CN104544543A - Electronic cigarette smoke solution prepared through black tea leaf extract - Google Patents
Electronic cigarette smoke solution prepared through black tea leaf extract Download PDFInfo
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- CN104544543A CN104544543A CN201410848645.0A CN201410848645A CN104544543A CN 104544543 A CN104544543 A CN 104544543A CN 201410848645 A CN201410848645 A CN 201410848645A CN 104544543 A CN104544543 A CN 104544543A
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/10—Chemical features of tobacco products or tobacco substitutes
- A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
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- A—HUMAN NECESSITIES
- A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
- A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
- A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
- A24B15/18—Treatment of tobacco products or tobacco substitutes
- A24B15/24—Treatment of tobacco products or tobacco substitutes by extraction; Tobacco extracts
- A24B15/241—Extraction of specific substances
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- A24F47/002—
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Abstract
The invention relates to an electronic cigarette smoke solution prepared through black tea leaf extract. The electronic cigarette smoke solution is prepared from the following components in parts by mass: 1 to 25 parts of black tea leaf extract, 2 to 25 parts of tobacco extract, 0.5 to 15 parts of tobacco flavor, 50 to 80 parts of propylene glycol, 5 to 30 parts of glycerinum, and 2 to 5 parts of edible alcohol. According to the electronic cigarette smoke solution prepared through the black tea leaf extract, the special black tea leaf extract is mixed with the special tobacco extract, so that the electronic cigarette smoke solution is rich in fragrance, coordinated in perfume, and high in sense of satisfaction; the disadvantages of insufficient fragrance and taste of the electronic cigarette smoke solution can be improved to some extent; meanwhile, the tea essential oil contains a plurality of effective ingredients which bring a healthcare effect to some extent.
Description
Technical field
The present invention relates to a kind of tobacco juice for electronic smoke utilizing black tea leaf extract to prepare, belong to electronic cigarette technical field.
Background technology
Along with the progressively enforcement of the international Framework Convention on Tobacco Control and the enhancing gradually of health of people consciousness, traditional cigarette selling market is subject to powerful impact.In order to tackle change and the consumer demand in market, the novel tobacco goods of a class less harmful receive showing great attention to of domestic and international each large tobacco enterprise and extensively study.Wherein, electronic cigarette, as a class staple product in novel tobacco goods, is to contain or not to be atomized into particulate containing nicotine solution, directly to be sucked by consumer.Electronic cigarette generates smog sensation owing to taking atomizing type, does not produce tar and CO, produces second-hand-cigarette harm hardly simultaneously, be regarded as non-harmful smoking cessation product or substitute of tobacco.Particularly showed powerful development trend in European and American developed countries in the last few years, data show world's electronic cigarette gross sales amount over nearly 3 years average annual growth rate up to 40%.Wherein only at American market, within 2013, electronic cigarette gross sales amount is more than 1,000,000,000 dollars, increases nearly one times than 2012.
The market potential that electronic cigarette is huge excites broad interest and the further investigation of each large tobacco enterprises and individuals.Current existing atomization technique can produce good atomizing effect, to electronic cigarette smoker with the impression of swallowing clouds and blowing out fog, but is but barely satisfactory compared with traditional cigarette on mouthfeel, fragrance.Improving the most important thing that electronic cigarette formula of liquid is the research of current electronic cigarette, is the core technology that tobacco enterprise bases oneself upon in electronic cigarette industry and develops.
In order to simulate the fragrance of traditional cigarette, fragrance and mouthfeel to the full extent, solution the most general at present adds tobacco extract in tobacco juice.Tobacco extractive technique mainly comprises the means of different combinations such as steam distillation, solvent extraction, simultaneous distillation method, enzymolysis extraction, supercritical extraction, molecularly distilled and extracts aroma component in tobacco.Tobacco juice for electronic smoke is mixed to get according to a certain ratio by the essential oil of tobaccos and Alevaire, flavouring essence for tobacco that extract acquisition, although but smoking result shows that the tobacco juice obtained by this approach is containing certain this perfume of tobacco, mouthfeel and fragrance enrich degree and also have larger gap compared with traditional cigarette.Trace it to its cause and may be: on the one hand different extraction means extraction efficiency is different, Partial Tobacco aroma component cannot greater efficiency be transferred in extract; On the other hand, tobacco, without combustion process, lacks the fragrance component produced through cracking in extract.In order to make up the deficiency of tobacco extract further, finding a kind of plant with tobacco with similarity, improving through blending, formula, prepare the abundant and obvious tobacco juice for electronic smoke of feature of fragrance.
Tealeaves and tobacco are that present people live the two indispensable large class consumer goods.Both have numerous similarity, as the odor type of tealeaves and tobacco seemingly, the fragrance matter contained in tealeaves is similar to tobacco.Meanwhile, tealeaves special causes perfume (or spice) and health-care components, as catechin, caffeine, abundant mineral matter, vitamin and other active ingredient flavonols, saponin etc. containing self again.Tobacco extract is mixed with into electronic cigarette liquid by a certain percentage with tea extract, not only can supplements the shortcoming of tobacco aroma concentration deficiency, make fragrance component abundanter; The harm simultaneously can alleviating or suppress tobacco to bring containing much active ingredient in tea extraction liquid.It is reported that the application study of Tea Polyphenols in Tea has a lot of aspect, comprise anticancer, anti-oxidant and delay senility, antibacterial and antiviral, reducing blood lipid, lipid-antioxidant activity effect, pigment protective effect, deodorant, anticaries action, the several functions such as suppression atherosclerotic.Tea Polyphenols has become the focus of medicine, the exploitation of food circle.Cigarette is pungent and fragrant, the sweet and delicate fragrance in tea Tianjin, uses together and can bring out the best in each other.
Tea tree is because of differences such as hereditary capacity, growing environment, geographical situation and sweats, and all there is some difference to make chemical composition in tealeaves and content, tea leaf quality and odor type.Black tea belongs to full fermented tea, is with suitable new tea tooth leaf for raw material, through the tea that the series of process process such as wither, knead (cutting), fermentation, drying is refined.Black tea leaf there occurs the chemical reaction centered by Tea Polyphenols enzymatic oxidation, chemical composition change in fresh leaf is larger, Tea Polyphenols reduces more than 90%, Tea Polyphenols is oxidized, polymerization, form the huge theaflavins of molecular weight and thearubigin class, aroma substance obviously increases than fresh leaf, formation black tea red soup red autumnal leaves, the qualitative characteristics that fragrance is fragrant and sweet, flavour is sweet and pure.The kind of black tea is more, and the natural place of production is also just comparatively wide, according to the method for its processing and the tea shape of product, generally can be divided into three major types again: souchong, congou tea, red fannings and black tea tea are precious.Representational category comprises: Wuyi Mountain, fujian Lapsang souchong, Qimen, Anhui time, lake red time, Yunnan black tea time, peaceful red time, suitable red time, redder time, river red time, Fujian red time etc.Black tea is rich in the various nutrient elements such as carrotene, vitamin A, calcium, phosphorus, magnesium, potassium, caffeine, isoleucine, leucine, lysine, glutamic acid, alanine, asparatate, there is warm stomach health, benefit of refreshing oneself thinks of, dispelling fatigue, elimination oedema, antidiarrheal, antibacterial, strengthen the effects such as immune.Black tea also contributes to gastro-intestinal digestion, can promote appetite, can effectively prevent and treat myocardial infarction, strong cardiac muscle function, reduce blood glucose value and hypertension, prevent to decay tooth and poison by food etc.Research and analyse result and show that the main aromatic components of black tea is: geraniol, linalool and oxide thereof, phenmethylol, 2 phenylethyl alcohol, gaultherolin, dihydroactinidiolide etc., the component of the precursor substance of its fragrance mainly polyester class, terpene compound, unsaturated fatty acids and some other thermal degradation.
Summary of the invention
The object of the present invention is to provide a kind of tobacco juice for electronic smoke utilizing black tea leaf extract to prepare, improve existing tobacco juice for electronic smoke mouthfeel not good, the shortcomings such as fragrance is not enough.The present invention obtains the black tea leaf extract of different cultivars by supercritical extract, it is mixed with specific tobacco extract afterwards, is aided with suitable essence spice for cigarette and Alevaire, can prepare that fragrance enriches, the tobacco juice for electronic smoke of comfortable taste.
The present invention is achieved by the following technical solutions:
A first aspect of the present invention provides a kind of tobacco juice for electronic smoke utilizing black tea leaf extract to prepare, comprise following component according to the mass fraction: black tea leaf extract 1 ~ 25 part, tobacco extract 2 ~ 25 parts, flavouring essence for tobacco 0.5 ~ 15 part, propane diols 50 ~ 80 parts, glycerine 5 ~ 30 parts, edible alcohol 2 ~ 5 parts.
Preferably, described a kind of tobacco juice for electronic smoke, comprises following component according to the mass fraction: black tea leaf extract 5 ~ 20 parts, tobacco extract 8 ~ 17 parts, flavouring essence for tobacco 2 ~ 12 parts, propane diols 55 ~ 75 parts, glycerine 10 ~ 25 parts, edible alcohol 2 ~ 4 parts.
Optimum, described tobacco juice for electronic smoke, comprises following component according to the mass fraction: black tea leaf extract 15 parts, tobacco extract 12 parts, flavouring essence for tobacco 7 parts, propane diols 70 parts, glycerine 20 parts, edible alcohol 3 parts.
Described black tea leaf extract be by Lapsang souchong, Qimen, the Anhui time, the lake red time, the Yunnan black tea time, the peaceful red time, should the red time, the redder time, the river red time, in the red time of Fujian one or more combination through extracting obtained concentrate.
The extract of black tea leaf described in the present invention can adopt method conventional in prior art to obtain.
Preferably, the extracting method of described black tea leaf extract is: get black tea leaf crushed after being dried, then carries out supercritical extract and obtains black tea leaf extract.
Preferably, the extracting method of described black tea leaf extract is: get black tea leaf crushed after being dried, then carries out supercritical CO
2extraction obtains black tea leaf extract.
Preferably, described black tea leaf be selected from Lapsang souchong, Qimen, the Anhui time, the lake red time, the Yunnan black tea time, the peaceful red time, should the red time, the redder time, the river red time, any one or multiple combination in the red time of Fujian.
Preferably, after dry, Measuring Moisture Content of Tea percentage by weight is less than 20%, and after more excellent drying, Measuring Moisture Content of Tea percentage by weight is less than 10%.
Preferably, described black tea leaf grinding particle size is 10 ~ 70 orders, is more preferably 25 orders.
Preferably, described supercritical CO
2the extracting pressure of extraction is 10 ~ 50MPa; Preferred extracting pressure is 25MPa.
Preferably, described supercritical CO
2the extraction temperature of extraction is 10 ~ 60 DEG C; More excellent extraction temperature is 45 DEG C.
Preferably, described supercritical CO
2the extraction time of extraction is 1 ~ 10h; Preferred extraction time is 3h.
Preferably, described tobacco extract is selected from the tobacco leaf of one or more the combination in osculant flue-cured tobacco, burley tobaccos and Dark sun-cured or pipe tobacco through extracting obtained extract.
Preferably, described tobacco extract is mass ratio is 1:(0.9 ~ 1.1) osculant flue-cured tobacco and the tobacco leaf of burley tobaccos or pipe tobacco through extracting obtained concentrate.
Tobacco extract described in the present invention can adopt method conventional in prior art to obtain.
Preferably, the extracting method of described tobacco extract, for: get tobacco leaf or pipe tobacco, crushed after being dried powdered, be placed in solvent and carry out ultrasonic extraction, through sedimentation, filtration and reduced pressure concentration i.e. obtained described tobacco extract.
Preferably, the grinding particle size of described tobacco leaf or pipe tobacco is 40 ~ 100 orders, is more preferably 40 ~ 60 orders.
Preferably, described ultrasonic extraction process, the mass ratio of tobacco leaf or pipe tobacco powder and solvent is 1:(2 ~ 5); Be more preferably 1:(2.5 ~ 3.5).
Preferably, described solvent is deionized water or ethanol.
Preferably, the temperature of described ultrasonic extraction is 30 ~ 60 DEG C, is more preferably 40 ~ 60 DEG C.
Preferably, the time of described ultrasonic extraction is 2 ~ 5 hours, is more preferably 3.5 ~ 4.5 hours.
Preferably, under 50 ~ 90 DEG C of conditions, decompression is revolved and is desolventized to obtain tobacco extract, and more excellent is 60 ~ 80 DEG C.
The present invention does not have special restriction to the kind of described tobacco essence and source, adopts flavouring essence for tobacco well known to those skilled in the art.
Preferably; described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2; 6; 6-trimethyl-2-cyclohexene-1; 4-diketone, 2-hydroxyl-3,5,5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine and 2; 3,5-trimethylpyrazine.
Preferably, described flavouring essence for tobacco is the component being selected from following weight percent: 1 ~ 10% Ethyl vanillin, 1 ~ 10% benzyl acetate, 1 ~ 8% furfural, 4 ~ 20% dorinones, 2 ~ 15% β-damascone, 10 ~ 30% Megastigmatrienones, 2 ~ 15% dihydroactinidiolides, 1 ~ 8% dimethyl succinate, 1 ~ 5%2, 6, 6-trimethyl-2-cyclohexene-1, 4-diketone, 1 ~ 5%2-hydroxyl-3, 5, 5-trimethyl-2-cyclonene, 3 ~ 15% geranyl acetones, 5 ~ 30% alpha, beta-lonones, 3 ~ 15% phenmethylols, 2 ~ 7% palmitic acids, 1 ~ 4% isovaleric acid, 1 ~ 4%2-methylvaleric acid, 1 ~ 3% indoles, 1 ~ 3% pyridine, 1 ~ 5%3-acetylpyridine and 1 ~ 5%2, 3, 5-trimethylpyrazine, and to meet summation be 100wt%.
Preferably, described flavouring essence for tobacco is following several formula (percentage by weight):
Formula one: 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Said components is mixed in vortex oscillator.
Formula two: 15% dorinones, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol; Said components is mixed in vortex oscillator.
Formula three: 15% dorinones, 30% Megastigmatrienone, 5%2,3,5-trimethylpyrazines, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 12% phenmethylol.
Formula four: 30% Megastigmatrienones, 5% benzyl acetate, 6% furfural, 8% Ethyl vanillin, 7% palmitic acid, 3%2,3,5-trimethylpyrazines, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 15% phenmethylol.
Formula five: 15% dorinones, 30% Megastigmatrienone, 5%2,3,5-trimethylpyrazines, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% alpha, beta-lonone, 12% phenmethylol.
Preferably, described glycerine and propane diols are food grade product.
Second aspect present invention provides the preparation method of aforementioned electronic tobacco juice, for described each composition mix and blend is mixed and be get final product.
Third aspect present invention provides aforementioned electronic tobacco juice and is preparing the purposes in electronic cigarette.
Compared with prior art, the present invention has following beneficial effect:
(1) the present invention utilizes supercritical carbon dioxide extraction means to obtain the derived essential oil of black tea leaf, farthest maintains this perfume of black tea.
(2) the present invention is by mixing black tea extract with tobacco extract, and make tobacco juice for electronic smoke fragrance abundanter, fragrance is coordinated more, to some extent solves the shortcoming of tobacco juice for electronic smoke fragrance and taste deficiency.
(3) tobacco juice for electronic smoke of the present invention generates smog sensation owing to taking atomizing type, does not produce tar and CO, does not produce second-hand-cigarette harm simultaneously.
(4) the present invention is by adding the black tea leaf essential oil of multiple effect composition, warm stomach health, benefit of refreshing oneself thinks of, dispelling fatigue, elimination oedema, antidiarrheal, antibacterial, strengthen the effects such as immune.
Detailed description of the invention
Below by way of specific instantiation, technical scheme of the present invention is described.Should be understood that one or more method steps that the present invention mentions do not repel and before and after described combination step, also to there is additive method step or can also insert additive method step between these steps clearly mentioned; Should also be understood that these embodiments are only not used in for illustration of the present invention to limit the scope of the invention.And, except as otherwise noted, the numbering of various method steps is only the convenient tool differentiating various method steps, but not be ordering or the enforceable scope of restriction the present invention of restriction various method steps, the change of its relativeness or adjustment, when changing technology contents without essence, when being also considered as the enforceable category of the present invention.
Embodiment 1:
The preparation of tobacco extract: get osculant cured tobacco leaf sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, be crushed to 40 ~ 100 orders.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h under 50 ± 5 DEG C of conditions, afterwards standing sedimentation 4h, sand core funnel filters to get filtrate, and 70 ± 10 DEG C of vacuum rotary steams are concentrated into 3mL, obtain tobacco extract.
The supercritical preparation process of black tea leaf extract: take Wuyi Mountain Lapsang souchong 100g, grinds as 20-30 order powder through pulverizer, and load in the extraction kettle of 1L, control extracting pressure is 25MPa, and extraction temperature is 50 DEG C, regulates supercritical CO
2flow be 25L/h, extraction time is 3h.The supercritical fluid being dissolved with extract after extraction is reduced pressure by choke valve, and enter in separating still and become gas, extract is separated out in separating still, is collected in receiving bottle and namely obtains black tea leaf extract.
Flavouring essence for tobacco (percentage by weight): 8% dorinone, 5% β-damascone, 13% Megastigmatrienone, 24% alpha, beta-lonone, 9% Ethyl vanillin, 7% benzyl acetate, 5% furfural, 5% phenmethylol, 4% palmitic acid, 12% dihydroactinidiolide, 8% dimethyl succinate.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
A kind of tobacco juice for electronic smoke preparation utilizing black tea leaf extract to prepare, black tea leaf extract 15 parts, tobacco extract 12 parts, flavouring essence for tobacco 7 parts, propane diols 70 parts, glycerine 20 parts, edible alcohol 3 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Embodiment 2:
The preparation of tobacco extract: get burley tobaccos tobacco sample dry 3h in 40 DEG C of baking ovens, after being cooled to room temperature, be crushed to 40 ~ 100 orders.Take the conical flask that 100g offal is placed in 1L, add 300mL deionized water, ultrasonic extraction 4h, standing sedimentation 4h afterwards under 50 ± 5 DEG C of conditions, sand core funnel filters to get filtrate, and 70 ± 10 DEG C of vacuum rotary steams are concentrated into 3mL, obtain tobacco extract.
The supercritical preparation process of black tea leaf extract: take Qimen kung fu tea 100g, grinds as 45-55 order powder through pulverizer, and load in the extraction kettle of 1L, control extracting pressure is 40MPa, and extraction temperature is 35 DEG C, regulates supercritical CO
2flow be 35L/h, extraction time is 5h.The supercritical fluid being dissolved with extract after extraction is reduced pressure by choke valve, and enter in separating still and become gas, extract is separated out in separating still, is collected in receiving bottle and namely obtains black tea leaf extract.
Flavouring essence for tobacco (percentage by weight): 15% dorinone, 3% indoles, 15% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 9% alpha, beta-lonone, 15% phenmethylol.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
A kind of tobacco juice for electronic smoke preparation utilizing black tea leaf extract to prepare, following components in mass portion number meter batching: black tea leaf extract 5 parts, tobacco extract 17 parts, flavouring essence for tobacco 12 parts, propane diols 75 parts, glycerine 25 parts, edible alcohol 4 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Embodiment 3:
Prepared by tobacco extract: get Dark sun-cured tobacco sample, extract, extracting method is with embodiment 1.
The supercritical preparation process of black tea leaf extract: claim the red kung fu tea 100g in lake, grind as 10-20 order powder through pulverizer, load in the extraction kettle of 1L, control extracting pressure is 50MPa, and extraction temperature is 55 DEG C, regulates supercritical CO
2flow be 20L/h, extraction time is 7h.The supercritical fluid being dissolved with extract after extraction is reduced pressure by choke valve, and enter in separating still and become gas, extract is separated out in separating still, is collected in receiving bottle and namely obtains black tea leaf extract.
Flavouring essence for tobacco (percentage by weight): 15% dorinone, 30% Megastigmatrienone, 5%2,3,5-trimethylpyrazine, 8% Ethyl vanillin, 4% palmitic acid, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 12% phenmethylol.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
A kind of tobacco juice for electronic smoke preparation utilizing black tea leaf extract to prepare, following components in mass portion number meter batching: black tea leaf extract 20 parts, tobacco extract 8 parts, flavouring essence for tobacco 2 parts, propane diols 55 parts, glycerine 10 parts, edible alcohol 2 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Embodiment 4:
Prepared by tobacco extract: get osculant flue-cured tobacco and the mixing of burley tobaccos tobacco leaf that mass ratio is 1:1, then extract obtained tobacco extract according to the mode of embodiment 1.
The supercritical preparation process of black tea leaf extract: take Yunnan black tea kung fu tea 100g, grinds as 20-30 order powder through pulverizer, and load in the extraction kettle of 1L, control extracting pressure is 25MPa, and extraction temperature is 45 DEG C, regulates supercritical CO
2flow be 25L/h, extraction time is 3h.The supercritical fluid being dissolved with extract after extraction is reduced pressure by choke valve, and enter in separating still and become gas, extract is separated out in separating still, is collected in receiving bottle and namely obtains black tea leaf extract.
Flavouring essence for tobacco (percentage by weight): 30% Megastigmatrienone, 5% benzyl acetate, 6% furfural, 8% Ethyl vanillin, 7% palmitic acid, 3%2,3,5-trimethylpyrazine, 9% dihydroactinidiolide, 2% dimethyl succinate, 15% geranyl acetone, 15% phenmethylol.Said components is mixed in vortex oscillator.
Glycerine and propane diols are food grade product.
A kind of tobacco juice for electronic smoke preparation utilizing black tea leaf extract to prepare, following components in mass portion number meter batching: black tea leaf extract 1 part, tobacco extract 25 parts, flavouring essence for tobacco 15 parts, propane diols 80 parts, glycerine 30 parts, edible alcohol 5 parts, vortex oscillator mixes and obtains tobacco juice for electronic smoke.
Comparative example 1 (not containing black tea leaf extract)
Prepared by tobacco juice for electronic smoke, following components in mass portion number meter batching: tobacco extract 12 parts, flavouring essence for tobacco 7 parts, propane diols 70 parts, glycerine 20 parts, edible alcohol 3 parts.
Wherein tobacco extract composition and extracting mode, flavouring essence for tobacco formula are with embodiment 1.
Comparative example 2 (not containing tobacco extract)
Prepared by tobacco juice for electronic smoke, below each component batching according to the mass fraction: black tea leaf extract 15 parts, flavouring essence for tobacco 7 parts, propane diols 70 parts, glycerine 20 parts, edible alcohol 3 parts.
Wherein tobacco extract composition and extracting mode, flavouring essence for tobacco formula are with embodiment 1.
Comparative example 3 (not containing flavouring essence for tobacco)
Prepared by tobacco juice for electronic smoke, by following components in mass portion number batching: black tea leaf extract 15 parts, and tobacco extract 12 parts, propane diols 70 parts, glycerine 20 parts, edible alcohol 3 parts.
Tobacco extract composition and extracting method, black tea leaf extract component and extracting method thereof are with embodiment 1.
Tobacco juice for electronic smoke liquid in above-described embodiment and comparative example is added in electronic cigarette device and carries out sensory effects evaluation respectively.
Sensory effects evaluation method comprises the following steps:
(1) 9 evaluation indexes are provided with, comprise excitant, satisfaction, concentration, comfort level, feature style, tobacco perfume, aroma quality, perfume quantity and the amount of being fuming, and give different score value according to the Different Effects degree of every evaluation index to tobacco juice for electronic smoke aesthetic quality.
Described excitant refers to: suck the discomfort that flue gas comprises oral cavity to sense organ, throat and nasal cavity produce that tobacco juice for electronic smoke produces through atomization and be subject to.
Described satisfaction refers to: the flue gas strength that tobacco juice for electronic smoke produces through atomization, concentration and note are to the comprehensive impression that sense organ produces.
Described concentration refers to: the impression of tobacco juice for electronic smoke oral cavity filling degree when the flue gas firm suction inlet that atomization produces.
Described comfort level refers to: the impact of flue gas on oral cavity level of comfort after sucking oral cavity and exhalation that tobacco juice for electronic smoke produces through atomization.
Described feature style refers to: a kind of tobacco juice for electronic smoke is different from the sense organ Main Differences performance of other homogeneous e cigarette tobacco juices in joyful sense.
Described tobacco perfume (or spice) refers to: in process of smokeing panel test, sensory feel is to the breath of this perfume (or spice) of tobacco.
Described aroma quality refers to: felt the good and bad degree of pleasant breath in process of smokeing panel test by sense of smell and the sense of taste.
Described perfume quantity refers to: in process of smokeing panel test by oral cavity and nasal cavity weigh pleasant breath amount number.
The described amount of being fuming refers to: tobacco juice for electronic smoke through atomization produce exhaust gas volumn number.
(2) member of smoking of 9 people is set, everyone a tobacco juice for electronic smoke sensory quality assessment table, adopt the marking mode secretly commented, adopt the overall method of smokeing panel test that circulates, tobacco juice for electronic smoke is aspirated, according to the implication of 9 sensory quality assessment index score values in table 1, adopt hundred-mark system point system to carry out comprehensive grading to the aesthetic quality of tobacco juice for electronic smoke, every evaluation index is by five points, ten point system or the scoring of ten the five-grade marking systems.The concrete meaning of the score value of tobacco juice for electronic smoke evaluation index sees the following form 1:
The score value implication table of table 1 tobacco juice for electronic smoke sensory quality assessment index
(3) evaluation method: according to the evaluation index in table 1 and score value, member of smoking tackles each evaluation index and carries out sensory quality assessment, and records its evaluation result, and the minimum score unit of score value is 0.5.
(4) result statistics: remove minimum point and a best result in the sensory quality assessment result of all members of smoking, calculate the arithmetic mean of instantaneous value of remaining effective single item evaluation index scoring, result retains two-decimal, the sensory quality assessment comprehensive grading of last tobacco juice for electronic smoke is the arithmetic mean of instantaneous value sum calculating the scoring of each single index, obtain total score, result retains a decimal.
The tobacco juice for electronic smoke prepared in the tobacco juice for electronic smoke containing black tea leaf extract prepared in embodiment 1-4 and comparative example 1-3 is added in electronic cigarette and carries out sensory quality assessment.Concrete evaluation result is in table 2, and in table 2, the scoring of every evaluation index is that the arithmetic average that 9 members of smoking effectively mark is divided.
Table 2 tobacco juice for electronic smoke sensory effects evaluation result
Table 2 result shows, when in above-described embodiment, tobacco juice for electronic smoke is embodied in suction, fog is dense, perfume quantity is enriched, have alcohol and the fragrant and sweet gas of wine, camphorwood is fragrant obviously, and sweet sense and fine and smooth degree increase obviously, stimulate and reduce, fragrance is harmonious, and pleasant impression is comfortable, shortens the aesthetic quality's difference with traditional cigarette.But the difference of the black tea kind used, Tobacco Types, extract adding proportion, essence spice for cigarette adding proportion, can produce Different Effects to investigated 9 indexs.
Claims (10)
1. the tobacco juice for electronic smoke utilizing black tea leaf extract to prepare, comprises following component according to the mass fraction: black tea leaf extract 1 ~ 25 part, tobacco extract 2 ~ 25 parts, flavouring essence for tobacco 0.5 ~ 15 part, propane diols 50 ~ 80 parts, glycerine 5 ~ 30 parts, edible alcohol 2 ~ 5 parts.
2. a kind of tobacco juice for electronic smoke utilizing black tea leaf extract to prepare as claimed in claim 1, it is characterized in that, described tobacco extract is selected from the tobacco leaf of any one or multiple combination in osculant flue-cured tobacco, burley tobaccos and Dark sun-cured or pipe tobacco through extracting obtained extract.
3. a kind of tobacco juice for electronic smoke utilizing black tea leaf extract to prepare as claimed in claim 2, it is characterized in that, the extracting method of described tobacco extract is: get tobacco leaf or pipe tobacco, crushed after being dried powdered, be placed in solvent and carry out ultrasonic extraction, through sedimentation and filtration, reduced pressure concentration i.e. obtained described tobacco extract.
4. a kind of tobacco juice for electronic smoke utilizing black tea leaf extract to prepare as claimed in claim 3, is characterized in that, described tobacco extracting method also to comprise any one of following characteristics or multinomial:
(1) grinding particle size of described tobacco leaf or pipe tobacco is 40 ~ 100 orders;
(2) described ultrasonic extraction process, the mass ratio of tobacco leaf or pipe tobacco powder and solvent is 1:(2 ~ 5);
(3) described solvent is deionized water or ethanol;
(4) temperature of described ultrasonic extraction is 30 ~ 60 DEG C;
(5) time of described ultrasonic extraction is 2 ~ 5 hours;
(6) under 50 ~ 90 DEG C of conditions, described filtrate decompression is revolved and desolventizes to obtain tobacco extract.
5. a kind of tobacco juice for electronic smoke utilizing black tea leaf extract to prepare as claimed in claim 1, it is characterized in that, described black tea extract is Lapsang souchong, Qimen, the Anhui time, the lake red time, the Yunnan black tea time, the peaceful red time, should red time, redder time, river red time, one or more in the red time of Fujian are through extracting obtained concentrate.
6. a kind of tobacco juice for electronic smoke utilizing black tea leaf extract to prepare as claimed in claim 5, it is characterized in that, the extracting method of described black tea leaf extract is: get black tea leaf crushed after being dried, then carries out supercritical extract and obtains black tea leaf extract.
7. a kind of tobacco juice for electronic smoke utilizing black tea leaf extract to prepare as claimed in claim 6, it is characterized in that, the extracting method of described black tea leaf extract is: get black tea leaf crushed after being dried, then carries out supercritical CO
2extraction obtains black tea leaf extract.
8. a kind of tobacco juice for electronic smoke utilizing black tea leaf extract to prepare as claimed in claim 7, it is characterized in that, described extracting method also comprises any one or multinomial in following characteristics:
(1) dried black tea leaf moisture weight percentage is less than 20%;
(2) described black tea powder size is 10 ~ 70 orders;
(3) described supercritical CO
2the extracting pressure of extraction is 10 ~ 50MPa;
(4) described supercritical CO
2the extraction temperature of extraction is 10 ~ 60 DEG C;
(5) described supercritical CO
2the extraction time of extraction is 1 ~ 10h.
9. a kind of tobacco juice for electronic smoke utilizing black tea leaf extract to prepare as claimed in claim 1, it is characterized in that, described flavouring essence for tobacco is selected from Ethyl vanillin, benzyl acetate, furfural, dorinone, β-damascone, Megastigmatrienone, dihydroactinidiolide, dimethyl succinate, 2, 6, 6-trimethyl-2-cyclohexene-1, 4-diketone, 2-hydroxyl-3, 5, 5-trimethyl-2-cyclonene, geranyl acetone, alpha, beta-lonone, phenmethylol, palmitic acid, isovaleric acid, 2 methyl valeric acid, indoles, pyridine, 3-acetylpyridine and 2, 3, one or more combinations in 5-trimethylpyrazine.
10. the preparation method of the tobacco juice for electronic smoke according to the arbitrary claim of claim 1 ~ 9, for directly each component being mixed in setting ratio, to obtain final product.
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Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105011352A (en) * | 2015-08-06 | 2015-11-04 | 云南中烟工业有限责任公司 | Green tea scent type electronic cigarette liquid |
| CN105029696A (en) * | 2015-06-17 | 2015-11-11 | 云南中烟工业有限责任公司 | Black tea glycerol triacetate extract and application thereof in cigarettes |
| CN106723352A (en) * | 2016-12-30 | 2017-05-31 | 广东中烟工业有限责任公司 | A kind of method and a kind of cigarette filter for lifting cigarette comfort level |
| CN110506979A (en) * | 2019-09-12 | 2019-11-29 | 深圳雾芯科技有限公司 | Flavour compositions and electronic cigarette liquid comprising the flavour compositions |
| CN112438419A (en) * | 2019-08-27 | 2021-03-05 | 深圳波顿香料有限公司 | Preparation method of bud tea extract and application of bud tea extract in essence and electronic cigarette oil |
| CN113694717A (en) * | 2021-08-18 | 2021-11-26 | 武汉理工大学 | Chemical deodorant for garbage transfer station and preparation method and application thereof |
| CN114634841A (en) * | 2022-03-11 | 2022-06-17 | 吉林烟草工业有限责任公司 | Vitamin milk tea essence, preparation method thereof and cigarette |
Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101919584A (en) * | 2010-08-16 | 2010-12-22 | 深圳市如烟生物科技有限公司 | Slimming functional electronic cigarette liquid |
| CN101926505A (en) * | 2010-08-09 | 2010-12-29 | 深圳市如烟生物科技有限公司 | Caffeine electronic cigarette liquid |
| CN102960852A (en) * | 2012-11-14 | 2013-03-13 | 湖北中烟工业有限责任公司 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
| CN103653234A (en) * | 2012-08-30 | 2014-03-26 | 徐兵 | Aerosolization suction product with caffeine and the like and insomnia treatment function |
| CN103989245A (en) * | 2014-06-06 | 2014-08-20 | 山东中烟工业有限责任公司 | Chinese flue-cured tobacco type electronic cigarette liquid capable of effectively reducing oral cavity sweet greasy feeling |
| CN103989244A (en) * | 2014-06-06 | 2014-08-20 | 山东中烟工业有限责任公司 | Chinese style flue-cured tobacco odor type electronic cigarette tobacco juice capable of improving smoking satisfaction sense |
| CN104068467A (en) * | 2014-07-01 | 2014-10-01 | 安徽中烟工业有限责任公司 | Electronic cigarette liquid rich in plant flavone |
-
2014
- 2014-12-31 CN CN201410848645.0A patent/CN104544543A/en active Pending
Patent Citations (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101926505A (en) * | 2010-08-09 | 2010-12-29 | 深圳市如烟生物科技有限公司 | Caffeine electronic cigarette liquid |
| CN101919584A (en) * | 2010-08-16 | 2010-12-22 | 深圳市如烟生物科技有限公司 | Slimming functional electronic cigarette liquid |
| CN103653234A (en) * | 2012-08-30 | 2014-03-26 | 徐兵 | Aerosolization suction product with caffeine and the like and insomnia treatment function |
| CN102960852A (en) * | 2012-11-14 | 2013-03-13 | 湖北中烟工业有限责任公司 | Light-fragrance electronic cigarette atomized smoke solution and preparation method thereof |
| CN103989245A (en) * | 2014-06-06 | 2014-08-20 | 山东中烟工业有限责任公司 | Chinese flue-cured tobacco type electronic cigarette liquid capable of effectively reducing oral cavity sweet greasy feeling |
| CN103989244A (en) * | 2014-06-06 | 2014-08-20 | 山东中烟工业有限责任公司 | Chinese style flue-cured tobacco odor type electronic cigarette tobacco juice capable of improving smoking satisfaction sense |
| CN104068467A (en) * | 2014-07-01 | 2014-10-01 | 安徽中烟工业有限责任公司 | Electronic cigarette liquid rich in plant flavone |
Non-Patent Citations (2)
| Title |
|---|
| 于建军: "《卷烟工艺学》", 30 July 2003 * |
| 陈宗懋: "《中国茶经》", 30 May 1992 * |
Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105029696A (en) * | 2015-06-17 | 2015-11-11 | 云南中烟工业有限责任公司 | Black tea glycerol triacetate extract and application thereof in cigarettes |
| CN105011352A (en) * | 2015-08-06 | 2015-11-04 | 云南中烟工业有限责任公司 | Green tea scent type electronic cigarette liquid |
| CN105011352B (en) * | 2015-08-06 | 2016-06-01 | 云南中烟工业有限责任公司 | A kind of green tea flavor electronic cigarette tobacco tar |
| CN106723352A (en) * | 2016-12-30 | 2017-05-31 | 广东中烟工业有限责任公司 | A kind of method and a kind of cigarette filter for lifting cigarette comfort level |
| CN112438419A (en) * | 2019-08-27 | 2021-03-05 | 深圳波顿香料有限公司 | Preparation method of bud tea extract and application of bud tea extract in essence and electronic cigarette oil |
| CN110506979A (en) * | 2019-09-12 | 2019-11-29 | 深圳雾芯科技有限公司 | Flavour compositions and electronic cigarette liquid comprising the flavour compositions |
| WO2021046917A1 (en) * | 2019-09-12 | 2021-03-18 | 深圳雾芯科技有限公司 | Flavor composition and e-liquid comprising flavor composition |
| CN113694717A (en) * | 2021-08-18 | 2021-11-26 | 武汉理工大学 | Chemical deodorant for garbage transfer station and preparation method and application thereof |
| CN114634841A (en) * | 2022-03-11 | 2022-06-17 | 吉林烟草工业有限责任公司 | Vitamin milk tea essence, preparation method thereof and cigarette |
| CN114634841B (en) * | 2022-03-11 | 2023-11-21 | 吉林烟草工业有限责任公司 | Vitamin milk tea essence, preparation method thereof and cigarette |
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