CN103989245B - The Chinese style flue-cured tobacco odor type tobacco juice for electronic smoke of the sweet soapy feeling in a kind of effective reduction oral cavity - Google Patents

The Chinese style flue-cured tobacco odor type tobacco juice for electronic smoke of the sweet soapy feeling in a kind of effective reduction oral cavity Download PDF

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CN103989245B
CN103989245B CN201410250173.9A CN201410250173A CN103989245B CN 103989245 B CN103989245 B CN 103989245B CN 201410250173 A CN201410250173 A CN 201410250173A CN 103989245 B CN103989245 B CN 103989245B
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tobacco
electronic smoke
extract
dpg
essence
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CN201410250173.9A
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Chinese (zh)
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CN103989245A (en
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周仕禄
刘仕民
王钧
牟会南
刘晓芊
郑宏伟
刘江
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山东中烟工业有限责任公司
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Abstract

The invention discloses the application of DPG in tobacco juice for electronic smoke preparation, the tobacco juice for electronic smoke prepared when also disclosing application, be made up of the raw material of following mass percent: Yunnan tobacco extract 1-8%, tobacco aromatics 1-5%, flavouring essence for tobacco 0.5-3%, flavoring essence 1-5%, natural nicotine 0.8-2%, natural plant extraction elite 0.5-5%, DPG 30-95%, surplus is one or more in propane diols, glycerine, alcohol, sorbierite, distilled water; Wherein, natural plant extraction elite is cloves, sweet osmanthus, tussilago, Chinese trumpet creeper Radix Glycyrrhizae (2 ~ 4) in mass ratio: (1 ~ 2): (1 ~ 2): (1 ~ 2): (1 ~ 2) mixes, through supercritical CO 2extract the extract obtained.Also disclose the preparation method of this tobacco juice for electronic smoke, tobacco juice for electronic smoke of the present invention contains Chinese style flue-cured tobacco extract and essence spice for cigarette composition, comparatively close with traditional Chinese flue-cured tobacco flavor types cigarette in fragrance, mouthfeel, improves suction satisfaction.

Description

The Chinese style flue-cured tobacco odor type tobacco juice for electronic smoke of the sweet soapy feeling in a kind of effective reduction oral cavity

Technical field

The present invention relates to the Chinese style flue-cured tobacco odor type tobacco juice for electronic smoke of the sweet soapy feeling in a kind of effective reduction oral cavity, belong to electronic cigarette technical field.

Background technology

Along with progressively enforcement, the development of global Tobacco Control campaign and the carrying forward vigorously of State Bureau's lowering harm and decreasing coking of " Framework Convention on Tobacco Control ", the degree of concern of people to health improves day by day, makes cigarette living environment just increasingly serious.In order to satisfied different consumer demand, the product of various simulation cigarette continues to bring out, wherein general with electronic cigarette, and particularly American-European countries's acquisition is extensively approved and achieves great development in the world, people have generally had science and objectively judgement more to electronic cigarette, and the progress of electronic cigarette product self is also being accelerated and promoting this industry to be in progress towards optimum and healthy direction.But, tobacco juice for electronic smoke is now sold in market, mostly has that to suck sweet soapy feeling in rear oral cavity overweight, to the very uncomfortable sensation of people's one, and tobacco flavor is too weak, the domestic consumer that get used to suction Chinese style flue-cured tobacco odor type cigarette can not be met, seriously constrain the development of electronic cigarette.

DPG has another name called dipropylene glycol, is a kind of odorless, colourless, water-soluble and hygroscopic liquid, is mainly used in essence, spices and cosmetic field at present, not yet has the report being applied to tobacco juice for electronic smoke.

Summary of the invention

The object of the present invention is to provide the application of DPG in tobacco juice for electronic smoke preparation.

Another object of the present invention is to provide a kind of tobacco juice for electronic smoke utilizing DPG to prepare.

For achieving the above object, the present invention adopts following technical scheme:

The application of DPG in tobacco juice for electronic smoke preparation, in tobacco juice for electronic smoke, the mass percent of DPG is 30-95%;

Utilize a tobacco juice for electronic smoke prepared by DPG, be made up of the raw material of following mass percent:

Yunnan tobacco extract 1-8%, tobacco aromatics 1-5%, flavouring essence for tobacco 0.5-3%, flavoring essence 1-5%, natural nicotine 0.8-2%, natural plant extraction elite 0.5-5%, DPG 30-95%, surplus is one or more in propane diols, glycerine, alcohol, sorbierite, distilled water;

Wherein, natural plant extraction elite is cloves, sweet osmanthus, tussilago, Chinese trumpet creeper, Radix Glycyrrhizae (2 ~ 4) in mass ratio: (1 ~ 2): (1 ~ 2): (1 ~ 2): (1 ~ 2) mixes, through supercritical CO 2extract the extract obtained;

Cloves, tussilago, Chinese trumpet creeper, Radix Glycyrrhizae are the kind that " Chinese Pharmacopoeia " (version in 2010) is recorded, and its quality all meets the requirement under each kind item; Sweet osmanthus is the flower of Oleaceae plants sweet osmanthus (Osmanthus fragrans).

Preferably, this tobacco juice for electronic smoke is made up of the raw material of following mass percent:

Yunnan tobacco extract 2-8%, tobacco aromatics 1-5%, flavouring essence for tobacco 0.5-3%, flavoring essence 1-5%, natural nicotine 0.8-2%, natural plant extraction elite 1-5%, DPG 50-70%, surplus is one or more in propane diols, glycerine, alcohol, sorbierite, distilled water;

The preparation method of this tobacco juice for electronic smoke, comprises the following steps:

(1) preparation of tobacco extract: by drying tobacco, pulverizes, adds the water of 8-10 times amount, ultrasonic extraction 30-60 minute, and filter, filtrate reduced in volume to relative density is 1.05-1.10 (50 DEG C of survey), obtains tobacco extract;

(2) preparation of natural plant extraction elite: take cloves, sweet osmanthus, tussilago, Chinese trumpet creeper and Radix Glycyrrhizae by mass parts, pulverizes, and crosses 80-100 mesh sieve, through supercritical CO 2extraction, extracting pressure is 20-25MPa, CO 2flow is 20-30L/h, and extraction time is 1-2h, and entrainer is 95% ethanol;

(3) by one or more in tobacco extract, natural plant extraction elite, tobacco aromatics, flavouring essence for tobacco, flavoring essence, natural nicotine, DPG and propane diols, glycerine, alcohol, sorbierite, distilled water, add in mass ratio, mixing, to obtain final product.

Beneficial effect of the present invention is:

(1) tobacco juice for electronic smoke of the present invention is using DPG as solvent, and during suction, in oral cavity, sweet soapy feeling obviously reduces, and comfort is better;

(2) tobacco juice for electronic smoke of the present invention contains Chinese style flue-cured tobacco extract and essence spice for cigarette composition, comparatively close with traditional Chinese flue-cured tobacco flavor types cigarette in fragrance, mouthfeel, improves suction satisfaction.

(3) also contain natural plant extraction elite in tobacco juice for electronic smoke of the present invention, wherein, cloves: fragrant odour, has effect of warming middle energizer to descend adverse-rising qi, can be used for deficiency-cold in spleen and stomach, and hiccup is vomitted; Sweet osmanthus: fragrant odour, has stomach invigorating, reduces phlegm, promotes the production of body fluid, effect of flat liver, can be used for the many coughs for the treatment of phlegm, toothache halitosis; Tussilago: gas is fragrant, has moistening lung to lower qi, relieving cough and reducing sputum effect, coughs for new chronic cough, dyspnea and cough with excessive sputum, labor is coughed hemoptysis; Chinese trumpet creeper: gas delicate fragrance, has effect of Yin nourishing and lung moistening, preventing phlegm from forming and stopping coughing; Above-mentioned 5 taste medicines all have fragrance smell, aroma quality and the perfume quantity of tobacco juice for electronic smoke can be increased, but also there is Yin nourishing and lung moistening, preventing phlegm from forming and stopping coughing, effects such as flat liver of promoting the production of body fluid, smoking while, also serve the effect of certain health care.

Detailed description of the invention

The present invention is further illustrated in conjunction with the embodiments, should be noted that following explanation is only to explain the present invention, not limits its content.

Embodiment 1:

Utilize a tobacco juice for electronic smoke prepared by DPG, be made up of the raw material of following mass percent:

Yunnan tobacco extract 5%, tobacco aromatics 3%, flavouring essence for tobacco 2%, flavoring essence 3%, natural nicotine 1.5%, natural plant extraction elite 3%, DPG 70%, surplus is that propane diols, glycerine, alcohol, sorbierite are with the miscible mixed liquor of equal-volume;

Wherein, natural plant extraction elite is the 2:1:1:1:1 mixing in mass ratio of cloves, sweet osmanthus, tussilago, Chinese trumpet creeper, Radix Glycyrrhizae, through supercritical CO 2extract the extract obtained;

The fragrance-enhancing tobacco material (QY021) that tobacco aromatics provides for Shanghai Qi Yuan essence and flavoring agent Co., Ltd;

Flavouring essence for tobacco is the fragrance-enhancing tobacco material (BD010) that Shenzhen BoDun spice Co., Ltd produces;

Flavoring essence is the heterocyclic material that Wutong Aroma Chemicals Co., Ltd. produces;

The purity of natural nicotine is greater than 98%.

The preparation method of this tobacco juice for electronic smoke is:

(1) preparation of tobacco extract: be dry, pulverize by Yunnan tobacco, gets 30g Yunnan tobacco powder, add the water of 240ml, ultrasonic extraction 60 minutes, filter, filtrate reduced in volume to relative density is 1.05-1.10 (50 DEG C of survey), obtains tobacco extract;

(2) preparation of natural plant extraction elite: take cloves 30g, sweet osmanthus 15g, tussilago 15g, Chinese trumpet creeper 15g and Radix Glycyrrhizae 15g, pulverizes, and crosses 100 mesh sieves, through supercritical CO 2extraction, extracting pressure is 25MPa, CO 2flow is 20L/h, and extraction time is 1.5h, and entrainer is 95% ethanol;

(3) by tobacco extract, natural plant extraction elite, tobacco aromatics, flavouring essence for tobacco, flavoring essence, natural nicotine, DPG and propane diols, glycerine, alcohol, sorbierite mixed liquor, add in mass ratio, mixing, to obtain final product.

Embodiment 2:

Utilize a tobacco juice for electronic smoke prepared by DPG, be made up of the raw material of following mass percent:

Yunnan tobacco extract 2%, tobacco aromatics 5%, flavouring essence for tobacco 0.5%, flavoring essence 5%, natural nicotine 0.8%, natural plant extraction elite 5%, DPG 30%, surplus is propane diols;

Wherein, natural plant extraction elite is the 4:1:1:1:2 mixing in mass ratio of cloves, sweet osmanthus, tussilago, Radix Glycyrrhizae, through supercritical CO 2extract the extract obtained;

The source of tobacco aromatics, flavouring essence for tobacco, flavoring essence and natural nicotine is with embodiment 1.

The preparation method of this tobacco juice for electronic smoke is:

(1) preparation of tobacco extract: be dry, pulverize by Yunnan tobacco, gets 30g Yunnan tobacco powder, add the water of 270ml, ultrasonic extraction 30 minutes, filter, filtrate reduced in volume to relative density is 1.05-1.10 (50 DEG C of survey), obtains tobacco extract;

(2) preparation of natural plant extraction elite: take cloves 40g, sweet osmanthus 10g, tussilago 10g, Chinese trumpet creeper 10g and Radix Glycyrrhizae 20g, pulverizes, and crosses 80 mesh sieves, through supercritical CO 2extraction, extracting pressure is 20MPa, CO 2flow is 30L/h, and extraction time is 2h, and entrainer is 95% ethanol;

(3) by tobacco extract, natural plant extraction elite, tobacco aromatics, flavouring essence for tobacco, flavoring essence, natural nicotine, DPG and propane diols, add in mass ratio, mixing, to obtain final product.

Embodiment 3:

Utilize a tobacco juice for electronic smoke prepared by DPG, be made up of the raw material of following mass percent:

Yunnan tobacco extract 8%, tobacco aromatics 1%, flavouring essence for tobacco 3%, flavoring essence 1%, natural nicotine 2%, natural plant extraction elite 1%, DPG 50%, surplus be propane diols, glycerine, alcohol, sorbierite, distilled water with any than miscible mixed liquor;

Wherein, natural plant extraction elite is the 2:1.5:2:1.5:1 mixing in mass ratio of cloves, sweet osmanthus, tussilago, Chinese trumpet creeper, Radix Glycyrrhizae, through supercritical CO 2extract the extract obtained;

The source of tobacco aromatics, flavouring essence for tobacco, flavoring essence and natural nicotine is with embodiment 1.

The preparation method of this tobacco juice for electronic smoke is:

(1) preparation of tobacco extract: be dry, pulverize by Yunnan tobacco, gets 30g Yunnan tobacco powder, add the water of 300ml, ultrasonic extraction 45 minutes, filter, filtrate reduced in volume to relative density is 1.05-1.10 (50 DEG C of survey), obtains tobacco extract;

(2) preparation of natural plant extraction elite: take cloves 20g, sweet osmanthus 15g, tussilago 20g, Chinese trumpet creeper 15g and Radix Glycyrrhizae 10g, pulverizes, and crosses 100 mesh sieves, through supercritical CO 2extraction, extracting pressure is 25MPa, CO 2flow is 25L/h, and extraction time is 1h, and entrainer is 95% ethanol;

(3) by tobacco extract, natural plant extraction elite, tobacco aromatics, flavouring essence for tobacco, flavoring essence, natural nicotine, DPG and propane diols, glycerine, alcohol, sorbierite, distilled water mixed liquor, add in mass ratio, mixing, to obtain final product.

Embodiment 4:

Utilize a tobacco juice for electronic smoke prepared by DPG, be made up of the raw material of following mass percent:

Yunnan tobacco extract 1%, tobacco aromatics 1%, flavouring essence for tobacco 0.5%, flavoring essence 1%, natural nicotine 0.8%, natural plant extraction elite 0.5%, DPG 95%, surplus is propane diols;

Wherein, natural plant extraction elite is the 3:2:1:1:1 mixing in mass ratio of cloves, sweet osmanthus, tussilago, Chinese trumpet creeper, Radix Glycyrrhizae, through supercritical CO 2extract the extract obtained;

The source of tobacco aromatics, flavouring essence for tobacco, flavoring essence and natural nicotine is with embodiment 1.

The preparation method of this tobacco juice for electronic smoke is:

(1) preparation of tobacco extract: be dry, pulverize by Yunnan tobacco, gets 30g Yunnan tobacco powder, add the water of 300ml, ultrasonic extraction 45 minutes, filter, filtrate reduced in volume to relative density is 1.05-1.10 (50 DEG C of survey), obtains tobacco extract;

(2) preparation of natural plant extraction elite: take cloves 30g, sweet osmanthus 20g, tussilago 10g, Chinese trumpet creeper 10g and Radix Glycyrrhizae 10g, pulverizes, and crosses 100 mesh sieves, through supercritical CO 2extraction, extracting pressure is 25MPa, CO 2flow is 25L/h, and extraction time is 1h, and entrainer is 95% ethanol;

(3) by tobacco extract, natural plant extraction elite, tobacco aromatics, flavouring essence for tobacco, flavoring essence, natural nicotine, DPG and propane diols, add in mass ratio, mixing, to obtain final product.

Embodiment 5:

Utilize a tobacco juice for electronic smoke prepared by DPG, be made up of the raw material of following mass percent:

Yunnan tobacco extract 5%, tobacco aromatics 3%, flavouring essence for tobacco 2%, flavoring essence 2%, natural nicotine 1.5%, natural plant extraction elite 3%, DPG 60%, surplus is that propane diols, glycerine, alcohol are with the miscible mixed liquor of equal-volume;

Wherein, natural plant extraction elite is the 2.5:1.5:1.5:1.5:1.5 mixing in mass ratio of cloves, sweet osmanthus, tussilago, Chinese trumpet creeper, Radix Glycyrrhizae, through supercritical CO 2extract the extract obtained;

The source of tobacco aromatics, flavouring essence for tobacco, flavoring essence and natural nicotine is with embodiment 1.

The preparation method of this tobacco juice for electronic smoke is:

(1) preparation of tobacco extract: be dry, pulverize by Yunnan tobacco, gets 30g Yunnan tobacco powder, add the water of 300ml, ultrasonic extraction 45 minutes, filter, filtrate reduced in volume to relative density is 1.05-1.10 (50 DEG C of survey), obtains tobacco extract;

(2) preparation of natural plant extraction elite: take cloves 25g, sweet osmanthus 15g, tussilago 15g, Chinese trumpet creeper 15g and Radix Glycyrrhizae 15g, pulverizes, and crosses 100 mesh sieves, through supercritical CO 2extraction, extracting pressure is 25MPa, CO 2flow is 25L/h, and extraction time is 1h, and entrainer is 95% ethanol;

(3) by tobacco extract, natural plant extraction elite, tobacco aromatics, flavouring essence for tobacco, flavoring essence, natural nicotine, DPG and propane diols, glycerine, alcohol with the miscible mixed liquor of equal-volume, add in mass ratio, mixing, to obtain final product.

Embodiment 6:

Sensory quality assessment is tested:

(1) experiment material: tobacco juice for electronic smoke prepared by the embodiment of the present invention 1,2,3,4,5 is as sample.

(2) electronic cigarette sensory quality assessment standard:

With reference to patent " a kind of tobacco juice for electronic smoke utilizing strong-flavor tobacco leaf to prepare " (number of patent application: 201310030063.7) arrange 7 assessment items, the maximum scale of each assessment item is 9 points, each assessment item is all divided into scoring unit with 1, specifically in table 1.

Table 1 electronic cigarette sensory quality assessment standard

Score value Aroma quality Perfume quantity Sweet soapy feeling Excitant Assorted gas Strength Pleasant impression 9 Very well Sufficient Very light Very little Very light Very large Very well 8 Good Foot Light Little Gently Greatly Good 7 Better More sufficient Lighter Less Lighter Larger Better 6 Slightly good Still sufficient Slightly light Slightly little Still light Slightly large Slightly good 5 In In In In In In In

4 Slightly poor Slightly Slightly dense Slightly large Slightly heavy Slightly little Slightly poor 3 Poor Lighter Denseer Larger Heavier Less Poor 2 Difference Flat Dense Greatly Heavy Little Difference 1 Very poor Very light Dense Very large Very heavy Very little Very poor

(3) evaluation method: provide sample and sensory quality assessment standard scale to the expert that smokes panel test, by form requirement, indices is smoked panel test.

(4) result statistics: the smoking result of all experts that smokes panel test is all effective, and the individual event smoking result of the expert that respectively smokes panel test is asked arithmetic mean of instantaneous value, and result remains to 1 decimal, and the arithmetic mean of instantaneous value of each individual event is added and, obtain total score, the results are shown in Table 2.

Table 2 sensory quality assessment result

Sample Aroma quality Perfume quantity Sweet soapy feeling Excitant Assorted gas Strength Pleasant impression Add up to Embodiment 1 7.8 7.6 7.6 8.0 7.8 7.8 7.6 54.2 Embodiment 2 7.6 7.8 7.4 7.6 7.5 7.6 7.4 52.9 Embodiment 3 7.4 7.6 7.5 7.5 7.6 7.6 7.5 52.7 Embodiment 4 7.2 7.1 7.8 7.6 7.4 7.3 7.2 51.6 Embodiment 5 7.5 7.4 7.4 7.6 7.5 7.4 7.5 52.3

Above-described embodiment is the present invention's preferably embodiment; but embodiments of the present invention are not restricted to the described embodiments; one of ordinary skill in the art should be understood that; on the basis of technical scheme of the present invention, those skilled in the art do not need to pay various amendment or distortion that creative work can make still within protection scope of the present invention.

Claims (5)

1. a tobacco juice for electronic smoke, is characterized in that, is made up of the raw material of following mass percent:
Yunnan tobacco extract 1-8%, tobacco aromatics 1-5%, flavouring essence for tobacco 0.5-3%, flavoring essence 1-5%, natural nicotine 0.8-2%, natural plant extraction elite 0.5-5%, DPG 30-95%, surplus is one or more in propane diols, glycerine, alcohol, sorbierite, distilled water;
Wherein, natural plant extraction elite is cloves, sweet osmanthus, tussilago, Chinese trumpet creeper, Radix Glycyrrhizae (2 ~ 4) in mass ratio: (1 ~ 2): (1 ~ 2): (1 ~ 2): (1 ~ 2) mixes, through supercritical CO 2extract the extract obtained.
2. tobacco juice for electronic smoke as claimed in claim 1, it is characterized in that, be made up of the raw material of following mass percent: Yunnan tobacco extract 2-8%, tobacco aromatics 1-5%, flavouring essence for tobacco 0.5-3%, flavoring essence 1-5%, natural nicotine 0.8-2%, natural plant extraction elite 1-5%, DPG 50-70%, surplus is one or more in propane diols, glycerine, alcohol, sorbierite, distilled water.
3. tobacco juice for electronic smoke as claimed in claim 1, it is characterized in that, be made up of the raw material of following mass percent: Yunnan tobacco extract 5%, tobacco aromatics 3%, flavouring essence for tobacco 2%, flavoring essence 3%, natural nicotine 1.5%, natural plant extraction elite 3%, DPG 50%, surplus be propane diols, glycerine, alcohol, sorbierite with arbitrarily than miscible mixed liquor.
4. tobacco juice for electronic smoke as claimed in claim 1, it is characterized in that, be made up of the raw material of following mass percent: Yunnan tobacco extract 2%, tobacco aromatics 5%, flavouring essence for tobacco 0.5%, flavoring essence 5%, natural nicotine 0.8%, natural plant extraction elite 5%, DPG 30%, surplus is propane diols.
5. tobacco juice for electronic smoke as claimed in claim 1, it is characterized in that, be made up of the raw material of following mass percent: Yunnan tobacco extract 8%, tobacco aromatics 1%, flavouring essence for tobacco 3%, flavoring essence 1%, natural nicotine 2%, natural plant extraction elite 1%, DPG 60%, surplus be propane diols, glycerine, alcohol, sorbierite, distilled water with any than miscible mixed liquor.
CN201410250173.9A 2014-06-06 2014-06-06 The Chinese style flue-cured tobacco odor type tobacco juice for electronic smoke of the sweet soapy feeling in a kind of effective reduction oral cavity CN103989245B (en)

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