoke | |
| CN103989245B (en) | The Chinese style flue-cured tobacco odor type tobacco juice for electronic smoke of the sweet soapy feeling in a kind of effective reduction oral cavity | |
| CN103989244B (en) | A kind of Chinese style tobacco juice for electronic smoke and preparation method thereof | |
| CN104489913A (en) | E-cigarette nicotine liquid with functions of heat clearing and fire removing | |
| CN104544554A (en) | Electronic cigarette smoke solution with blood fat decreasing function | |
| CN104839885B (en) | A kind of electronic cigarette liquid and preparation method thereof of improvement | |
| CN104489903A (en) | E-cigarette nicotine liquid with function of tranquilizing by nourishing the heart | |
| CN103070472A (en) | Electronic cigarette liquid capable of effectively improving sensory quality of electronic cigarette | |
| CN104544546A (en) | Electronic cigarette smoke solution with appetite improving and digestion prompting functions | |
| CN104544549A (en) | Electronic cigarette smoke solution prepared through green tea leaf extract | |
| CN104544552A (en) | Electronic cigarette smoke solution prepared through oolong leaf extract | |
| CN104544543A (en) | Electronic cigarette smoke solution prepared through black tea leaf extract | |
| CN103070473A (en) | Electronic cigarette tobacco juice prepared from faint scent tobacco leaves | |
| CN105343203A (en) | Tobacco tar of electronic cigarette and preparation method of tobacco tar | |
| CN110419765A (en) | A kind of preparation method and preparation facilities of electronic cigarette tobacco tar | |
| CN102090712B (en) | Method for preparing coarse extract of peanut shell total flavones and application thereof in cigarettes | |
| CN103113989A (en) | Tobacco essence capable of improving cigarette taste and aroma | |
| CN106307602A (en) | Electronic cigarette liquid for freshening breath |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| SE01 | Entry into force of request for substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| RJ01 | Rejection of invention patent application after publication |
Application publication date: 20150408 |
|
| RJ01 | Rejection of invention patent application after publication |