CN103989244B - A kind of Chinese style tobacco juice for electronic smoke and preparation method thereof - Google Patents

A kind of Chinese style tobacco juice for electronic smoke and preparation method thereof Download PDF

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CN103989244B
CN103989244B CN201410249859.6A CN201410249859A CN103989244B CN 103989244 B CN103989244 B CN 103989244B CN 201410249859 A CN201410249859 A CN 201410249859A CN 103989244 B CN103989244 B CN 103989244B
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tobacco
glycerine
extract
electronic smoke
essence
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CN201410249859.6A
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Chinese (zh)
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CN103989244A (en
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刘仕民
周仕禄
王钧
刘晓芊
刘伟
郑宏伟
张新龙
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山东中烟工业有限责任公司
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Abstract

The invention discloses a kind of tobacco juice for electronic smoke, it is made up of the raw material of following mass percent: tobacco extract 5 10%, tobacco aromatics 2 4%, flavouring essence for tobacco 1 3%, flavoring essence 2 6%, natural nicotine 1 2%, natural plant extraction elite 1 4%, two glycerine 30 85%, one or more in balance of propane diols, glycerine, alcohol, butanediol, triethylene glycol;Wherein natural plant extraction elite is agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Long Ye, leaf of negundo chastetree (1~3) in mass ratio: (1~2): (1~2): (1~2): (1~2): (1~2) mixes, through supercritical CO2The extract being obtained by extraction.Also disclosing the preparation method of this tobacco juice for electronic smoke, the tobacco juice for electronic smoke of the present invention contains Chinese style flue-cured tobacco extract and essence spice for cigarette composition, is closer to traditional Chinese flue-cured tobacco flavor types cigarette, improves suction satisfaction in terms of fragrance, mouthfeel.

Description

A kind of Chinese style tobacco juice for electronic smoke and preparation method thereof

Technical field

The present invention relates to a kind of Chinese style tobacco juice for electronic smoke and preparation method thereof, belong to electronic cigarette technical field.

Background technology

With progressively the implementing of " Framework Convention on Tobacco Control ", the whole world development of Tobacco Control campaign and State Bureau's lowering harm and decreasing coking Carry forward vigorously, healthy degree of concern is improved by people day by day, makes cigarette living environment just increasingly serious.In order to meet difference Consumer demand, the product of various simulation cigarette continues to bring out, wherein universal with electronic cigarette, and in the world Particularly American-European countries obtains and is widely recognized as and achieves great development, and people have generally had more science and objectively to electronic cigarette Judging, the progress of self of electronic cigarette product is also being accelerated and is being promoted this industry towards optimum and healthy direction progress.But, city Now sell tobacco juice for electronic smoke on field, mostly there is sweet sense in sucking rear oral cavity overweight, give the very uncomfortable sensation of people's one, and Tobacco flavor is too weak, it is impossible to meets the domestic consumer that get used to aspirate Chinese style flue-cured tobacco odor type cigarette, seriously constrains electronics The development of cigarette.

Two glycerine have another name called contracting two glycerine, are a kind of yellow viscous liquid, and the easy moisture absorption is dissolved in water and ethanol, does not dissolves in ether, It is currently mainly used as emulsifying agent, defoamer and replaces glycerine to be used for stamp, but not yet having the report being applied to tobacco juice for electronic smoke Road.

Content of the invention

It is an object of the invention to provide application in tobacco juice for electronic smoke preparation for two glycerine.

It is a further object of the present invention to provide a kind of tobacco juice for electronic smoke utilizing two glycerine to prepare.

For achieving the above object, the present invention adopts the following technical scheme that

Application in tobacco juice for electronic smoke preparation for two glycerine, in tobacco juice for electronic smoke, the mass percent of two glycerine is 30-85%;

A kind of tobacco juice for electronic smoke utilizing two glycerine to prepare, is made up of the raw material of following mass percent:

Tobacco extract 5-10%, tobacco aromatics 2-4%, flavouring essence for tobacco 1-3%, flavoring essence 2-6%, natural nicotine 1-2%, sky Right plant extraction elite 1-4%, two glycerine 30-85%, in balance of propane diols, glycerine, alcohol, butanediol, triethylene glycol Plant or several;

Wherein, tobacco extract is selected from Yunnan tobacco extract, Tobacco In Guangxi extract or Hubei tobacco extract;

Natural plant extraction elite is agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Long Ye, leaf of negundo chastetree (1~3) in mass ratio: (1~2): (1~2): (1~2): (1~2): (1~2) mixes, through supercritical CO2The extract being obtained by extraction;

Agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Long Ye, leaf of negundo chastetree are the product that " Chinese Pharmacopoeia " (version in 2010) is recorded Kind, its quality all meets the requirement under each kind item.

Preferably, this tobacco juice for electronic smoke is made up of the raw material of following mass percent:

Tobacco extract 6-8%, tobacco aromatics 2-4%, flavouring essence for tobacco 1-3%, flavoring essence 3-5%, natural nicotine 1-2%, sky Right plant extraction elite 2-4%, two glycerine 50-80%, in balance of propane diols, glycerine, alcohol, butanediol, triethylene glycol Plant or several;

The preparation method of this tobacco juice for electronic smoke, comprises the following steps:

(1) preparation of tobacco extract: by drying tobacco, pulverizes, the water of addition 8-10 times amount, ultrasonic extraction 30-60 minute, Filtering, filtrate reduced in volume to relative density is 1.05-1.10 (50 DEG C of survey), obtains tobacco extract;

(2) preparation of natural plant extraction elite: by mass parts weigh agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Long Ye and Leaf of negundo chastetree, pulverizes, and crosses 80-100 mesh sieve, through supercritical CO2Extraction, extracting pressure is 20-25MPa, CO2Flow is 20-30L/h, Extraction time is 1-2h, and entrainer is 95% ethanol;

(3) by tobacco extract, tobacco aromatics, flavouring essence for tobacco, flavoring essence, natural nicotine, natural plant extraction elite, One or more in two glycerine, and propane diols, glycerine, alcohol, butanediol, triethylene glycol, add in mass ratio, mix, Obtain.

The beneficial effects of the present invention is:

(1) tobacco juice for electronic smoke of the present invention is using two glycerine as solvent, and during suction, in oral cavity, sweet sense substantially reduces, comfort More preferably;

(2) tobacco juice for electronic smoke of the present invention contains Chinese style flue-cured tobacco extract and essence spice for cigarette composition, in terms of fragrance, mouthfeel It is closer to traditional Chinese flue-cured tobacco flavor types cigarette, improve suction satisfaction.

(3) tobacco juice for electronic smoke of the present invention contains natural plant extraction elite, wherein, agalloch eaglewood: fragrant odour, has promoting the circulation of qi and stops Bitterly, warming middle energizer to arrest vomiting, effect that gas of receiving is relievingd asthma;Santal: smell delicate fragrance;In promoting the circulation of qi temperature, being used for cold obstruction causing qi stagnation, chest diaphragm does not relaxes; Bee saage: fragrant odour;Acute turpinia leaf: fragrant odour, has clearing heat and detoxicating, effect of reducing pharyngeal swelling;Long Ye: gas is micro-, There is the effect moistening the lung and relieve the cough;Leaf of negundo chastetree: fragrant odour, has and eliminates the phlegm, cough-relieving, the effect relievingd asthma;Above-mentioned 6 taste medicines have mostly Have the smell of natural aromatic, add aroma quality and the perfume quantity of tobacco juice, but also have moisten the lung and relieve the cough, eliminating phlegm and relieving asthma, profit pharynx Effect of detumescence, while smoking, also acts certain medical care effect.

Detailed description of the invention

The present invention is further illustrated in conjunction with the embodiments, it should explanation, the description below merely to explain the present invention, Not its content is defined.

Embodiment 1:

A kind of tobacco juice for electronic smoke utilizing two glycerine to prepare, is made up of the raw material of following mass percent:

Yunnan tobacco extract 8%, tobacco aromatics 3%, flavouring essence for tobacco 2%, flavoring essence 4%, natural nicotine 1.5%, natural plant Thing extracts elite 3%, and two glycerine 50%, balance of propane diols, glycerine, alcohol, butanediol, triethylene glycol are miscible with equal-volume Mixed liquor;

Wherein, natural plant extraction elite is agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Long Ye, leaf of negundo chastetree in mass ratio 2: 1.5:1.5:1.5:1.5:1.5 mixes, through supercritical CO2The extract being obtained by extraction;

The fragrance-enhancing tobacco material (QY021) that tobacco aromatics provides for Shanghai Qi Yuan essence and flavoring agent Co., Ltd;

Flavouring essence for tobacco is the fragrance-enhancing tobacco material (BD010) that Shenzhen BoDun spice Co., Ltd produces;

Flavoring essence is the heterocyclic material that Wutong Aroma Chemicals Co., Ltd. produces;

The purity of natural nicotine is more than 98%.

The preparation method of this tobacco juice for electronic smoke is:

(1) preparation of tobacco extract: dry, pulverize Yunnan tobacco, takes 30g Yunnan tobacco powder, adds the water of 240ml, Ultrasonic extraction 40 minutes, filters, and filtrate reduced in volume to relative density is 1.05-1.10 (50 DEG C of survey), obtains tobacco extract;

(2) preparation of natural plant extraction elite: weigh agalloch eaglewood 20g, santal 15g, banksia rose 15g, acute turpinia leaf 15g, dragon Leaf 15g and leaf of negundo chastetree 15g, pulverizes, and crosses 100 mesh sieves, through supercritical CO2Extraction, extracting pressure is 25MPa, CO2Flow is 20L/h, Extraction time is 1.5h, and entrainer is 95% ethanol;

(3) by tobacco extract, natural plant extraction elite, tobacco aromatics, flavouring essence for tobacco, flavoring essence, natural nicotine, Two glycerine and propane diols, glycerine, alcohol, butanediol, triethylene glycol mixed liquor, add in mass ratio, mixes, to obtain final product.

Embodiment 2:

A kind of tobacco juice for electronic smoke utilizing two glycerine to prepare, is made up of the raw material of following mass percent:

Tobacco In Guangxi extract 5%, tobacco aromatics 4%, flavouring essence for tobacco 1%, flavoring essence 6%, natural nicotine 1%, natural plant Thing extracts elite 4%, two glycerine 30%, balance of propane diols, the mixed liquor of triethylene glycol;

Wherein, natural plant extraction elite is agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Long Ye, leaf of negundo chastetree in mass ratio 3: 1:2:1:2:1 mixes, through supercritical CO2The extract being obtained by extraction;

The source of tobacco aromatics, flavouring essence for tobacco, flavoring essence and natural nicotine is with embodiment 1.

The preparation method of this tobacco juice for electronic smoke is:

(1) preparation of tobacco extract: dry, pulverize Yunnan tobacco, takes 30g Guangxi tobacco leaf powder, adds the water of 270ml, Ultrasonic extraction 30 minutes, filters, and filtrate reduced in volume to relative density is 1.05-1.10 (50 DEG C of survey), obtains tobacco extract;

(2) preparation of natural plant extraction elite: weigh agalloch eaglewood 30g, santal 10g, banksia rose 20g, acute turpinia leaf 10g, dragon Leaf 20g and leaf of negundo chastetree 10g pulverizes, and crosses 80 mesh sieves, through supercritical CO2Extraction, extracting pressure is 20MPa, CO2Flow is 30L/h, Extraction time is 2h, and entrainer is 95% ethanol;

(3) by tobacco extract, natural plant extraction elite, tobacco aromatics, flavouring essence for tobacco, flavoring essence, natural nicotine, Two glycerine and the mixed liquor of propane diols, triethylene glycol, add in mass ratio, mixes, to obtain final product.

Embodiment 3:

A kind of tobacco juice for electronic smoke utilizing two glycerine to prepare, is made up of the raw material of following mass percent:

Hubei tobacco extract 10%, tobacco aromatics 2%, flavouring essence for tobacco 3%, flavoring essence 2%, natural nicotine 2%, natural plant Thing extracts elite 1%, two glycerine 65%, balance of triethylene glycol;

Wherein, natural plant extraction elite is agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Long Ye, leaf of negundo chastetree in mass ratio 2: 2:1:2:1:2 mixes, through supercritical CO2The extract being obtained by extraction;

The source of tobacco aromatics, flavouring essence for tobacco, flavoring essence and natural nicotine is with embodiment 1.

The preparation method of this tobacco juice for electronic smoke is:

(1) preparation of tobacco extract: dry, pulverize Hubei tobacco leaf, takes 30g Yunnan tobacco powder, adds the water of 300ml, Ultrasonic extraction 45 minutes, filters, and filtrate reduced in volume to relative density is 1.05-1.10 (50 DEG C of survey), obtains tobacco extract;

(2) preparation of natural plant extraction elite: weigh agalloch eaglewood 20g, santal 20g, banksia rose 10g, acute turpinia leaf 20g, dragon Leaf 10g and leaf of negundo chastetree 20g, pulverizes, and crosses 100 mesh sieves, through supercritical CO2Extraction, extracting pressure is 25MPa, CO2Flow is 25L/h, Extraction time is 1h, and entrainer is 95% ethanol;

(3) by tobacco extract, natural plant extraction elite, tobacco aromatics, flavouring essence for tobacco, flavoring essence, natural nicotine, Two glycerine and triethylene glycol, add in mass ratio, mixes, to obtain final product.

Embodiment 4:

A kind of tobacco juice for electronic smoke utilizing two glycerine to prepare, is made up of the raw material of following mass percent:

Yunnan tobacco extract 5%, tobacco aromatics 2%, flavouring essence for tobacco 1%, flavoring essence 2%, natural nicotine 1%, natural plant Thing extracts elite 1%, two glycerine 85%, balance of propane diols;

Wherein, natural plant extraction elite is agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Long Ye, leaf of negundo chastetree in mass ratio 2: 1:1:1:1:1 mixes, through supercritical CO2The extract being obtained by extraction;

The source of tobacco aromatics, flavouring essence for tobacco, flavoring essence and natural nicotine is with embodiment 1.

The preparation method of this tobacco juice for electronic smoke is:

(1) preparation of tobacco extract: dry, pulverize Yunnan tobacco, takes 30g Yunnan tobacco powder, adds the water of 300ml, Ultrasonic extraction 45 minutes, filters, and filtrate reduced in volume to relative density is 1.05-1.10 (50 DEG C of survey), obtains tobacco extract;

(2) preparation of natural plant extraction elite: weigh agalloch eaglewood 20g, santal 10g, banksia rose 10g, acute turpinia leaf 10g, dragon Leaf 10g and leaf of negundo chastetree 10g, pulverizes, and crosses 100 mesh sieves, through supercritical CO2Extraction, extracting pressure is 25MPa, CO2Flow is 25L/h, Extraction time is 1h, and entrainer is 95% ethanol;

(3) by tobacco extract, natural plant extraction elite, tobacco aromatics, flavouring essence for tobacco, flavoring essence, natural nicotine, Two glycerine and propane diols, add in mass ratio, mixes, to obtain final product.

Embodiment 5:

A kind of tobacco juice for electronic smoke utilizing two glycerine to prepare, is made up of the raw material of following mass percent:

Yunnan tobacco extract 6%, tobacco aromatics 3%, flavouring essence for tobacco 1%, flavoring essence 2%, natural nicotine 1.5%, natural plant Thing extracts elite 3%, two glycerine 80%, balance of butanediol;

Wherein, natural plant extraction elite is agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Long Ye, leaf of negundo chastetree in mass ratio 2: 1.5:2:1.5:2:1.5 mixes, through supercritical CO2The extract being obtained by extraction;

The source of tobacco aromatics, flavouring essence for tobacco, flavoring essence and natural nicotine is with embodiment 1.

The preparation method of this tobacco juice for electronic smoke is:

(1) preparation of tobacco extract: dry, pulverize Yunnan tobacco, takes 30g Yunnan tobacco powder, adds the water of 300ml, Ultrasonic extraction 45 minutes, filters, and filtrate reduced in volume to relative density is 1.05-1.10 (50 DEG C of survey), obtains tobacco extract;

(2) preparation of natural plant extraction elite: weigh agalloch eaglewood 20g, santal 15g, banksia rose 20g, acute turpinia leaf 15g, dragon Leaf 20g and leaf of negundo chastetree 15g, pulverizes, and crosses 100 mesh sieves, through supercritical CO2Extraction, extracting pressure is 25MPa, CO2Flow is 25L/h, Extraction time is 1h, and entrainer is 95% ethanol;

(3) by tobacco extract, natural plant extraction elite, tobacco aromatics, flavouring essence for tobacco, flavoring essence, natural nicotine, Two glycerine and butanediol, add in mass ratio, mixes, to obtain final product.

Embodiment 6:

Sensory quality assessment is tested:

(1) experiment material: the embodiment of the present invention the 1st, the 2nd, the 3rd, the 4th, 5 preparation tobacco juice for electronic smoke as sample.

(2) electronic cigarette sensory quality assessment standard:

Set with reference to patent " a kind of tobacco juice for electronic smoke utilizing strong-flavor tobacco leaf to prepare " (number of patent application: 201310030063.7) Putting 7 assessment items, the maximum scale of each assessment item is 9 points, and each assessment item is all divided into scoring unit with 1, tool Body is shown in Table 1.

Table 1 electronic cigarette sensory quality assessment standard

(3) evaluation method: provide sample and sensory quality assessment standard scale to the expert that smokes panel test, by form requirement, indices is entered Row is smoked panel test.

(4) result statistics: the smoking result of all experts that smoke panel test is all effective, and the individual event smoking result of the expert that respectively smokes panel test is asked arithmetic Mean value, result retains to 1 decimal, and the arithmetic mean of instantaneous value to each individual event adds and obtains total score, the results are shown in Table 2.

Table 2 sensory quality assessment result

Sample Aroma quality Perfume quantity Sweet sense Excitant Miscellaneous gas Strength Pleasant impression Add up to Embodiment 1 7.6 7.5 7.7 7.8 7.6 7.9 7.6 53.7 Embodiment 2 7.4 7.6 7.4 7.4 7.8 7.6 7.5 52.7 Embodiment 3 7.5 7.4 7.6 7.6 7.5 8.0 7.6 53.2 Embodiment 4 7.3 7.2 7.4 7.6 7.6 7.2 7.2 51.5 Embodiment 5 7.4 7.2 7.5 7.4 7.3 7.8 7.6 52.2

Above-described embodiment is the present invention preferably embodiment, but embodiments of the present invention being not restricted to the described embodiments, One of ordinary skill in the art should be understood that, on the basis of technical scheme, those skilled in the art do not need to pay wound The property made work can make various modification or deformation still within protection scope of the present invention.

Claims (7)

1. a tobacco juice for electronic smoke, it is characterised in that be made up of the raw material of following mass percent:
Tobacco extract 5-10%, tobacco aromatics 2-4%, flavouring essence for tobacco 1-3%, flavoring essence 2-6%, natural nicotine 1-2%, natural plant Thing extracts elite 1-4%, two glycerine 30-85%, one or more in balance of propane diols, glycerine, alcohol, butanediol, triethylene glycol;
Wherein, tobacco extract is selected from Yunnan tobacco extract, Tobacco In Guangxi extract or Hubei tobacco extract, is by drying tobacco, Pulverizing, adding the water of 8-10 times amount, ultrasonic extraction 30-60 minute, filter, filtrate reduced in volume to relative density is 1.05-1.10, The extract obtaining;
Natural plant extraction elite is agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Long Ye, leaf of negundo chastetree (1~3) in mass ratio: (1~ 2): (1~2): (1~2): (1~2): (1~2) mixes, through supercritical CO2The extract being obtained by extraction.
2. tobacco juice for electronic smoke as claimed in claim 1, it is characterised in that be made up of the raw material of following mass percent: tobacco carries Take thing 6-8%, tobacco aromatics 2-4%, flavouring essence for tobacco 1-3%, flavoring essence 3-5%, natural nicotine 1-2%, natural plant extraction essence China 2-4%, two glycerine 50-80%, one or more in balance of propane diols, glycerine, alcohol, butanediol, triethylene glycol.
3. tobacco juice for electronic smoke as claimed in claim 1, it is characterised in that be made up of the raw material of following mass percent: Yunnan Tobacco Grass extract 8%, tobacco aromatics 3%, flavouring essence for tobacco 2%, flavoring essence 4%, natural nicotine 1.5%, natural plant extraction elite 3%, Two glycerine 50%, balance of propane diols, glycerine, alcohol, butanediol, triethylene glycol are with the miscible mixed liquor of equal-volume.
4. tobacco juice for electronic smoke as claimed in claim 1, it is characterised in that be made up of the raw material of following mass percent: Tobacco In Guangxi Extract 5%, tobacco aromatics 4%, flavouring essence for tobacco 1%, flavoring essence 6%, natural nicotine 1%, natural plant extraction elite 4%, two Glycerine 30%, balance of propane diols, the mixed liquor of triethylene glycol.
5. tobacco juice for electronic smoke as claimed in claim 1, it is characterised in that be made up of the raw material of following mass percent: Hubei tobacco Extract 10%, tobacco aromatics 2%, flavouring essence for tobacco 3%, flavoring essence 2%, natural nicotine 2%, natural plant extraction elite 1%, Two glycerine 65%, balance of triethylene glycol.
6. the preparation method of a tobacco juice for electronic smoke as claimed in claim 1, it is characterised in that by tobacco extract, natural plants Extraction elite, tobacco aromatics, flavouring essence for tobacco, flavoring essence, natural nicotine, two glycerine and propane diols, glycerine, alcohol, fourth two One or more in alcohol, triethylene glycol, add by mass percentage, mix, to obtain final product.
7. the preparation method of tobacco juice for electronic smoke as claimed in claim 6, it is characterised in that the preparation method of natural plant extraction elite For: weigh agalloch eaglewood, santal, the banksia rose, acute turpinia leaf, Long Ye, leaf of negundo chastetree by mass parts, pulverize, cross 80-100 mesh sieve, through surpassing Critical CO2Extraction, extracting pressure is 20-25MPa, CO2Flow is 20-30L/h, and extraction time is 1-2h, and entrainer is 95% ethanol, Obtain.
CN201410249859.6A 2014-06-06 2014-06-06 A kind of Chinese style tobacco juice for electronic smoke and preparation method thereof CN103989244B (en)

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CN103610229A (en) * 2013-12-09 2014-03-05 李建伟 Nicotine liquid of electronic cigarette
CN103720030A (en) * 2013-12-13 2014-04-16 浙江中烟工业有限责任公司 Electronic cigarette liquid prepared from tobacco powder extractive and preparation method of electronic cigarette liquid

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